{"id":88200,"date":"2017-06-27T06:30:35","date_gmt":"2017-06-26T22:30:35","guid":{"rendered":"\/\/m.iemloyee.com\/?p=88200"},"modified":"2017-06-26T15:05:55","modified_gmt":"2017-06-26T07:05:55","slug":"%e3%80%90%e6%8a%95%e7%a8%bf%e5%be%85%e5%ae%9a%e3%80%91%e8%83%a1%e5%8a%b2%e6%9d%be%ef%bc%86%e9%ab%98%e5%b3%b0jacs%ef%bc%9a%e5%be%ae%e8%a7%82%e5%bd%a2%e8%b2%8c%e5%92%8c%e7%94%b5%e5%ad%90%e7%bb%93","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=88200","title":{"rendered":"\u80e1\u52b2\u677e\uff06\u9ad8\u5cf0JACS\uff1a\u5fae\u89c2\u5f62\u8c8c\u548c\u7535\u5b50\u7ed3\u6784\u53cc\u91cd\u8c03\u63a7\u4f7f\u78b1\u5f0f\u78b3\u9178\u76d0\u7c7b\u6750\u6599\u53ef\u7528\u4e8e\u9ad8\u6548\u7535\u50ac\u5316\u5168\u6c34\u5206\u89e3"},"content":{"rendered":"

\"\"
\n <\/strong>\u6750\u6599\u4eba\u9996\u5c4a\u79d1\u6280\u8d44\u8baf\u5199\u4f5c\u5927\u8d5b\u81ea5\u670813\u65e5\u53d1\u5e03\u5f81\u7a3f\u901a\u77e5\u4ee5\u6765\uff08\u53c2\u8d5b\u8be6\u60c5\u8bf7\u6233\u6211<\/a>\uff09\u53d7\u5230\u8bfb\u8005\u4eec\u7684\u5e7f\u6cdb\u5173\u6ce8\u3002\u611f\u8c22\u652f\u6301\u5355\u4f4dTaylor\u00a0&\u00a0Francis\u00a0Group\uff0c\u79d1\u5b66\u51fa\u7248\u793e\uff0cMDPI\uff0cNational Science Review\uff0cChinese Science Bulletin\uff0cScience China Materials\uff0cScience China Chemistry \uff0cNano-Micro Letters\u5bf9\u672c\u6b21\u5927\u8d5b\u7684\u652f\u6301\uff01\u672c\u6587\u7531\u4e2d\u56fd\u79d1\u5b66\u9662\u5316\u5b66\u7814\u7a76\u6240\u6c5f\u6587\u6770\u535a\u58eb\u6295\u7a3f\u3002<\/p>\n

