{"id":77808,"date":"2017-05-19T06:30:13","date_gmt":"2017-05-18T22:30:13","guid":{"rendered":"\/\/m.iemloyee.com\/?p=77808"},"modified":"2017-05-18T20:37:34","modified_gmt":"2017-05-18T12:37:34","slug":"%e9%83%ad%e7%8e%89%e5%9b%bd%ef%bc%86%e5%90%b4%e9%9b%84%e4%bc%9faem-%e4%b8%80%e7%a7%8d%e9%ab%98%e6%80%a7%e8%83%bd%e5%85%a8%e9%92%92%e6%b6%b2%e6%b5%81%e7%94%b5%e6%b1%a0%e7%94%a8%e5%a4%8d%e5%90%88","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=77808","title":{"rendered":"\u90ed\u7389\u56fd\uff06\u5434\u96c4\u4f1fAEM: \u4e00\u79cd\u9ad8\u6027\u80fd\u5168\u9492\u6db2\u6d41\u7535\u6c60\u7528\u590d\u5408\u7535\u6781"},"content":{"rendered":"

\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/span><\/p>\n

\u5316\u77f3\u71c3\u6599\u5f15\u8d77\u7684\u73af\u5883\u548c\u80fd\u6e90\u77ed\u7f3a\u95ee\u9898\u8feb\u4f7f\u4eba\u7c7b\u5bfb\u627e\u5408\u9002\u7684\u89e3\u51b3\u65b9\u6cd5\u2014\u2014\u6e05\u6d01\u3001\u53ef\u518d\u751f\u80fd\u6e90\uff0c\u5982\u98ce\u80fd\u3001\u592a\u9633\u80fd\u7b49\u3002\u6e05\u6d01\u80fd\u6e90\u7684\u95f4\u65ad\u6027\u548c\u4e0d\u7a33\u5b9a\u6027\u9020\u6210\u5927\u91cf\u7535\u80fd\u7684\u6d6a\u8d39\uff0c\u4e9f\u9700\u5927\u578b\u50a8\u80fd\u8bbe\u5907\u4ee5\u63d0\u9ad8\u5176\u5229\u7528\u7387\u3002\u5168\u9492\u6db2\u6d41\u7535\u6c60\u8868\u73b0\u51fa\u4f4e\u6210\u672c\u3001\u9ad8\u6548\u7387\u3001\u9ad8\u5faa\u73af\u6027\u80fd\u3001\u5bb9\u91cf\u548c\u529f\u7387\u53ef\u7075\u6d3b\u8bbe\u8ba1\u7b49\u4f18\u70b9\uff0c\u6210\u4e3a\u5f53\u524d\u6700\u5177\u6709\u5e94\u7528\u524d\u666f\u7684\u5927\u89c4\u6a21\u50a8\u80fd\u88c5\u7f6e\u4e4b\u4e00\u3002\u76ee\u524d\u9488\u5bf9\u7535\u6781\u6750\u6599\u7684\u7814\u7a76\u4e3b\u8981\u662f\u78b3\u7535\u6781\u3002\u7279\u522b\u662f\u77f3\u58a8\u6be1\u7535\u6781\u5177\u6709\u5f88\u5f3a\u7684\u8010\u9178\u8150\u6027\u3001\u4f18\u826f\u7684\u5bfc\u7535\u6027\u3001\u5728\u8f83\u5bbd\u7684\u7535\u52bf\u8303\u56f4\u5185\u8868\u73b0\u4e3a\u5316\u5b66\u60f0\u6027\u548c\u4f4e\u6210\u672c\u7b49\u7279\u70b9, \u4ece\u800c\u5728\u9492\u7535\u6c60\u5f97\u5230\u4e86\u5e7f\u6cdb\u5e94\u7528\u3002\u7136\u800c\u77f3\u58a8\u6be1\u7535\u6781\u8868\u73b0\u51fa\u4f4e\u7684\u7535\u5316\u5b66\u6d3b\u6027\uff0c\u6291\u5236\u9492\u7535\u6c60\u5927\u7535\u6d41\u653e\u7535\u6027\u80fd\u548c\u7535\u6c60\u6548\u7387\uff0c\u963b\u788d\u4e86\u5176\u5728\u9492\u7535\u6c60\u4e2d\u7684\u53d1\u5c55\u3002\u56e0\u6b64\uff0c\u5f00\u53d1\u4e00\u79cd\u9ad8\u7535\u5316\u5b66\u6d3b\u6027\u7684\u7535\u6781\u6750\u6599\u5bf9\u4e8e\u9492\u7535\u6c60\u5728\u4ea7\u4e1a\u5316\u63a8\u5e7f\u4e0a\u5177\u6709\u91cd\u5927\u610f\u4e49\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/span><\/p>\n

