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3\u3001 \u81ea\u52a8\u89e3\u6790\u672a\u77e5\u7eb3\u7c73\u6676\u4f53\u7684\u539f\u5b50\u7ed3\u6784<\/strong><\/p>\n

\u8fd1\u4e9b\u5e74\uff0c\u4ee5\u745e\u5178\u65af\u5fb7\u54e5\u5c14\u6469\u5927\u5b66\u7684\u90b9\u6653\u4e1c\u6559\u6388\u4e3a\u4ee3\u8868\u7684\u79d1\u5b66\u5bb6\u4eec\u53d1\u5c55\u4e86\u81ea\u52a8\u6536\u96c6\u7535\u5b50\u884d\u5c04\u82b1\u6837\u5e76\u89e3\u6790\u7eb3\u7c73\u6750\u6599\u4e2d\u539f\u5b50\u6392\u5217\u7684\u65b9\u6cd5\uff0c\u8fd9\u4e9b\u65b9\u6cd5\u90fd\u51cf\u5f31\u4e86\u7535\u5b50\u884d\u5c04\u52a8\u529b\u5b66\u6548\u5e94\uff0c\u4f7f\u5f97\u7535\u5b50\u884d\u5c04\u53ef\u4ee5\u50cf X-\u5c04\u7ebf\u5355\u6676\u884d\u5c04\u4e00\u6837\u89e3\u6790\u6676\u4f53\u7684\u539f\u5b50\u6392\u5217\u7ed3\u6784\u3002\u8fd9\u4e9b\u65b9\u6cd5\u4e3b\u8981\u5305\u62ec\u65cb\u8fdb\u7535\u5b50\u884d\u5c04(PED\uff0c Procession electron diffraction)\u53ca\u7535\u5b50\u884d\u5c04\u4e09\u7ef4\u91cd\u6784(ADT, Automated diffraction tomograpHy; RED, Rotation electron\u00a0diffraction)\uff0c\u5df2\u89e3\u6790\u51fa\u6cb8\u77f3\u3001\u91d1\u5c5e\u6709\u673a\u9aa8\u67b6(MOFs, Metal-organic frameworks )\u3001\u5171\u4ef7\u6709\u673a\u9aa8\u67b6(COFs, Covalent-organic frameworks )\u7b49\u591a\u79cd\u7eb3\u7c73\u6750\u6599\u7684\u539f\u5b50\u6392\u5217\u7ed3\u6784\u3002\u65cb\u8fdb\u7535\u5b50\u884d\u5c04 PED \u662f\u91c7\u7528\u7c7b\u4f3c X-\u5c04\u7ebf\u884d\u5c04\u4e2d\u7684\u65cb\u8fdb\u6280\u672f\uff0c\u53ea\u4e0d\u8fc7\u6837\u54c1\u4e0d\u503e\u659c\uff0c\u800c\u662f\u5c06\u7535\u5b50\u675f\u5c0f\u89d2\u5ea6\u503e\u659c\uff0c\u5e76\u6cbf\u4e0e\u900f\u5c04\u7535\u955c\u5149\u8f74\u540c\u8f74\u7684\u9525\u9762\u5728\u6837\u54c1\u8868\u9762\u626b\u63cf\uff0c\u5728\u6b64\u8fc7\u7a0b\u4e2d\u7528\u8f6f\u4ef6\u81ea\u52a8\u6536\u96c6\u6bcf\u4e00\u5e45\u7535\u5b50\u884d\u5c04\u82b1\u6837\uff0c\u5e76\u8fdb\u884c\u5408\u5e76\u5206\u6790\uff0c\u8fd9\u6837\u53ef\u5927\u5927\u51cf\u5c11\u591a\u91cd\u6563\u5c04\u4ece\u800c\u53ef\u4ee5\u5927\u5927\u51cf\u5f31\u52a8\u529b\u5b66\u6548\u5e94\uff0c\u4f7f\u5f97\u9274\u5b9a\u7a7a\u95f4\u7fa4\u76f8\u5bf9\u5bb9\u6613\uff0c\u5e76\u4e14\u901a\u8fc7\u884d\u5c04\u5f3a\u5ea6\u7684\u5206\u6790\u63ed\u793a\u7eb3\u7c73\u6750\u6599\u7684\u539f\u5b50\u6392\u5217\u7ed3\u6784\u3002\u5df2\u7528\u8fd9\u79cd\u65b9\u6cd5\u89e3\u6790\u4e86\u6cb8\u77f3\u5982 MCM-22\uff0c SSZ-48\uff0c ITQ-40 \u7b49\u7684\u6676\u4f53\u7ed3\u6784\uff0c\u5982\u56fe 5 \u4e3a SSZ-48 \u4e09\u4e2a\u6676\u5e26\u8f74\u7684\u7535\u5b50\u884d\u5c04\u53ca\u7531\u6b64\u5f97\u51fa\u7684\u7ed3\u6784\u6a21\u578b\u3002\u73b0\u5728\uff0c\u5df2\u6709\u5546\u4e1a\u5316\u7684\u63a7\u5236\u7535\u5b50\u675f\u65cb\u8fdb\u7684\u786c\u4ef6\u53ca\u914d\u5957\u7684\u91c7\u96c6\u3001\u5206\u6790\u884d\u5c04\u56fe\u7684\u8f6f\u4ef6\u3002<\/p>\n