\u3010\u5f15\u8a00\u3011<\/strong><\/span><\/p>\n

\u80fd\u6e90\u4f5c\u4e3a\u4eba\u7c7b\u793e\u4f1a\u751f\u4ea7\u6d3b\u52a8\u7684\u57fa\u77f3\uff0c\u662f\u751f\u4ea7\u529b\u53d1\u5c55\u7684\u6700\u4e3b\u8981\u63a8\u52a8\u529b\u3002\u5f00\u53d1\u65b0\u578b\u53ef\u6301\u7eed\u80fd\u6e90\u662f\u89e3\u51b3\u5de8\u5927\u80fd\u6e90\u9700\u6c42\u4ee5\u53ca\u4f7f\u7528\u4f20\u7edf\u78b3\u57fa\u80fd\u6e90\u5f15\u8d77\u7684\u73af\u5883\u95ee\u9898\u7684\u5fc5\u7531\u4e4b\u8def\u3002\u6c22\u80fd\u662f\u4e00\u79cd\u7406\u60f3\u7684\u80fd\u6e90\u8f7d\u4f53\uff0c\u5177\u6709\u80fd\u91cf\u5bc6\u5ea6\u9ad8\u3001\u53ef\u5faa\u73af\u5229\u7528\u3001\u7eff\u8272\u73af\u4fdd\u7b49\u4f18\u70b9\u3002\u7535\u89e3\u6c34\u7531\u4e8e\u73af\u5883\u53cb\u597d\u3001\u4ea7\u54c1\u7eaf\u5ea6\u9ad8\u4ee5\u53ca\u65e0\u78b3\u6392\u653e\u7b49\u4f18\u70b9\uff0c\u5df2\u6210\u4e3a\u6700\u5177\u6709\u5e94\u7528\u524d\u666f\u7684\u7eff\u8272\u5236\u6c22\u65b9\u6cd5\u4e4b\u4e00\u3002\u4f46\u9650\u5236\u7535\u89e3\u6c34\u5927\u89c4\u6a21\u5e94\u7528\u7684\u6700\u91cd\u8981\u74f6\u9888\u662f\u5982\u4f55\u5927\u5e45\u964d\u4f4e\u5176\u7535\u80fd\u6d88\u8017\uff0c\u56e0\u800c\u964d\u4f4e\u5236\u6c22\u6210\u672c<\/strong>\u3002\u5176\u5173\u952e\u662f\u5982\u4f55\u964d\u4f4e\u7535\u6781\u4e0a\u9633\u6781\u6790\u6c27\u53cd\u5e94\u548c\u9634\u6781\u6790\u6c22\u53cd\u5e94\u7684\u8fc7\u7535\u4f4d\uff0c\u5b9e\u73b0\u5728\u4f4e\u7535\u4f4d\u4e0b\u7684\u5927\u7535\u6d41\u4ea7\u6c22<\/strong>\u3002\u8fc4\u4eca\u4e3a\u6b62\uff0c\u8d35\u91d1\u5c5e\u6750\u6599\u88ab\u516c\u8ba4\u4e3a\u4f18\u5f02\u7684\u6790\u6c27\u548c\u6790\u6c27\u50ac\u5316\u5242\uff0c\u4f46\u5176\u8f83\u9ad8\u7684\u6210\u672c\u548c\u8d44\u6e90\u532e\u4e4f\u7684\u7f3a\u70b9\u9650\u5236\u4e86\u8fd9\u4e9b\u6750\u6599\u7684\u5e7f\u6cdb\u5e94\u7528\u3002\u56e0\u6b64\uff0c\u53d1\u5c55\u53ef\u66ff\u4ee3\u7684\u5ec9\u4ef7\u3001\u6613\u5236\u5907\u4e14\u9ad8\u6548\u7684\u975e\u8d35\u91d1\u5c5e\u7535\u89e3\u6c34\u50ac\u5316\u5242\u6210\u4e3a\u8fd1\u51e0\u5e74\u7684\u7814\u7a76\u70ed\u70b9\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n

\u78b1\u5f0f\u78b3\u9178\u76d0\u5236\u5907\u65b9\u6cd5\u7b80\u5355\u3001\u7ecf\u6d4e\u3001\u73af\u4fdd\uff0c\u4f46\u5176\u7535\u50ac\u5316\u5206\u89e3\u6c34\u7684\u6027\u80fd\u5f88\u5dee\u3002\u8fd1\u65e5\uff0c\u4e2d\u56fd\u79d1\u5b66\u9662\u5316\u5b66\u7814\u7a76\u6240\u80e1\u52b2\u677e\u7814\u7a76\u5458\u8bfe\u9898\u7ec4<\/strong>\u4e0e\u5b89\u5fbd\u5e08\u8303\u5927\u5b66\u9ad8\u5cf0\u6559\u6388\u7814\u7a76\u7ec4<\/strong>\u5171\u540c\u7814\u7a76\u53d1\u73b0\uff0c\u901a\u8fc7\u5411\u78b1\u5f0f\u78b3\u9178\u94b4\u4e2d\u5f15\u5165\u9530\uff0c\u5b9e\u73b0\u5bf9\u5176\u5fae\u89c2\u5f62\u8c8c\u548c\u7535\u5b50\u7ed3\u6784\u7684\u53cc\u91cd\u8c03\u63a7<\/strong>\uff0c\u53ef\u4ee5\u5927\u5e45\u5ea6\u63d0\u5347\u5176\u7535\u89e3\u6c34\u50ac\u5316\u6027\u80fd\uff0c\u4f7f\u539f\u672c\u6ca1\u6709\u5e94\u7528\u524d\u666f\u7684\u78b1\u5f0f\u78b3\u9178\u76d0\u7c7b\u6750\u6599\u6210\u4e3a\u53ef\u4e0e\u6700\u8fd1\u62a5\u9053\u7684\u9ad8\u6027\u80fd\u786b\u5316\u7269\uff0c\u78f7\u5316\u7269\u7b49\u5ab2\u7f8e\u7684\u3001\u53ef\u5728\u5927\u7535\u6d41\u4e0b\u5de5\u4f5c\u7684\u65b0\u578b\u53cc\u529f\u80fd\u5168\u6c34\u5206\u89e3\u7535\u50ac\u5316\u5242<\/strong>\uff0c\u76f8\u5173\u6210\u679c\u53d1\u8868\u4e8eJournal of the American Chemical Society\u6742\u5fd7\u4e0a\u3002<\/p>\n

