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Kobayashi\u7b49\u7528XANES\u7814\u7a76\u4e86LiNi0.80Co0.15Al0.05O2\u6b63\u6781\u6750\u6599\u3002XANES\u68c0\u6d4b\u5230\u9897\u7c92\u8868\u9762\u542b\u6709Li2Co3<\/span>\u548c\u5176\u5b83\u989d\u5916\u7acb\u65b9\u76f8\u6742\u8d28[7]\u3002<\/span><\/p>\n

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\u5229\u7528\u521d\u7ea7X\u5c04\u7ebf\u5149\u5b50\u6216\u5176\u5b83\u5fae\u89c2\u79bb\u5b50\u6fc0\u53d1\u5f85\u6d4b\u7269\u8d28\u4e2d\u7684\u539f\u5b50\uff0c\u4f7f\u4e4b\u4ea7\u751f\u8367\u5149\uff08\u6b21\u7ea7X\u5c04\u7ebf\uff09\u800c\u8fdb\u884c\u7269\u8d28\u6210\u5206\u5206\u6790\u548c\u5316\u5b66\u6001\u7814\u7a76\u7684\u65b9\u6cd5\u3002\u6309\u6fc0\u53d1\u3001\u8272\u6563\u548c\u63a2\u6d4b\u65b9\u6cd5\u7684\u4e0d\u540c\uff0c\u5206\u4e3aX\u5c04\u7ebf\u5149\u8c31\u6cd5\uff08\u6ce2\u957f\u8272\u6563\uff09\u548cX\u5c04\u7ebf\u80fd\u8c31\u6cd5\uff08\u80fd\u91cf\u8272\u6563\uff09\u3002\u6839\u636e\u8272\u6563\u65b9\u5f0f\u4e0d\u540c\uff0cX\u5c04\u7ebf\u8367\u5149\u5206\u6790\u4eea\u76f8\u5e94\u5206\u4e3aX\u5c04\u7ebf\u8367\u5149\u5149\u8c31\u4eea\uff08\u6ce2\u957f\u8272\u6563\uff09\u548cX\u5c04\u7ebf\u8367\u5149\u80fd\u8c31\u4eea\uff08\u80fd\u91cf\u8272\u6563\uff09\u3002XRF\u88ab\u5de5\u4e1a\u754c\u5e7f\u6cdb\u5e94\u7528\u4e8e\u9502\u79bb\u5b50\u7535\u6c60\u6750\u6599\u4e3b\u6210\u5206\u53ca\u6742\u8d28\u5143\u7d20\u5206\u6790\u3002\u5bf9\u67d0\u4e9b\u5143\u7d20\u68c0\u51fa\u9650\u53ef\u4ee5\u8fbe\u523010-9<\/sup>\u7684\u91cf\u7ea7\u3002<\/span><\/p>\n

2\u3001\u5f62\u8c8c\u8868\u5f81<\/strong><\/span><\/p>\n

\uff081\uff09\u626b\u63cf\u7535\u955c\uff08SEM\uff09<\/span><\/p>\n

\u6536\u96c6\u6837\u54c1\u8868\u9762\u7684\u4e8c\u6b21\u7535\u5b50\u4fe1\u606f\uff0c\u53cd\u5e94\u6837\u54c1\u7684\u8868\u9762\u5f62\u8c8c\u548c\u7c97\u7cd9\u7a0b\u5ea6\uff0c\u5e26\u6709EDS\u914d\u4ef6\u7684SEM\u53ef\u4ee5\u8fdb\u4e00\u6b65\u5206\u6790\u5143\u7d20\u79cd\u7c7b\u3001\u5206\u5e03\u4ee5\u53ca\u534a\u5b9a\u91cf\u7684\u5206\u6790\u5143\u7d20\u542b\u91cf\u3002\u867d\u7136SEM\u7684\u5206\u8fa8\u7387\u8fdc\u5c0f\u4e8eTEM\uff0c\u4f46\u5b83\u4ecd\u662f\u8868\u5f81\u7535\u6c60\u6750\u6599\u7684\u9897\u7c92\u5927\u5c0f\u548c\u8868\u9762\u5f62\u8c8c\u7684\u6700\u57fa\u672c\u7684\u5de5\u5177<\/span><\/p>\n

