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\u5f15\u8a00<\/strong><\/span><\/h3>\n

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\u8d85\u8f7b\u6750\u6599\u7684\u6027\u80fd\u4e3b\u8981\u53d6\u51b3\u4e8e\u5b83\u7684\u7ed3\u6784\uff08\u5b54\u9699\u548c\u56fa\u4f53\u6210\u5206\u5728\u7a7a\u95f4\u4e0a\u7684\u5206\u5e03\uff09\u548c\u56fa\u4f53\u6210\u5206\u7684\u6027\u80fd\uff08\u521a\u5ea6\u3001\u5f3a\u5ea6\u7b49\uff09\u3002\u73b0\u6709\u7684\u8d85\u8f7b\u6750\u6599\u6709\u4e8c\u6c27\u5316\u7845\u6c14\u51dd\u80f6\uff08\u03c1\u2265 1 mg\/cm3<\/sup>\uff09\u3001\u78b3\u7eb3\u7c73\u7ba1\u6c14\u51dd\u80f6\uff08\u03c1\u22654mg\/cm3<\/sup> \uff09\u3001 \u91d1 \u5c5e \u6ce1 \u6cab\uff08\u03c1\u226510mg\/cm3<\/sup>\uff09\u3001\u805a\u5408\u7269\u6ce1\u6cab\uff08\u03c1\u22658mg\/cm3<\/sup> \uff09\u3001\u8d85\u8f7b\u7684\u6c2e\u5316\u787c\u6ce1\u6cab\uff08\u03c1\u2265 1.6mg\/cm3<\/sup>\uff09\u4ee5\u53ca\u91d1\u5c5e\u5fae\u6676\u683c\uff08\u03c1\u2265 0.9mg\/cm3<\/sup>\uff09\u7b49\u3002<\/p>\n

1.\u6c14\u51dd\u80f6<\/strong><\/span><\/h3>\n

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1.1\u00a0<\/b>\u7845\u7cfb\u6c14\u51dd\u80f6<\/h4>\n

\u7845\u7cfb\u7684\u6c14\u51dd\u80f6\u662f\u6c14\u51dd\u80f6\u4e2d\u6700\u4f20\u7edf\u4e5f\u662f\u6700\u5e38\u89c1\u7684\u4e00\u7c7b\u3002 \u7845\u7cfb\u6c14\u51dd\u80f6\u4e2d\u4e3b\u8981\u7684\u5c31\u662f\u4e8c\u6c27\u5316\u7845\u6c14\u51dd\u80f6\uff0c\u88ab\u79f0\u4f5c\u201c\u84dd\u70df\u201d\u3001\u201c\u56fa\u4f53\u70df\u201d\u3002 Tilloton\u7b49\u901a\u8fc7\u6539\u826f\u7684\u4e24\u6b65\u6eb6\u80f6-\u51dd\u80f6\u8fc7\u7a0b\u5236\u5907\u51fa\u4e86\u65e0\u88c2\u7f1d\u3001\u5bc6\u5ea6\u57283-80 mg\/cm3<\/sup>\u7684\u900f\u660e\u4e8c\u6c27\u5316\u7845\u6c14\u51dd\u80f6\u6750\u6599\u3002 \u5f97\u5230\u7684\u4e8c\u6c27\u5316\u7845\u6c14\u51dd\u80f6\u7684\u5bc6\u5ea6\u66f4\u4f4e\u3002 \u800cKoncon\u7b49\u901a\u8fc7\u8d85\u4e34\u754c\u7684\u4e59\u9187\u5e72\u71e5\u4e24\u6b65\u6eb6\u80f6\u2043\u51dd\u80f6\u8fc7\u7a0b\u5f97\u5230\u7684\u4e8c\u6c27\u5316\u7845\u6c14\u51dd\u80f6\uff0c\u5bc6\u5ea6\u66f4\u5c0f\uff0c\u5176\u6700\u5c0f\u5bc6\u5ea6\u53ef\u8fbe\u52302.3mg\/cm3<\/sup>\u3002<\/p>\n

1.2 \u78b3\u7cfb\u6c14\u51dd\u80f6<\/h4>\n

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\u00a02.\u00a0<\/strong>\u6ce1\u6cab\u6750\u6599<\/strong><\/span><\/h3>\n