\u7814\u7a76\u4eba\u5458\u5229\u7528\u4e00\u6b65\u6c34\u70ed\u6cd5\uff0c\u76f4\u63a5\u5728\u6ce1\u6cab\u954d\u57fa\u5e95\u4e0a\u751f\u957f\u4e86\u9530\u63ba\u6742\u7684\u78b1\u5f0f\u78b3\u9178\u94b4\u7eb3\u7c73\u7247\u9635\u5217\uff0c\u4e0e\u5df2\u62a5\u9053\u7684\u786b\u5316\u7269\u3001\u7852\u5316\u7269\u3001\u78f7\u5316\u7269\u7b49\u9ad8\u6548\u7684\u50ac\u5316\u5242\u76f8\u6bd4\uff0c\u5236\u5907\u5de5\u827a\u7b80\u5355\u3001\u7ecf\u6d4e\u3001\u7eff\u8272\u65e0\u6c61\u67d3\uff0c\u6613\u4e8e\u5927\u89c4\u6a21\u751f\u4ea7\u3002\u5c06\u6240\u5f97\u6750\u6599\u7528\u4f5c\u6790\u6c27\u50ac\u5316\u5242\uff0c\u572830 mA\/cm2<\/sup>\u5904\u7684\u8fc7\u7535\u4f4d\u4ec5\u4e3a294 mV\uff0c\u663e\u8457\u4f18\u4e8e\u6b64\u524d\u62a5\u9053\u7684\u8be5\u7c7b\u6750\u6599\u7684\u6790\u6c27\u50ac\u5316\u6027\u80fd\u3002\u540c\u65f6\uff0c\u901a\u8fc7\u8fd9\u79cd\u53cc\u91cd\u8c03\u63a7\u8fd8\u5728\u8fd9\u7c7b\u6750\u6599\u4e0a\u9996\u6b21\u5b9e\u73b0\u4e86\u4f18\u5f02\u7684\u6790\u6c22\u50ac\u5316\u6027\u80fd\u3002\u572810 mA\/cm2<\/sup>\u5904\u7684\u8fc7\u7535\u4f4d\u4ec5\u4e3a180 mV\u3002\u8fdb\u4e00\u6b65\u5c06\u6240\u5236\u5907\u7684\u9530\u63ba\u6742\u78b1\u5f0f\u78b3\u9178\u94b4\u4f5c\u4e3a\u65b0\u578b\u53cc\u529f\u80fd\u7535\u6781\u7ec4\u88c5\u6210\u5168\u6c34\u5206\u89e3\u88c5\u7f6e\uff0c\u572810 mA\/cm2<\/sup>\u5904\u7684\u69fd\u538b\u4ec5\u4e3a1.68 V\u3002\u7814\u7a76\u4eba\u5458\u8fd8\u53d1\u73b0\uff0c\u4e0d\u540c\u9530\u6bd4\u4f8b\u63ba\u6742\u53ef\u4ee5\u6709\u6548\u8c03\u63a7\u78b1\u5f0f\u78b3\u9178\u94b4\u7684\u5f62\u8c8c\uff0c\u4ece\u800c\u66b4\u9732\u66f4\u591a\u7684\u50ac\u5316\u6d3b\u6027\u4f4d\u6570\u91cf\uff0c\u5e76\u4e14\u6709\u52a9\u4e8e\u7ef4\u6301\u5176\u4e0e\u57fa\u5e95\u7262\u56fa\u63a5\u89e6\uff0c\u4f5c\u4e3a\u6790\u6c27\u50ac\u5316\u5242\uff0c\u5728\u8fc7\u7535\u4f4d\u4e3a462 mV\u5904\u53ef\u7a33\u5b9a\u8f93\u51fa1000 mA\/cm2<\/sup>\u3002\u6b64\u5916\uff0c\u5b9e\u9a8c\u548c\u7406\u8bba\u8ba1\u7b97\u90fd\u8bc1\u5b9e\uff0c\u9530\u5143\u7d20\u7684\u5f15\u5165\u8c03\u63a7\u4e86\u78b1\u5f0f\u78b3\u9178\u94b4\u4e2d\u94b4\u5143\u7d20\u7684\u7535\u5b50\u7ed3\u6784\uff0c\u4ece\u800c\u52a0\u901f\u4e86\u6790\u6c22\u548c\u6790\u6c27\u7684\u7535\u50ac\u5316\u8fc7\u7a0b\u3002\u8be5\u5de5\u4f5c\u901a\u8fc7\u8c03\u63a7\u50ac\u5316\u5242\u7684\u5fae\u89c2\u5f62\u8c8c\u548c\u7535\u5b50\u7ed3\u6784\uff0c\u5927\u5e45\u5ea6\u63d0\u9ad8\u4e86\u6d3b\u6027\u8f83\u4f4e\u6750\u6599\u7684\u50ac\u5316\u6d3b\u6027\uff0c\u62d3\u5bbd\u4e86\u7535\u89e3\u6c34\u50ac\u5316\u5242\u7684\u9009\u62e9\u8303\u56f4\uff0c\u6709\u52a9\u4e8e\u7406\u89e3\u50ac\u5316\u5242\u7684\u6784\u6548\u5173\u7cfb\uff0c\u5e76\u4e3a\u5f00\u53d1\u65b0\u578b\u3001\u9ad8\u6548\u3001\u4f4e\u6210\u672c\u7535\u50ac\u5316\u5242\u63d0\u4f9b\u4e86\u5d2d\u65b0\u7684\u601d\u8def\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

