{"id":63343,"date":"2017-02-04T06:30:47","date_gmt":"2017-02-03T22:30:47","guid":{"rendered":"\/\/m.iemloyee.com\/?p=63343"},"modified":"2017-02-06T12:30:27","modified_gmt":"2017-02-06T04:30:27","slug":"%e5%ad%a6%e6%9c%af%e5%b9%b2%e8%b4%a7%e4%b8%a8%e8%b0%83%e5%88%b6%e5%b7%ae%e7%a4%ba%e6%89%ab%e6%8f%8f%e9%87%8f%e7%83%ad%e6%b3%95%e5%9c%a8%e9%ab%98%e5%88%86%e5%ad%90%e6%9d%90%e6%96%99%e4%b8%ad%e7%9a%84","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=63343","title":{"rendered":"\u5b66\u672f\u5e72\u8d27\u4e28\u8c03\u5236\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\u5728\u9ad8\u5206\u5b50\u6750\u6599\u4e2d\u7684\u5e94\u7528"},"content":{"rendered":"

\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\uff08Differential scanning calorimetry ,\u7b80\u79f0DSC\uff09\u662f\u8868\u5f81\u805a\u5408\u7269\u6027\u80fd\u7684\u4e00\u79cd\u975e\u5e38\u5feb\u901f\u6709\u6548\u7684\u5206\u6790\u65b9\u6cd5\uff0c\u5728\u9ad8\u5206\u5b50\u3001\u5316\u5b66\u54c1\u3001\u98df\u54c1\u548c\u836f\u7269\u7b49\u9886\u57df\u6709\u975e\u5e38\u5e7f\u6cdb\u7684\u5e94\u7528\u3002\u8c03\u5236\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\u00a0\uff08Modelated Differential scanning calorimetry\uff0c\u7b80\u79f0\u00a0MDSC\uff09\u662f\u57fa\u4e8e\u4f20\u7edfDSC\u53d1\u5c55\u8d77\u6765\u7684\u4e00\u79cd\u5206\u6790\u6280\u672f\uff0cMDSC\u540c\u65f6\u4f7f\u7528\u4e24\u4e2a\u5347\u6e29\u901f\u7387\uff1a\u5176\u4e00\u662f\u7ebf\u6027\u5347\u6e29\u901f\u7387\uff0c\u63d0\u4f9b\u4e0e\u4f20\u7edfDSC\u76f8\u7c7b\u4f3c\u7684\u4fe1\u606f\uff1b\u53e6\u4e00\u662f\u6b63\u5f26\u6216\u8c03\u5236\u5347\u6e29\u901f\u7387\uff0c\u53ef\u540c\u65f6\u8fdb\u884c\u8bd5\u6837\u70ed\u5bb9\u6d4b\u91cf\uff0c\u5229\u7528\u5085\u91cc\u53f6\u53d8\u6362\u53ef\u5c06\u4ea7\u751f\u7684\u70ed\u6d41\u91cf\u5373\u65f6\u5206\u89e3\u6210\u70ed\u5bb9\u6210\u5206\u548c\u52a8\u529b\u5b66\u6210\u5206\u3002\u5bf9MDSC\u800c\u8a00\uff0c\u70ed\u5bb9\u6210\u5206\u662f\u53ef\u9006\u70ed\u6d41\u91cf\uff08\u5305\u62ec\u73bb\u7483\u5316\u8f6c\u53d8\u3001\u5927\u90e8\u5206\u7684\u7194\u878d\u7b49\uff09\uff0c\u800c\u52a8\u529b\u5b66\u6210\u5206\u662f\u4e0d\u53ef\u9006\u70ed\u6d41\u91cf\uff08\u5305\u62ec\u7ed3\u6676\u3001\u56fa\u5316\u3001\u6325\u53d1\u3001\u5206\u89e3\u3001\u5206\u5b50\u677e\u5f1b\u548c\u5316\u5b66\u53cd\u5e94\u7b49\uff09\u3002MDSC\u603b\u70ed\u6d41\u4fe1\u53f7\u662f\u6240\u6709\u70ed\u8f6c\u53d8\u7684\u603b\u548c\uff0c\u4e0e\u4f20\u7edfDSC\u76f8\u540c\u3002<\/p>\n