\u6ce1\u6cab\u6750\u6599\u3001\u6c14\u51dd\u80f6\u4ee5\u53ca\u4e4b\u540e\u8981\u4ecb\u7ecd\u7684\u70b9\u9635\u6750\u6599\u5747\u5c5e\u4e8e\u591a\u5b54\u6750\u6599\u3002 \u591a\u5b54\u6750\u6599\u662f\u751f\u7269\u6750\u6599\u4e2d\u666e\u904d\u5b58\u5728\u7684\u4e00\u79cd\u5178\u578b\u7ed3\u6784\uff0c\u5e76\u5728\u52a8\u690d\u7269\u7b49\u751f\u7269\u4f53\u5185\u53d1\u6325\u7740\u4e0d\u53ef\u66ff\u4ee3\u7684\u751f\u7269\u4f5c\uff0c\u5982\u5e38\u89c1\u7684\u6728\u6750\u3001\u73ca\u745a\u3001\u9aa8\u5934\u7b49\u5929\u7136\u591a\u5b54\u7ed3\u6784\u7684\u6750\u6599\u80fd\u591f\u957f\u671f\u627f\u53d7\u5de8\u5927\u7684\u8f7d\u8377\u3002\u591a\u5b54\u6750\u6599\u7531\u56fa\u4f53\u9aa8\u67b6\u548c\u5927\u91cf\u7684\u5b54\u9699\u7ec4\u6210\uff0c\u5b54\u9699\u7684\u5b58\u5728\u964d\u4f4e\u4e86\u6750\u6599\u7684\u8d28\u91cf\uff0c\u540c\u65f6\u4e5f\u589e\u5927\u4e86\u6750\u6599\u7684\u6bd4\u8868\u9762\u79ef\u3002\u591a\u5b54\u6750\u6599\u6309\u7167\u7ed3\u6784\u89c4\u5219\u7a0b\u5ea6\u5212\u5206\u4e3a\u4e24\u79cd\u7c7b\u578b\uff0c\u4e00\u7c7b\u662f\u65e0\u5e8f\u591a\u5b54\u6750\u6599\uff0c\u5982\u6c14\u51dd\u80f6\u548c\u6ce1\u6cab\u6750\u6599\u3002 \u53e6\u4e00\u7c7b\u662f\u6709\u5e8f\u591a\u5b54\u7ed3\u6784\u7684\u6750\u6599\uff0c\u5982\u70b9\u9635\u6750\u6599\u3002<\/p>\n

\u6ce1\u6cab\u6750\u6599\u4f5c\u4e3a\u4e00\u79cd\u542b\u6709\u65e0\u5e8f\u5b54\u9699\u7684\u591a\u5b54\u6750\u6599\uff0c\u6309\u7167\u5b54\u9699\u7684\u5f62\u6001\u53ef\u5206\u4e3a\u5f00\u5b54\u6ce1\u6cab\u548c\u95ed\u5b54\u6ce1\u6cab\u3002\u5f00\u5b54\u6ce1\u6cab\u6307\u7684\u662f\u5b54\u9699\u4e0e\u5b54\u9699\u95f4\u76f8\u901a\uff0c\u95ed\u5b54\u6ce1\u6cab\u5373\u5b54\u9699\u8868\u9762\u662f\u95ed\u5408\u7684\uff0c\u5b54\u9699\u4e0e\u5b54\u9699\u95f4\u88ab\u56fa\u4f53\u9aa8\u67b6\u6240\u9694\u5f00\u3002\u800c\u6309\u7167\u6ce1\u6cab\u6750\u8d28\u7684\u4e0d\u540c\uff0c\u53ef\u5206\u4e3a\u91d1\u5c5e\u6ce1\u6cab\u3001\u78b3\u7cfb\u6ce1\u6cab\u548c\u805a\u5408\u7269\u6ce1\u6cab\u3002 \u4e0b\u9762\u5c31\u6309\u7167\u6750\u8d28\u7684\u4e0d\u540c\u5bf9\u8d85\u8f7b\u6ce1\u6cab\u6750\u6599\u8fdb\u884c\u4ecb\u7ecd\u3002<\/p>\n