\u56fe<\/strong>1 <\/strong>\u50ac\u5316\u5242\u7684\u7269\u76f8\u5206\u6790<\/strong><\/span><\/p>\n

\"\"<\/p>\n

\u50ac\u5316\u5242\u7684XRD\u8c31\u56fe\u3002<\/p>\n

\u56fe<\/strong>2<\/strong>\u50ac\u5316\u5242\u7684\u5f62\u8c8c\u5206\u6790<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a) CoCH\u7684SEM\u56fe\u3002<\/p>\n

(b) Co1.5<\/sub>Mn0.5<\/sub>CH\u7684SEM\u56fe\u3002<\/p>\n

(c) Co1<\/sub>Mn1<\/sub>CH\u7684SEM\u56fe\u3002<\/p>\n

(d) Co0.5<\/sub>Mn1.5<\/sub>CH\u7684SEM\u56fe\u3002<\/p>\n

(e) MnCO3<\/sub>\u7684SEM\u56fe\u3002<\/p>\n

(f) Co1<\/sub>Mn1<\/sub>CH\u7684TEM\u56fe\uff0c\u63d2\u56fe\u662f\u7ea2\u6846\u5904\u653e\u5927\u7684\u9ad8\u500dTEM\u56fe\u3002<\/p>\n

\u56fe<\/strong>3 <\/strong>\u4e0d\u540c\u50ac\u5316\u5242\u7684\u50ac\u5316\u6d3b\u6027\u7684\u6bd4\u8f83\u53ca\u7a33\u5b9a\u6027\u6d4b\u8bd5<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a) Cox<\/sub>Mny<\/sub>CH\u6837\u54c1\u7684\u7535\u5316\u5b66\u6d3b\u6027\u9762\u79ef\u4e0eCo\/Mn\u6bd4\u4f8b\u7684\u5173\u7cfb\u56fe\u3002<\/p>\n

(b) Cox<\/sub>Mny<\/sub>CH\u6837\u54c1\u7684\u6790\u6c27\u6781\u5316\u66f2\u7ebf\u3002<\/p>\n

(c) Cox<\/sub>Mny<\/sub>CH\u6837\u54c1\u7684\u6790\u6c22\u6781\u5316\u66f2\u7ebf\u3002<\/p>\n

(d) Co1<\/sub>Mn1<\/sub>CH\u6837\u54c1\u7684\u6790\u6c27\u4e0e\u6790\u6c22\u7a33\u5b9a\u6027\u66f2\u7ebf\u3002<\/p>\n

\u56fe<\/strong>4 <\/strong>\u79bb\u5b50\u4ea4\u6362\u6cd5\u7814\u7a76<\/strong>Mn<\/strong>\u5bf9<\/strong>Co<\/strong>\u7535\u5b50\u7ed3\u6784\u7684\u5f71\u54cd\u53ca\u7406\u8bba\u8ba1\u7b97\u7ed3\u679c<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a) CoMnCH-ce (\u79bb\u5b50\u4ea4\u6362\u6cd5\u5236\u5907\u6837\u54c1) \u4e0eCoCH\u7684EDS\u80fd\u8c31\u5206\u6790\uff0c\u63d2\u56fe\u662fCoMnCH-ce\u7684\u5149\u5b66\u7167\u7247\u3002<\/p>\n

(b) CoMnCH-ce\u4e0eCoCH\u7684\u7535\u5316\u5b66\u6d3b\u6027\u9762\u79ef\u6bd4\u8f83\u66f2\u7ebf\u3002<\/p>\n

