{"id":53057,"date":"2016-11-24T14:00:42","date_gmt":"2016-11-24T06:00:42","guid":{"rendered":"\/\/m.iemloyee.com\/?p=53057"},"modified":"2016-11-25T22:47:45","modified_gmt":"2016-11-25T14:47:45","slug":"adv-mater-%e4%ba%8c%e7%bb%b4%e5%99%bb%e5%90%a9%e7%ba%b3%e7%b1%b3%e7%89%87%e4%b8%8e%e7%9f%b3%e5%a2%a8%e7%83%af%e5%a0%86%e5%8f%a0%e5%b1%82%e5%bc%82%e8%b4%a8%e7%bb%93%e8%86%9c%e4%bd%9c%e4%b8%ba","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=53057","title":{"rendered":"Adv. Mater.: \u4e8c\u7ef4\u567b\u5429\u7eb3\u7c73\u7247\u4e0e\u77f3\u58a8\u70ef\u5806\u53e0\u5c42\u5f02\u8d28\u7ed3\u819c\u4f5c\u4e3a\u9ad8\u500d\u7387\u9ad8\u5bb9\u91cf\u5168\u56fa\u6001\u8d5d\u7535\u5bb9\u5668\u7535\u6781"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u968f\u7740\u4fbf\u643a\u5f0f\u548c\u53ef\u7a7f\u6234\u5f0f\u7535\u5b50\u4ea7\u54c1\u7684\u5feb\u901f\u53d1\u5c55,\u672a\u6765\u7684\u50a8\u80fd\u8bbe\u5907\u9664\u4e86\u53d8\u5f97\u8f7b\u8584\u5b9e\u60e0\u5916,\u8fd8\u9700\u8981\u5177\u5907\u8d85\u5f3a\u7684\u67d4\u6027\u3002\u5168\u56fa\u6001\u8d85\u7ea7\u7535\u5bb9\u5668\uff08ASSSs\uff09\u5177\u6709\u6781\u5f3a\u7684\u5668\u68b0\u67d4\u6027\u548c\u5b89\u5168\u6027\uff0c\u5728\u7535\u5b50\u8bbe\u5907\u7684\u5236\u9020\u8fc7\u7a0b\u4e2d\u88ab\u8ba4\u4e3a\u662f\u4e00\u79cd\u5f88\u597d\u7684\u9ad8\u529f\u7387\u6e90\u3002\u4f46\u603b\u4f53\u4e0a\uff0c\u7eb3\u7c73\u78b3\u57fa\u5e95\uff08\u5982\u6d3b\u6027\u70ad\u3001\u78b3\u7eb3\u7c73\u7ba1\u3001\u77f3\u58a8\u70ef\uff09ASSSs\u7684\u4f53\u79ef\u6bd4\u7535\u5bb9\u4f4e\uff0c\u800c\u4ee5\u5bfc\u7535\u805a\u5408\u7269\u548c\u91d1\u5c5e\u6c27\u5316\u7269\u4e3a\u57fa\u5e95\u7684\u8d5dASSSs\u500d\u7387\u6027\u80fd\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u8f83\u5dee\uff0c\u8fd9\u4e9b\u7f3a\u70b9\u6781\u5927\u7684\u9650\u5236\u5b83\u4eec\u5728\u5b9e\u9645\u751f\u6d3b\u4e2d\u7684\u5e94\u7528\u3002\u56e0\u6b64\uff0c\u5f00\u53d1\u4e00\u79cd\u5177\u6709\u5927\u4f53\u79ef\u6bd4\u7535\u5bb9\uff0c\u51fa\u8272\u7684\u500d\u7387\u6027\u80fd\u548c\u9ad8\u5faa\u73af\u6027\u7684\u65b0\u578b\u7535\u6781\u6750\u6599\u5bf9ASSSs\u6765\u8bf4\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u4e2d\u56fd\u79d1\u5b66\u9662\u5927\u8fde\u5316\u5b66\u7269\u7406\u7814\u7a76\u6240\u5434\u5fe0\u5e05\u7814\u7a76\u5458\u3001\u5fb7\u56fd\u9a6c\u666e\u6240\u7684<\/strong>Klaus M\u00fcllen<\/strong>\u6559\u6388\u4ee5\u53ca\u5fb7\u7d2f\u65af\u987f\u6280\u672f\u5927\u5b66\u7684\u51af\u65b0\u4eae\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u7684\u56e2\u961f<\/strong>\u5728Advanced Materials<\/strong>\u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u9898\u4e3a\u201cStacked-Layer Heterostructure Films of 2D Thiophene Nanosheets and Graphene for High-Rate All-Solid-State Pseudocapacitors with Enhanced Volumetric Capacitance<\/strong>\u201d\u7684\u6587\u7ae0\u3002\u8be5\u7814\u7a76\u56e2\u961f\u9996\u6b21\u5229\u7528\u567b\u5429\uff08TP\uff09\u7eb3\u7c73\u7247\u548c\u7535\u5316\u5b66\u5265\u79bb\u7684\u77f3\u58a8\u70ef\uff08EG\uff09\u5236\u5907\u51fa\u5806\u53e0\u5c42\u5f02\u8d28\u7ed3\u819c\uff08TP\/EG\uff09\uff0c\u5e76\u5c06\u5176\u5e94\u7528\u4e8e\u9ad8\u500d\u7387\u3001\u67d4\u6027\u5316ASSSs (TP\/EG-ASSSs)\u548c\u5fae\u578b\u8d85\u7ea7\u7535\u5bb9\u5668\uff08TP\/EG-MSCs\uff09\u3002\u7814\u7a76\u56e2\u961f\u901a\u8fc7\u4f9d\u6b21\u4ea4\u66ff\u6c89\u79efEG\u7eb3\u7c73\u7247\u548c\u6c27\u5316\u8fd8\u539f\u6027\u5bfc\u7535TP\u7eb3\u7c73\u7247\u7684\u65b9\u6cd5\u83b7\u5f97\u5f02\u8d28\u7ed3\u819c\uff0c\u518d\u5c06\u6240\u5236\u5907\u7684\u819c\u76f4\u63a5\u8f6c\u79fb\u5230\u805a\u5bf9\u82ef\u4e8c\u7532\u9178\u4e59\u4e8c\u9187\u916f\uff08PET\uff09\u57fa\u5e95\u4e0a\u5e76\u7528\u4f5c\u67d4\u6027\u8d85\u7ea7\u7535\u5bb9\u5668\u7684\u65e0\u7c98\u5408\u5242\u548c\u65e0\u6dfb\u52a0\u5242\u7535\u6781\u3002\u8be5\u56e2\u961f\u6240\u5236\u6210\u7684TP\/EG-ASSSs\u7684\u9762\u79ef\u6bd4\u7535\u5bb9\u7ea6\u4e3a3.9 mF\/cm2<\/sup>\uff0c\u4f53\u79ef\u6bd4\u7535\u5bb9\u7ea6\u4e3a375 F\/cm3<\/sup>\uff0c\u80fd\u91cf\u5bc6\u5ea6\u4e3a13 mWh\/cm3<\/sup>,\u529f\u7387\u5bc6\u5ea6\u4e3a776 W\/cm3<\/sup>\u3002\u540c\u65f6\uff0c\u6240\u5236\u6210\u7684TP\/EG-MSCs\u5177\u6709\u8d85\u9ad8\u500d\u7387\u6027\u80fd\uff0c\u80fd\u591f\u5728\u9ad8\u81f31000 V\/s\u7684\u500d\u7387\u4e0b\u5de5\u4f5c\u3002\u5728100 V\/s\u7684\u500d\u7387\u4e0b\uff0cTP\/EG-MSCs\u9762\u79ef\u6bd4\u7535\u5bb9\u4e3a1.30 mF\/cm2<\/sup>\uff0c\u4f53\u79ef\u6bd4\u7535\u5bb9\u4e3a123 F\/cm3<\/sup>\u3002\u53e6\u5916\uff0c\u8fd9\u79cd\u8d85\u67d4\u6027\u7684TP\/EG-MSCs\u5728\u4e0d\u540c\u7684\u5f2f\u66f2\u72b6\u6001\u4e0b\u90fd\u5177\u6709\u5f88\u7a33\u5b9a\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe1: TP\u548cEG\u7eb3\u7c73\u7247\u7684\u7ed3\u6784\u548c\u5f62\u8c8c\u7279\u6027<\/strong><\/p>\n