\u8fd1\u65e5\uff0c\u6765\u81ea\u4e2d\u79d1\u9662\u5316\u5b66\u6240\u90ed\u7389\u56fd\u7814\u7a76\u5458\uff0c\u6e56\u5357\u519c\u4e1a\u5927\u5b66\u5434\u96c4\u4f1f\u526f\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\uff09\u7b49\u4eba\u901a\u8fc7\u6c34\u70ed\u53cd\u5e94\u5c06\u8fd8\u539f\u6c27\u5316\u77f3\u58a8\u70ef\u539f\u4f4d\u751f\u957f\u5728\u77f3\u58a8\u6be1\u7ea4\u7ef4\u8868\u9762\u5236\u5907\u6210\u590d\u5408\u7535\u6781\u3002\u4e0e\u7a7a\u767d\u7535\u6781\u76f8\u6bd4\uff0c\u8be5\u590d\u5408\u7535\u6781\u5bf9\u6b63\u8d1f\u6781\u9492\u79bb\u5b50\u5747\u8868\u73b0\u51fa\u66f4\u4f18\u5f02\u7684\u7535\u50ac\u5316\u6027\u80fd\uff0c\u5927\u5927\u63d0\u9ad8\u4e86\u7535\u6c60\u7535\u538b\u6548\u7387\u548c\u653e\u7535\u5bb9\u91cf\uff0c\u6700\u5927\u7535\u6d41\u5bc6\u5ea6\u8fbe\u5230300 mA cm-2<\/sup>\uff0c\u7279\u522b\u5728\u7535\u6d41\u5bc6\u5ea6\u4e3a150 mA cm-2<\/sup>\u6761\u4ef6\u4e0b\u5145\u653e\u7535500\u5708\u8868\u73b0\u51fa\u7a33\u5b9a\u7684\u80fd\u91cf\u6548\u7387\uff0c\u901a\u8fc7\u4e00\u7cfb\u5217\u7814\u7a76\u8868\u660e\u7535\u6781\u8868\u9762\u7684\u542b\u6c27\u5b98\u80fd\u56e2\u4e0e\u6c27\u5316\u77f3\u58a8\u70ef\u8868\u9762\u6d3b\u6027\u5b98\u80fd\u56e2\u53cd\u5e94\u751f\u6210\u5185\u8868\u9762\u9ad8\u5bfc\u7535\u548c\u5916\u8868\u9762\u9ad8\u50ac\u5316\u6d3b\u6027\u7684\u8fd8\u539f\u6c27\u5316\u77f3\u58a8\u70ef\u5c42\u3002rGO-GF\u590d\u5408\u7535\u6781\u7684\u5f62\u6210\u673a\u7406\u5982\u4e0b\u56fe\uff1a<\/p>\n