(c) CoMnCH-ce\u4e0eCoCH\u7684\u6790\u6c27\u6781\u5316\u66f2\u7ebf\u3002<\/p>\n

(d) CoMnCH-ce\u4e0eCoCH\u7684Co 2p3\/2\u8c31\u56fe\u3002<\/p>\n

(e) CoMnCH\u4e0eCoCH\u4e2d\u94b4\u5143\u7d20\u76843d\u8f68\u9053\u7535\u5b50\u6001\u5bc6\u5ea6\u66f2\u7ebf\u3002<\/p>\n

(f) CoMnCH\u4e0eCoCH\u4e2d\u94b4\u5143\u7d20\u76843d\u8f68\u9053\u7535\u5b50\u6570\u3002<\/p>\n

(a) Co1<\/sub>Mn1<\/sub>CH\u5168\u6c34\u5206\u89e3\u6027\u80fd\u6d4b\u8bd5\u66f2\u7ebf\uff0c\u63d2\u56fe\u662f\u5168\u6c34\u5206\u89e3\u65f6\u7684\u5149\u5b66\u7167\u7247\u3002<\/p>\n

(b) Co1<\/sub>Mn1<\/sub>CH\u5168\u6c34\u5206\u89e3\u7a33\u5b9a\u6027\u6d4b\u8bd5\u66f2\u7ebf\uff0c\u63d2\u56fe\u662f\u7a33\u5b9a\u6027\u6d4b\u8bd5\u540eCo1<\/sub>Mn1<\/sub>CH\u7684SEM\u56fe\u3002<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/span><\/p>\n

\u672c\u6587\u62a5\u9053\u4e86\u4e00\u79cd\u751f\u957f\u5728\u6ce1\u6cab\u954d\u57fa\u5e95\u4e0a\u7684\u9530\u63ba\u6742\u78b1\u5f0f\u78b3\u9178\u94b4\u7eb3\u7c73\u7247\u9635\u5217\uff0c\u5728\u78b1\u6027\u6761\u4ef6\u4e0b\u5c55\u73b0\u51fa\u4e86\u8f83\u9ad8\u7684\u7535\u50ac\u5316\u6790\u6c22\u548c\u6790\u6c27\u50ac\u5316\u6d3b\u6027\uff0c\u53ef\u4ee5\u5ab2\u7f8e\u6700\u8fd1\u62a5\u9053\u7684\u5404\u79cd\u65b0\u578b\u53cc\u529f\u80fd\u5168\u6c34\u5206\u89e3\u7535\u50ac\u5316\u5242\uff0c\u5982\u6c27\u5316\u7269\uff0c\u786b\u5316\u7269\uff0c\u78f7\u5316\u7269\u7b49\uff0c\u5e76\u4e14\u53d1\u73b0\uff0c\u9530\u63ba\u6742\u53ef\u5b9e\u73b0\u5bf9\u50ac\u5316\u5242\u5fae\u89c2\u5f62\u8c8c\u4ee5\u53ca\u7535\u5b50\u7ed3\u6784\u7684\u53cc\u91cd\u8c03\u63a7\uff0c\u8fd9\u4e00\u7814\u7a76\u62d3\u5bbd\u4e86\u7535\u89e3\u6c34\u50ac\u5316\u5242\u7684\u9009\u62e9\u8303\u56f4\uff0c\u6709\u52a9\u4e8e\u7406\u89e3\u50ac\u5316\u5242\u7684\u6784\u6548\u5173\u7cfb\uff0c\u5e76\u4e3a\u5f00\u53d1\u65b0\u578b\u3001\u9ad8\u6548\u3001\u4f4e\u6210\u672c\u7535\u50ac\u5316\u5242\u63d0\u4f9b\u4e86\u5d2d\u65b0\u7684\u601d\u8def\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Electronic and Morphological Dual Modulation of Cobalt Carbonate Hydroxides by Mn Doping toward Highly Efficient and Stable Bifunctional Electrocatalysts for Overall Water Splitting<\/a> (J. Am. Chem. Soc<\/em>., 2017, DOI:10.1021\/jacs.7b03507)<\/p>\n

\u672c\u6587\u7531\u4e2d\u56fd\u79d1\u5b66\u9662\u5316\u5b66\u7814\u7a76\u6240\u6c5f\u6587\u6770\u535a\u58eb\u6295\u7a3f\uff0c\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u7ec4\u80cc\u9006\u65f6\u5149\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

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