{"id":95608,"date":"2017-08-17T06:30:59","date_gmt":"2017-08-16T22:30:59","guid":{"rendered":"\/\/m.iemloyee.com\/?p=95608"},"modified":"2017-08-14T19:53:52","modified_gmt":"2017-08-14T11:53:52","slug":"%e4%b8%ad%e7%a7%91%e5%a4%a7%e4%bf%9e%e4%b9%a6%e5%ae%8fangew-chem-int-ed-%ef%bc%9a%e5%a4%a7%e8%a7%84%e6%a8%a1%e5%88%b6%e5%a4%87zns%c2%b7deta0-5%e4%bd%9c%e4%b8%ba%e7%a1%ab%e7%ba%b3%e7%b1%b3","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=95608","title":{"rendered":"\u4e2d\u79d1\u5927\u4fde\u4e66\u5b8fAngew. Chem. Int. Ed.\uff1a\u5927\u89c4\u6a21\u5236\u5907ZnS\u00b7(DETA)0.5\u4f5c\u4e3a\u786b\u7eb3\u7c73\u590d\u5408\u6750\u6599\u9634\u6781\u524d\u9a71\u4f53"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/span><\/p>\n

\u91d1\u5c5e\u786b\u5316\u7269-\u80fa\u6742\u5316\u7eb3\u7c73\u6750\u6599\u2014\u2014\u4f5c\u4e3a\u529f\u80fd\u6027\u65e0\u673a\u7eb3\u7c73\u6750\u6599\u524d\u9a71\u4f53\u2014\u2014\u5c55\u73b0\u51fa\u4f18\u5f02\u7684\u7279\u6027\u3002\u901a\u8fc7\u5c06\u6709\u673a\u80fa\u5206\u5b50\u5f15\u5165\u91d1\u5c5e\u786b\u5316\u7269\u7684\u5c42\u72b6\u4e3b\u4f53\u5185\uff0c\u53ef\u4ee5\u8c03\u8282\u5176\u7eb3\u7c73\u6750\u6599\u7269\u5316\u7279\u6027\uff1b\u8fd8\u53ef\u4ee5\u6539\u53d8\u6709\u673a\u80fa\u6210\u5206\uff0c\u5f71\u54cd\u91d1\u5c5e\u786b\u5316\u7269\u6676\u4f53\u751f\u957f\u65b9\u5411\u5f97\u5230\u9700\u6c42\u7684\u7cbe\u7ec6\u7eb3\u7c73\u7ed3\u6784\u3002\u7136\u800c\uff0c\u91d1\u5c5e\u786b\u5316\u7269-\u80fa\u6742\u5316\u7eb3\u7c73\u6750\u6599\u90fd\u662f\u901a\u8fc7\u6c34\u70ed\u6cd5\u6216\u8005\u6eb6\u5242\u70ed\u6cd5\u5236\u5907\uff0c\u65e0\u6cd5\u91cf\u4ea7\u4f7f\u5f97\u8be5\u6280\u672f\u53d1\u5c55\u53d7\u9650\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n

\u4e2d\u56fd\u79d1\u5b66\u6280\u672f\u5927\u5b66\u5316\u5b66\u7cfb\u4fde\u4e66\u5b8f\u6559\u6388\u548c\u59da\u5b8f\u658c\u6559\u6388<\/strong>\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u8fd1\u65e5\u5728\u56fd\u9645\u9876\u7ea7\u671f\u520aAngew. Chem. Int. Ed.<\/strong>\u53d1\u8868\u4e86\u9898\u4e3a\u201cLarge-Scale Syntheses of Zinc Sulfide\u00b7(Diethylenetriamine)0.5<\/sub> Hybrids as Precursors for Sulfur Nanocomposite Cathodes<\/strong>\u201d\u7684\u6587\u7ae0\u3002\u7531\u4e8e\u8be5\u7bc7\u8bba\u6587\u7814\u7a76\u5185\u5bb9\u7684\u91cd\u8981\u6027\uff0c\u5c06\u5176\u8bc4\u9009\u4e3aVIP(Very Important Paper)<\/strong>\u6587\u7ae0\u3002\u5728\u524d\u4eba\u57fa\u7840\u4e0a\uff0c\u8be5\u7814\u7a76\u53d1\u73b0\u4e00\u79cd\u7b80\u5355\u3001\u9ad8\u6548\u4e14\u53ef\u5927\u89c4\u6a21\u5236\u5907<\/strong>\u9ad8\u5ea6\u6709\u5e8f\u548c\u9ad8\u8d28\u91cf\u7684ZnS\u00b7(DETA)0.5<\/sub>\u6742\u5316\u7eb3\u7c73\u5e26\u548c\u7eb3\u7c73\u7247\u6676\u7684\u65b9\u6cd5\u2014\u2014\u6709\u673a\u80fa\u8f85\u52a9\u56de\u6d41\u6cd5\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

