{"id":97893,"date":"2017-08-27T14:00:44","date_gmt":"2017-08-27T06:00:44","guid":{"rendered":"\/\/m.iemloyee.com\/?p=97893"},"modified":"2017-08-23T21:22:16","modified_gmt":"2017-08-23T13:22:16","slug":"adv-mater-%ef%bc%9a%e4%bd%9c%e4%b8%ba%e8%83%b6%e4%bd%93%e7%ba%b3%e7%b1%b3%e6%99%b6%e8%a1%a8%e9%9d%a2%e5%ae%98%e8%83%bd%e5%8c%96%e7%9a%84%e7%ae%80%e4%be%bf%e9%80%9a%e7%94%a8%e6%96%b9%e6%b3%95","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=97893","title":{"rendered":"Adv. Mater. \uff1a\u4f5c\u4e3a\u80f6\u4f53\u7eb3\u7c73\u6676\u8868\u9762\u5b98\u80fd\u5316\u7684\u7b80\u4fbf\u901a\u7528\u65b9\u6cd5\u7684\u786b\u9187-\u70ef\u5316\u53cd\u5e94"},"content":{"rendered":"<p><strong>\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n<p> \u901a\u5e38\u4f7f\u7528\u6cb9\u9178\uff08OA\uff09\u548c\u6cb9\u80fa\uff08OAm\uff09\u6765\u4f5c\u4e3a\u65e0\u673a\u7eb3\u7c73\u6676\u4f53\uff08NC\uff09\u7a33\u5b9a\u5316\u7684\u8868\u9762\u914d\u4f53\u3002NC\u8868\u9762\u7684\u758f\u6c34\u6027\u548c\u60f0\u6027\u9650\u5236\u4e86\u5176\u5728\u751f\u7269\u533b\u5b66\u9886\u57df\u7684\u53d1\u5c55\uff0c\u56e0\u6b64\uff0c\u5bf9\u5176\u8fdb\u884c\u8868\u9762\u6539\u6027\u5fc5\u4e0d\u53ef\u5c11\u7684\u3002\u672c\u6587\u62a5\u9053\u4e86\u901a\u8fc7\u7d2b\u5916\u7ebf\u8bf1\u5bfc\u7684\u786b\u9187-\u70ef\u5316\u5b66\u6539\u6027NCs\u7684\u65b9\u6cd5\uff0c\u5176\u4e2d\u786b\u9187\u5c01\u7aef\u7684\u805a\u4e59\u4e8c\u9187\uff08HS-PEG\uff09\u53ca\u5176\u884d\u751f\u7269\u53ef\u76f4\u63a5\u4e0eOA\/OAm\u914d\u4f53\u4e00\u6b65\u5f62\u6210\u5171\u4ef7\u8fde\u63a5\u3002\u901a\u8fc7\u8fd9\u79cd\u65b9\u6cd5\uff0c\u5404\u79cd\u4e0d\u540c\u7ec4\u6210\u3001\u4e0d\u540c\u5f62\u6001\u7684\u758f\u6c34NC\u80fd\u591f\u4e0e\u6d3b\u6027\u57fa\u56e2\u5b98\u80fd\u5316\u8fdb\u800c\u8f6c\u79fb\u5230\u6c34\u4e2d\u3002\u4f5c\u4e3a\u6982\u5ff5\u8bc1\u660e\uff0c\u8be5\u6cd5\u6210\u529f\u7528\u4e8e\u6784\u5efa\u57fa\u4e8e\u4e0a\u53d8\u9891\u53d1\u5149\u5206\u6790\u68c0\u6d4b\u6297\u751f\u7269\u7d20\u86cb\u767d\u7684\u4f20\u611f\u5668\u3002\u8be5\u6cd5\u4e3a\u4e0d\u540c\u5e94\u7528\u7684NC\u8bbe\u8ba1\u548c\u8c03\u6574\u8868\u9762\u7279\u6027\u63d0\u4f9b\u4e86\u65b0\u601d\u8def\u3002<\/p>\n<p><strong>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n<p>\u7eb3\u7c73\u6750\u6599\u4ee5\u5176\u5c3a\u5bf8\u3001\u5f62\u72b6\u548c\u7ec4\u6210\u6548\u679c\uff0c\u5c55\u73b0\u51fa\u72ec\u7279\u7684\u7269\u7406\u6027\u80fd\uff0c\u8fd1\u51e0\u5341\u5e74\u6765\uff0c\u7eb3\u7c73\u6676\u4f53\uff08NCs\uff09\u5728\u751f\u7269\u533b\u5b66\u3001\u5149\u7535\u5b50\u5668\u4ef6\u3001\u50ac\u5316\u3001\u4f20\u611f\u5668\u3001\u65b0\u80fd\u6e90\u6280\u672f\u548c\u7eb3\u7c73\u590d\u5408\u6750\u6599\u7b49\u9886\u57df\u53d6\u5f97\u4e86\u5de8\u5927