\"\"<\/p>\n

\u77f3\u58a8\u6be1\u7ea4\u7ef4\u8868\u9762\u4e0a\u7684\u542b\u6c27\u5b98\u80fd\u56e2\u80fd\u591f\u4e0e\u6c27\u5316\u77f3\u58a8\u70ef\u7f3a\u9677\u4f4d\u70b9\u4e0a\u7684\u542b\u6c27\u548c\u542b\u6c22\u57fa\u56e2\u53d1\u751f\u4ea4\u8054\u53cd\u5e94\u3002rGO\u548c\u77f3\u58a8\u6be1\u7ea4\u7ef4\u4e4b\u95f4\u5f62\u6210\u7684\u5316\u5b66\u952e\u548c\u7269\u7406\u5438\u9644\u80fd\u591f\u5728\u77f3\u58a8\u6be1\u7ea4\u7ef4\u8868\u9762\u5f62\u6210\u8f83\u5f3a\u7684\u7c98\u9644\u4f5c\u7528\u529b\u3002\u540c\u65f6\u6c27\u5316\u77f3\u58a8\u70ef\u5206\u5b50\u95f4\u7684\u8131\u6c34\uff0c\u6709\u52a9\u4e8e\u5728\u77f3\u58a8\u6be1\u7ea4\u7ef4\u8868\u9762\u751f\u957f\u5927\u5c3a\u5bf8\u7684\u8fd8\u539f\u77f3\u58a8\u70ef\u5c42\uff0c\u63d0\u9ad8\u590d\u5408\u7535\u6781\u7684\u6bd4\u8868\u9762\u79ef\u3002\u590d\u5408\u7535\u6781\u8868\u73b0\u51fa\u4e30\u5bcc\u7684\u542b\u6c27\u5b98\u80fd\u56e2\uff0c\u9ad8\u7684\u5bfc\u7535\u7387\uff0c\u663e\u8457\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u7535\u5316\u5b66\u6027\u80fd\u7ed3\u679c\u663e\u793a\u5728200 mA cm-2<\/sup>\uff0c\u7535\u538b\u6548\u7387\u4e3a74.5%\uff0c\u80fd\u91cf\u6548\u7387\u4e3a72.0%\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

\u56fe<\/strong>1 rGO-GF<\/strong>\u590d\u5408\u7535\u6781\u7684\u5f62\u8c8c\u8868\u5f81<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a)\u77f3\u58a8\u6be1; (b)\u5faa\u73af\u524d (c)\u5faa\u73af\u540e; (d)\u66f4\u9ad8\u500d\u7387; (e) rGO-GF\u590d\u5408\u7535\u6781; (f)\u4f7f\u7528FIB-SEM \u8bb0\u5f55SEM\u56fe; (b), (c),(e), (f)\u4e2dSEM\u56fe\u4e2d\u4f7f\u7528\u7684\u6c27\u5316\u77f3\u58a8\u70ef\u6d53\u5ea6\u4e3a2 g L-1<\/sup>\u3002<\/p>\n

\u00a0<\/strong>\u56fe<\/strong>2 rGO-GF<\/strong>\u590d\u5408\u7535\u6781\u7684\u5143\u7d20\u7ec4\u6210\u4e0e\u7ed3\u6784\u5206\u6790<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a) GF, rGO-1-GF, rGO-2-GF, \u548c rGO-3-GF \u7535\u6781\u6750\u6599\u7684XPS\u56fe\u8c31; (b) \u5728\u9ad8\u5206\u8fa8\u7387\u4e0b\u62df\u5408C1\u5cf0 (c) \u5728\u9ad8\u5206\u8fa8\u7387\u4e0b\u62df\u5408O1s\u5cf0 \uff1b(d) \u548c (e) \u5316\u5b66\u7ec4\u6210\uff1b (f)\u6c27\u5316\u77f3\u58a8\u70ef\u548c\u8fd8\u539f\u6c27\u5316\u77f3\u58a8\u70ef\u7684\u62c9\u66fc\u5149\u8c31\u3002<\/p>\n

\u56fe<\/strong>3 rGO-GF<\/strong>\u590d\u5408\u7535\u6781\u7684<\/strong>CV<\/strong>\u548c<\/strong>EIS<\/strong>\u6d4b\u8bd5<\/strong><\/span><\/p>\n

\"\"<\/p>\n

(a) \u5728\u5faa\u73af\u4f0f\u5b89\u6d4b\u8bd5\u7535\u89e3\u6db20.05 MVOSO4<\/sub> +3.0 M H2<\/sub>SO4<\/sub>\u5206\u522b\u5bf9 GF, rGO-1-GF, rGO-2-GF, and rGO-3-GF \u7535\u6781\u6750\u6599\u7684\u5faa\u73af\u4f0f\u5b89\u6d4b\u8bd5\uff0c\u626b\u901f\u4e3a10 mV s-1<\/sup>\uff1b (b) GF, rGO-1-GF, rGO-2-GF \u548c rGO-3-GF\u7684\u4ea4\u6d41\u963b\u6297\u6d4b\u8bd5\u3002<\/p>\n