2.1 \u91d1\u5c5e\u6ce1\u6cab<\/h4>\n

\u91d1\u5c5e\u6ce1\u6cab\u662f\u4e0a\u4e16\u7eaa80\u5e74\u4ee3\u540e\u671f\u624d\u8fc5\u901f\u53d1\u5c55\u8d77\u6765\u7684\u4e00\u79cd\u7ed3\u6784\u529f\u80fd\u6750\u6599\u3002\u91d1\u5c5e\u6ce1\u6cab\u4e0d\u4ec5\u5177\u6709\u91d1\u5c5e\u672c\u8eab\u7684\u5bfc\u7535\u5bfc\u70ed\u6027\uff0c\u4e5f\u7531\u4e8e\u8be5\u79cd\u6ce1\u6cab\u7684\u7ed3\u6784\u5177\u6709\u8bf8\u5982\u8f7b\u8d28\u3001\u9ad8\u6bd4\u8868\u9762\u3001\u521a\u6027\u5927\u3001\u51cf\u632f\u6548\u679c\u597d\u7b49\u7269\u7406\u6027\u80fd\uff0c\u6240\u4ee5\u4f5c\u4e3a\u65b0\u578b\u7684\u529f\u80fd\u6750\u6599\u5177\u6709\u5e7f\u6cdb\u7684\u5e94\u7528\uff0c\u5982\u6c7d\u8f66\u4ee5\u53ca\u822a\u5929\u98de\u673a\u7684\u5236\u9020\u4e2d\u3002\u4f46\u662f\u968f\u7740\u78b3\u7cfb\u6ce1\u6cab\u4ee5\u53ca\u70b9\u9635\u6750\u6599\u7684\u51fa\u73b0\uff0c\u91d1\u5c5e\u6ce1\u6cab\u4e0d\u8bba\u662f\u4ece\u6750\u8d28\u8fd8\u662f\u7ed3\u6784\u6765\u8bf4\uff0c\u5176\u5e94\u7528\u90fd\u53d7\u5230\u4e86\u4e00\u5b9a\u7684\u9650\u3002 \u800c\u4e14\uff0c\u91d1\u5c5e\u6ce1\u6cab\u7684\u5bc6\u5ea6\u867d\u5c5e\u4e8e\u8f7b\u8d28\uff0c\u4f46\u662f\u8fbe\u5230\u8d85\u8f7b\u8303\u56f4\u7684\u5374\u4e0d\u591a\u3002Taappan \u7b49\u5728\u60f0\u6027\u6c14\u4f53\u4e2d\u5c06\u6d3b\u6027\u914d\u4f53\u82ef\u5e76\u4e09\u5511(BTA)\u4e0e\u91d1\u5c5e\u94c1\u914d\u4f4d\uff0c\u901a\u8fc7\u5c06\u914d\u4f4d\u4f53\u81ea\u8513\u5ef6\u71c3\u70e7\u7684\u65b9\u6cd5\u5f97\u5230\u94c1\u7684\u91d1\u5c5e\u6ce1\u6cab\uff08\u56fe 1\uff09\u3002\u8fd9\u79cd\u6ce1\u6cab\u7684\u5bc6\u5ea6\u53ef\u8fbe\u523011 mg\/cm3<\/sup>\uff0c\u6bd4\u8868\u9762\u79ef\u4e3a 270m2<\/sup>\/g\u3002\u4ed6\u4eec\u8fd8\u901a\u8fc7\u8fd9\u79cd\u65b9\u6cd5\u5f97\u5230\u4e86\u94b4\u3001\u954d\u3001\u94dc\u7684\u91d1\u5c5e\u6ce1\u6cab\u3002<\/p>\n

<\/h5>\n
\u56fe 1 \u94c1\u6ce1\u6cab\uff1a(a) \u94c1\u6ce1\u6cab\u548c\u672a\u71c3\u70e7\u7684Fe-BTA\uff1b(b)\u914d\u4f4d\u4f53\u81ea\u8513\u5ef6\u71c3\u70e7\u6cd5\u5236\u5907\u7684\u94c1\u6ce1\u6cab SEM\u00a0\u56fe (1\u03bcm)\uff1b\uff08c\uff09 \u56fe(b)\u7684\u653e\u5927\u56fe(200nm)<\/h5>\n

2.2 \u78b3\u7cfb\u6ce1\u6cab<\/h4>\n

\u78b3\u7cfb\u6ce1\u6cab\u7ecf\u5e38\u7531\u91d1\u5c5e\u6ce1\u6cab\u4f5c\u50ac\u5316\u5242\u5728\u5176\u57fa\u7840\u4e0a\u52a0\u5de5\u5f97\u6765\u3002 \u4f46\u662f\u4e0e\u91d1\u5c5e\u6ce1\u6cab\u76f8\u6bd4\u78b3\u7cfb\u6ce1\u6cab\u5177\u6709\u66f4\u591a\u7684\u529f\u80fd\u3002\u5982\u7531Wu\u7b49\u5236\u5907\u5f97\u5230\u76843D\u77f3\u58a8\u70ef\u6ce1\u6cab\u662f\u901a\u8fc7\u954d\u6ce1\u6cab\u505a\u727a\u7272\u6a21\u677f\uff0c\u5c06\u7535\u5904\u7406\u8fc7\u540e\u7684\u8584\u77f3\u58a8\u70ef\u6c89\u79ef\u5728\u6a21\u677f\u4e0a\uff0c\u7136\u540e\u5728FeCl3<\/sub>\/HCl\u7684\u6df7\u5408\u6eb6\u6db2\u4e2d\u5c06\u6a21\u677f\u8150\u8680\u6389\u5f97\u5230\u7684\u3002\u8fd9\u79cd\u77f3\u58a8\u70ef\u6ce1\u6cab\u53ef\u7528\u4f5c\u8d85\u7ea7\u7535\u5bb9\u5668\u3002 \u5176\u5728\u6c34\u7535\u89e3\u8d28\u4e2d\uff0c\u5f53\u7535\u6d41\u5bc6\u5ea6\u4e3a0.5A\/g\u65f6\uff0c\u53ef\u63d0\u4f9b113.2F\/g\u7684\u7535\u5bb9\u91cf\uff0c\u4e14\u5728\u5faa\u73af1000\u6b21\u4e4b\u540e\uff0c\u4ecd\u53ef\u4ee5\u4fdd\u630190%\u7684\u7535\u5bb9\u91cf\u3002<\/p>\n

Chen \u7b49\u5219\u5229\u7528CVD\u7684\u65b9\u6cd5\u7528\u7532\u70f7\u505a\u78b3\u6e90\uff0c\u5728\u954d\u6ce1\u6cab\u4e0a\u53cd\u5e94\u540e\u901a\u8fc7\u5728 FeCl3<\/sub>\/HCl\u7684\u6df7\u5408\u6eb6\u6db2\u4e2d\u5c06\u6a21\u677f\u8150\u8680\u6389\uff0c\u4ece\u800c\u5f97\u5230\u5bc6\u5ea6\u7ea6\u4e3a2-3 mg\/cm3<\/sup>\u7684\u77f3\u58a8\u70ef\u6ce1\u6cab(\u56fe2)\u3002<\/p>\n

