{"id":58450,"date":"2016-12-27T14:00:16","date_gmt":"2016-12-27T06:00:16","guid":{"rendered":"\/\/m.iemloyee.com\/?p=58450"},"modified":"2017-03-04T10:36:21","modified_gmt":"2017-03-04T02:36:21","slug":"adv-mater-%e5%9c%ba%e6%95%88%e5%ba%94%e5%a2%9e%e5%bc%bamos2%e7%ba%b3%e7%b1%b3%e7%89%87%e7%9a%84%e6%9e%90%e6%b0%a2%e5%8f%8d%e5%ba%94%e5%82%ac%e5%8c%96%e6%b4%bb%e6%80%a7","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=58450","title":{"rendered":"Adv.Mater.:\u573a\u6548\u5e94\u589e\u5f3aMoS2\u7eb3\u7c73\u7247\u7684\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u6d3b\u6027"},"content":{"rendered":"<p><strong><span style=\"color: #ff0000;\">\u3010\u5f15\u8a00\u3011<\/span><\/strong><\/p>\n<p>\u6c22\u6c14\u5177\u6709\u5f88\u9ad8\u7684\u80fd\u91cf\u5bc6\u5ea6\uff0c\u662f\u4e00\u79cd\u7eff\u8272\u7684\u6e05\u6d01\u80fd\u6e90\u3002\u5206\u89e3\u6c34\u662f\u4e00\u79cd\u5e38\u89c1\u7684\u5236\u5907\u6c22\u6c14\u7684\u65b9\u6cd5\uff0c\u5305\u62ec\u6790\u6c22\u53cd\u5e94\uff08HER\uff09\u548c\u6790\u6c27\u53cd\u5e94\u3002\u4e00\u79cd\u9ad8\u6027\u80fd\u7684\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u5242\u9700\u8981\u5177\u5907\u9ad8\u901f\u7684\u7535\u5b50\u4f20\u8f93\u80fd\u529b\uff0c\u5177\u6709\u9ad8\u5bc6\u5ea6\u7684\u50ac\u5316\u6d3b\u6027\u4f4d\u70b9\uff0c\u4ee5\u53ca\u8f83\u4e3a\u5408\u9002\u7684\u5438\u9644\u6c22\u539f\u5b50\u7684\u5409\u5e03\u65af\u81ea\u7531\u80fd\u3002\u91d1\u5c5ePt\u53ef\u4ee5\u6ee1\u8db3\u4e0a\u8ff0\u6761\u4ef6\uff0c\u662f\u4e00\u79cd\u4f18\u5f02\u7684\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u5242\u3002\u4f46\u662fPt\u5728\u81ea\u7136\u754c\u4e2d\u50a8\u91cf\u7a00\u5c11\uff0c\u9650\u5236\u4e86\u5176\u5728\u5de5\u4e1a\u751f\u4ea7\u4e2d\u7684\u5e94\u7528\u3002\u6240\u4ee5\u627e\u5230\u4e00\u79cd\u9ad8\u6027\u80fd\u3001\u4f4e\u6210\u672c\u7684\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u5242\u662f\u5341\u5206\u5fc5\u8981\u7684\u3002\u7406\u8bba\u8ba1\u7b97\u8868\u660e\u4e8c\u786b\u5316\u94bc\uff08MoS<sub>2<\/sub>\uff09\u53ef\u4ee5\u66ff\u4ee3Pt\u4f5c\u4e3a\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u5242\uff0c\u4f46\u662f\u6d3b\u6027\u4f4d\u70b9\u7684\u70ed\u529b\u5b66\u4e0d\u7a33\u5b9a\u6027\u548c\u8f83\u4f4e\u7684\u7535\u5bfc\u7387\u6210\u4e3a\u4e86\u5b83\u7684\u9650\u5236\u56e0\u7d20\u3002\u4eba\u4eec\u91c7\u7528\u5f88\u591a\u65b9\u6cd5\u6765\u589e\u52a0MoS<sub>2<\/sub>\u7684\u50ac\u5316\u6d3b\u6027\uff0c\u4f8b\u5982\u63a7\u5236\u5f62\u8c8c\u548c\u7ed3\u6784\uff0c\u589e\u52a0\u7f3a\u9677\u4f5c\u4e3a\u6d3b\u6027\u4f4d\u70b9\u4ee5\u53ca\u4e0e\u5176\u4ed6\u6750\u6599\u590d\u5408\u6765\u589e\u52a0\u7535\u5b50\u4f20\u8f93\u901f\u7387\u7b49\u7b49\u3002\u4ece\u4ee5\u524d\u5bf9MoS<sub>2<\/sub>\u6676\u4f53\u7ba1\u7684\u7814\u7a76\u6765\u770b\uff0c\u7535\u573a\u6548\u5e94\u53ef\u4ee5\u540c\u65f6\u51cf\u5c11\u63a5\u89e6\u7535\u963b\u548cMoS<sub>2<\/sub>\u7684\u8584\u5c42\u7535\u963b\uff0c\u4ece\u800c\u5f97\u5230\u66f4\u5feb\u7684\u7535\u5b50\u4f20\u8f93\u901f\u7387\u3002\u56e0\u6b64\uff0c\u7535\u573a\u6548\u5e94\u53ef\u80fd\u4f1a\u4f7fMoS<sub>2<\/sub>\u5177\u6709\u66f4\u597d\u7684\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u6d3b\u6027\u3002<\/p>\n<p><strong><span