\"\"<\/p>\n

\u56fe 5 SSZ-48 \u4e09\u4e2a\u6676\u5e26\u8f74\u7684\u7535\u5b50\u884d\u5c04\u53ca\u7ed3\u6784\u6a21\u578b<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe 6 \u7531 RED \u91cd\u6784\u7684 ZIF-7 \u4e09\u7ef4\u5012\u6613\u7a7a\u95f4\u70b9\u9635\u53ca\u7ecf\u8fc7\u7cbe\u4fee\u540e\u7684\u7ed3\u6784\u6a21\u578b<\/strong><\/p>\n

PED \u6280\u672f\u901a\u5e38\u662f\u6cbf\u7740\u6676\u4f53\u7684\u67d0\u4e2a\u6676\u5e26\u8f74\u65cb\u8fdb\uff0c\u8981\u6c42\u8f6c\u6b63\u6676\u4f53\u7684\u5e26\u8f74\uff0c\u800c\u7535\u5b50\u884d\u5c04\u7684\u4e09\u7ef4\u91cd\u6784\u6280\u672f ADT \u548c RED \u662f\u4f7f\u6837\u54c1\u8fdb\u884c\u5927\u89d2\u5ea6\u8303\u56f4\u7684\u503e\u8f6c(\u901a\u5e38\ufe6330\u00ba\u5230 +30\u00ba )\uff0c\u65e0\u9700\u8f6c\u6b63\u6676\u4f53\u7684\u5e26\u8f74\uff0c\u53ef\u6cbf\u4efb\u610f\u5e26\u8f74\u8fdb\u884c\u6570\u636e\u91c7\u96c6\uff0c\u56e0\u6b64\u6bd4 PED \u6280\u672f\u66f4\u6709\u4f18\u52bf\u3002\u6bd4\u5982\u7531\u90b9\u6653\u4e1c\u6559\u6388\u56e2\u961f\u5f00\u53d1\u7684 RED \u6280\u672f\u662f\u5728\u63a7\u5236\u6d4b\u89d2\u53f0\u5373\u6837\u54c1\u65cb\u8f6c\u7684\u540c\u65f6\uff0c\u63a7\u5236\u7535\u5b50\u675f\u7684\u504f\u8f6c\uff0c\u901a\u5e38\u6837\u54c1\u6bcf\u8f6c 2\u00ba\uff0d3\u00ba\uff0c\u7535\u5b50\u675f\u540c\u65f6\u503e\u8f6c 0.1\u00ba\uff0d0.4\u00ba\uff0c\u8fd9\u6837\u907f\u514d\u4e86\u52a8\u529b\u5b66\u6548\u5e94\uff0c\u5e94\u7528\u8f6f\u4ef6\u5728\u4e0d\u5230\u4e00\u4e2a\u5c0f\u65f6\u4e4b\u5185\u53ef\u91c7\u96c6\u4e0a\u5343\u5f20\u7535\u5b50\u884d\u5c04\u56fe\uff0c\u4e4b\u540e\u518d\u8fdb\u884c\u8c31\u56fe\u878d\u5408\u3001\u5355\u80de\u786e\u5b9a\u3001\u6307\u6570\u6807\u5b9a\u3001\u5f3a\u5ea6\u63d0\u53d6\u7b49\u6570\u636e\u5904\u7406\uff0c\u4e4b\u540e\u53ef\u5e94\u7528\u4e0e X-\u5c04\u7ebf\u5355\u6676\u89e3\u6790\u76f8\u540c\u7684\u65b9\u6cd5\u8fdb\u884c\u7ed3\u6784\u89e3\u6790\u53ca\u7cbe\u4fee\uff0c\u5982\u56fe 