\"fig1\"<\/p>\n

(a)\u901a\u8fc7\u7531Ph2TPh\u5355\u4f53\u7ec4\u6210\u7684\u805a\u5408\u7269\u7684\u81ea\u7ec4\u88c5\u6765\u5236\u5907TP\u7eb3\u7c73\u7247\uff0c\u8be5Ph2TPh\u5355\u4f53\u662f\u7531\u6eb6\u89e3\u5728\u90bb\u4e8c\u6c2f\u82ef\uff08DCB\uff09\u4e2d\u76841,2,3-\u4e09\u5511\u5355\u5143\u8fde\u63a5\u800c\u6210\uff1b<\/p>\n

(b)\u7a33\u5b9a\u7684TP\u6eb6\u6db2\u7684\u5149\u5b66\u56fe\u50cf\uff0cDCB\u6eb6\u6db2\u4e2d\u5355\u4f53\u5355\u5143\u7684\u6eb6\u5ea6\u4e3a1\u00d710-4<\/sup> mol\/L\uff1b<\/p>\n

(c)TP\u7eb3\u7c73\u7247\u7684TEM\u56fe\u50cf\uff0c\u63d2\u56fe\u662fTP\u7eb3\u7c73\u7247\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(d)TP\u7eb3\u7c73\u7247\u7684AFM\u56fe\u50cf\uff1b<\/p>\n

