{"id":75901,"date":"2017-05-11T06:30:15","date_gmt":"2017-05-10T22:30:15","guid":{"rendered":"\/\/m.iemloyee.com\/?p=75901"},"modified":"2017-05-11T08:40:54","modified_gmt":"2017-05-11T00:40:54","slug":"%e6%8a%95%e7%a8%bf%e5%be%85%e5%ae%9aadv-funct-mater-%ef%bc%9a%e5%9f%ba%e4%ba%8e%e9%bb%91%e7%a3%b7%e7%ba%b3%e7%b1%b3%e7%89%87%e7%9a%84%e8%87%aa%e4%be%9b%e7%94%b5%e5%85%89%e6%8e%a2%e6%b5%8b%e5%99%a8","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=75901","title":{"rendered":"AFM\u5185\u9875\u5c01\u5e95\u8bba\u6587\uff1a\u57fa\u4e8e\u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u81ea\u4f9b\u7535\u5149\u63a2\u6d4b\u5668\u6784\u7b51\u4e0e\u6027\u80fd"},"content":{"rendered":"<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-80260\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/346337042478569632.jpg\" alt=\"\" width=\"600\" height=\"800\" \/><\/p>\n<p><strong><b>\u3010<\/b><\/strong><strong><b>\u5f15\u8a00<\/b><\/strong>\u3011<\/p>\n<p>\u5149\u63a2\u6d4b\u5668\u662f\u4e00\u79cd\u80fd\u591f\u5c06\u5149\u4fe1\u53f7\u8f6c\u6362\u4e3a\u7535\u4fe1\u53f7\u7684\u88c5\u7f6e\uff0c\u5176\u5728\u8bf8\u591a\u9886\u57df\u90fd\u6709\u7740\u5e7f\u6cdb\u7684\u5e94\u7528\u3002\u5728\u534a\u5bfc\u4f53\u5149\u7535\u5b50\u9886\u57df\uff0c\u4e8c\u7ef4\u8fc7\u6e21\u65cf\u91d1\u5c5e\u786b\u65cf\u5316\u5408\u7269\u56e0\u5176\u72ec\u7279\u7684\u5c42\u72b6\u7ed3\u6784\u4ee5\u53ca\u5149\u7535\u6027\u8d28\u800c\u88ab\u7528\u4e8e\u5149\u7535\u63a2\u6d4b\u5668\u7684\u7814\u7a76\u3002\u7136\u800c\uff0c\u8f83\u4f4e\u7684\u7535\u8f93\u8fd0\u6027\u80fd\u4ee5\u53ca\u6709\u9650\u7684\u80fd\u5e26\u53d8\u5316\u8303\u56f4\u6781\u5927\u7684\u9650\u5236\u4e86\u5176\u5728\u5149\u7535\u63a2\u6d4b\u9886\u57df\u7684\u5b9e\u9645\u5e94\u7528\u3002<\/p>\n<p> \u8fd1\u65e5\uff0c\u9ed1\u78f7\u4f5c\u4e3a\u4e00\u79cd\u534a\u5bfc\u4f53\u6027\u7684\u8303\u5fb7\u534e\u5c42\u72b6\u6750\u6599\u5c55\u73b0\u51fa\u9ad8\u7684\u8f7d\u6d41\u5b50\u8fc1\u79fb\u7387\u3001\u5404\u5411\u5f02\u6027\u7684\u5149\u7535\u7279\u6027\u3001\u53ef\u8c03\u63a7\u7684\u76f4\u63a5\u5e26\u9699\u4ee5\u53ca\u9ad8\u7684\u5f00\u5173\u6bd4\uff0c\u56e0\u6b64\u88ab\u4eba\u4eec\u8ba4\u4e3a\u662f\u5236\u9020\u5149\u63a2\u6d4b\u5668\u7684\u7406\u60f3\u6750\u6599\u4e4b\u4e00\u3002\u540c\u65f6\uff0c\u7814\u7a76\u8868\u660e\u51cf\u5c0f\u5c42\u72b6\u6750\u6599\u7684\u539a\u5ea6\u80fd\u591f\u6709\u6548\u63d0\u9ad8\u6750\u6599\u7684\u7535\u8f93\u8fd0\u6