\u7684\u8fdb\u6b65\u3002\u76ee\u524d\uff0c\u9ad8\u8d28\u91cf\u7684NC\u901a\u5e38\u901a\u8fc7\u70ed\u5206\u89e3\u5728\u9ad8\u6cb8\u70b9\u6709\u673a\u6eb6\u5242\u4e2d\u5236\u9020\u3002\u6cb9\u9178\uff08OA\uff09\u548c\u6cb9\u80fa\uff08OAm\uff09\u4e3b\u8981\u7528\u4f5cNCs\u8868\u9762\u7684\u5c01\u7aef\u5242\u8fdb\u800c\u7a33\u5b9a\u5316\u3002\u7136\u800c\uff0c\u60f0\u6027\u70f7\u70c3\u4e0d\u80fd\u9002\u5e94\u5404\u79cd\u60c5\u51b5\uff0c\u8fdb\u4e00\u6b65\u7684\u8868\u9762\u6539\u6027\u662f\u5176\u5e94\u7528\u7684\u5fc5\u7136\u53d1\u5c55\u3002\u4e3a\u6b64\uff0c\u5df2\u7ecf\u5efa\u7acb\u4e86\u4e00\u4e9b\u7528\u4e8e\u8f6c\u5316\u548c\u5b98\u80fd\u5316\u758f\u6c34NCs\u7684\u65b9\u6cd5\uff0c\u5305\u62ec\u4e8c\u6c27\u5316\u7845\u6d82\u5c42\u3001\u914d\u4f53\u4ea4\u6362\u3001OA\u914d\u4f53\u7684\u6c27\u5316\u3001\u4e24\u4eb2\u6027\u5171\u805a\u7269\u9644\u7740\u548c\u70ef\u70c3\u590d\u5206\u89e3\u7b49\u3002\u7136\u800c\uff0c\u8fd9\u4e9b\u65b9\u6cd5\u5404\u5177\u5c40\u9650\u6027\u3002\u56e0\u6b64\uff0c\u5f00\u53d1\u4e00\u79cd\u7b80\u5355\u3001\u9ad8\u6548\u3001\u591a\u529f\u80fd\u7684\u5de5\u7a0bNC\u4ecd\u7136\u662f\u4e00\u4e2a\u5de8\u5927\u7684\u6311\u6218\u3002<\/p>\n<p>\u8fd1\u671f\uff0c\u6765\u81ea<strong>\u4e2d\u79d1\u9662\u957f\u6625\u5e94\u5316\u6240\u7684\u6797\u541b\u7814\u7a76\u5458\u3001\u7a0b\u5b50\u6cf3\u7814\u7a76\u5458\u00a0<\/strong>\u548c<strong>\u54c8\u5c14\u6ee8\u5de5\u7a0b\u5927\u5b66<\/strong>\u7684<strong>\u6768\u98d8\u840d\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u7b49\u4eba\u5728<strong>Advanced Materials<\/strong>\u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u5173\u4e8e\u7eb3\u7c73\u6676\u8868\u9762\u5b98\u80fd\u5316\u7684\u6587\u7ae0\uff0c\u9898\u4e3a\u201c<strong>Thiol\u2013Ene Click Reaction as a Facile and General Approach for Surface Functionalization of Colloidal Nanocrystals<\/strong>\u201d\u3002\u6587\u4e2d\u63cf\u8ff0\u4e86\u4e00\u79cd\u5229\u7528\u786b\u9187\u9009\u62e9\u53cd\u5e94\u5bf9NC\u8fdb\u884c\u8868\u9762\u5b98\u80fd\u5316\uff0c\u5b83\u53ef\u4ee5\u5728\u4e00\u4e2a\u5355\u4e00\u6b65\u9aa4\u5185\u5c06\u758f\u6c34\u6027NCs\u5feb\u901f\u8f6c\u5316\u4e3a\u6c34\u6eb6\u6027NC\uff081\u5c0f\u65f6\u5185\u5b8c\u6210\uff0c\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u4e0d\u5fc5\u9664\u53bb\u6c27\u6c14\u3001\u52a0\u70ed\u5904\u7406\uff0c\u4e5f\u4e0d\u4f1a\u7834\u574f\u539f\u59cb\u8868\u9762\u3002<\/p>\n<p><strong>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n<p><strong>\u56fe1 \u901a\u8fc7\u786b\u9187\u70ef\u952e\u5728NC\u4e0a\u63a5\u679dHS-PEG-R\u7684\u5408\u6210\u65b9\u6cd5\u53ca\u53cd\u5e94\u673a\u7406\u793a\u610f\u56fe<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-97894 