style=\"color: #ff0000;\">\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/span><\/strong><\/p>\n<p>\u8fd1\u65e5\uff0c<strong>\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u7684<span style=\"color: #ff0000;\">\u9ea6\u7acb\u5f3a\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/span>\u3001<span style=\"color: #ff0000;\">\u664f\u68a6\u96e8\u535a\u58eb\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/span><\/strong>\u5728Advanced Materials\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cField Effect Enhanced Hydrogen Evolution Reaction of MoS<sub>2<\/sub> Nanosheets\u201d\u7684\u6587\u7ae0\u3002\u7528\u5355\u4e2aMoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u6210\u529f\u5236\u5907\u4e86\u7535\u573a\u8c03\u8282\u7684\u6790\u6c22\u53cd\u5e94\u8bbe\u5907\u6765\u63a2\u7a76\u7535\u573a\u6548\u5e94\u5bf9\u50ac\u5316\u53cd\u5e94\u7684\u5f71\u54cd\u3002\u968f\u7740\u7535\u573a\u7684\u5f15\u5165\uff0cMoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u7684\u50ac\u5316\u6027\u80fd\u5f97\u5230\u4e86\u660e\u663e\u7684\u63d0\u9ad8\u3002\u5728\u7535\u6d41\u5bc6\u5ea6\u4e3a100 mA \u00b5m<sup>-2<\/sup>\u6761\u4ef6\u4e0b\u7684\u6700\u4f4e\u8fc7\u7535\u4f4d\u53ef\u8fbe\u523038 mV\uff0c\u5728\u80cc\u6805\u7535\u538b\u4e3a5 V\u65f6\u7684\u5854\u83f2\u5c14\u659c\u7387\u503c\u964d\u4f4e\u5230\u6ca1\u6709\u7535\u573a\u65f6\u7684\u4e00\u534a\u3002\u7814\u7a76\u7ed3\u679c\u8bc1\u660e\u4e86\u7535\u573a\u6548\u5e94\u901a\u8fc7\u964d\u4f4e\u901a\u9053\u7535\u963b\u3001\u52a0\u5feb\u7535\u8377\u4f20\u8f93\u53ef\u4ee5\u6709\u6548\u5730\u589e\u5f3aMoS<sub>2<\/sub>\u7684\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u6d3b\u6027\u3002<\/p>\n<p><strong><span style=\"color: #ff0000;\">\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/span><\/strong><\/p>\n<p><strong>\u56fe1 MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u7535\u573a\u8c03\u8282\u6790\u6c22\u53cd\u5e94\u88c5\u7f6e\u5236\u5907\u7684\u4e09\u7ef4\u539f\u7406\u56fe\u3002<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-58455\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0001.png\" alt=\"\" width=\"600\" height=\"417\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0001.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0001-300x209.