<\/h5>\n
\u56fe 2\u00a0\u77f3\u58a8\u70ef\u6ce1\u6cab\uff1a\uff08a\uff09170\u00d7220\u00a0mm2<\/sup>\u00a0\u81ea\u652f\u6491\u77f3\u58a8\u70ef\u6ce1\u6cab\u7684\u7167\u7247\uff1b(b)\u77f3\u58a8\u70ef\u6ce1\u6cab\u7684 SEM\u00a0\u7167\u7247<\/h5>\n

2.3 \u805a\u5408\u7269\u6ce1\u6cab<\/h4>\n

\u805a\u5408\u7269\u6ce1\u6cab\u540c\u6837\u5177\u5907\u8f7b\u8d28\u9ad8\u5f3a\u7684\u6027\u8d28\uff0c\u540c\u65f6\u7531\u4e8e\u805a\u5408\u7269\u7279\u6709\u7684\u6027\u8d28\uff0c\u805a\u5408\u7269\u901a\u5e38\u5177\u6709\u5f62\u72b6\u53ef\u5851\u6027\u53ca\u8bb0\u5fc6\u529f\u80fd\u3002Singha\u00a0\u7b49\u5229\u7528\u4e8c\u6c27\u5316\u78b3\u6c14\u4f53\u53d1\u6ce1\u7684\u65b9\u6cd5\u5236\u5907\u5f97\u5230\u4e00\u79cd\u5bc6\u5ea6\u4e3a 15mg\/cm3<\/sup>\u7684\u805a\u6c28\u916f\u6ce1\u6cab.\u8fd9\u79cd\u805a\u5408\u7269\u6ce1\u6cab\u5177\u6709\u597d\u7684\u5f62\u72b6\u8bb0\u5fc6\u529f\u80fd\u548c\u751f\u7269\u76f8\u5bb9\u3002Shastri\u7b49\u901a\u8fc7\u78b3\u6c22\u5316\u5408\u7269\u9897\u7c92\u505a\u6a21\u677f\u5236\u5907\u5f97\u5230\u4e00\u79cd\u4f4e\u5bc6\u5ea6\u7684\u5927\u5b54\u805a\u4e73\u9178\u6ce1\u6cab\u3002\u8fd9\u79cd\u6ce1\u6cab\u5177\u6709\u826f\u597d\u7684\u5f62\u72b6\u53ef\u5851\u6027\uff0c\u53ef\u7528\u4e8e\u56fa\u4f53\u652f\u6491\u548c\u533b\u7597\u8bbe\u5907\u3002\u4e5f\u53ef\u7528\u4f5c\u70ed\u548c\u673a\u68b0\u7edd\u7f18\u4f53\u3002 \u7528\u78b3\u6c22\u5316\u5408\u7269\u9897\u7c92\u505a\u6a21\u7248\u53ef\u4ee5\u63a7\u5236\u6ce1\u6cab\u7a7a\u9699\u7684\u5b54\u5f84\u5927\u5c0f\u548c\u5f62\u72b6\uff0c\u4e3a\u5236\u5907\u591a\u5b54\u6750\u6599\u63d0\u4f9b\u4e86\u4e00\u4e2a\u5f88\u597d\u7684\u63a7\u5236\u5b54\u9699\u7684\u65b9\u6cd5\u3002\u4ee5\u4e0a\u603b\u7ed3\u53ef\u4ee5\u770b\u51fa\uff0c\u91d1\u5c5e\u6ce1\u6cab\u3001\u78b3\u7cfb\u6ce1\u6cab\u548c\u805a\u5408\u7269\u6ce1\u6cab\u7684\u4f4e\u5bc6\u5ea6\u90fd\u662f\u901a\u8fc7\u6ce1\u6cab\u7ed3\u6784\u7684\u591a\u5b54\u6027\u6765\u5b9e\u73b0\u7684\u3002 \u4f46\u662f\u6ce1\u6cab\u7684\u5b54\u9699\u4e0e\u6c14\u51dd\u80f6\u76f8\u6bd4\uff0c\u901a\u5e38\u5b54\u7684\u5c3a\u5bf8\u8f83\u5927\u4f46\u662f\u5b54\u9699\u5ea6\u4e0d\u8db3\uff0c\u8fd9\u4e5f\u662f\u73b0\u6709\u7684\u6ce1\u6cab\u6750\u6599\u6ca1\u6709\u6c14\u51dd\u80f6\u5bc6\u5ea6\u66f4\u4f4e\u7684\u539f\u56e0\u3002<\/p>\n