\u4e0e\u4f20\u7edfDSC\u76f8\u6bd4,MDSC\u6709\u4ee5\u4e0b\u51e0\u4e2a\u4f18\u70b9\uff1a(1)\u80fd\u591f\u901a\u8fc7\u6e29\u5ea6\u8c03\u5236\u5c06\u603b\u70ed\u6d41\u62c6\u5206\u4e3a\u53ef\u9006\u70ed\u6d41\u548c\u4e0d\u53ef\u9006\u70ed\u6d41\uff0c\u4ece\u800c\u53ef\u4ee5\u5206\u79bb\u76f8\u4e92\u8986\u76d6\u7684\u8f6c\u53d8\uff1b(2)\u540c\u65f6\u5177\u6709\u8f83\u9ad8\u7684\u7075\u654f\u5ea6\u548c\u5206\u8fa8\u7387\uff0c\u56e0\u800c\u5728\u68c0\u6d4b\u8f83\u5f31\u8f6c\u53d8\u65f6\u66f4\u5177\u4f18\u52bf\uff1b(3)\u51c6\u786e\u6d4b\u5b9a\u00a0\u805a\u5408\u7269\u7684\u521d\u59cb\u7ed3\u6676\u5ea6\uff1b(4)\u80fd\u591f\u76f4\u63a5\u6d4b\u91cf\u6bd4\u70ed\u5bb9\uff1b(5)\u80fd\u591f\u5b9e\u73b0\u5728\u53cd\u5e94\u6216\u52a8\u529b\u5b66\u8fc7\u7a0b\u70ed\u5bb9\u53d8\u5316\u7684\u51c6\u7b49\u6e29\u6d4b\u91cf\u3002<\/p>\n

\u8fd1\u5e74\u6765,MDSC\u5907\u53d7\u9ad8\u5206\u5b50\u754c\u79d1\u7814\u4eba\u5458\u7684\u4eb2\u7750\uff0c\u5728\u7814\u7a76\u9ad8\u5206\u5b50\u6750\u6599\u7684\u73bb\u7483\u5316\u8f6c\u53d8\u3001\u7ed3\u6676\uff0d\u7194\u878d\u3001\u70ed\u5bb9\u53d8\u5316\u7b49\u9886\u57df\u5f97\u5230\u4e86\u8f83\u4e3a\u5e7f\u6cdb\u7684\u5e94\u7528\uff0c\u5f97\u5230\u4e86\u5927\u91cf\u4f20\u7edfDSC\u6240\u96be\u4ee5\u68c0\u6d4b\u7684\u6570\u636e\uff0c\u4f7f\u4e00\u4e9b\u96be\u4ee5\u7406\u89e3\u7684\u73b0\u8c61\u5f97\u5230\u4e86\u89e3\u91ca\u8bf4\u660e\u3002\u4e0b\u9762\u5c06\u5bf9MDSC\u8fd1\u5e74\u6765\u5728\u9ad8\u5206\u5b50\u6750\u6599\u4e2d\u7684\u6700\u65b0\u7814\u7a76\u5e94\u7528\u505a\u8be6\u7ec6\u4ecb\u7ecd\u3002<\/p>\n

1\u00a0<\/b><\/strong>\u73bb\u7483\u5316\u8f6c\u53d8\u53ca\u70ed\u7113\u677e\u5f1b\u7684\u7cbe\u786e\u6d4b\u91cf<\/b><\/strong><\/h3>\n

\u6d4b\u91cf\u73bb\u7483\u5316\u8f6c\u53d8\u548c\u73bb\u7483\u5316\u8f6c\u53d8\u6e29\u5ea6\uff08Tg<\/sub>\uff09\u662fDSC\u6280\u672f\u4e2d\u6700\u5e38\u89c1\u7684\u5e94\u7528\uff0c\u5bf9\u4e8e\u65e0\u5b9a\u5f62\u9ad8\u5206\u5b50\u6765\u8bf4\uff0c\u5176\u7269\u7406\u6027\u8d28\u968f\u7740\u65f6\u95f4\u4f1a\u53d1\u751f\u53d8\u5316\uff0c\u6837\u54c1\u5411\u5e73\u8861\u6001\u677e\u5f1b\uff08\u70ed\u7113\u677e\u5f1b\uff09\uff0c\u70ed\u7113\u677e\u5f1b\u4f34\u968f\u7740\u73bb\u7483\u5316\u8f6c\u53d8\u8fc7\u7a0b\u5728\u4f20\u7edfDSC\u70ed\u6d41\u66f2\u7ebf\u4e0a\u5f62\u6210\u53e0\u52a0\u3002\u4e3a\u4e86\u5f97\u5230\u51c6\u786e\u7684Tg<\/sub>\uff0c\u4e00\u822c\u5148\u8981\u5c06\u6837\u54c1\u52a0\u70ed\u81f3Tg<\/sub>\u4ee5\u4e0a\u53bb\u9664\u70ed\u5386\u53f2\uff0c\u964d\u6e29\u540e\u518d\u6b21\u5347\u6e29\u6d4b\u8bd5\uff0c\u53d6\u7b2c\u4e8c\u6b21\u5347\u6e29\u66f2\u7ebf\u6765\u6807\u5b9aTg<\/sub>\u3002\u7136\u800c\uff0c\u5e76\u975e\u6240\u6709\u7684\u6837\u54c1\u90fd\u80fd\u53bb\u9664\u70ed\u5386\u53f2\u540e\u4e8c\u6b21\u5347\u6e29\u6d4b\u8bd5\uff0c\u4f8b\u5982\u70ed\u56fa\u6027\u805a\u5408\u7269\u7b49\u3002MDSC\u80fd\u591f\u901a\u8fc7\u6e29\u5ea6\u8c03\u5236\u5c06\u603b\u70ed\u6d41\u62c6\u5206\u4e3a\u53ef\u9006\u70ed\u6d41\u548c\u4e0d\u53ef\u9006\u70ed\u6d41\uff0c\u70ed\u7113\u677e\u5f1b\u5c5e\u4e8e\u4e0d\u53ef\u9006\u8fc7\u7a0b\uff0c\u51fa\u73b0\u5728\u4e0d\u53ef\u9006\u70ed\u6d41\u4e2d\uff0c\u800c\u73bb\u7483\u5316\u8f6c\u53d8\u5c5e\u4e8e\u53ef\u9006\u8fc7\u7a0b\uff0c\u51fa\u73b0\u5728\u53ef\u9006\u70ed\u6d41\u4e2d\uff0c\u4ece\u800c\u5f97\u5230\u51c6\u786e\u7684Tg<\/sub>\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/span><\/b>1<\/span><\/b>\u3000<\/span><\/b>ABS<\/span><\/b>\u6811\u8102\u7684<\/span><\/b>MDSC<\/span><\/b>\u5347\u6e29\u66f2\u7ebf<\/span><\/b><\/p>\n