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72471-18.png\" alt=\"\" width=\"700\" height=\"390\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72471-18.png 700w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72471-18-300x167.png 300w\" sizes=\"(max-width: 700px) 100vw, 700px\" \/><\/p>\n<p><strong>\u56fe2 \u4e0a\u8f6c\u6362\u53d1\u5149\u7eb3\u7c73\u9897\u7c92\uff08UCNP\uff09\u63a5\u679dHS-PEG1000\u524d\u540e\u56fe\u50cf<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-97895 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72472-19.png\" alt=\"\" width=\"700\" height=\"904\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72472-19.png 700w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72472-19-232x300.png 232w\" sizes=\"(max-width: 700px) 100vw, 700px\" \/><\/p>\n<p>\uff08A\uff09\u5177\u6709OA\u5c01\u7aef\u7684NaYF4\uff1aYb\uff0cTm @ NaYF4Yb UCNP\u7684TEM\u56fe\u50cf\uff1b<\/p>\n<p>\uff08B\uff09\u63a5\u679dHS-PEG1000\u540e\u7684TEM\u56fe\u50cf\uff1b<\/p>\n<p>\uff08C\uff09\u63a5\u679dHS-PEG1000\u524d\uff08\u5de6\uff09\u540e\uff08\u53f3\uff09UCNP\u5728\u6c34\u4e2d\u7684\u5206\u6563\u884c\u4e3a\u7684\u7167\u7247\uff1b<\/p>\n<p>\uff08D\uff09UCNPs-OA\uff08a\uff09\u548c\u63a5\u679dHS-PEG1000\uff08b\uff09\u5728N2\u6c14\u6c1b\u4e0b\u8fdb\u884c\u7684TGA\u66f2\u7ebf\u3002\uff1b<\/p>\n<p>\uff08E\uff09UCNP\u7684X\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\uff08XPS\uff09\uff1b<\/p>\n<p>\uff08F\uff09\u7528HS-PEG1000\u4fee\u9970\u524d\u540e\u7684\u9ad8\u5206\u8fa8\u7387S2p\u5cf0\u3002<\/p>\n<p><strong>\u56fe3 UCNP\u4e0a\u914d\u4f53\u5206\u5b50\u7684\u7ea2\u5916\u56fe\u50cf<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-97896 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72473-13.png\" alt=\"\" width=\"570\" height=\"244\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72473-13.png 570w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72473-13-300x128.png 300w\" sizes=\"(max-width: 570px) 100vw, 570px\" \/><\/p>\n<p>\uff08A\uff09<strong>a.<\/strong>OA\u7684UCNP\u7ea2\u5916\u5149\u8c31\uff1b<strong>b.<\/strong>HS-PEG1000\u7ea2\u5916\u5149\u8c31\uff1b<strong>c.<\/strong>\u901a\u8fc7\u786b\u9187\u9009\u62e9\u53cd\u5e94\u7684\u63a5\u679dHS-PEG1000\u7684UCNP\u7ea2\u5916\u5149\u8c31\u3002<\/p>\n<p>\uff08B\uff09\u653e\u5927\u6bd4\u8f83\u3002<\/p>\n<p><strong>\u56fe4 \u63a2\u7a76\u786b\u9187\u70ef\u952e\u70b9\u53cd\u5e94\u76841 H NMR\u5149\u8c31<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-97897 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72474-11.png\" alt=\"\" width=\"606\" height=\"725\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72474-11.png 606w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72474-11-251x300.png 