3.\u5fae\u70b9\u9635\u6750\u6599<\/strong><\/span><\/h3>\n

\u5fae\u70b9\u9635\u6750\u6599\u662f\u8fd1\u5e74\u6765\u5174\u8d77\u7684\u4e00\u79cd\u65b0\u9896\u7684\u591a\u529f\u80fd\u8d85\u8f7b\u6750\u6599\u3002 \u5c24\u5176\u662f\u4ece 2011\u00a0\u5e74 Schaedler \u7b49\u5236\u5907\u5f97\u5230\u8d85\u8f7b\u591a\u5b54\u5fae\u70b9\u9635\u954d\u6750\u6599(\u03c1 \u2265 0.9mg\/cm3<\/sup>)\u00a0<\/sup>\u6210\u4e3a\u5f53\u65f6\u201c\u4e16\u754c\u4e0a\u6700\u8f7b\u7684\u6750\u6599\u201d\u4ee5\u6765\uff0c\u5fae\u70b9\u9635\u6750\u6599\u7684\u7814\u7a76\u5c31\u6c79\u6d8c\u800c\u81f3\u3002Xiong\u5df2\u7ecf\u5bf9\u5fae\u70b9\u9635\u6750\u6599\u7684\u79cd\u7c7b\u3001\u6027\u80fd\u3001\u7528\u9014\u7b49\u65b9\u9762\u8fdb\u884c\u4e86\u4e00\u5b9a\u7684\u603b\u7ed3\u3002 \u5fae\u70b9\u9635\u6750\u6599\u6700\u5927\u7684\u7279\u70b9\u662f\u5176\u7ed3\u6784\u7684\u6709\u5e8f\u6027\u3002 \u5fae\u70b9\u9635\u6750\u6599\u4e0e\u6ce1\u6cab\u76f8\u6bd4\u662f\u4e00\u79cd\u5468\u671f\u6027\u6709\u5e8f\u7684\u591a\u5b54\u6750\u6599\u3002 \u5b54\u9699\u65e0\u5e8f\u7684\u6750\u6599\u76f8\u5bf9\u6bd4\u8868\u9762\u79ef\u9ad8\uff0c\u8868\u89c2\u5bc6\u5ea6\u5c0f\uff0c\u6709\u5e8f\u7ed3\u6784\u76f8\u6bd4\u8fd9\u65b9\u9762\u7684\u6027\u8d28\u4f1a\u7a0d\u5fae\u5dee\u4e00\u70b9\uff0c\u4f46\u662f\u7531\u4e8e\u5176\u6709\u5e8f\u6027\u4f7f\u5f97\u6750\u6599\u5177\u6709\u9ad8\u7684\u786c\u5ea6\u548c\u5f3a\u5ea6\u3002\u800c\u9ad8\u5f3a\u5ea6\u6750\u6599\u5728\u5e94\u7528\u65b9\u9762\u66f4\u5360\u4f18\u52bf\u3002\u4ece\u56fe3\u5c31\u53ef\u4ee5\u770b\u51fa\u70b9\u9635\u6750\u6599\u5728\u673a\u68b0\u5f3a\u5ea6\u65b9\u9762\u7684\u4f18\u52bf\u3002<\/p>\n

<\/h5>\n
\u56fe 3 \u00a0\u73b0\u6709\u6750\u6599\u7684\u5f3a\u5ea6\u4e0e\u5bc6\u5ea6\u7684\u5173\u7cfb\u56fe<\/h5>\n

3.1 \u91d1\u5c5e\u5fae\u70b9\u9635\u6750\u6599<\/h4>\n

\u91d1\u5c5e\u5fae\u70b9\u9635\u6750\u6599\u662f\u6700\u5148\u51fa\u73b0\u7684\u5fae\u70b9\u9635\u6750\u6599\u7684\u7c7b\u578b\u30022011\u5e74\u7f8e\u56fd\u52a0\u5dde\u5927\u5b66\u6b27\u6587\u5206\u6821\u548c\u52a0\u5dde\u7406\u5de5\u5927\u5b66\u7684\u7814\u7a76\u8005\u4eec(Schaedler \u7b49) \u5229\u7528\u81ea\u8513\u5ef6\u5149\u805a\u5408\u6cd5\u5236\u5907\u5f97\u5230\u7684\u786b\u9187\u2043\u70ef\u805a\u5408\u7269\u5fae\u70b9\u9635\u4f5c\u4e3a\u6a21\u677f\uff0c\u4e4b\u540e\u518d\u6a21\u677f\u4e0a\u8fdb\u884c\u5316\u5b66\u9540\u954d\uff0c\u518d\u5c06\u6a21\u677f\u523b\u8680\u6389\u5f97\u5230\u6b63\u516b\u9762\u4f53\u7a7a\u5fc3\u7ba1\u5fae\u6676\u683c\u954d\u6750\u6599\uff0c\u9996\u6b21\u5236\u5907\u51fa\u4e86\u7ed3\u6784\u53ef\u63a7\u3001\u6750\u6599\u5229\u7528\u7387\u9ad8\u7684\u8d85\u8f7b\u591a\u5b54\u5fae\u70b9\u9635\u6750\u6599\uff0c\u5bc6\u5ea6\u6700\u5c0f\u53ef\u8fbe0.9mg\/cm3<\/sup>\u8be5\u6750\u6599\u80fd\u91cf\u5438\u6536\u5f3a\u4e0e\u5f39\u6027\u4f53\u76f8\u4f3c\u3002\u8be5\u6750\u6599\u7684\u8fd9\u4e9b\u4f18\u5f02\u7684\u6027\u80fd\u5f52\u56e0\u4e8e\u6750\u6599\u5728\u7ed3\u6784\u4e0a\u7684\u591a\u7ea7\u6b21\u5c3a\u5ea6\u7ed3\u6784\uff08\u4ece\u7eb3\u7c73\u5230\u5fae\u7c73\u81f3\u6beb\u7c73\uff09\uff0c\u8fd9\u79cd\u5c3a\u5ea6\u7ed3\u6784\u53ef\u4ece\u56fe4\u4e2d\u8868\u73b0\u51fa\u6765\u3002<\/p>\n