027\u80fd\uff0c\u6539\u5584\u80fd\u5e26\u7ed3\u6784\u5e76\u6709\u5229\u4e8e\u63d0\u5347\u6750\u6599\u7684\u5149\u63a2\u6d4b\u80fd\u529b\uff0c\u6240\u4ee5\u5c11\u5c42\u9ed1\u78f7\u7eb3\u7c73\u7247\u5728\u5149\u7535\u9886\u57df\u5177\u6709\u6781\u5927\u7684\u5e94\u7528\u4ef7\u503c\u3002\u5c3d\u7ba1\u5982\u6b64\uff0c\u9ed1\u78f7\u7eb3\u7c73\u7247\u66b4\u9732\u5728\u7a7a\u6c14\u4e2d\u65f6\u4f1a\u4e0d\u53ef\u907f\u514d\u5730\u906d\u53d7\u6c27\u5316\u635f\u5bb3\uff0c\u8fd9\u6781\u5927\u5730\u963b\u788d\u4e86\u5176\u5e94\u7528\u5f00\u53d1\u3002\u4e3a\u6b64\uff0c\u5c06\u9ed1\u78f7\u7eb3\u7c73\u7247\u8fd0\u7528\u5728\u5149\u63a2\u6d4b\u9886\u57df\u540c\u65f6\u4fdd\u8bc1\u5176\u7a33\u5b9a\u6027\u5bf9\u9ad8\u6027\u80fd\u5149\u63a2\u6d4b\u5668\u7684\u53d1\u5c55\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n<p><strong><b>\u3010<\/b><\/strong><strong><b>\u6210\u679c\u7b80\u4ecb<\/b><\/strong>\u3011<\/p>\n<p>\u8fd1\u65e5\uff0c<strong>\u6e58\u6f6d\u5927\u5b66\u949f\u5efa\u65b0\u6559\u6388\u56e2\u961f\u7684\u7941\u7965\uff08\u901a\u8baf\u4f5c\u8005\uff09\u526f\u6559\u6388\u8bfe\u9898\u7ec4\u548c\u6df1\u5733\u5e02\u9ed1\u78f7\u5149\u7535\u6280\u672f\u5de5\u7a0b\u5b9e\u9a8c\u5ba4\u4e3b\u4efb\u6df1\u5733\u5927\u5b66\u5f20\u6657\uff08\u901a\u8baf\u4f5c\u8005\uff09\u6559\u6388\u8bfe\u9898\u7ec4<\/strong>\u8fd1\u671f\u5728Advanced Functional Materials\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cEnvironmentally Robust Black Phosphorus Nanosheets in Solution: Application for Self-Powered Photodetector\u201d\u7684\u5185\u5c01\u5e95\u6587\u7ae0\u3002<\/p>\n<p> \u8be5\u56e2\u961f\u9009\u7528KOH\u4f5c\u4e3a\u7535\u89e3\u8d28\uff0c\u5728\u6eb6\u6db2\u7684\u73af\u5883\u4e0b\u6d4b\u8bd5\u4e86\u6db2\u76f8\u5265\u79bb\u5236\u5907\u7684\u5c11\u5c42\u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u81ea\u4f9b\u7535\u5149\u63a2\u6d4b\u6027\u80fd\u4ee5\u53ca\u5176\u7a33\u5b9a\u6027\u3002\u7814\u7a76\u53d1\u73b0\uff0c\u9ed1\u78f7\u7eb3\u7c73\u7247\u5728KOH\u7535\u89e3\u6db2\u4e2d\u7684\u5149\u7535\u6d41\u80fd\u8fbe\u5230265\u00a0nA\/cm<sup>2<\/sup>\uff0c\u4e00\u5468\u4e4b\u540e\u5176\u5149\u7535\u6d41\u5927\u5c0f\u4ecd\u6709103 