6 \u4e3a\u5e94\u7528 RED \u6280\u672f\u89e3\u6790\u7684\u4e00\u79cd MOFs (ZIF-7)\u7684\u7ed3\u6784\u3002\u7531\u6b64\u53ef\u89c1\uff0c\u5e94\u7528 RED \u8fd9\u79cd\u6280\u672f\u53ef\u5c06\u900f\u5c04\u7535\u955c\u53d1\u5c55\u6210\u4e3a\u80fd\u591f\u89e3\u6790\u7eb3\u7c73\u6676\u4f53\u672a\u77e5\u7ed3\u6784\u7684\u7535\u5b50\u884d\u5c04\u4eea\uff0c\u9884\u8ba1\u5c06\u5728\u7eb3\u7c73\u6676\u4f53\u7ed3\u6784\u7814\u7a76\u65b9\u9762\u53d1\u6325\u975e\u5e38\u91cd\u8981\u4f5c\u7528\u3002\u5f53\u7136\uff0c\u7535\u5b50\u884d\u5c04\u89e3\u6790\u6676\u4f53\u7ed3\u6784\u76ee\u524d\u5b58\u5728\u7684\u4e00\u4e2a\u4e3b\u8981\u95ee\u9898\u662f\u7535\u5b50\u675f\u5bf9\u6837\u54c1\u7684\u635f\u4f24\uff0c\u901a\u8fc7\u4f4e\u6e29\u7b49\u65b9\u6cd5\u53ef\u51cf\u5f31\u635f\u4f24\u3002<\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u900f\u5c04\u7535\u955c\u7535\u5b50\u884d\u5c04\u5728\u6676\u4f53\u7ed3\u6784\u5206\u6790\u65b9\u9762\u5177\u6709\u91cd\u8981\u7684\u5e94\u7528\u524d\u666f\uff0c\u5728\u5df2\u6709\u786c\u4ef6\u548c\u8f6f\u4ef6\u7684\u57fa\u7840\u4e0a\uff0c\u5316\u5b66\u6240\u5206\u6790\u6d4b\u8bd5\u4e2d\u5fc3\u7535\u955c\u7ec4\u5df2\u7ecf\u521d\u6b65\u5f00\u5c55\u4e86\u7eb3\u7c73\u6750\u6599\u751f\u957f\u65b9\u5411\u5224\u5b9a\u4ee5\u53ca\u672a\u77e5\u6676\u4f53\u6676\u80de\u53c2\u6570\u786e\u5b9a\u7684\u5de5\u4f5c\uff0c\u5982\u679c\u80fd\u591f\u914d\u5907\u7535\u5b50\u884d\u5c04\u4e09\u7ef4\u91cd\u6784\u6280\u672f\u6240\u9700\u7684\u914d\u4ef6\uff0c \u6211\u4eec\u5c06\u80fd\u591f\u6df1\u5165\u5f00\u5c55\u672a\u77e5\u7eb3\u7c73\u6676\u4f53\u7ed3\u6784\u89e3\u6790\u7684\u5de5\u4f5c\uff0c\u5f25\u8865\u5e38\u89c4 X-\u5c04\u7ebf\u884d\u5c04\u6280\u672f\u4e0d\u80fd\u89e3\u6790\u7eb3\u7c73\u6676\u4f53\u7ed3\u6784\u7684\u4e0d\u8db3\u3002<\/p>\n