<\/h5>\n
\u56fe4\u00a0 \u5fae\u70b9\u9635\u954d\u7684\u5236\u5907\u6b65\u9aa4\u53ca\u7ed3\u6784\u5c42\u6b21\u56fe<\/h5>\n

Wang\u00a0\u7b49\u901a\u8fc73D \u6253\u5370\u7684\u65b9\u6cd5\u5236\u5907\u4e86\u805a\u5408\u7269\u70b9\u9635\uff0c\u7136\u540e\u5728\u5176\u8868\u9762\u8fdb\u884c\u5316\u5b66\u9540\u94dc\uff0c\u518d\u901a\u8fc7\u6052\u6e29(60\u2103)\u6d78\u6ce1\u5728\u6c22\u6c27\u5316\u94a0\u6eb6\u6db2\u4e2d\u3001\u65f6\u95f4\u4e3a24h\u7684\u65b9\u6cd5\u5c06 \u805a \u5408 \u7269 \u6a21 \u677f \u53bb \u9664\u3002 \u5f97 \u5230 \u4e86 \u6700 \u5c0f \u5bc6 \u5ea6 \u53ef \u8fbe7.2 mg \/cm3<\/sup>\u7684\u7a7a\u5fc3\u91d1\u5c5e\u94dc\u5fae\u70b9\u9635\u3002<\/p>\n

3.2 \u9676\u74f7\u5fae\u70b9\u9635\u6750\u6599<\/h4>\n

\u9676\u74f7\u662f\u4eba\u7c7b\u751f\u6d3b\u548c\u751f\u4ea7\u4e2d\u4e0d\u53ef\u6216\u7f3a\u7684\u4e00\u79cd\u6750\u6599\uff0c\u7531\u4e8e\u8f83\u9ad8\u7684\u5f3a\u5ea6\u3001\u786c\u5ea6\u53ca\u8010\u9ad8\u6e29\u3001\u6297\u8150\u8680\u6027\u7b49\u7279\u70b9\uff0c\u5176\u5e94\u7528\u8303\u56f4\u904d\u53ca\u5404\u4e2a\u9886\u57df\u3002 \u5c24\u5176\u5728\u6211\u56fd\uff0c\u9676\u74f7\u5236\u54c1\u4ece\u53e4\u81f3\u4eca\u90fd\u5728\u4eba\u4eec\u7684\u65e5\u5e38\u751f\u6d3b\u4e2d\u8d77\u7740\u91cd\u8981\u7684\u4f5c\u7528\u3002 \u4f46\u662f\u7531\u4e8e\u5176\u6613\u788e\u4e14\u5bf9\u4e8e\u88c2\u7f1d\u7684\u654f\u611f\u6027\uff0c\u5bf9\u4e8e\u5236\u5907\u7ed3\u6784\u6750\u6599\u6765\u8bf4\u4e0d\u662f\u6700\u4f18\u7684\u9009\u62e9\u3002\u9676\u74f7\u70b9\u9635\u6750\u6599\u4e0d\u4ec5\u8d85\u8f7b\u3001\u5f3a\u8d28\u4e14\u53ef\u5728\u4e00\u5b9a\u7a0b\u5ea6\u4e0a\u514b\u670d\u5176\u8106\u6027\u3002<\/p>\n