\u674e\u6587\u4fca\u7b49\u5229\u7528\u5bc6\u5c01\u8f6c\u79fb\u76d2\u8f6c\u79fb\u6837\u54c1\u7684\u57fa\u7840\u4e0a\uff0c\u91cd\u65b0\u8bbe\u8ba1\u4e86\u9488\u5bf9\u91d1\u5c5e\u9502\u7535\u6781\u7684\u626b\u63cf\u7535\u955c\u7684\u6837\u54c1\u6258\u67b6\uff0c\u7814\u7a76\u4e86\u91d1\u5c5e\u9502\u7535\u6781\u5728Li\u7684\u5d4c\u5165\u548c\u8131\u51fa\u8fc7\u7a0b\u4e2d\u8868\u9762\u5b54\u6d1e\u548c\u679d\u6676\u7684\u5f62\u6210\u8fc7\u7a0b[8]\u3002<\/span><\/p>\n

\uff082\uff09\u900f\u5c04\u7535\u955c\uff08TEM\uff09<\/span><\/p>\n

\u6750\u6599\u7684\u8868\u9762\u548c\u754c\u9762\u7684\u5f62\u8c8c\u548c\u7279\u6027\uff0c\u5728\u5173\u4e8e\u8868\u9762\u5305\u8986\u4ee5\u53ca\u9610\u8ff0\u8868\u9762SEI\u7684\u6587\u732e\u4e2d\u591a\u6709\u4ecb\u7ecd\u3002TEM\u4e5f\u53ef\u4ee5\u914d\u7f6e\u80fd\u8c31\u9644\u4ef6\u6765\u5206\u6790\u5143\u7d20\u7684\u79cd\u7c7b\u3001\u5206\u5e03\u7b49\u3002\u4e0eSEM\u76f8\u6bd4TEM\u80fd\u89c2\u5bdf\u5230\u66f4\u5c0f\u7684\u9897\u7c92\uff0c\u5e76\u4e14\u9ad8\u5206\u8fa8\u900f\u5c04\u7535\u955c\u53ef\u4ee5\u5bf9\u6676\u683c\u8fdb\u884c\u89c2\u5bdf\uff0c\u539f\u4f4dTEM\u7684\u529f\u80fd\u66f4\u52a0\u5f3a\u5927\uff0c\u5728TEM\u7535\u955c\u8154\u4f53\u4e2d\u7ec4\u88c5\u539f\u4f4d\u7535\u6c60\uff0c\u540c\u65f6\u501f\u52a9\u4e8eTEM\u7684\u9ad8\u5206\u8fa8\u7279\u6027\uff0c\u5bf9\u7535\u6c60\u6750\u6599\u5728\u5faa\u73af\u8fc7\u7a0b\u4e2d\u7684\u5f62\u8c8c\u548c\u7ed3\u6784\u6f14\u5316\u8fdb\u884c\u5b9e\u65f6\u7684\u6d4b\u91cf\u548c\u5206\u6790<\/span><\/p>\n

\u9ec4\u5efa\u5b87\u7b49\u5229\u7528\u539f\u4f4d\u6837\u54c1\u6746\u5bf9SnO2\u5728\u79bb\u5b50\u6db2\u4f53\u4e2d\u5d4c\u8131\u9502\u8fc7\u7a0b\u4e2d\u7684\u5f62\u8c8c\u548c\u7ed3\u6784\u6f14\u5316\u8fdb\u884c\u4e86\u539f\u4f4d\u8868\u5f81\u3002\u968f\u540e\uff0c\u4ed6<\/span>\u4eec\u5bf9TEM\u539f\u4f4d\u7535\u6c60\u5b9e\u9a8c\u7684\u88c5\u7f6e\u8fdb\u884c\u4e86\u6539\u8fdb\uff0c\u5229\u7528\u5728\u91d1\u5c5eLi\u4e0a\u81ea\u7136\u751f\u4ea7\u7684\u6c27\u5316\u9502\u4f5c\u4e3a\u7535\u89e3\u8d28\uff0c\u4ee3\u66ff\u4e86\u539f\u5148\u4f7f\u7528\u7684\u79bb\u5b50\u6db2\u4f53\uff0c\u63d0\u9ad8\u4e86\u5b9e\u9a8c\u7684\u7a33\u5b9a\u6027\uff0c\u66f4\u597d\u5730\u4fdd\u62a4\u4e86\u7535\u955c\u8154\u4f53[9,10]\u3002<\/span><\/p>\n

\u6269\u5c55\u9605\u8bfb\uff1a\u5b66\u672f\u5e72\u8d27\u2502\u539f\u4f4d\u900f\u5c04\u7535\u955c\u5728\u6750\u6599\u6c14\u6db2\u76f8\u5316\u5b66\u53cd\u5e94\u7814\u7a76\u4e2d\u7684\u4f5c\u7528<\/a><\/p>\n