nA\/cm<sup>2<\/sup>\u3002\u7ed3\u679c\u8868\u660e\uff0c\u9ed1\u78f7\u7eb3\u7c73\u7247\u5728KOH\u7535\u89e3\u6db2\u4e2d\u5177\u6709\u4f18\u5f02\u7684\u5149\u63a2\u6d4b\u80fd\u529b\u4ee5\u53ca\u826f\u597d\u7684\u7a33\u5b9a\u6027\u3002\u4e0d\u4ec5\u5982\u6b64\uff0c\u901a\u8fc7\u5bf9KOH\u7535\u89e3\u6db2\u7684\u6d53\u5ea6\u548c\u504f\u538b\u8fdb\u884c\u8c03\u63a7\uff0c\u6709\u6548\u7684\u63d0\u5347\u4e86\u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u5149\u63a2\u6d4b\u6027\u80fd\u3002\u672c\u5de5\u4f5c\u4e0d\u4ec5\u5f97\u5230\u4e86\u9ed1\u78f7\u7eb3\u7c73\u7247\u5149\u63a2\u6d4b\u6027\u80fd\u548c\u7535\u89e3\u6db2\u6d53\u5ea6\u7684\u5173\u7cfb\uff0c\u8fd8\u8bf4\u660e\u9ed1\u78f7\u7eb3\u7c73\u7247\u4f5c\u4e3a\u4f4e\u529f\u8017\u5149\u63a2\u6d4b\u5668\u4ef6\u4e2d\u5177\u6709\u826f\u597d\u7684\u6027\u80fd\u4e0e\u6f5c\u529b\u3002<\/p>\n<p>\u8be5\u7814\u7a76\u5f97\u5230\u4e86\u6df1\u5733\u5e02\u9ed1\u78f7\u5149\u7535\u6280\u672f\u5de5\u7a0b\u5b9e\u9a8c\u5ba4\uff0c\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u91cd\u5927\u53ca\u91cd\u70b9\u9879\u76ee\uff0c\u6df1\u5733\u5e02\u91cd\u70b9\u79d1\u6280\u9879\u76ee\u7b49\u591a\u9879\u57fa\u91d1\u7684\u652f\u6301\u3002<\/p>\n<p><strong><b>\u3010<\/b><\/strong><strong><b>\u56fe\u6587\u5bfc\u8bfb<\/b><\/strong><strong><b>\u3011<\/b><\/strong><\/p>\n<p><strong><b>\u56fe1\uff1a\u4e8c\u7ef4\u9ed1\u78f7\u7eb3\u7c73\u7247\u6db2\u76f8\u5265\u79bb\u7684\u5236\u5907\u793a\u610f\u56fe\u4ee5\u53ca<\/b><\/strong><strong><b>\u5f62\u8c8c\u7ed3\u6784\u8868\u5f81<\/b><\/strong><\/p>\n<p><strong><b><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-75904\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72471-10.jpg\" alt=\"\" width=\"600\" height=\"591\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72471-10.jpg 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72471-10-300x296.jpg 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/b><\/strong><\/p>\n<p>(a) \u6db2\u76f8\u5265\u79bb\u5236\u5907\u5c11\u5c42\u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u6d41\u7a0b\u793a\u610f\u56fe\uff1b<\/p>\n<p>(b-c) SEM\u4ee5\u53caEDS\u5206\u6790\uff1b<\/p>\n<p>(d) TEM\u5206\u6790\uff1b<\/p>\n<p>(e) HRTEM\u56fe\uff1b<\/p>\n<p>(f) \u5bf9\u5e94\u7684\u884d\u5c04\u82b1\u6837\uff1b<\/p>\n<p>(g) \u9ed1\u78f7\u7eb3\u7c73\u7247\u5728NMP\u6eb6\u6db2\u4e2d\u7684\u7d2b\u5916\u53ef\u89c1\u5149\u8c31\u8868\u5f81\uff1b<\/p>\n<p>(h) \u5757\u72b6\u9ed1\u78f7\u548c\u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u62c9\u66fc\u5149\u8c31\u5206\u6790\uff1b<\/p>\n<p>(i) \u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u5149\u81f4\u53d1\u5149\u8c31\u3002<\/p>\n<p> <strong><b>\u56fe2\uff1a\u57fa\u4e8e\u9ed