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a)\u00a0Si\u57fa\u5e95\uff08\u84dd\u8272\uff09\u8868\u9762\u4e0a\u6709300 nm\u7684SiO<sub>2<\/sub>\uff08\u7c89\u8272\uff09\u548c5 nm\/50 nm\u7684Cr\/Au\u7535\u6781<\/p>\n<p>b)\u00a0\u901a\u8fc7\u673a\u68b0\u5265\u79bb\u6cd5\u5236\u5907\u7684MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\uff08\u7d2b\u8272\uff09\u8f6c\u79fb\u5230SiO<sub>2<\/sub>\u8868\u9762\u4e0a<\/p>\n<p>c)\u00a0\u7528\u7535\u5b50\u675f\u5e73\u5370\u672f\u56fa\u5b9aMoS<sub>2<\/sub>\u7eb3\u7c73\u7247\uff0c\u4e4b\u540e\u5728\u70ed\u84b8\u9540\u673a\u4e0a\u6c89\u79ef5 nm\/150 nm Cr\/Au<\/p>\n<p>d)\u00a0\u901a\u8fc7\u7535\u5b50\u675f\u5e73\u5370\u672f\u5c06\u5149\u523b\u80f6\uff08PMMA\uff09\u8986\u76d6\u5230\u5e26\u6709\u88f8\u9732MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u7684\u7845\u7247\u4e0a\uff0c\u5916\u9732\u7684\u9ad8\u7535\u5bfc\u7845\u57fa\u5e95\u662f\u7528\u6765\u65bd\u52a0\u80cc\u6805\u7535\u538b\u7684<\/p>\n<p>e-h)\u00a0\u5728\u4e0d\u540c\u88c5\u914d\u72b6\u6001\u4e0bMoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u7535\u573a\u8c03\u8282\u6790\u6c22\u53cd\u5e94\u88c5\u7f6e\u7684\u5149\u5b66\u5f71\u50cf\uff0c\u5206\u522b\u5bf9\u5e94\u4e8e\uff08a-d\uff09\u3002<\/p>\n<p><strong>\u56fe2\u00a0MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u4ee5\u53ca\u6790\u6c22\u53cd\u5e94\u88c5\u7f6e\u7684\u8868\u9762\u5f62\u8c8c\u3002<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-58456\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0002.png\" alt=\"\" width=\"600\" height=\"458\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0002.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0002-300x229.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a) MoS<sub>2<\/sub>\u7eb3\u7c73\u7247HER\u88c5\u7f6e\u7684FESEM\u56fe\u50cf<\/p>\n<p>b)\u00a0MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u7684\u539f\u5b50\u529b\u663e\u5fae\u955c\u56fe\u50cf<\/p>\n<p>c)\u00a0HER\u50ac\u5316\u6d4b\u91cf\u4e2d\u4e09\u7535\u6781\u7684\u793a\u610f\u56fe<\/p>\n<p>d)\u00a0\u50ac\u5316\u6d4b\u91cf\u7684\u5b9e\u7269\u8fde\u63a5\u56fe\u3002<\/p>\n<p><strong>\u56fe3 \u4e0d\u540c\u6837\u54c1\u53ca\u4e0d\u540c\u6805\u7535\u538b\u4e0b\u7684\u6027\u80fd\u8868\u5f81\u3002<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-58457\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0003.png\" alt=\"\" width=\"600\" height=\"463\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0003.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0003-300x232.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a)\u00a0\u7a7a\u767d\u8bd5\u6837\uff0cAu\u7535\u6781\uff0cMoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u548cPt\u7684HER\u6781\u5316\u66f2\u7ebf<\/p>\n<p>b)\u00a0\u521d\u59cbMoS<sub>2<\/sub>\u7eb3\u7c73\u7247\uff0c\u7ecf\u8fc7\u7535\u89e3\u6db2\u6d78\u6e0d\u540e\u7684MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u548c\u7ecf\u8fc7\u7535\u5316\u5b66\u6d4b\u91cf\u540e\u7684\u7eb3\u7c73\u7247\u7684\u62c9\u66fc\u5149\u8c31<\/p>\n<p>c)\u00a0\u5728\u4e0d\u540c\u80cc\u6805\u7535\u538b\u4e0b\u7684HER\u6781\u5316\u66f2\u7ebf\uff0c\u6700\u597d\u7684\u50ac\u5316\u6027\u80fd\u51fa\u73b0\u5728\u6805\u7535\u538b\u4e3a5 V\u7684\u65f6\u5019<\/p>\n<p>d)\u00a0\u4e0d\u540c\u80cc\u6805\u7535\u538b\u5bf9\u5e94\u7684\u5854\u83f2\u5c14\u659c\u7387\u3002<\/p>\n<p><strong>\u56fe4 \u4e0d\u540c\u7535\u538b\u4e0bMoS<sub>2<\/sub>\u7eb3\u7c73\u7247HER\u88c5\u7f6e\u7684\u80fd\u5e26\u60c5\u51b5\u3002<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-58458\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0004.png\" alt=\"\" width=\"600\" height=\"363\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0004.