\u56fe 1. \u6eb6\u5242\u70ed\u6cd5\/\u56de\u6d41\u6cd5\u5236\u5907ZnS\u00b7(DETA)0.5<\/sub>\u6bd4\u8f83<\/h3>\n

\"\"<\/p>\n

a.<\/strong> \u6eb6\u5242\u70ed\u6cd5\u4e0e\u56de\u6d41\u6cd5\u53cd\u5e94\u7cfb\u7edf\u7684\u4e0d\u540c\uff1b<\/p>\n

b<\/strong>\u548cc.<\/strong> \u6eb6\u5242\u70ed\u6cd5\u548c\u56de\u6d41\u6cd5\u5236\u5907\u7684ZnS\u00b7(DETA)0.5<\/sub>\u7eb3\u7c73\u7247\u6676\u7684SEM\u56fe\u50cf\uff0c\u5185\u7f6e\u5c0f\u56fe\u4e3a\u4ea7\u54c1\u4ea7\u91cf\u5206\u522b\u4e3a10.04g\u548c15.18g\u3002<\/p>\n

\u56fe 2. \u4e0d\u540c\u6eb6\u5242\u6210\u5206\u4e0b\u56de\u6d41\u6cd5\u5236\u5907\u7684ZnS\u00b7(DETA)0.5<\/sub>\u7eb3\u7c73\u6750\u6599\u5f62\u8c8c<\/h3>\n

\"\"<\/p>\n

a-f.<\/strong> 220\u2103\uff0c\u4e0d\u540c\u6c34\u542b\u91cf\u4e0b(\u53bb\u79bb\u5b50\u6c34:DETA)\u5236\u5907\u7684ZnS\u00b7(DETA)0.5<\/sub>\u7eb3\u7c73\u6750\u6599\u7684TEM\u56fe\u7247,\u6807\u5c3a\uff1aa\uff1a500 nm\uff0cb-f\uff1a1 \u03bcm\u3002<\/p>\n

\u56fe 3. ZnS\u7eb3\u7c73\u5e26\u548c\u7eb3\u7c73\u7247\u6676\u7684\u8868\u5f81<\/h3>\n

\"\"<\/p>\n

a<\/strong>\u548cb.<\/strong> \u5236\u5907\u7684ZnS\u7eb3\u7c73\u5e26\u548c\u7eb3\u7c73\u7247\u6676TEM\u56fe\u7247\uff1b<\/p>\n

c.<\/strong> ZnS\u7eb3\u7c73\u5e26\u548c\u7eb3\u7c73\u7247\u6676\u7684\u7c89\u672bXRD\uff1b<\/p>\n

d.<\/strong> ZnS\u7eb3\u7c73\u5e26AFM\u56fe\u7247\uff1b<\/p>\n

e<\/strong>\u548cf.<\/strong> ZnS\u7eb3\u7c73\u5e26AFM\u56fe\u548cHRTEM\u56fe\u3002<\/p>\n

\u56fe 4. ZnS\u7eb3\u7c73\u7247\u6676\u7684\u4fee\u9970\u53ca\u5176\u5e94\u7528<\/h3>\n

\"\"<\/p>\n

a.<\/strong> ZnS@C\u7684HRTEM\u56fe\uff1b<\/p>\n

b<\/strong>\u548cc.<\/strong> S@C\u7684TEM\u548cTGA\uff1b<\/p>\n

d-g.<\/strong> \u4f5c\u4e3aLi-S\u7535\u6c60\u8d1f\u6781\u6027\u80fd\u4f18\u5f02\u7684S@C\/CNTs\/BCs\uff0cd\uff1a\u666e\u901a\u7167\u7247\uff0ce\uff1a\u6a2a\u65ad\u9762\u56fe\uff0cf\uff1a\u6a2a\u65ad\u9762\u7684SEM\u653e\u5927\u56fe\uff0cg\uff1a\u957f\u5faa\u73af\u5bff\u547d\u3002<\/p>\n

