{"id":93316,"date":"2017-07-27T06:30:46","date_gmt":"2017-07-26T22:30:46","guid":{"rendered":"\/\/m.iemloyee.com\/?p=93316"},"modified":"2017-07-26T20:21:30","modified_gmt":"2017-07-26T12:21:30","slug":"npg-asia-mater-%e5%8f%af%e8%a7%81%e5%85%89%e9%a9%b1%e5%8a%a8%e5%8f%8c%e9%87%91%e5%b1%9eau-rh%e6%a0%b8%e5%a3%b3%e7%ba%b3%e7%b1%b3%e6%99%b6%e5%82%ac%e5%8c%96%e5%89%82%e9%ab%98%e6%95%88%e4%ba%a7","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=93316","title":{"rendered":"NPG Asia Mater.: \u53ef\u89c1\u5149\u9a71\u52a8\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u50ac\u5316\u5242\u9ad8\u6548\u4ea7\u6c22"},"content":{"rendered":"<p><span style=\"color: #0000ff;\"><strong>\u3010\u5f15\u8a00\u3011<\/strong><\/span><\/p>\n<p>\u6c22\u662f\u4e00\u79cd\u73af\u4fdd\u7684\u53ef\u518d\u751f\u80fd\u6e90\u8f7d\u4f53\uff0c\u5177\u6709\u5b89\u5168\u3001\u9ad8\u6548\u3001\u53ef\u6301\u7eed\u6027\u548c\u6e05\u6d01\u65e0\u6c61\u67d3\u7b49\u7279\u6027\u3002\u7531\u4e8e\u4f20\u7edf\u5316\u77f3\u80fd\u6e90\u9762\u4e34\u67af\u7aed\u7684\u5371\u673a\u548c\u4e25\u91cd\u7684\u6c61\u67d3\u95ee\u9898\uff0c\u6c22\u80fd\u6e90\u7684\u5f00\u53d1\u548c\u4f7f\u7528\u88ab\u5e7f\u6cdb\u5173\u6ce8\u3002\u76ee\u524d\uff0c\u57fa\u7840\u7814\u7a76\u4e2d\u5236\u6c22\u65b9\u5f0f\u4e3b\u8981\u6709\u7535\u89e3\u6c34\u5236\u6c22\u3001\u592a\u9633\u80fd\u5236\u6c22\u548c\u5316\u5b66\u5236\u6c22\u7b49\uff0c\u5747\u9700\u8981\u9ad8\u6d3b\u6027\u3001\u9ad8\u7a33\u5b9a\u6027\u50ac\u5316\u5242\uff0c\u56e0\u6b64\uff0c\u5f00\u53d1\u4f4e\u6210\u672c\u3001\u9ad8\u6548\u80fd\u7684\u5236\u6c22\u50ac\u5316\u5242\u662f\u80fd\u6e90\u3001\u50ac\u5316\u548c\u6750\u6599\u9886\u57df\u7684\u7814\u7a76\u70ed\u70b9<strong>\u3002<\/strong><\/p>\n<p><span style=\"color: #0000ff;\"><strong>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n<p>\u8fd1\u65e5\uff0c\u9655\u897f\u5e08\u8303\u5927\u5b66\u9648\u715c\u6559\u6388\u8bfe\u9898\u7ec4\u5236\u5907\u51fa\u7531\u8d85\u8584Rh\u7eb3\u7c73\u7247\u4e3a\u58f3\u7684\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u3002\u57fa\u4e8e\u539f\u5b50\u7ea7\u539a\u5ea6\u4e8c\u7ef4Rh\u7eb3\u7c73\u7247\u7684\u8d85\u8584\u7ed3\u6784\uff0c\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u5177\u6709\u8f83\u9ad8\u7684\u6bd4\u8868\u9762\u79ef\u548c\u539f\u5b50\u5229\u7528\u7387\uff0c\u5176\u5bf9\u6c34\u5408\u80bc\u6c34\u89e3\u4ea7\u6c22\u8868\u73b0\u51fa\u975e\u5e38\u9ad8\u7684\u6d3b\u6027\u3002\u5728\u5149\u7167\u6761\u4ef6\u4e0b\uff0c\u4f9d\u8d56\u4e8eAu\u4e8c\u5341\u9762\u4f53\u6838\u7684\u5c40\u57df\u8868\u9762\u7b49\u79bb\u5b50\u4f53\u5171\u632f\uff08LSPR\uff09\u7279\u6027\uff0c\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u663e\u793a\u51fa\u5149\u589e\u5f3a\u7684\u50ac\u5316\u6d3b\u6027\u3002\u8be5\u9879\u5de5\u4f5c\u4ee5\u201c<a