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2016\/12\/adma201604464-fig-0004-300x182.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>a)\u00a0\u5728\u4e0d\u540c\u6805\u7535\u538b\u4e0b\uff080-10 V\uff09\u7684MoS<sub>2<\/sub>\u7eb3\u7c73\u7247HER\u88c5\u7f6e\u7684I-V\u66f2\u7ebf<\/p>\n<p>b)\u00a0MoS<sub>2<\/sub>\u7eb3\u7c73\u7247HER\u88c5\u7f6e\u7684\u901a\u9053\u7535\u5bfc\u53d8\u5316\u8d8b\u52bf\u3002MoS<sub>2<\/sub>\u7eb3\u7c73\u7247HER\u88c5\u7f6e\u7684\u80fd\u5e26\u968f\u7740\u6805\u7535\u538b\u7684\u4e0d\u540c\u800c\u53d8\u5316<\/p>\n<p>c)\u00a0\u88c5\u7f6e\u5728\u95ed\u5408\u7ebf\u8def\u4f46\u4e0d\u52a0\u4efb\u4f55\u6805\u7535\u538b\u6761\u4ef6\u4e0b\u7684\u6807\u51c6\u72b6\u6001<\/p>\n<p>d)\u00a0\u88c5\u7f6e\u5728\u5916\u52a0\u6b63\u6805\u7535\u538b\u4e0b\u7684\u80fd\u5e26\u60c5\u51b5<\/p>\n<p>e)\u00a0\u88c5\u7f6e\u5728\u5916\u52a0\u8d1f\u6805\u7535\u538b\u4e0b\u7684\u80fd\u5e26\u60c5\u51b5\u3002<\/p>\n<p><strong><span style=\"color: #ff0000;\">\u3010\u7ed3\u8bba\u3011<\/span><\/strong><\/p>\n<p>\u8be5\u7814\u7a76\u5de5\u4f5c\u6210\u529f\u5236\u5907\u4e86\u4ee5MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u4e3a\u57fa\u7840\u7684\u6790\u6c22\u53cd\u5e94\u88c5\u7f6e\uff0c\u901a\u8fc7\u5f15\u5165\u7535\u573a\u6765\u63a2\u7a76\u7535\u573a\u6548\u5e94\u5bf9MoS<sub>2<\/sub>\u50ac\u5316\u6d3b\u6027\u7684\u5f71\u54cd\u3002\u7ed3\u679c\u8bc1\u660e\u6b63\u7535\u573a\u7684\u5f15\u5165\u4f7f\u5f97MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u7684\u50ac\u5316\u6d3b\u6027\u663e\u8457\u63d0\u9ad8\u3002\u5728\u5f15\u51655 V\u7684\u6805\u7535\u538b\u540e\uff0cMoS<sub>2<\/sub>\u7684\u50ac\u5316\u53cd\u5e94\u8fc7\u7535\u4f4d\u4ece240 mV\u964d\u4f4e\u523038 mV\uff0c\u8fd9\u4e00\u7ed3\u679c\u5728\u6027\u80fd\u4e0a\u5df2\u7ecf\u80fd\u591f\u548cPt\u76f8\u6bd4\u3002\u901a\u8fc7\u80fd\u5e26\u7406\u8bba\uff0c\u6211\u4eec\u53ef\u4ee5\u5f97\u51fa\u50ac\u5316\u6d3b\u6027\u7684\u63d0\u9ad8\u4e3b\u8981\u5f52\u56e0\u4e8e\u7535\u573a\u7684\u5f15\u5165\u63d0\u9ad8\u4e86MoS<sub>2<\/sub>\u7eb3\u7c73\u7247\u7684\u901a\u9053\u7535\u5bfc\u3002\u8fd9\u4e00\u901a\u8fc7\u5f15\u5165\u7535\u573a\u6765\u63d0\u9ad8\u6790\u6c22\u53cd\u5e94\u50ac\u5316\u6d3b\u6027\u7684\u7b56\u7565\u4e5f\u53ef\u4ee5\u5e94\u7528\u4e8e\u5176\u4ed6\u7535\u5316\u5b66\u53cd\u5e94\u8fc7\u7a0b\u5f53\u4e2d\uff0c\u5177\u6709\u975e\u5e38\u91cd\u8981\u7684\u610f\u4e49\u3002<\/p>\n<p>\u539f\u6587\u94fe\u63a5\uff1a<a href=\"http:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/adma.201604464\/full\" target=\"_blank\">Field Effect Enhanced Hydrogen Evolution Reaction of MoS<sub>2<\/sub> 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