1\u78f7\u7eb3\u7c73\u7247\u5149\u63a2\u6d4b\u5668<\/b><\/strong><strong><b>\u7684<\/b><\/strong><strong><b>\u6027\u80fd<\/b><\/strong><strong><b>\u7814\u7a76<\/b><\/strong><\/p>\n<p><strong><b><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-75905\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72472-8.jpg\" alt=\"\" width=\"600\" height=\"441\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72472-8.jpg 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72472-8-300x221.jpg 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/b><\/strong><\/p>\n<p>\u6d4b\u8bd5\u9ed1\u78f7\u7eb3\u7c73\u7247\u57280.1 M KOH\u7535\u89e3\u6db2\u4e2d\u5149\u63a2\u6d4b\u6027\u80fd\uff1a<\/p>\n<p>(a) \u7ebf\u6027\u4f0f\u5b89\u7279\u6027\u66f2\u7ebf\uff1b<\/p>\n<p>(b)\u00a0\u4e0d\u540c\u5149\u5f3a\u5ea6\u4e0b\u7684\u5149\u54cd\u5e94\u80fd\u529b\uff1b<\/p>\n<p>(c)\u00a0\u4e0d\u540c\u5149\u5f3a\u4e0b\u5149\u7535\u6d41\u548c\u5149\u8f6c\u6362\u6548\u7387\u7684\u5206\u6790\uff1b<\/p>\n<p>(d)\u00a0\u4e0d\u540c\u6ce2\u957f\u5149\u6e90(360 nm, 405 nm, 436 nm and 546 nm)\u7167\u5c04\u4e0b\u7684\u4f0f\u5b89\u7279\u6027\u66f2\u7ebf\uff1b<\/p>\n<p>(e) \u81ea\u4f9b\u7535\u5149\u63a2\u6d4b\u6027\u80fd\uff1b<\/p>\n<p>(f)\u00a0\u57280.3 V\u548c0.6 V\u504f\u538b\u4e0b\u7684\u5149\u63a2\u6d4b\u6027\u80fd\u3002<\/p>\n<p> <strong><b>\u56fe3\uff1a\u9ed1\u78f7\u7eb3\u7c73\u7247\u5728\u78b1\u6027KOH\u6eb6\u6db2\u4e2d\u7684\u7a33\u5b9a\u6027<\/b><\/strong><\/p>\n<p><strong><b><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-75906\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72473-7.jpg\" alt=\"\" width=\"600\" height=\"479\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72473-7.jpg 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72473-7-300x240.jpg 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/b><\/strong><\/p>\n<p>(a) \u5faa\u73af\u7a33\u5b9a\u6027\u6d4b\u8bd5\uff1b<\/p>\n<p>(b)\u00a0\u957f\u65f6\u95f4\u81ea\u4f9b\u7535\u9ed1\u78f7\u7eb3\u7c73\u7247\u5149\u63a2\u6d4b\u5668\u7a33\u5b9a\u6027\u6d4b\u8bd5\uff1b<\/p>\n<p>(c)\u00a0\u9ed1\u78f7\u7eb3\u7c73\u7247\u5149\u63a2\u6d4b\u5668\u7684\u57281\u5c0f\u65f6\u30011\u5929\u30011\u5468\u4ee5\u53ca1\u4e2a\u6708\u540e\u7684\u5149\u54cd\u5e94\u7279\u5f81\u5206\u6790\u3002<\/p>\n<p> <strong><b>\u56fe4\uff1a\u4e0d\u540cKOH\u6d53\u5ea6\u4e0b\u7684\u9ed1\u78f7<\/b><\/strong><strong><b>\u7eb3\u7c73\u7247<\/b><\/strong><strong><b>\u81ea\u4f9b\u7535\u5149\u63a2\u6d4b\u5668\u6027\u80fd\u5206\u6790<\/b><\/strong><\/p>\n<p><strong><b><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-75907\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72474-7.jpg\" alt=\"\" width=\"600\" height=\"430\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72474-7.jpg 