\u5982\u56fe1\u91c7\u7528MDSC\u6d4b\u5b9aABS\u6811\u8102\uff08\u4e19\u70ef\u8148\uff0d\u4e01\u4e8c\u70ef\uff0d\u82ef\u4e59\u70ef\u6811\u8102\uff09\u53ca\u5176\u5171\u6df7\u7269\u57fa\u4f53\u6811\u8102\u7684Tg<\/sub>\uff0c\u5e76\u7814\u7a76\u4e86ABS\u6811\u8102\u7684\u5347\u6e29\u8fc7\u7a0b\u4e0e\u57fa\u7840\u5347\u6e29\u901f\u7387\u3001\u8c03\u5236\u632f\u5e45\u7684\u76f8\u5173\u6027\u3002MDSC\u603b\u70ed\u6d41\u66f2\u7ebf\u4e0e\u4f20\u7edfDSC\u70ed\u6d41\u66f2\u7ebf\u76f8\u540c\uff0c\u5728\u53ef\u9006\u70ed\u6d41\u4e2d\u68c0\u6d4b\u5230\u4e86ABS\u7684\u73bb\u7483\u5316\u8f6c\u53d8\uff0c\u5728\u4e0d\u53ef\u9006\u70ed\u6d41\u66f2\u7ebfTg<\/sub>\u9644\u8fd1\u51fa\u73b0\u4e86\u70ed\u7113\u677e\u5f1b\u7684\u5438\u70ed\u5cf0\uff0cMDSC\u5c06\u8fd9\u4e24\u79cd\u8f6c\u53d8\u8fdb\u884c\u4e86\u5206\u79bb\uff0c\u66f4\u7cbe\u786e\u5730\u6d4b\u5b9a\u4e86ABS\u6811\u8102\u7684Tg<\/sub>\u4e3a109.06\u2103\uff0c\u800c\u4e0d\u662f\u603b\u70ed\u6d41\u66f2\u7ebf\u5f97\u5230\u7684106.09\u2103\u3002<\/p>\n

2\u00a0<\/b><\/strong>\u534a\u7ed3\u6676\u805a\u5408\u7269\u7684\u7814\u7a76<\/b><\/strong><\/h3>\n

