{"id":70481,"date":"2017-03-14T06:30:46","date_gmt":"2017-03-13T22:30:46","guid":{"rendered":"\/\/m.iemloyee.com\/?p=70481"},"modified":"2017-03-12T14:41:36","modified_gmt":"2017-03-12T06:41:36","slug":"%e6%b5%99%e6%b1%9f%e5%a4%a7%e5%ad%a6macromolecules-%e7%bb%93%e6%99%b6%e9%a9%b1%e5%8a%a8%e5%be%ae%e7%b1%b3%e7%ba%a7%e8%81%9a%e5%90%88%e7%89%a9%e6%b7%b7%e5%90%88%e5%8d%95%e6%99%b6%e5%92%8c%e7%ba%b3","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=70481","title":{"rendered":"\u6d59\u6c5f\u5927\u5b66Macromolecules: \u7ed3\u6676\u9a71\u52a8\u5fae\u7c73\u7ea7\u805a\u5408\u7269\u6df7\u5408\u5355\u6676\u548c\u7eb3\u7c73\u7ea7\u7ed3\u6676\u80f6\u675f\u7684\u5171\u7ec4\u88c5\u884c\u4e3a"},"content":{"rendered":"

\u3010\u5f15\u8a00<\/strong>\u3011<\/p>\n

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\u3010\u6210\u679c\u4ecb\u7ecd<\/strong>\u3011<\/p>\n

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\u3010\u56fe\u6587\u5bfc\u8bfb<\/strong>\u3011<\/p>\n

\u56fe<\/strong>1<\/strong>\u4e3a<\/strong>BCP\/PE<\/strong>\u7684\u8d28\u91cf\u6bd4<\/strong>(WBCP<\/sub>\/WPE<\/sub>)<\/strong>\u4e3a<\/strong>0.4\/1<\/strong>\u7684\u6df7\u5408\u7269\u5728<\/strong>75o<\/sup>C<\/strong>\uff0c<\/strong>DMF<\/strong>\u6eb6\u5242\u4e2d\u7ed3\u6676\u5236\u5f97\u6df7\u5408\u5355\u6676\u7684\u900f\u5c04\u7535\u955c\uff08<\/strong>TEM<\/strong>\uff09<\/strong>(a)<\/strong>\u548c\u7535\u5b50\u884d\u5c04\u56fe<\/strong>(SAED)(b)<\/strong>\u3002<\/strong><\/p>\n

a:PE100<\/sub>-b-PtBA48<\/sub>\/PE52<\/sub>\u5728DMF\u6eb6\u5242\u4e2d\u8f83\u5dee\u7684\u6eb6\u89e3\u6027\uff0c\u5728TEM\u4e2d\u8868\u73b0\u4e3a\u622a\u9762\u4e3a\u83f1\u5f62\u7684\u6676\u4f53\uff1b<\/p>\n

b:[110]\u4e0e[200]\u884d\u5c04\u6591\u70b9\u4e3a\u5178\u578bPE\u659c\u65b9\u6676\u4f53\u7684\u7279\u5f81\uff0c\u7531\u6b64\u5f97\u51faPE100<\/sub>-b-PtBA48<\/sub>\/PE52<\/sub>\u5171\u6df7\u7269\u7684\u6676\u4f53\u4e3a\u5355\u6676\u3002<\/p>\n

\u56fe<\/strong>2<\/strong>\u4e3a<\/strong>WBCP<\/sub>\/WPE<\/sub><\/strong>\u4e3a<\/strong>0.4\/1<\/strong>\u7684\u6df7\u5408\u7269\u5728<\/strong>75o<\/sup>C<\/strong>\uff0c<\/strong>DMF<\/strong>\u6eb6\u5242\u4e2d\u7ed3\u6676\u5236\u5f97\u6df7\u5408\u5355\u6676\u7684\u539f\u5b50\u7c92\u663e\u5fae\u955c\uff08<\/strong>AFM<\/strong>\uff09\u7684\u9ad8\u5ea6\u56fe\u3002<\/strong><\/p>\n

<\/strong><\/p>\n

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\u56fe<\/strong>3<\/strong>\u4e3a<\/strong>BCP\/PE <\/strong>\u5171\u6df7\u7269\u6df7\u5408\u5355\u6676<\/strong>(a)<\/strong>\uff0c\u5171\u7ec4\u88c5\u4f53<\/strong>(b)<\/strong>\uff0c\u67f1\u72b6\u80f6\u675f\u7684\u7ed3\u6784<\/strong>(c)<\/strong><\/p>\n