Meza \u7b49\u5c31\u8bc1\u5b9e\u4e86\u7eb3\u7c73\u7ea7\u7684\u9676\u74f7\u6750\u6599\u540c\u65f6\u5177\u5907\u8d85\u8f7b\u3001\u6bd4\u5f3a\u5ea6\u9ad8\u7684\u7b49\u7279\u6027\uff0c\u4e14\u53ef\u5728\u538b\u529b\u8fbe\u523050%\u65f6\uff0c\u4ecd\u53ef\u6062\u590d\u539f\u5f62\u3002\u8fd9\u79cd\u6750\u6599\u901a\u8fc7\u53cc\u5149\u5b50\u5149\u523b\u6280\u672f\u5f97\u5230\u805a\u5408\u7269\u6a21\u578b\uff0c\u7528\u5176\u505a\u6a21\u677f\uff0c\u901a\u8fc7\u539f\u5b50\u5c42\u6c89\u79ef\u9540\u4e0a\u4e00\u5c42\u7eb3\u7c73\u7ea7\u7684\u6c27\u5316\u94dd\u819c\uff0c\u5e76\u901a\u8fc7\u6c27\u6c14\u7b49\u79bb\u5b50\u4f53\u5c06\u805a\u5408\u7269\u6a21\u677f\u523b\u8680\u6389\uff0c\u5f97\u5230\u539a\u5ea6\u4e3a5-60nm\u7684\u4e2d\u7a7a\u6c27\u5316\u94dd\u9676\u74f7\u70b9\u9635\uff08\u56fe5\uff09\uff0c\u5bf9\u5e94\u7684\u5bc6\u5ea6\u4e3a6.3-258mg\/cm3<\/sup>\u3002\u8fd9\u79cd\u8d85\u8f7b\u7684\u9676\u74f7\u6750\u6599\u5177\u6709\u80fd\u91cf\u50a8\u5b58\u7684\u529f\u80fd\uff0c\u5e76\u53ef\u4ee5\u901a\u8fc7\u6539\u53d8\u539a\u5ea6\/\u534a\u5f84\u6bd4\u503c\u7684\u5927\u5c0f\uff0c\u51cf\u5c0f\u548c\u6291\u5236\u6750\u6599\u7684\u8106\u6027\u65ad\u88c2\u3002Meza\u7b49\u8fd8\u5229\u7528\u8fd9\u79cd\u65b9\u6cd5\u5f97\u5230\u539a\u5ea6\u4e3a75nm\u7684\u4e2d\u7a7a\u6c2e\u5316\u949b\u7eb3\u7c73\u70b9\u9635\uff0c\u8fd9\u79cd\u6750\u6599\u5177\u6709\u8f83\u597d\u7684\u673a\u68b0\u5f3a\u5ea6\uff0c\u5c48\u670d\u5e94\u529b\u53ef\u4ee5\u8fbe\u52301.75GPa\u3002<\/p>\n

<\/h5>\n
\u56fe 5 \u4e2d\u7a7a\u6c27\u5316\u94dd\u7eb3\u7c73\u70b9\u9635\uff1a(a)170\u00d7220\u00a0mm2<\/sup>\u00a0\u81ea\u652f\u6491\u77f3\u58a8\u70ef\u6ce1\u6cab\u7684\u7167\u7247\uff1b(b) \u77f3\u58a8\u70ef\u6ce1\u6cab\u7684SEM \u7167\u7247<\/h5>\n

3.3 \u78b3\u7cfb\u5fae\u70b9\u9635\u6750\u6599<\/h4>\n

\u4e0a\u8ff0\u5df2\u7ecf\u8bf4\u660e\u78b3\u6750\u6599\u5177\u6709\u4f18\u826f\u7684\u6027\u80fd\uff0c\u6545\u5404\u79cd\u8d85\u8f7b\u6750\u6599\u5747\u6709\u78b3\u7cfb\u6750\u8d28\u7684\u53c2\u4e0e\u3002 \u5fae\u70b9\u9635\u6750\u6599\u4e5f\u4e0d\u4f8b\u5916\uff0cJacobsen \u7b49\u57283D\u6253\u5370\u7684\u5149\u654f\u6811\u8102\u5fae\u70b9\u9635\u6750\u6599\u8868\u9762\u6d78\u6e0d\u4e19\u70ef\u8148\uff0c\u7136\u540e\u9ad8\u6e29\u70e7\u8680\u5f97\u5230\u4e86\u8d85\u8f7b\u7684\u73bb\u7483\u78b3\u5fae\u70b9\u9635\uff0c\u8fd9\u79cd\u6750\u6599\u7684\u538b\u7f29\u5f3a\u5ea6\u53ef\u8fbe\u523010.2MPa\u3002<\/p>\n

\u5fae\u70b9\u9635\u6750\u6599\u4f5c\u4e3a\u4e00\u79cd\u53ef\u8bbe\u8ba1\u6027\u5f88\u5f3a\u7684\u65b0\u578b\u8d85\u8f7b\u6750\u6599\u79cd\u7c7b\uff0c\u5df2\u7ecf\u5f97\u5230\u4e86\u4e00\u4e9b\u6027\u80fd\u4f18\u5f02\u7684\u8d85\u8f7b\u6750\u6599\u30023D \u6253\u5370\u7b49\u79d1\u6280\u7684\u7ed3\u5408\u4e3a\u70b9\u9635\u6750\u6599\u7684\u53d1\u5c55\u63d0\u4f9b\u652f\u6301\u548c\u4fdd\u8bc1\u3002 \u8fd9\u79cd\u6750\u6599\u7684\u7ed3\u6784\u66f4\u5229\u4e8e\u5f97\u5230\u529b\u5b66\u6027\u80fd\u5f3a\u7684\u8d85\u8f7b\u6750\u6599\uff0c\u8fd9\u5c31\u4f7f\u5f97\u5230\u5bc6\u5ea6\u66f4\u4f4e\u3001\u529b\u5b66\u6027\u80fd\u66f4\u5f3a\u7684\u6750\u6599\u5f97\u5230\u4e86\u8fdb\u4e00\u6b65\u7684\u53d1\u5c55\u3002<\/p>\n