251w\" sizes=\"(max-width: 606px) 100vw, 606px\" \/><\/p>\n<p>\uff08A\uff09\u5206\u6563\u5728CDCl3\u4e2d\u7684OA-\u5c01\u7aef\u7684NaYF4\u76841H NMR\u8c31\uff1b<\/p>\n<p>\uff08B\uff09\u901a\u8fc7\u786b\u9187-\u5355\u916f\u53cd\u5e94\uff0c\u7ecfHS-PEG1000\u4fee\u9970\u540e\u76841H NMR\u8c31\u3002<\/p>\n<p><strong>\u56fe5 \u786b\u9187\u70ef\u952e\u70b9\u53cd\u5e94\u7684\u8868\u9762\u6539\u6027\u65b9\u6cd5\u7684\u793a\u610f\u56fe<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-97898 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72475-7.png\" alt=\"\" width=\"700\" height=\"415\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72475-7.png 700w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72475-7-300x178.png 300w\" sizes=\"(max-width: 700px) 100vw, 700px\" \/><\/p>\n<p>\uff08A\uff09\u7528\u4e8eOAm\u5c01\u7aef\u7684Fe3O4 NC\uff1b<\/p>\n<p>\uff08B\uff09OAm \/ OA\u5c01\u7aef\u7684Cu9S5 NC\u548cOAm\u5c01\u7aef\u7684WS2\uff1b<\/p>\n<p>\uff08C\uff09Gd\u7eb3\u7c73\u7247\u3002 \u7167\u7247\u663e\u793a\u4e86NCs\u5728H2O\u548c\u5df1\u70f7\u6df7\u5408\u7269\u4e2d\u7684\u6539\u6027\u524d\u540e\u7684\u53ef\u6eb6\u6027\u3002<\/p>\n<p><strong>\u56fe6 UCNPs-OA\u548cUCNPs-PEG1000\u7684\u53d1\u5149\u7279\u6027\u56fe<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-97899 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72476-4.png\" alt=\"\" width=\"700\" height=\"805\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72476-4.png 700w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72476-4-261x300.png 261w\" sizes=\"(max-width: 700px) 100vw, 700px\" 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Ag-\u751f\u7269\u7d20\u7684\u6df7\u5408\u7269\u7684\u53d1\u5c04\u5f3a\u5ea6\uff09\u3002<\/p>\n<p><strong>\u56fe7 \u4e0a\u8f6c\u6362\u53d1\u5149\u5171\u632f\u80fd\u91cf\u8f6c\u79fb\uff08LRET\uff09\u7684\u8fc7\u7a0b\u7684\u793a\u610f\u56fe<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-97900 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72477-2.png\" alt=\"\" width=\"700\" height=\"451\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72477-2.png 700w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/08\/\u56fe\u72477-2-300x193.png 300w\" sizes=\"(max-width: 700px) 100vw, 700px\" 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href=\"http:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/adma.201604878\/full\" target=\"_blank\" rel=\"noopener\"> Thiol\u2013Ene Click Reaction as a Facile and General Approach\u00a0for Surface Functionalization of Colloidal Nanocrystals<\/a><\/strong><a href=\"http:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/adma.201604878\/full\">\uff08<\/a>Adv. 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