href=\"http:\/\/www.nature.com\/am\/journal\/v9\/n7\/full\/am2017114a.html\">Bimetallic AuRh nanodendrites consisting of Au icosahedroncores and atomically ultrathin Rh nanoplate shells: synthesis and light-enhanced catalytic activity<\/a>\u201d\u4e3a\u9898\u5728\u7ebf\u53d1\u8868\u4e8eNature\u51fa\u7248\u96c6\u56e2\u65d7\u4e0b\u5b66\u672f\u520a\u7269 <strong><em>NPG Asia Materials <\/em><\/strong>(NPG Asia Mater. 9, e407. DOI: 10.1038\/am.2017.114.)\u3002\u8be5\u8bba\u6587\u7531\u9655\u897f\u5e08\u8303\u5927\u5b66\u4f5c\u4e3a\u552f\u4e00\u7814\u7a76\u5355\u4f4d\u72ec\u7acb\u5b8c\u6210\uff0c\u7b2c\u4e00\u4f5c\u8005\u662f\u9655\u897f\u5e08\u8303\u5927\u5b66\u6750\u6599\u79d1\u5b66\u4e0e\u5de5\u7a0b\u5b66\u9662\u7855\u58eb\u7814\u7a76\u751f\u5eb7\u6c38\u5f3a\u540c\u5b66\uff0c\u901a\u8baf\u4f5c\u8005\u4e3a\u9655\u897f\u5e08\u8303\u5927\u5b66\u6750\u6599\u79d1\u5b66\u4e0e\u5de5\u7a0b\u5b66\u9662\u91d1\u666e\u519b\u526f\u6559\u6388\u548c\u9648\u715c\u6559\u6388\u3002<\/p>\n<p><span style=\"color: #0000ff;\"><strong>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n<p><strong>\u56fe1. <\/strong><strong>Au@Rh<\/strong><strong>\u53cc\u91d1\u5c5e\u6838\u58f3<\/strong><strong>\u7eb3\u7c73\u7ed3\u6784\u7269\u7684\u7269\u7406\u8868\u5f81<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-93317\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f1.jpg\" alt=\"\" width=\"680\" height=\"686\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f1.jpg 680w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f1-150x150.jpg 150w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f1-297x300.jpg 297w\" sizes=\"(max-width: 680px) 100vw, 680px\" \/><\/p>\n<p>\uff08a\uff09Au @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684\u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff09\u56fe\u50cf\uff0c\u63d2\u56fe\uff1a\u653e\u5927SEM\u56fe\u50cf\u3002<\/p>\n<p>\uff08b\uff09Au @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684EDX\u80fd\u8c31\u5206\u6790\u3002<\/p>\n<p>\uff08c\uff09Au @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684Au 4f\u548cRh 3d XPS\u5149\u8c31\u3002<\/p>\n<p>\uff08d\uff09Au @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684XRD\u56fe\u3002<\/p>\n<p>\uff08e\uff09\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684\u9ad8\u5206\u8fa8\u7387TEM\uff08HRTEM\uff09\u56fe\u50cf\u3002<\/p>\n<p>\uff08f\uff09\u9ad8\u89d2\u5ea6\u73af\u5f62\u6697\u573a\u626b\u63cfTEM\u56fe\u50cf\uff0c\u4ee5\u53ca\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u5404\u5143\u7d20\u7684EDX\u9762\u626b\u63cf\u548c\u7ebf\u626b\u63cf\u56fe\u3002<\/p>\n<p>\uff08g\uff09\u8d85\u8584Rh\u7eb3\u7c73\u7247\u58f3\u5c42\u653e\u5927\u7684HRTEM\u56fe\u50cf\u3002\u9876\u90e8\u63d2\u56fe\uff1a\u8fdb\u4e00\u6b65\u653e\u5927HRTEM\u56fe\u50cf\uff1b\u5e95\u90e8\u63d2\u56fe\uff1a\u76f8\u5e94\u7684\u5085\u91cc\u53f6\u53d8\u6362\uff08FFT\uff09\u56fe\u50cf\u3002<\/p>\n<p>\uff08h\uff09\u8d85\u8584Rh\u7eb3\u7c73\u7247\u7684HRTEM\u56fe\u3002<\/p>\n<p>\uff08i\uff09\u901a\u8fc7\u5f3a\u8d85\u58f0\u5904\u7406\u83b7\u5f97\u7684Rh\u7eb3\u7c73\u7247\u7684\u539f\u5b50\u529b\u663e\u5fae\u955c\u56fe\u50cf\u3002<\/p>\n<p><strong>\u56fe2. Au @ Rh<\/strong><strong>\u6838\u58f3\u7eb3\u7c73\u6676\u7684\u5f62\u6210\u673a\u7406<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-93318\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f2.jpg\" alt=\"\" width=\"680\" height=\"791\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f2.jpg 680w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f2-258x300.jpg 258w\" sizes=\"(max-width: 680px) 100vw, 680px\" \/><\/p>\n<p>\uff08a\uff09UV-vis\u5149\u8c31\uff0c\u63d2\u56fe\uff1a\u5c40\u90e8\u653e\u5927\u7684\u7d2b\u5916\u5149\u8c31\u3002<\/p>\n<p>\uff08b\uff09\u4e0d\u540c\u65f6\u95f4\u5b9e\u9645\u53cd\u5e94\u4f53\u7cfb\u7684\u7167\u7247\u3002<\/p>\n<p>\uff08c\uff09TEM\u56fe\u50cf\u548c\uff08d\uff09\u76f8\u5bf9\u5e94\u76840.5\uff0c1\uff0c2\u548c6\u5c0f\u65f6\u53d6\u51fa\u7684\u53cd\u5e94\u4e2d\u95f4\u4f53\u7684XRD\u56fe\u8c31\u3002<\/p>\n<p>\uff08e\uff09\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684\u5f62\u6210\u8fc7\u7a0b\u793a\u610f\u56fe\u3002<\/p>\n<p><strong>\u56fe<\/strong><strong>3. \u53cc<\/strong><strong>\u91d1\u5c5eAu @ Rh<\/strong><strong>\u6838\u58f3\u7eb3\u7c73<\/strong><strong>\u6676\u7684\u50ac\u5316\u6027\u80fd<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-93319\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f4.jpg\" alt=\"\" width=\"680\" height=\"584\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f4.jpg 680w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/07\/am2017114f4-300x258.jpg 300w\" sizes=\"(max-width: 680px) 100vw, 