Jiang\u7b49\u5728\u91d1\u5c5e\u5fae\u70b9\u9635\u3001\u9676\u74f7\u5fae\u70b9\u9635\u4ee5\u53ca\u78b3\u7cfb\u5fae\u70b9\u9635\u65b9\u9762\u8fdb\u884c\u4e86\u76f8\u5e94\u7684\u7814\u7a76\uff0c\u5229\u75283D \u6253\u5370\u6280\u672f\u5f97\u5230\u91d1\u521a\u77f3\u7ed3\u6784\u7684\u9ad8\u805a\u7269\u6a21\u578b\uff0c\u5e76\u901a\u8fc7\u5316\u5b66\u9540\u954d\u3001\u70e7\u8680\u6a21\u677f\u7684\u65b9\u6cd5\u5f97\u5230\u4e86\u5bc6\u5ea6\u4e3a19 mg\/cm3<\/sup>\u7684\u7a7a\u5fc3\u954d\u5fae\u70b9\u9635\uff08\u56fe6\uff09\uff0c\u63a5\u8fd1\u8d85\u8f7b\u6750\u6599\u7684\u8303\u56f4\u3002<\/p>\n

<\/h5>\n
\u56fe 6\u00a0\u7a7a\u5fc3\u954d\u5fae\u70b9\u9635\uff1a(a)\u7a7a\u5fc3\u954d\u5fae\u70b9\u9635\u7684\u7167\u7247\uff1b(b)\u7a7a\u5fc3\u954d\u5fae\u70b9\u9635\u91d1\u521a\u77f3\u7ed3\u6784\u7684 SEM\u7167\u7247<\/h5>\n

4.\u00a0<\/strong>\u603b\u7ed3<\/strong><\/span><\/h3>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u5404\u79cd\u6750\u6599\u5747\u6709\u5176\u4f18\u70b9\u4e5f\u6709\u4e00\u5b9a\u7684\u7f3a\u9677\u3002 \u8d85\u8f7b\u6750\u6599\u7684\u7814\u7a76\u8fd8\u9700\u4ece\u4ee5\u4e0b3\u4e2a\u65b9\u9762\u8fdb\u884c\u7814\u7a76:<\/p>\n

(1)\u5229\u7528\u5404\u79cd\u6750\u6599\u7684\u4f18\u70b9\u6765\u5236\u5907\u590d\u5408\u7ed3\u6784\u578b\u7684\u8d85\u8f7b\u6750\u6599\u3002<\/p>\n

(2)\u8d85\u8f7b\u6750\u6599\u7684\u529f\u80fd\u5316\u3002<\/p>\n

(3)\u5bfb\u627e\u5176\u4ed6\u7ed3\u6784\u6765\u4e30\u5bcc\u8d85\u8f7b\u6750\u6599\u7684\u591a\u6837\u6027\u3002<\/p>\n

\u968f\u7740\u5fae\u578b 3D\u00a0\u6253\u5370\u7b49\u79d1\u6280\u7684\u53d1\u5c55\uff0c\u5236\u5907\u4f53\u79ef\u66f4\u5c0f\u3001\u8d28\u91cf\u66f4\u8f7b\u3001\u5f3a\u5ea6\u66f4\u9ad8\u7684\u5fae\u70b9\u9635\u6750\u6599\u5df2\u7ecf\u6210\u4e3a\u8d85\u8f7b\u6750\u6599\u53d1\u5c55\u7684\u8d8b\u52bf\u3002 \u76f8\u4fe1\u4ee5\u540e\u8fd8\u4f1a\u51fa\u73b0\u6027\u80fd\u66f4\u591a\u3001\u66f4\u597d\u7684\u5fae\u70b9\u9635\u6750\u6599\u4ee5\u53ca\u66f4\u4f18\u4e8e\u73b0\u6709\u7ed3\u6784\u7684\u8d85\u8f7b\u6750\u6599\uff0c\u5c24\u5176\u5728\u65b0\u7684\u589e\u6750\u5236\u9020\u65b9\u9762\u5c06\u4f1a\u53d1\u6325\u66f4\u5927\u7684\u4f5c\u7528\u3002<\/p>\n

\u539f\u6587\u94fe\u63a5\uff1a\u8d85\u8f7b\u6750\u6599<\/a><\/strong><\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u5b66\u672f\u5e72\u8d27\u7ec4 \u5927\u5b8b\u3001\u8def\u6960 \u00a0\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u7f16\u8f91\u6574\u7406\u3002<\/p>\n

\u6750\u6599\u4eba\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u8fd9\u91cc\u6c47\u96c6\u4e86\u5404\u5927\u9ad8\u6821\u7855\u535a\u751f\u3001\u4e00\u7ebf\u79d1\u7814\u4eba\u5458\u4ee5\u53ca\u884c\u4e1a\u4ece\u4e1a\u8005\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u7f16\u8f91\u90e8<\/a>\u3002<\/p>\n

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