\uff083\uff09\u539f\u5b50\u529b\u663e\u5fae\u955c\uff08AFM\uff09<\/span><\/p>\n

\u7eb3\u7c73\u7ea7\u5e73\u6574\u8868\u9762\u7684\u89c2\u5bdf\uff0c\u5728\u78b3\u6750\u6599\u7684\u8868\u5f81\u4e2d\u4f7f\u7528\u8f83\u591a\u3002<\/span><\/p>\n

3\u3001\u6676\u4f53\u7ed3\u6784\u8868\u5f81<\/strong><\/span><\/p>\n

\uff081\uff09X\u5c04\u7ebf\u884d\u5c04\u6280\u672f\uff08XRD\uff09<\/span><\/p>\n

\u901a\u8fc7XRD\uff0c\u53ef\u4ee5\u83b7\u5f97\u6750\u6599\u7684\u6676\u4f53\u7ed3\u6784\u3001\u7ed3\u6676\u5ea6\u3001\u5e94\u529b\u3001\u7ed3\u6676\u53d6\u5411\u3001\u8d85\u7ed3\u6784\u7b49\u4fe1\u606f\uff0c\u8fd8\u53ef\u4ee5\u53cd\u6620\u5757\u4f53\u6750\u6599\u5e73\u5747\u6676\u4f53\u7ed3\u6784\u6027\u8d28\uff0c\u5e73\u5747\u7684\u6676\u80de\u7ed3\u6784\u53c2\u6570\u53d8\u5316\uff0c\u62df\u5408\u540e\u53ef\u4ee5\u83b7\u53d6\u539f\u5b50\u5360\u4f4d\u4fe1\u606f<\/span><\/p>\n

Thurston\u7b49\u9996\u6b21\u5c06\u539f\u4f4d\u7684XRD\u6280\u672f\u5e94\u7528\u5230\u9502\u79bb\u5b50\u7535\u6c60\u4e2d\u3002\u901a\u8fc7\u5229\u7528\u540c\u6b65\u8f90\u5c04\u5149\u6e90\u7684\u786cX\u5c04\u7ebf\u63a2\u6d4b\u539f\u4f4d\u7535\u6c60\u88c5\u7f6e\u4e2d\u7684\u4f53\u7535\u6781\u6750\u6599\uff0c\u76f4\u89c2\u7684\u89c2\u5bdf\u5230\u6676\u683c\u81a8\u80c0\u548c\u6536\u7f29\u3001\u76f8\u53d8\u3001\u591a\u76f8\u5f62\u6210\u7684\u7ed3\u679c\u3002<\/span><\/p>\n

\uff082\uff09\u6269\u5c55X\u5c04\u7ebf\u5438\u6536\u7cbe\u7ec6\u8c31\uff08EXAFS\uff09<\/span><\/p>\n

\u901a\u8fc7X \u5c04\u7ebf\u4e0e\u6837\u54c1\u7684\u7535\u5b50\u76f8\u4e92\u4f5c\u7528\uff0c\u5438\u6536\u90e8\u5206\u7279\u5b9a\u80fd\u91cf\u7684\u5165\u5c04\u5149\u5b50\uff0c\u6765\u53cd\u6620\u6750\u6599\u5c40\u90e8\u7ed3\u6784\u5dee\u5f02\u4e0e\u53d8\u5316\u7684\u6280\u672f\uff0c\u5177\u6709\u4e00\u5b9a\u7684\u80fd\u91cf\u548c\u65f6\u95f4\u5206\u8fa8\u80fd\u529b\uff0c\u4e3b\u8981\u83b7\u5f97\u6676\u4f53\u7ed3\u6784\u4e2d\u5f84\u5411\u5206\u5e03\u3001\u952e\u957f\u3001\u6709\u5e8f\u5ea6\u3001\u914d\u4f4d\u6570\u7b49\u4fe1\u606f\uff1b\u901a\u5e38\u9700\u8981\u540c\u6b65\u8f90\u5c04\u5149\u6e90\u7684\u5f3a\u5149\u6e90\u6765\u5b9e\u73b0EXAFS \u5b9e\u9a8c<\/p>\n