DSC\u5e94\u7528\u4e8e\u534a\u7ed3\u6676\u805a\u5408\u7269\u7ed3\u6676\uff0d\u7194\u878d\u7684\u7814\u7a76\u5df2\u6709\u8f83\u957f\u7684\u5386\u53f2\uff0c\u7136\u800c\u4f20\u7edfDSC\u6709\u65f6\u4f1a\u5e26\u7ed9\u4eba\u4eec\u9519\u8bef\u7684\u7ed3\u679c\uff0c\u6bd4\u5982\u5bf9\u521d\u59cb\u7ed3\u6676\u5ea6\u7684\u6d4b\u8bd5\u8bef\u5dee\u53ef\u9ad8\u8fbe50%\u3002\u4e00\u822c\u6765\u8bf4\uff0c\u7ed3\u6676\u5c5e\u4e8e\u4e0d\u53ef\u9006\u8fc7\u7a0b\uff0c\u51fa\u73b0\u5728\u4e0d\u53ef\u9006\u70ed\u6d41\u4e2d\uff0c\u800c\u5927\u90e8\u5206\u7684\u7194\u878d\u5c5e\u4e8e\u53ef\u9006\u8fc7\u7a0b\uff0c\u51fa\u73b0\u5728\u53ef\u9006\u70ed\u6d41\u4e2d\u3002MDSC\u662f\u7528\u4e8e\u5206\u6790\u805a\u5408\u7269\u7ed3\u6676\uff0d\u7194\u878d\u8fc7\u7a0b\u975e\u5e38\u6709\u6548\u548c\u53ef\u9760\u7684\u65b9\u6cd5\u3002<\/p>\n

2.1\u00a0<\/b><\/strong>\u534a\u7ed3\u6676\u805a\u5408\u7269\u521d\u59cb\u7ed3\u6676\u5ea6\u7684\u6d4b\u91cf<\/b><\/strong><\/h4>\n

\u4f20\u7edfDSC\u53ea\u6709\u4e00\u6761\u603b\u70ed\u6d41\u66f2\u7ebf\uff0c\u5728\u5224\u65ad\u534a\u7ed3\u6676\u805a\u5408\u7269\u521d\u59cb\u7ed3\u6676\u5ea6\u4e0a\u4f1a\u51fa\u73b0\u8f83\u5927\u7684\u504f\u5dee\uff08\u5982\u56fe2\u6240\u793a\uff09\uff0c\u8fd9\u4e3b\u8981\u662f\u7531\u4e8e\u5927\u591a\u6570\u7684\u534a\u7ed3\u6676\u805a\u5408\u7269\u5728\u5347\u6e29\u8fc7\u7a0b\u4e2d\u4f1a\u7ecf\u5386\u201c\u6c89\u9ed8\u7ed3\u6676\u8fc7\u7a0b\u201d\uff0c\u800c\u4f20\u7edfDSC\u6d4b\u91cf\u7684\u662f\u805a\u5408\u7269\u5728\u4e00\u5b9a\u6e29\u5ea6\u548c\u65f6\u95f4\u51fa\u73b0\u7684\u70ed\u6d41\u6548\u5e94\u7684\u603b\u548c\uff0c\u800c\u805a\u5408\u7269\u6676\u4f53\u7194\u878d\u548c\u7ed3\u6676\u53ef\u80fd\u4f1a\u540c\u65f6\u53d1\u751f\uff0c\u56e0\u800c\u4f1a\u53d1\u751f\u5438\u70ed\u5cf0\u548c\u653e\u70ed\u5cf0\u7684\u53e0\u52a0\u3002MDSC\u53ef\u4ee5\u5c06\u7194\u878d\u548c\u7ed3\u6676\u8fc7\u7a0b\u5206\u79bb\u6210\u53ef\u9006\u70ed\u6d41\u548c\u4e0d\u53ef\u9006\u70ed\u6d41\u7684\u4fe1\u53f7\uff0c\u4ece\u800c\u5f97\u5230\u51c6\u786e\u7684\u521d\u59cb\u7ed3\u6676\u5ea6\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/span> <\/span><\/b>2 <\/span><\/b>\u00a0<\/span>\u6dec\u706b\u5c3c\u9f99<\/span><\/span><\/b>6<\/span><\/b>\u7684\u7ed3\u6676\u5ea6\u6d4b\u5b9a<\/span><\/span><\/b><\/p>\n

2.2\u00a0<\/b><\/strong>\u534a\u7ed3\u6676\u805a\u5408\u7269\u7ed3\u6676\uff0d\u7194\u878d\u8fc7\u7a0b\u7684\u7814\u7a76<\/b><\/strong><\/h4>\n

\u534a\u7ed3\u6676\u805a\u5408\u7269\u7684\u7ed3\u6676\uff0d\u7194\u878d\u8fc7\u7a0b\u6bd4\u8f83\u590d\u6742\uff0c\u53ef\u80fd\u5305\u62ec\u51b7\u7ed3\u6676\u3001\u91cd\u7ed3\u6676\u3001\u7ed3\u6676\u5b8c\u5584\u3001\u4e0e\u6b21\u6676\u6709\u5173\u7684\u70ed\u8f6c\u53d8\u7b49\u3002MDSC\u80fd\u628a\u4e00\u4e9b\u91cd\u53e0\u7684\u8f6c\u53d8\u5206\u79bb\u5f00\u6765\uff0c\u5e38\u7528\u6765\u7814\u7a76\u534a\u7ed3\u6676\u805a\u5408\u7269\u7684\u7ed3\u6676\uff0d\u7194\u878d\u8fc7\u7a0b\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/span><\/span><\/b>3<\/span><\/span><\/b>\u3000<\/span><\/span><\/b>PA6\/MWNT<\/span><\/span><\/b>\u00a0<\/span><\/span><\/b>(0.07%)<\/span><\/span><\/b>\u7eb3\u7c73\u590d\u5408\u6750\u6599<\/span><\/span><\/b>(a)<\/span><\/span><\/b>\u548c\u7eaf<\/span><\/span><\/b>PA6(b)<\/span><\/span><\/b>\u7684<\/span><\/span><\/b>MDSC<\/span><\/span><\/b>\u7194\u878d\u66f2\u7ebf<\/span><\/span><\/b><\/p>\n