<\/strong><\/p>\n

\u6839\u636eAFM\u7684\u7ed3\u679c\uff0c\u7c7b\u4f3c\u4e8eC198<\/sub>H398<\/sub>\u70f7\u70c3\u5728\u6eb6\u5242\u4e2d\u7ed3\u6676\u884c\u4e3a\uff0c PE100<\/sub>-b-PtBA48<\/sub>\/PE52<\/sub>\u4e2dPE\u65e0\u6cd5\u5b8c\u5168\u6392\u51fa\uff0cPtBA\u5d4c\u6bb5\u5728\u8868\u9762\u5f62\u62104nm\u7684\u8868\u5c42\uff0c\u5f62\u6210\u4e86\u5728AFM\u4e0a\u989d\u5916\u76848nm\u7684\u9ad8\u5ea6\uff0cPE\u6676\u4f53\u7684\u9ad8\u5ea6\u4e3a24nm\u3002\u67f1\u72b6\u80f6\u675f\u7684\u6838\u662f\u7531\u5355\u5c42PE\u5d4c\u6bb5\u6676\u4f53\u7ec4\u6210\uff0c\u4e0e\u6df7\u5408\u5355\u6676\u7684\u53cc\u5c42\u7ed3\u6784\u4e0d\u540c<\/p>\n

\u56fe<\/strong>4 <\/strong>\u4e0d\u540c<\/strong>WBCP<\/sub>\/WPE<\/sub><\/strong>\u5728<\/strong>DMF<\/strong>\u4e2d\u4e0d\u540c\u8d28\u91cf\u6bd4\u7684\u6837\u54c1\uff0c<\/strong>75o<\/sup>C<\/strong>\u7ed3\u6676\u7684<\/strong>TEM<\/strong>\u56fe<\/strong>,AFM<\/strong>\u56fe\u548c\u76f8\u4f4d\u89d2\u56fe<\/strong><\/p>\n

<\/strong><\/p>\n

a-b: WBCP<\/sub>\/WPE<\/sub>\u4e3a1\/1 \u548c2\/1\u7684\u6df7\u5408\u5355\u6676\u7684TEM\u56fe\uff0c\u5706\u7b52\u72b6\u80f6\u675f\u6cbf\u7740\u6df7\u5408\u5355\u6676\u4fa7\u9762\u751f\u957f\uff1b<\/p>\n

c:\u4e3aWBCP<\/sub>\/WPE<\/sub>=2\/1,75o<\/sup>C\u7ed3\u6676\u7684AFM\u9ad8\u5ea6\u56fe\uff0c\u4e0eb\u56fe\u5f62\u72b6\u76f8\u8fd1\uff1b<\/p>\n

d:\u4e3a\u5bf9\u5e94c\u7684\u9ad8\u5ea6\u56fe\uff0c PE\u5d4c\u6bb5\u7ed3\u6676\u4e3a12nm\uff0cPtBA\u5c42\u5728PE\u8868\u9762\u539a\u5ea6\u4e3a4nm\uff0c\u80f6\u675f\u9ad8\u5ea6\u4e3a20nm\uff0c\u4e0eAFM\u56fe\u543b\u5408\uff1b<\/p>\n

e:\u4e3aWBCP<\/sub>\/WPE<\/sub>=2\/1,75o<\/sup>C\u7ed3\u6676\u7684\u6676\u4f53\/\u80f6\u675f\u5171\u7ec4\u88c5\u4f53\u7684AFM\u76f8\u4f4d\u56fe\uff1b<\/p>\n

f:\u4e3aWBCP<\/sub>\/WPE<\/sub>=2\/1,75o<\/sup>C\u7ed3\u6676\u7684\u6676\u4f53\/\u80f6\u675f\u5171\u7ec4\u88c5\u4f53\u7684\u76f8\u4f4d\u89d2\u5206\u6790\uff0c\u6b64\u7ed3\u679c\u9a8c\u8bc1\u4e86\u6df7\u5408\u5355\u6676\u7684\u68af\u5ea6\u7ed3\u6784<\/p>\n

\u56fe<\/strong>5 <\/strong>\u4e3a<\/strong>WBCP<\/sub>\/WPE<\/sub>=1\/1<\/strong>\u5728<\/strong>DMF<\/strong>\u4e0d\u540c\u6e29\u5ea6\u7ed3\u6676\u7684<\/strong>TEM,<\/strong>\u7535\u5b50\u884d\u5c04<\/strong>(SAED)<\/strong>\u548c<\/strong>AFM<\/strong>\u9ad8\u5ea6\u56fe<\/strong><\/p>\n