\u4e3b\u8981\u53c2\u8003\u6587\u732e<\/strong><\/p>\n

1. \u5218\u6587\u897f\uff0c\u9ec4\u5b5d\u745b\uff0c\u9648\u7389\u5982\uff0c\u6750\u6599\u7ed3\u6784\u7684\u7535\u5b50\u663e\u5fae\u5206\u6790\uff0c\u5929\u6d25\u5927\u5b66\u51fa\u7248\u793e\uff0c 1989.<\/p>\n

2. \u90ed\u53ef\u4fe1\uff0c\u53f6\u6052\u5f3a\uff0c\u5434\u7389\u7428\uff0c\u7535\u5b50\u884d\u5c04\u56fe\u5728\u6676\u4f53\u5b66\u4e2d\u7684\u5e94\u7528\uff0c\u79d1\u5b66\u51fa\u7248\u793e\uff0c 1983.<\/p>\n

3.Yong Ding , Zhong Lin Wang, Structure analysis of nanowires and nanobelts by
\n transmission electron microscopy, J. PHys. Chem. B 2004, 108, 12280.<\/p>\n

4. Xiaodong Zou, Sven Hovm\u00f6ller, Electron crystallograpHy: imaging and single
\n crystal from powders, Acta Cyst. 2008, A64, 149.<\/p>\n

5. Tom Willhammar, Yifeng Yun, Xiaodong Zou, Structural determination of ordered
\n porous solids by electron crystallograpHy, Adv. Funct. Mater. 2014, 24,182.<\/p>\n

6. Wei Hua, Hong Chen, Zheng-Bao Yu, Xiaodong Zou, Jianhua Lin, Junliang Sun,
\n Tuning the pore size and shape in zeolites: a stable germanosilicate with 11-ring
\n channels solved by electron crystallograpHy, Angew Chem. Int. Ed. 2014, 53,5868.<\/p>\n

7. Peng Guo, Leifeng Liu, Yifeng Yun, Jie Su, Hermann Gies, Haiyan Zhang,
\n Feng-Shou Xiao, Xiaodong Zou, Ab initio Structure Solution of Interlayer Expanded
\n Zeolites by Rotation Electron Diffraction, Dalton Trans. 2014, 43, 10593.<\/p>\n

\u6d4b\u8bd5\u8c37<\/a><\/strong>\u662f\u6750\u6599\u4eba\u65d7\u4e0b\u4e13\u6ce8\u6750\u6599\u5206\u6790\u6d4b\u8bd5\u5e73\u53f0\uff0c\u63d0\u4f9b\u5305\u62ec\u529b\u5b66\u3001\u7269\u7406\u3001\u5316\u5b66\u3001\u7ed3\u6784\u5206\u6790\u7b49\u5206\u6790\u6d4b\u8bd5\u53ca\u5176\u76f8\u5173\u6570\u636e\u5206\u6790<\/strong>\uff0c\u63d0\u4f9b\u8bba\u6587\u6da6\u8272\u3001\u63d2\u56fe\u7ed8\u5236\u3001\u6750\u6599\u8ba1\u7b97\uff0c\u4e13\u5229\u64b0\u5199\u7b49\u670d\u52a1<\/strong>\u3002\u540c\u65f6\uff0c\u6b22\u8fce\u6709\u4e00\u6280\u4e4b\u957f\u7684\u6750\u6599\u4eba\u5165\u9a7b\u6d4b\u8bd5\u8c37\uff0c\u5411\u5e7f\u5927\u4f1a\u5458\u63d0\u4f9b\u670d\u52a1\uff0c\u626b\u7801\u76f4\u8fbe\u6d4b\u8bd5\u8c37\u670d\u52a1\u4e13\u533a\uff1a<\/p>\n

\"\"<\/p>\n

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