\u56fe<\/strong>4 rGO-GF<\/strong>\u590d\u5408\u7535\u6781\u7684\u5145\u653e\u7535\u6d4b\u8bd5<\/strong><\/span><\/p>\n

\"\"<\/p>\n

\u5206\u522b\u4f7f\u7528 GF \u548crGO-2-GF \u7535\u6781\u7684\u9492\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd (a) \u7535\u6d41\u5bc6\u5ea6\u4e3a150 mA cm-2<\/sup>; (b) VE, CE and (c) EE \u5728\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6(50, 100, 120, 150 mA cm-2<\/sup>); EE (d) \u653e\u7535\u5bb9\u91cf(e) \u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6(50, 100, 120, 150, 180, 200, 250, 300 mA cm-2<\/sup>); EE (f) rGO-2-GF\u5728150 mA cm-2<\/sup> \u4e0b\u7684\u957f\u5faa\u73af\u6d4b\u8bd5.<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/span><\/p>\n

rGO-GF\u590d\u5408\u7535\u6781\u6750\u6599\u7684\u5236\u5907\u8fc7\u7a0b\u5b89\u5168\u53ef\u9760\uff0c\u6210\u672c\u4f4e\u5ec9\uff0c\u5b89\u5168\u53ef\u9760\u3002\u4e0e\u539f\u59cb\u7684\u77f3\u58a8\u6be1\u7535\u6781\u76f8\u6bd4\uff0c\u8fd9\u79cdrGO-GF\u590d\u5408\u77f3\u58a8\u6be1\u7535\u6781\u7684\u7535\u50ac\u5316\u6d3b\u6027\u5f97\u5230\u6781\u5927\u5730\u63d0\u5347\uff0c\u540c\u65f6\u6709\u6548\u964d\u4f4e\u6781\u5316\u4f5c\u7528\uff0c\u63d0\u9ad8\u7535\u6d41\u5bc6\u5ea6\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u590d\u5408\u7535\u6781\u6027\u80fd\u63d0\u9ad8\u5f52\u56e0\u4e8e\u5feb\u901f\u7684\u7535\u5b50\u8f6c\u79fb\u901f\u5ea6\u548c\u4e30\u5bcc\u7684\u542b\u6c27\u5b98\u80fd\u56e2\u80fd\u591f\u52a0\u901frGO-GF\u7535\u6781\u8868\u9762\u7684\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\u901f\u7387\uff0c\u6709\u671b\u5728\u9492\u6db2\u6d41\u7535\u6c60\u4e2d\u5f97\u5230\u5e7f\u6cdb\u5e94\u7528\u3002<\/p>\n

\"\"<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aQ. Deng, P. Huang, W.-X. Zhou, Q. Ma, N. Zhou, H. Xie, W. Ling, C.-J. Zhou,Y.-X. Yin, X.-W. Wu,* X.-Y. Lu,* Y.-G.Guo*<\/em>\u00a0. A High-Performance Composite Electrode for Vanadium Redox Flow Batteries <\/a><\/strong>(Adv. Energy Mater. \uff0c2017\uff0c<\/strong>DOI: 10.1002\/aenm.201700461<\/em><\/strong> )<\/p>\n

\u7279\u522b\u611f\u8c22:<\/p>\n

\u6e56\u5357\u7701\u94f6\u5cf0\u65b0\u80fd\u6e90\u6709\u9650\u516c\u53f8\u4e3a\u672c\u5b9e\u9a8c\u63d0\u4f9b\u7684\u5b9e\u9a8c\u6750\u6599\u548c\u6280\u672f\u652f\u6301\uff0c\u5f97\u5230\u4e2d\u56fd\u56fd\u5bb6\u6770\u51fa\u9752\u5e74\u57fa\u91d1\uff08No. 51225204\uff09\uff0c\u6e56\u5357\u7701\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\uff08No. 2015JJ3074\uff09\u548c\u957f\u6c99\u5e02\u79d1\u6280\u5c40\u91cd\u70b9\u9879\u76ee\uff08No. KL403147-11)\u7684\u8d44\u91d1\u652f\u6301\u3002<\/p>\n

\u3010\u5434\u96c4\u4f1f\u526f\u6559\u6388\u7b80\u4ecb<\/strong>\u3011<\/p>\n

\"\"<\/p>\n

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