Jung\u7b49\u901a\u8fc7\u7528EXAFS\u5206\u6790\u7814\u7a76\u4e86\u5d4cSnOx\uff0fCuOx\u7684\u78b3\u7eb3\u7c73\u8d1f\u6781\u6750\u6599\u7684\u7535\u5316\u5b66\u6027\u8d28\uff0c\u8868\u660e\u5d4cSnOx\uff0fCuOx\u7684\u78b3\u7eb3\u7c73\u7ea4\u7ef4\u5177\u6709\u4e00\u4e2a\u65e0\u5e8f\u7684\u7ed3\u6784\uff0c\u5f62\u6210\u4e86SnOx\u9897\u7c92\u7684\u7279\u6b8a\u5206\u5e03\uff0c\u7531\u6b64\u5bfc\u81f4\u7535\u5316\u5b66\u6027\u80fd\u6709\u6240\u63d0\u5347[12]\u3002<\/span><\/p>\n

\uff083\uff09\u4e2d\u5b50\u884d\u5c04\uff08ND\uff09<\/span><\/p>\n

\u5f53\u9502\u79bb\u5b50\u7535\u6c60\u6750\u6599\u4e2d\u6709\u8f83\u5927\u7684\u539f\u5b50\u5b58\u5728\u65f6\uff0cX \u5c04\u7ebf\u5c06\u96be\u4ee5\u5bf9\u9502\u79bb\u5b50\u5360\u4f4d\u8fdb\u884c\u7cbe\u786e\u7684\u63a2\u6d4b\u3002\u4e2d\u5b50\u5bf9\u9502\u79bb\u5b50\u7535\u6c60\u6750\u6599\u4e2d\u7684\u9502\u8f83\u654f\u611f\uff0c\u56e0\u6b64\u4e2d\u5b50\u884d\u5c04\u5728\u9502\u79bb\u5b50\u7535\u6c60\u6750\u6599\u7684\u7814\u7a76\u4e2d\u53d1\u6325\u7740\u91cd\u8981\u4f5c\u7528\u3002<\/span><\/p>\n

Arbi\u7b49\u901a\u8fc7\u4e2d\u5b50\u884d\u5c04\u786e\u5b9a\u4e86\u9502\u79bb\u5b50\u7535\u6c60\u56fa\u6001\u7535\u89e3\u8d28\u6750\u6599LATP\u4e2d\u7684Li+\u5360\u4f4d[13]\u3002<\/span><\/p>\n

\uff084\uff09\u6838\u78c1\u5171\u632f\uff08NMR\uff09<\/span><\/p>\n

NMR\u5177\u6709\u9ad8\u7684\u80fd\u91cf\u5206\u8fa8\u3001\u7a7a\u95f4\u5206\u8fa8\u80fd\u529b\uff0c\u80fd\u591f\u63a2\u6d4b\u6750\u6599\u4e2d\u7684\u5316\u5b66\u4fe1\u606f\u5e76\u6210\u50cf\uff0c\u63a2\u6d4b\u679d\u6676\u53cd\u5e94\u3001\u6d4b\u5b9a\u9502\u79bb\u5b50\u81ea\u6269\u6563\u7cfb\u6570\u3001\u5bf9\u9897\u7c92\u5185\u90e8\u76f8\u8f6c\u53d8\u53cd\u5e94\u8fdb\u884c\u7814\u7a76<\/strong>\u3002<\/span><\/p>\n

Grey\u7b49\u5bf9NMR\u5728\u9502\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u6750\u6599\u4e2d\u7684\u7814\u7a76\u5f00\u5c55\u4e86\u5927\u91cf\u7684\u7814\u7a76\u5de5\u4f5c\u3002\u8868\u660e\u4ece\u6b63\u6781\u6750\u6599\u7684NMR\u8c31\u4e2d\u53ef\u4ee5\u5f97<\/span>\u5230\u4e30\u5bcc\u7684\u5316\u5b66\u4fe1\u606f\u53ca\u5c40\u90e8\u7535\u8377\u6709\u5e8f\u65e0\u5e8f\u7b49\u4fe1\u606f\uff0c\u5e76\u53ef\u4ee5\u63a2\u6d4b\u987a\u78c1\u6216\u91d1\u5c5e\u6001\u7684\u6750\u6599\uff0c\u8fd8\u53ef\u4ee5\u63a2\u6d4b\u63ba\u6742\u5e26\u6765\u7684\u7535\u5b50\u7ed3\u6784\u7684\u5fae\u5f31\u53d8\u5316\u6765\u53cd\u6620\u5143\u7d20\u5316\u5408\u6001\u4fe1\u606f\u3002\u53e6\u5916\u7ed3\u5408\u540c\u4f4d\u7d20\u793a\u8e2a\u8fd8\u53ef\u4ee5\u7814\u7a76\u7535\u6c60\u4e2d\u7684\u526f\u53cd\u5e94\u7b49[14]\u3002<\/span><\/p>\n