\u5982\u56fe3\u6240\u793a\u591a\u58c1\u78b3\u7eb3\u7c73\u7ba1MWNT\u5728\u5c3c\u9f996\u57fa\u4f53\u4e2d\u7684\u5f02\u76f8\u6210\u6838\u4f5c\u7528\uff0cMDSC\u53ef\u9006\u5347\u6e29\u66f2\u7ebf\u6709\u4e24\u4e2a\u7194\u878d\u5cf0\uff0c\u4e0d\u53ef\u9006\u5347\u6e29\u66f2\u7ebf\u5448\u73b0\u4e00\u4e2a\u5438\u70ed\u5cf0\u548c\u4e00\u4e2a\u653e\u70ed\u5cf0\uff0c\u8bf4\u660e\u5728\u4f4e\u6e29\u5904\u6709\u7ed3\u6676\u884c\u4e3a\uff0c\u5347\u6e29\u66f2\u7ebf\u4e2d\u7b2c\u4e00\u4e2a\u7194\u878d\u5cf0\u662f\u4f4e\u6e29\u7ed3\u6676\u4e0e\u7194\u878d\u5171\u540c\u4f5c\u7528\u7684\u7ed3\u679c\uff0c\u5728\u8f83\u4f4e\u6e29\u5ea6\uff0c\u5b8c\u5584\u5ea6\u8f83\u4f4e\u7684\u6676\u4f53\u5148\u7194\u878d\uff0c\u7194\u878d\u7684\u540c\u65f6\u53d1\u751f\u4e86\u518d\u7ed3\u6676\u5f97\u5230\u5b8c\u5584\u5ea6\u8f83\u9ad8\u7684\u6676\u4f53\uff0c\u8fd9\u4e9b\u5b8c\u5584\u5ea6\u8f83\u9ad8\u7684\u6676\u4f53\u5219\u5728\u9ad8\u6e29\u5904\u4e0e\u590d\u5408\u6750\u6599\u539f\u672c\u4ea7\u751f\u7684\u5b8c\u5584\u5ea6\u9ad8\u7684\u6676\u4f53\u4e00\u8d77\u7194\u878d\uff0c\u5373\u590d\u5408\u6750\u6599\u5728\u5347\u6e29\u8fc7\u7a0b\u4e2d\u51fa\u73b0\u4e86\u7194\u878d\uff0d\u7ed3\u6676\uff0d\u518d\u7194\u878d\u7684\u8fc7\u7a0b\u3002<\/p>\n

3\u00a0<\/b><\/strong>\u51c6\u7b49\u6e29\u6a21\u5f0f\u4e0b\u9ad8\u5206\u5b50\u7684\u7ed3\u6784\u53d8\u5316\u7814\u7a76<\/b><\/strong><\/h3>\n

\u5728\u7814\u7a76\u805a\u5408\u7269\u52a8\u529b\u5b66\u8fc7\u7a0b\u7684\u53cd\u5e94\u901f\u7387\u548c\u53cd\u5e94\u7a0b\u5ea6\u65f6\uff0c\u7ecf\u5e38\u4f1a\u9009\u62e9\u7b49\u6e29\u6a21\u5f0f\u3002\u5bf9\u4e8e\u4f20\u7edfDSC\u6765\u8bf4\uff0c\u6b64\u65f6\u5347\u6e29\u901f\u7387\u4e3a\u96f6\uff0c\u5373\u70ed\u5bb9\u9879\u4e3a\u96f6\u3002\u800cMDSC\u5bf9\u8bd5\u6837\u540c\u65f6\u65bd\u52a0\u4e24\u4e2a\u5347\u6e29\u901f\u7387\uff0c\u5e73\u5747\u5347\u6e29\u901f\u7387\u8bbe\u4e3a\u96f6\uff0c\u5219\u5e73\u5747\u6e29\u5ea6\u4fdd\u6301\u6052\u5b9a\uff0c\u800c\u632f\u5e45\u4e0d\u4e3a\u96f6\uff0c\u5373\u8c03\u5236\u5347\u6e29\u901f\u7387\u4e0d\u4e3a\u96f6\uff0c\u6b64\u65f6\u4fbf\u53ef\u6d4b\u91cf\u70ed\u5bb9\u548c\u6052\u6e29\u8fc7\u7a0b\u3001\u52a8\u529b\u5b66\u8fc7\u7a0b\uff08\u5982\u7ed3\u6676\u3001\u5316\u5b66\u53cd\u5e94\uff09\u7684\u70ed\u5bb9\u53d8\u5316\uff0c\u8fd9\u79cd\u6d4b\u8bd5\u6a21\u5f0f\u5373\u4e3a\u51c6\u7b49\u6e29\u6a21\u5f0f\uff08Quasi-isothermal\uff09\uff0c\u5728\u7814\u7a76\u9ad8\u5206\u5b50\u7684\u7ed3\u6784\u53d8\u5316\u65b9\u9762\u6709\u72ec\u7279\u7684\u4f18\u52bf\u3002<\/p>\n