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2017\/04\/\u56fe\u72474-7-300x215.jpg 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/b><\/strong><\/p>\n<p>(a) \u4e0d\u540cKOH\u7535\u89e3\u6db2\u6d53\u5ea6\u4e2d\u7684\u5149\u54cd\u5e94\u6d4b\u8bd5\uff1b<\/p>\n<p>(b)\u00a0\u62df\u5408\u5149\u54cd\u5e94\u66f2\u7ebf\u5f97\u5230\u54cd\u5e94\u65f6\u95f4\u5e38\u6570\uff1b<\/p>\n<p>(c)\u00a0\u4e0d\u540c\u7535\u89e3\u6db2\u6d53\u5ea6\u4e2d\u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u4ea4\u6d41\u963b\u6297\u6d4b\u8bd5\u3002<\/p>\n<p><strong><b>\u3010<\/b><\/strong><strong><b>\u5c0f\u7ed3<\/b><\/strong><strong><b>\u3011<\/b><\/strong><\/p>\n<p>\u8be5\u5de5\u4f5c\u5229\u7528\u6db2\u76f8\u5265\u79bb\u7684\u65b9\u6cd5\u5f97\u5230\u4e86\u5c11\u5c42\u9ed1\u78f7\u7eb3\u7c73\u7247\u5e76\u5c06\u5176\u7528\u4e8e\u6784\u5efa\u81ea\u4f9b\u7535\u5149\u63a2\u6d4b\u5668\u7684\u7535\u6781\u3002\u901a\u8fc7\u5149\u54cd\u5e94\u6d4b\u8bd5\uff0c\u65f6\u95f4\u5faa\u73af\u7a33\u5b9a\u6027\u6d4b\u8bd5\u4ee5\u53ca\u663e\u5fae\u62c9\u66fc\u8868\u5f81\u53d1\u73b0\u5728KOH\u7535\u89e3\u6db2\u7684\u73af\u5883\u4e0b\uff0c\u4e8c\u7ef4\u9ed1\u78f7\u7eb3\u7c73\u7247\u4e0d\u4ec5\u5177\u6709\u4f18\u5f02\u7684\u5149\u54cd\u5e94\u6027\u80fd\u8fd8\u5177\u6709\u826f\u597d\u7684\u7a33\u5b9a\u6027\u3002\u8fdb\u4e00\u6b65\u5b9e\u9a8c\u7ed3\u679c\u8868\u660e\uff0c\u901a\u8fc7\u6539\u53d8KOH\u7684\u6d53\u5ea6\u80fd\u591f\u6709\u6548\u8c03\u63a7\u9ed1\u78f7\u7eb3\u7c73\u7247\u7684\u5149\u63a2\u6d4b\u6027\u80fd\uff0c\u4ece\u800c\u63d0\u4f9b\u4e00\u79cd\u5f97\u5230\u4f18\u5f02\u5149\u63a2\u6d4b\u6027\u80fd\u4ee5\u53ca\u9ad8\u7a33\u5b9a\u9ed1\u78f7\u7eb3\u7c73\u7247\u5149\u63a2\u6d4b\u5668\u7684\u65b9\u6cd5\u3002<\/p>\n<p><strong><b>\u6587\u7ae0\u94fe\u63a5<\/b><\/strong>\uff1a<a href=\"http:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/adfm.201606834\/full\" target=\"_blank\" rel=\"noopener noreferrer\">Environmentally Robust Black Phosphorus Nanosheets in Solution: Application for Self\u2010Powered Photodetector <\/a>(Adv. Funct. 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