\uff085\uff09\u7403\u5dee\u6821\u6b63\u626b\u63cf\u900f\u5c04\u7535\u955c\uff08STEM\uff09<\/span><\/p>\n

\u7528\u9014\uff1a\u7528\u6765\u89c2\u5bdf\u539f\u5b50\u7684\u6392\u5e03\u60c5\u51b5<\/strong>\u3001\u539f\u5b50\u7ea7\u5b9e\u7a7a\u95f4\u6210\u50cf\uff0c\u53ef\u6e05\u6670\u770b\u5230\u6676\u683c\u4e0e\u539f\u5b50\u5360\u4f4d\uff1b\u5bf9\u6837\u54c1\u8981\u6c42\u9ad8\uff1b\u53ef\u4ee5\u5b9e\u73b0\u539f\u4f4d\u5b9e\u9a8c<\/span><\/p>\n

Oshima\u7b49\u5229\u7528\u73af\u5f62\u660e\u573a\u6210\u50cf\u7684\u7403\u5dee\u6821\u6b63\u626b\u63cf\u900f\u5c04\u663e\u5fae\u955c(ABF-STEM)\u89c2\u5bdf\u5230\u4e86Li2VO4\u4e2dLi\u3001V\u3001O\u5728\u5b9e\u7a7a\u95f4\u7684\u539f\u5b50\u6392\u5e03[15]\u3002<\/span><\/p>\n

\uff086\uff09Raman<\/span><\/p>\n

\u65e9\u671f\u7528\u62c9\u66fc\u5149\u8c31\u7814\u7a76LiC0O2\u7684\u6676\u4f53\u7ed3\u6784\uff0cLiC0O2\u4e2d\u6709\u4e24\u79cd\u62c9\u66fc\u6d3b\u6027\u6a21\u5f0f\uff0cCo\u2014O\u4f38\u7f29\u632f\u52a8Alg\u7684\u5cf0\u4e0eO\u2014Co\u2014O\u7684\u5f2f\u66f2\u632f\u52a8Eg\u7684\u5cf0[16]\u3002\u4e5f\u591a\u7528\u4e8e\u9502\u79bb\u5b50\u7535\u6c60\u4e2d\u78b3\u6750\u6599\u77f3\u58a8\u5316\u7a0b\u5ea6\u7684\u8868\u5f81\u5206\u6790\u3002<\/span><\/p>\n

4\u3001\u5b98\u80fd\u56e2\u7684\u8868\u5f81<\/strong><\/span><\/p>\n

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\uff081\uff09\u62c9\u66fc\u5149\u8c31\uff08RS\uff09<\/span><\/p>\n

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6\u3001\u6750\u6599\u5fae\u89c2\u529b\u5b66\u6027\u8d28<\/strong><\/span><\/p>\n

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7\u3001\u6750\u6599\u8868\u9762\u529f\u51fd\u6570<\/strong><\/span><\/p>\n

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\u76f8\u5173\u6587\u732e\uff1a<\/span><\/strong><\/p>\n

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[13]\u00a0Arbi K, Hoelzel M, Kuhn A, et al. Structural Factors That Enhance Lithium Mobility in Fast-Ion Li1+ x Ti2\u2013x Al x (PO4) 3 (0\u2264 x\u2264 0.4) Conductors Investigated by Neutron Diffraction in the Temperature Range 100\u2013500 K[J]. Inorganic chemistry, 2013, 52(16): 9290-9296.<\/span><\/p>\n

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[19] Nishimura S, Kobayashi G, Ohoyama K, et al. Experimental visualization of lithium diffusion in LixFePO4[J]. Nature materials, 2008, 7(9): 707-711.<\/span><\/p>\n

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[21]\u00a0Kobayashi H, Shikano M, Koike S, et al. Investigation of positive electrodes after cycle testing of high-power Li-ion battery cells: I. An approach to the power fading mechanism using XANES[J]. Journal of Power Sources, 2007, 174(2): 380-386.<\/a><\/span><\/p>\n

[22]\u00a0Nam K W, Bak S M, Hu E, et al. Combining In Situ Synchrotron X\u2010Ray Diffraction and Absorption Techniques with Transmission Electron Microscopy to Study the Origin of Thermal Instability in Overcharged Cathode Materials for Lithium\u2010Ion Batteries[J]. Advanced Functional Materials, 2013, 23(8): 1047-1063.<\/a><\/span><\/p>\n

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