<\/strong><\/p>\n

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b:\u4e3aa\u5bf9\u5e94\u7684\u67f1\u72b6\u80f6\u675f\u751f\u957f\u7684SAED\u56fe\uff0c\u7531b\u56fe\u5f97\u51fa\u67f1\u72b6\u80f6\u675f\u8d8b\u5411\u4e8e\u5728PE\u6676\u4f53\u7684[020]\u6676\u9762\u4e0a\u751f\u957f\uff1b<\/p>\n

d:\u572850 o<\/sup>C\u7ed3\u6676\u7684\u5355\u6676\u7684AFM\u56fe\uff0c\u8868\u9762\u8d77\u4f0f\u7684\u6676\u4f53\u5f88\u5c0f\uff0c<\/p>\n

e:\u4e3ad\u56fe\u7684\u5bf9\u5e94\u9ad8\u5ea6\u56fe\uff0c\u6df7\u5408\u5355\u6676\u9ad8\u5ea6\u4e3a32nm\uff0c\u7ed3\u679c\u9a8c\u8bc1\u4e8650 o<\/sup>C\u7ed3\u6676\u7684\u5355\u6676\u8fb9\u7f18\u80f6\u675f\u751f\u957f\u5f97\u8f83\u5c0f<\/p>\n

\u56fe<\/strong>6<\/strong>\u4e3a\u4e0d\u540c\u6eb6\u5242\u548c\u4e0d\u540c<\/strong>WBCP<\/sub>\/WPE<\/sub><\/strong>\u5728<\/strong>75o<\/sup>C<\/strong>\u7ed3\u6676\u7684\u7247\u72b6\u6676\u4f53\u7684<\/strong>TEM<\/strong>\u56fe<\/strong><\/p>\n

<\/strong><\/p>\n

a,b: \u6eb6\u5242\u4e3aVxylene\/VDMF<\/sub>\u4e3a1\/9\uff0cWBCP<\/sub>\/WPE<\/sub>\u4e3a0.4\/1 \u548c1\/1\u5171\u7ec4\u88c5\u4f53\u7684TEM\u56fe\uff0c\u6574\u4f53\u5f62\u72b6\u4ecd\u4e3a\u622a\u89d2\u68f1\u578b\uff0c\u8868\u793a\u4e8c\u7532\u82ef\u5bf9\u5171\u7ec4\u88c5\u884c\u4e3a\u7684\u6291\u5236\u4f5c\u7528\uff0c\u4f46\u5c11\u91cf\u7684\u4e8c\u7532\u82ef\u4e0d\u4f1a\u6539\u53d8BCP\u989d\u6784\u8c61\uff1b<\/p>\n

c,d:\u4e3aVxylene\/VDMF<\/sub>\u4e3a1\/1, WBCP<\/sub>\/WPE<\/sub>\u4e3a0.4\/1 \u548c1\/1\u5728b\u65b9\u5411\u4e0a\u7684\u5f62\u8c8c\uff0c\u7531\u6b64\u53ef\u4ee5\u5f97\u5230\u7ed3\u6676\u521d\u671f\u751f\u957f\u53d7\u9650\uff0c\u9020\u6210\u4e86\u5355\u6676\u7684\u900f\u955c\u5f62\u8c8c\uff1b<\/p>\n

\u4e8c\u7532\u82ef\u5bf9BCP\u6709\u66f4\u597d\u7684\u76f8\u5bb9\u6027\uff0c\u5728\u6eb6\u5242\u4e2d\u57fa\u672c\u4e0a\u770b\u4e0d\u5230\u67f1\u72b6\u80f6\u675f\uff0c\u8868\u793a\u51e0\u4e4e\u6240\u6709\u7684BCPs\u90fd\u8fdb\u5165\u4e86\u6df7\u5408\u5355\u6676\u4e2d\uff0c\u4f46\u67f1\u72b6\u80f6\u675f\u4ecd\u53ef\u4ee5\u5728\u66f4\u591a\u51cf\u5c11Vxylene\/VDMF<\/sub>\uff0c\u589e\u5927WBCP<\/sub>\/WPE<\/sub>\u7684\u6676\u4f53\u4e2d\u53d1\u73b0\u3002<\/p>\n

\u56fe<\/strong>7<\/strong>\u4e3a<\/strong>WBCP<\/sub>\/WPE<\/sub><\/strong>\u5728<\/strong>o-xylene\/DMF<\/strong>\u6eb6\u5242\u4e2d<\/strong>75o<\/sup>C<\/strong>\u901a\u8fc7\u4e24\u6b65\u6cd5\u7ed3\u6676\u5236\u5f97\u7684\u5171\u7ec4\u88c5\u4f53\uff0c\u5728\u4e0d\u540c\u5c3a\u5ea6\u4e0b\u7684<\/strong>TEM<\/strong>\u56fe<\/strong><\/p>\n

<\/strong><\/p>\n

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\u3010\u5c0f\u7ed3<\/strong>\u3011<\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Crystallization-Driven Co-Assembly of Micrometric Polymer Hybrid Single Crystals and Nanometric Crystalline Micelles<\/a> \uff08Macromolecules 2017, DOI: 10.1021\/acs.macromol.7b00105\uff09<\/p>\n

\u611f\u8c22\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u9ad8\u5206\u5b50\u7ec4Andy_chen\u63d0\u4f9b\u7d20\u6750\uff0c\u6750\u6599\u725b\u7f16\u8f91\u6574\u7406\u3002<\/p>\n

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