3.1\u00a0<\/b><\/strong>\u70ed\u5bb9\u503c\u7684\u51c6\u786e\u6d4b\u91cf<\/b><\/strong><\/h4>\n

\u4f20\u7edfDSC\u6d4b\u91cf\u6750\u6599\u7684\u6bd4\u70ed\u5bb9\u9700\u8981\u5728\u76f8\u540c\u7684\u6761\u4ef6\u4e0b\u8fde\u7eed\u8fdb\u884c\u4e09\u6b21\u5b9e\u9a8c\u3002MDSC\u6d4b\u91cf\u70ed\u5bb9\u7684\u4e00\u4e2a\u91cd\u8981\u4f18\u70b9\u5728\u4e8e\uff0c\u4e3a\u5f97\u5230\u4e00\u4e2a\u7cbe\u786e\u7684\u70ed\u5bb9\u503c\u4e0d\u9700\u8981\u4e00\u4e2a\u7a33\u5b9a\u7684\u57fa\u7ebf\uff0c\u53ef\u9006\u70ed\u5bb9\u7684\u6d4b\u91cf\u4ec5\u4ec5\u6839\u636e\u8c03\u5236\u70ed\u6d41\u4fe1\u53f7\u7684\u632f\u5e45\uff0c\u800c\u4e0d\u662f\u5b83\u7684\u5e73\u5747\u503c\u3002\u00a0\u91c7\u7528MDSC\u4e2d\u7684\u51c6\u7b49\u6e29\u6a21\u5f0f\u7814\u7a76\u805a\u5df1\u5185\u916fPCL\u7684\u7ed3\u6676\u8fc7\u7a0b\uff0c\u8bd5\u6837\u9996\u5148\u572870\u2103\u9884\u7194\uff0c\u7136\u540e\u4ee51\u2103\u00b7min-1<\/sup>\u964d\u6e29\u81f355\u2103\u8fdb\u884c\u51c6\u7b49\u6e29\u7ed3\u6676\uff0c\u632f\u5e45\u4e3a0.5\u2103\uff0c\u8c03\u5236\u5468\u671f\u4ece20S\u52301200s\u4e0d\u7b49\u3002\u7ed3\u6676\u8fc7\u7a0b\u7ed3\u675f\u540e\u5c06\u8bd5\u6837\u4ee510\u2103\u00b7min-1<\/sup>\u5347\u6e29\u81f370\u2103\uff0c\u8bd5\u6837\u5b8c\u5168\u7194\u878d\uff0c\u5c06\u7194\u878d\u7113\u4e0e100%\u7ed3\u6676PCL\u7194\u878d\u7113\u8fdb\u884c\u5bf9\u6bd4\uff0c\u5f97\u5230\u4e86PCL\u7684\u7ed3\u6676\u5ea6\uff0c\u7ed8\u5236\u51fa\u4e86\u70ed\u5bb9\u4e0e\u65f6\u95f4\u548c\u9891\u7387\u7684\u5173\u7cfb\u66f2\u7ebf\uff0c\u5982\u56fe4\u6240\u793a\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/span><\/span><\/b>4<\/span><\/b>\u3000<\/span><\/span><\/b>pcl<\/span><\/b>\u5728<\/span><\/span><\/b>55<\/span><\/b>\u2103<\/span>\u7b49\u6e29\u7ed3\u6676\u65f6\u70ed\u5bb9\u4e0e\u65f6\u95f4\u548c\u9891\u7387\u7684\u5173\u7cfb\u66f2\u7ebf<\/span><\/span><\/b><\/p>\n