680px\" \/><\/p>\n<p>\uff08a\uff09\u5728\u975e\u5149\u7167\u6761\u4ef6\u4e0b\uff0c\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\uff0c\u5546\u4e1aRh\u9ed1\u548c\u5355\u91d1\u5c5eRh\u7eb3\u7c73\u6676\u7684\u50ac\u5316\u6c34\u5408\u80bc\u4ea7\u6c22\u6027\u80fd\u3002\u63d2\u56fe\uff1a\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\uff0c\u5546\u4e1aRh\u9ed1\u548c\u5355\u91d1\u5c5eRh\u7eb3\u7c73\u6676\u7684\u50ac\u5316\u6c34\u5408\u80bc\u4ea7\u6c22\u7684TOF\u503c\u3002<\/p>\n<p>\uff08b\uff09\u5728\u975e\u5149\u7167\u6761\u4ef6\u4e0b\uff0c\u5206\u522b\u4e8e30\u2103\uff0c40\u2103\u548c50\u2103\u4e0b\uff0c\u5bf9\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684\u4ea7\u6c22\u4f53\u79ef-\u65f6\u95f4\u66f2\u7ebf\u3002\u63d2\u56fe\uff1a\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\uff0cln TOF\u4e0e1 \/ T\u7684\u5173\u7cfb\u66f2\u7ebf\u3002<\/p>\n<p>\uff08c\uff09\u572830\u2103\uff0c\u6709\u548c\u6ca1\u6709\u5149\u7167\u5c04\u7684\u60c5\u51b5\u4e0b\uff0c\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u7684\u50ac\u5316\u6c34\u5408\u80bc\u4ea7\u6c22\u6027\u80fd\u3002\u63d2\u56fe\uff1a\u76f8\u5bf9\u5e94\u7684\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u50ac\u5316\u6c34\u5408\u80bc\u4ea7\u6c22\u7684TOF\u503c\u3002<\/p>\n<p>\uff08d\uff09\u572830\u00b0C\u7684\u5149\u7167\u5c04\u6761\u4ef6\u4e0b\uff0c\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\u50ac\u5316\u6c34\u5408\u80bc\u4ea7\u6c22\u7684\u5faa\u73af\u8010\u4e45\u6027\u6d4b\u8bd5\u3002<\/p>\n<p><span style=\"color: #0000ff;\"><strong>\u3010\u5c55<\/strong><strong>\u671b<\/strong><strong>\u3011<\/strong><\/span><\/p>\n<p>Au\u7684\u5c40\u57df\u8868\u9762\u7b49\u79bb\u5171\u632f\uff08LSPR\uff09\u7279\u6027\u4e00\u76f4\u5907\u53d7\u5173\u6ce8\uff0c\u5236\u5907\u53cc\u91d1\u5c5eAu @ Rh\u6838\u58f3\u7eb3\u7c73\u6676\uff0c\u501f\u52a9\u8d85\u8584\u7684Rh\u7eb3\u7c73\u7247\uff0c\u4e0d\u4ec5\u53ef\u4ee5\u63d0\u9ad8Rh\u7684\u5229\u7528\u7387\uff0c\u6709\u6548\u5730\u63d0\u4f9b\u66f4\u591a\u7684\u50ac\u5316\u6d3b\u6027\u4f4d\u70b9\uff0c\u800c\u4e14\u53ef\u4ee5\u901a\u8fc7Au\u7684LSPR\u7279\u6027\u4ea7\u751f\u5149\u589e\u5f3a\u7684\u50ac\u5316\u6d3b\u6027\uff0c\u8fdb\u4e00\u6b65\u63d0\u9ad8\u4ea7\u6c22\u6027\u80fd\u7684\u540c\u65f6\uff0c\u7f13\u89e3\u5728\u5faa\u73af\u8fc7\u7a0b\u4e2d\u7eb3\u7c73\u9897\u7c92\u7684\u4f53\u79ef\u81a8\u80c0\uff0c\u56e0\u6b64\u8be5\u6838\u58f3\u7ed3\u6784\u5c06\u4e30\u5bcc\u548c\u62d3\u5c55Au\u548cRh\u7684\u5e94\u7528\u9014\u5f84\u3002<\/p>\n<p><strong>\u539f\u6587\u94fe\u63a5\uff1a<\/strong><a