\u3010\u5c55\u671b\u3011<\/span><\/strong><\/p>\n

\u8be5\u5de5\u4f5c\u4ecb\u7ecd\u4e86\u6709\u673a\u80fa\u8f85\u52a9\u56de\u6d41\u5236\u5907\u6709\u5e8fZnS\u00b7(DETA)0.5<\/sub>\u6742\u5316\u7eb3\u7c73\u5e26\u548c\u7eb3\u7c73\u7247\u6676\u7684\u9ad8\u4ea7\u91cf\u65b9\u6cd5\u3002ZnS\u548cS@C\u90fd\u662f\u901a\u8fc7ZnS\u00b7(DETA)0.5<\/sub>\u4f5c\u4e3a\u524d\u9a71\u4f53\u5236\u5907\u5f97\u5230\uff0cS@C\/CNTs\/BCs\u5728S@C\u7eb3\u7c73\u6750\u6599\u7684\u57fa\u7840\u4e0a\u5f97\u5230\u5e76\u5c55\u73b0\u51fa\u9ad8\u7684\u6bd4\u8868\u9762\u5bb9\u91cf\u548c\u5faa\u73af\u7a33\u5b9a\u6027\uff0c\u8fdc\u8fdc\u9ad8\u4e8e\u5176\u4ed6S\/C\u590d\u5408\u6750\u6599\u4f5c\u4e3aLi-S\u7535\u6c60\u8d1f\u6781\u65f6\u7684\u6027\u80fd\u3002\u8fd9\u4e00\u5236\u5907\u65b9\u6cd5\u4e3a\u91d1\u5c5e\u786b\u5316\u7269-\u80fa\u6742\u5316\u6750\u6599\u7684\u5927\u89c4\u6a21\u5e94\u7528\u5f00\u8f9f\u4e86\u4e00\u6761\u65b0\u7684\u9053\u8def\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Large-Scale Syntheses of Zinc Sulfide\u00b7(Diethylenetriamine)0.5<\/sub><\/a> Hybrids as Precursors for Sulfur Nanocomposite Cathodes<\/a><\/span> (<\/strong>Angew. Chem. Int. Ed., 2017, DOI: 10.1002\/anie.201706199)<\/strong><\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7eb3\u7c73\u5b66\u672f\u7ec4 Mr_PSP \u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u7f16\u8f91\u6574\u7406\u3002<\/p>\n

\u6750\u6599\u725b\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u8fd9\u91cc\u6c47\u96c6\u4e86\u5404\u5927\u9ad8\u6821<\/span>\u7855\u535a\u751f\u3001\u4e00\u7ebf\u79d1\u7814\u4eba\u5458\u4ee5\u53ca\u884c\u4e1a\u4ece\u4e1a\u8005\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u6750\u6599\u4eba\u7f16\u8f91\u90e8<\/a><\/span>\u3002<\/p>\n

\u53c2\u4e0e\u65b0\u80fd\u6e90\u8bdd\u9898\u8ba8\u8bba\u8bf7\u52a0\u5165\u201c\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u6750\u6599\u4ea4\u6d41\u7fa4 422065952\u201d\u3002<\/p>\n

\u6750\u6599\u6d4b\u8bd5\uff0c\u6570\u636e\u5206\u6790\uff0c\u4e0a<\/strong>\u6d4b\u8bd5\u8c37<\/strong><\/a><\/span>\uff01<\/strong><\/p>\n","protected":false},"excerpt":{"rendered":"

\u3010\u5f15\u8a00\u3011 \u91d1\u5c5e\u786b\u5316\u7269-\u80fa\u6742\u5316\u7eb3\u7c73\u6750\u6599\u2014\u2014\u4f5c\u4e3a\u529f\u80fd\u6027\u65e0\u673a\u7eb3\u7c73\u6750\u6599\u524d\u9a71\u4f53\u2014\u2014\u5c55\u73b0\u51fa\u4f18\u5f02\u7684\u7279\u6027\u3002\u901a\u8fc7\u5c06\u6709\u673a\u80fa\u5206\u5b50\u5f15\u5165\u91d1\u5c5e\u786b\u5316\u7269\u7684\u5c42\u72b6\u4e3b\u4f53\u5185\uff0c\u53ef\u4ee5\u8c03\u8282\u5176\u7eb3\u7c73\u6750\u6599\u7269\u5316\u7279\u6027…<\/p>\n","protected":false},"author":3267,"featured_media":95609,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[215],"tags":[54,129],"class_list":["post-95608","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-jiedu","tag-making","tag-battery"],"_links":{"self":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/95608"}],"collection":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/users\/3267"}],"replies":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=95608"}],"version-history":[{"count":11,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/95608\/revisions"}],"predecessor-version":[{"id":96487,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/95608\/revisions\/96487"}],"wp:featuredmedia":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/media\/95609"}],"wp:attachment":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=95608"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=95608"},{"taxonomy":"post_tag","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=95608"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}