3.2\u00a0<\/b><\/strong>\u805a\u5408\u7269<\/b><\/strong>RAF<\/b><\/strong>\u7684\u7814\u7a76<\/b><\/strong><\/h4>\n

\u534a\u7ed3\u6676\u805a\u5408\u7269\u4e00\u822c\u5e38\u88ab\u63cf\u8ff0\u4e3a\u7531\u7ed3\u6676\u533a\u548c\u65e0\u5b9a\u5f62\u533a\u6784\u6210\u3002\u4f46\u662f\uff0c\u4eba\u4eec\u5728\u5bf9\u534a\u7ed3\u6676\u805a\u5408\u7269\u8fdb\u884cDSC\uff0c\u6d4b\u8bd5\u65f6\u5e38\u4f1a\u53d1\u73b0\uff1a\u5728\u73bb\u7483\u5316\u8f6c\u53d8\u9644\u8fd1\u7684\u70ed\u7113\u677e\u5f1b\u5f3a\u5ea6\u660e\u663e\u4f4e\u4e8e\u65e0\u5b9a\u5f62\u805a\u5408\u7269\uff0c\u8fd9\u662f\u65e0\u5b9a\u5f62\u533a\u6240\u4e0d\u80fd\u89e3\u91ca\u7684\uff0c\u7814\u7a76\u53d1\u73b0\u8fd9\u662f\u7531\u4e8e\u5728\u534a\u7ed3\u6676\u805a\u5408\u7269\u4e2d\u5b58\u5728\u4e00\u79cd\u521a\u6027\u65e0\u5b9a\u5f62\u7ec4\u5206\u3002\u7814\u7a76\u8868\u660e\uff0cRAF\u662f\u4f4d\u4e8e\u805a\u5408\u7269\u7ed3\u6676\u533a\u548c\u65e0\u5b9a\u5f62\u533a\u754c\u9762\u5904\u7684\u5177\u6709\u7eb3\u7c73\u5c3a\u5ea6\u7684\u4e00\u79cd\u7279\u6b8a\u7ed3\u6784\uff0c\u5728Tg<\/sub>\u4ee5\u4e0a\u65f6RAF\u4f9d\u65e7\u662f\u65e0\u5b9a\u5f62\u7ed3\u6784\u4e14\u4fdd\u6301\u73bb\u7483\u6001\u5b58\u5728\uff0c\u5982\u56fe5\u6240\u793a\u3002RAF\u7684\u5f62\u6210\u548c\u6d88\u5931\u6709\u975e\u5e38\u5f3a\u7684\u65f6\u95f4\u548c\u6e29\u5ea6\u4f9d\u8d56\u6027\uff0c\u56e0\u800c\u53ef\u4ee5\u901a\u8fc7\u6539\u53d8MDSC\u7684\u6d4b\u8bd5\u6761\u4ef6\u6765\u68c0\u6d4bRAF\u7684\u53d8\u5316\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/span><\/span><\/b>5 <\/span><\/b>\u6676\u4f53\u3001<\/span><\/span><\/b>RAF<\/span><\/b>\u548c<\/span><\/span><\/b>MAF<\/span><\/b>\u6392\u5217\u793a\u610f\u56fe<\/span><\/span><\/b><\/p>\n

4 \u7ed3\u8bed<\/b><\/strong><\/h3>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u8fd1\u5e74\u6765MDSC\u5728\u7814\u7a76\u9ad8\u5206\u5b50\u6750\u6599\u7684\u73bb\u7483\u5316\u8f6c\u53d8\u3001\u7ed3\u6676\u3001\u7194\u878d\u7b49\u590d\u6742\u76f8\u53d8\u9886\u57df\u53d6\u5f97\u4e86\u8f83\u5927\u7684\u8fdb\u6b65\uff0c\u5bf9\u4eba\u4eec\u8ba4\u8bc6\u9ad8\u5206\u5b50\u6750\u6599\u7684\u672c\u8d28\u53d1\u6325\u4e86\u975e\u5e38\u91cd\u8981\u7684\u4f5c\u7528\u3002\u5c06MDSC\u4e0e\u5176\u5b83\u5148\u8fdb\u7684\u68c0\u6d4b\u624b\u6bb5\u8054\u5408\u5e94\u7528\u4e8e\u9ad8\u5206\u5b50\u7814\u7a76\u5c06\u662f\u672a\u6765\u7684\u53d1\u5c55\u8d8b\u52bf\u3002\u4f46\u662f\uff0cMDSC\u6d4b\u8bd5\u6548\u7387\u8f83\u4f4e\uff08\u57fa\u7840\u5347\u6e29\u901f\u7387\u6162\uff09\uff0c\u4e0d\u80fd\u5b8c\u5168\u66ff\u4ee3\u4f20\u7edfDSC\uff0c\u4e00\u822c\u5148\u8fdb\u884c\u4f20\u7edfDSC\u6d4b\u8bd5\uff0c\u5f53\u7ed3\u679c\u96be\u4ee5\u89e3\u91ca\u548c\u5206\u8fa8\u65f6\u624d\u9700\u8fdb\u884cMDSC\u6d4b\u8bd5\u3002\u5176\u6b21\uff0cMDSC\u6d4b\u8bd5\u6761\u4ef6\u7684\u9009\u62e9\u8981\u6c42\u8f83\u9ad8\uff0c\u4e3b\u8981\u5305\u62ec\uff1a\u5347\u6e29\u901f\u7387\u3001\u8c03\u5236\u5468\u671f\u3001\u8c03\u5236\u632f\u5e45\u7b49\uff0c\u6d4b\u8bd5\u6761\u4ef6\u7684\u9009\u62e9\u76f4\u63a5\u5f71\u54cd\u7ed3\u679c\u7684\u51c6\u786e\u6027\uff0c\u9700\u8981\u6709\u4e30\u5bcc\u7684\u7ecf\u9a8c\u79ef\u7d2f\u624d\u80fd\u5f97\u5230\u6709\u4ef7\u503c\u7684\u6570\u636e\u3002<\/p>\n