href=\"http:\/\/www.nature.com\/am\/journal\/v9\/n7\/full\/am2017114a.html\">Bimetallic AuRh nanodendrites consisting of Au icosahedron cores and atomically ultrathin Rh nanoplate shells: synthesis and light-enhanced catalytic activity<\/a> (<em>NPG Asia Materials<\/em> (2017) <strong>9<\/strong>, e407; doi:10.1038\/am.2017.114)<\/p>\n<p><span style=\"color: #0000ff;\"><strong>\u3010\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n<p><a href=\"http:\/\/clxy.snnu.edu.cn\/home\/showjs\/386\"><strong>\u9648\u715c<\/strong><\/a>\u6559\u6388\uff0c\u9655\u897f\u5e08\u8303\u5927\u5b66\u6750\u6599\u79d1\u5b66\u4e0e\u5de5\u7a0b\u5b66\u9662\u5148\u8fdb\u80fd\u6e90\u8f6c\u5316\u6750\u6599\u4e0e\u5668\u4ef6\u521b\u65b0\u56e2\u961f\u6838\u5fc3\u6210\u5458\u3002\u957f\u671f\u81f4\u529b\u4e8e\u57fa\u4e8e\u8d35\u91d1\u5c5e\u7eb3\u7c73\u6676\u7684\u5f62\u8c8c\u63a7\u5236\u548c\u754c\u9762\u7ed3\u6784\/\u50ac\u5316\u6d3b\u6027\u76f8\u5173\u7684\u7814\u7a76\uff0c\u4f5c\u4e3a\u7b2c\u4e00\/\u901a\u8baf\u4f5c\u8005\u5728<em>Nano Energy, NPG Asia Materials, ACS Catalysis, Scientific Reports, Chemistry\u2013A European Journal, Nanoscale, Journal of Materials Chemistry A, Nano Research,<\/em> <em>ACS Applied Materials &amp; Interfaces<\/em>,<em> The Journal of Physical Chemistry C, Langmuir<\/em>\u7b49\u671f\u520a\u53d1\u8868SCI\u8bba\u658780\u4f59\u7bc7(\u88ab\u5f152400\u4f59\u6b21\uff0cH-index\u4e3a30\uff0ci10-index\u4e3a67)\uff0c10\u7bc7\u8bba\u6587\u5165\u9009ESI\u9ad8\u88ab\u5f15\u8bba\u6587(<em>J. Power Sources <\/em>2010, 195, 4129; <em>Int. J. Hydrogen Energy<\/em>. 2010, 35, 10109; <em>Int. J. Hydrogen Energy<\/em>. 2012, 37, 2993; <em>Appl. Catal. B: Environ. <\/em>2013, 129, 394; <em>J. Phys. Chem. C.<\/em> 2013, 117, 9826; <em>CrystEngComm<\/em> 2014, 16, 1606; <em>Chem. Eur. J.<\/em>2014, 20, 585; <em>ACS Appl. Mater. Interfaces <\/em>2014, 6, 7301; <em>Nano Energy <\/em>2015, 12, 824; <em>Nano Res<\/em>. 2016, 9, 755)\u3002\u8fd9\u4e00\u7cfb\u5217\u754c\u9762\u7ed3\u6784\/\u50ac\u5316\u6d3b\u6027\u76f8\u5173\u7814\u7a76\u7279\u8272\u9c9c\u660e\uff0c\u53d7\u5230\u56fd\u9645\u540c\u884c\u7684\u5e7f\u6cdb\u8ba4\u53ef\uff0c\u76f8\u7ee7\u53d7\u5230<em>Journal of Energy Chemistry<\/em>\u3001<em>Journal of Materials Research<\/em>\u548c<em>Science Bulletin<\/em>\u7b49\u671f\u520a\u9080\u8bf7\u64b0\u5199\u4e13\u9898\u6587\u7ae0\u548c\u7ec4\u7ec7\u4e13\u520a\u53d1\u8868\u3002<\/p>\n<p><span style=\"color: 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