\u53c2\u8003\u6587\u732e<\/b><\/strong><\/h3>\n

[1]\u738b\u8273\u8272, \u9b4f\u5fd7\u52c7, \u7533\u51ef\u534e,\u7b49. \u8c03\u5236\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\u5728\u9ad8\u5206\u5b50\u6750\u6599\u4e2d\u7684\u5e94\u7528[J]. \u9ad8\u5206\u5b50\u901a\u62a5, 2016(3):16-22.<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u5b66\u672f\u5e72\u8d27\u7ec4zhengzheng666\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u7f16\u8f91\u6574\u7406\u3002<\/p>\n

\u6750\u6599\u4eba\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u8fd9\u91cc\u6c47\u96c6\u4e86\u5404\u5927\u9ad8\u6821\u7855\u535a\u751f\u3001\u4e00\u7ebf\u79d1\u7814\u4eba\u5458\u4ee5\u53ca\u884c\u4e1a\u4ece\u4e1a\u8005\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u7f16\u8f91\u90e8<\/u><\/a>\u3002<\/p>\n

\u6750\u6599\u4eba\u7f51\u5411\u5404\u5927\u56e2\u961f\u8bda\u5fc3\u7ea6\u7a3f\uff0c\u8bfe\u9898\u7ec4\u6700\u65b0\u6210\u679c\u3001\u65b9\u5411\u603b\u7ed3\u3001\u56e2\u961f\u8bbf\u8c08\u3001\u5b9e\u9a8c\u6280\u80fd\u7b49\u7686\u53ef\u6295\u7a3f\uff0c\u4f18\u79c0\u7a3f\u4ef6\u4e00\u7ecf\u5f55\u7528\uff0c\u6211\u4eec\u4f1a\u5949\u4e0a\u7a3f\u916c\uff0c\u8bf7\u8054\u7cfb\uff1a\u90ae\u7bb1tougao@cailiaoren.com \u6216 QQ\uff1a97482208\u3002<\/p>\n

\u4eea\u5668\u8bbe\u5907\u3001\u8bd5\u5242\u8017\u6750\u3001\u6750\u6599\u6d4b\u8bd5\u3001\u6570\u636e\u5206\u6790\uff0c\u627e\u6750\u6599\u4eba<\/u><\/a>\u3001\u4e0a\u6d4b\u8bd5\u8c37<\/u><\/a>\uff01<\/p>\n","protected":false},"excerpt":{"rendered":"

\u5dee\u793a\u626b\u63cf\u91cf\u70ed\u6cd5\uff08Differential scanning calorimetry ,\u7b80\u79f0DSC\uff09\u662f\u8868\u5f81\u805a\u5408\u7269\u6027\u80fd\u7684\u4e00\u79cd\u975e\u5e38\u5feb\u901f\u6709\u6548\u7684\u5206\u6790\u65b9\u6cd5\uff0c\u5728\u9ad8\u5206\u5b50\u3001\u5316\u5b66\u54c1…<\/p>\n","protected":false},"author":395,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[4],"tags":[],"class_list":["post-63343","post","type-post","status-publish","format-standard","hentry","category-ganhuo"],"_links":{"self":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/63343"}],"collection":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/users\/395"}],"replies":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=63343"}],"version-history":[{"count":22,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/63343\/revisions"}],"predecessor-version":[{"id":63848,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/63343\/revisions\/63848"}],"wp:attachment":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=63343"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=63343"},{"taxonomy":"post_tag","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=63343"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}