(e)TP\u7eb3\u7c73\u7247\u7684\u9ad8\u5ea6\u8f6e\u5ed3\uff0c\u539a\u5ea6\u7ea6\u4e3a3.5 nm\uff1b<\/p>\n

(f)\u7a33\u5b9aEG\u6eb6\u6db2\u7684\u7684\u5149\u5b66\u56fe\u50cf\uff0c\u5728DMF\u6eb6\u5242\u4e2dEG\u7684\u6eb6\u5ea6\u4e3a0.1 mg\/L\uff1b<\/p>\n

(g)EG\u7eb3\u7c73\u7247\u7684SEM\u56fe\u50cf\uff0c\u63d2\u56fe\u662fEG\u7eb3\u7c73\u7247\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(h)EG\u7eb3\u7c73\u7247\u7684AFM\u56fe\u50cf\uff1b<\/p>\n

(i)EG\u7eb3\u7c73\u7247\u7684\u9ad8\u5ea6\u8f6e\u5ed3\uff0c\u539a\u5ea6\u7ea6\u4e3a1.0 nm\u3002<\/p>\n

\u56fe2:TP\/EG\u5f02\u8d28\u7ed3\u8584\u819c\u7684\u8868\u5f81<\/strong><\/p>\n

\"fig2\"<\/p>\n

(a)\u81ea\u7531\u7ad9\u7acbTP\/EG\u5f02\u8d28\u7ed3\u8584\u819c\u7684SEM\u56fe\uff0c\u5de6\u4e0a\u7684\u63d2\u56fe\u662f\u5728PET\u57fa\u5e95\u4e0a\u5236\u5907\u7684\u8584\u819c\uff0c\u53f3\u4e0b\u7684\u63d2\u56fe\u662f\u5f02\u8d28\u7ed3\u8584\u819c\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(b)TP\/EG\u5f02\u8d28\u7ed3\u8584\u819c\u7684\u8868\u9762\u5f62\u8c8c\uff1b<\/p>\n

(c)\u7531\u53f0\u9636\u4eea\u6d4b\u91cf\u5f97\u5230TP\/EG\u5f02\u8d28\u7ed3\u8584\u819c\u7684\u76f8\u5e94\u539a\u5ea6\uff1b<\/p>\n

(d)TP\/EG\u5f02\u8d28\u7ed3\u8584\u819c\u7684SEM\u9876\u89c6\u56fe\uff0c\u63d2\u56fe\u662f\u5f02\u8d28\u7ed3\u8584\u819c\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(e)TP\/EG\u5f02\u8d28\u7ed3\u8584\u819c\u9ad8\u5206\u8fa8SEM\u9876\u89c6\u56fe\uff0c\u8868\u660e\u77f3\u58a8\u70ef\u5b58\u5728\u8936\u76b1\u3002<\/p>\n

\u56fe3\uff1aTP\/EG-ASSSs\u7684\u7535\u5316\u5b66\u8868\u5f81<\/strong><\/p>\n

\"fig3\"<\/p>\n

(a)\u67d4\u6027TP\/EG-ASSSs\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

(b)\u57281 mV\/s\u81f3500 mV\/s\u8303\u56f4\u5185\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u83b7\u5f97\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(c)\u57281 V\/s\u81f3100 V\/s\u8303\u56f4\u5185\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u83b7\u5f97\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(d)TP\/EG-ASSSs\u548cEG-ASSSs\u7684\u4f53\u79ef\u6bd4\u5bb9\u91cf\uff1b<\/p>\n

(e)TP\/EG-ASSSs\u548cEG-ASSSs\u7684Ragone\u56fe<\/p>\n

(f)TP\/EG-ASSSs\u548cEG-ASSSs\u7684\u963b\u6297\u76f8\u4f4d\u89d2\u4e0e\u9891\u7387\u7684\u51fd\u6570\u5173\u7cfb\u56fe\uff0c\u63d2\u56fe\u662fTP\/EG-ASSSs\u548cEG-ASSSs\u7684\u9ad8\u9891\u7387Nyquist\u56fe\uff1b<\/p>\n

(g)TP\/EG-ASSSs\u5728\u4e0d\u540c\u5f2f\u66f2\u89d2\u5ea6\u4e0b\u6d4b\u8bd5\u7684\u5f2f\u66f2\u793a\u610f\u56fe\uff1b<\/p>\n

(h)TP\/EG-ASSSs\u5728\u4e0d\u540c\u5f2f\u66f2\u89d2\u5ea6\u4e0b\u6d4b\u8bd5\u83b7\u5f97\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(i)\u626b\u63cf\u901f\u7387\u4e3a100 mV\/s\u65f6TP\/EG-ASSSs\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002<\/p>\n

\u56fe4\uff1aTP\/EG-MSCs\u7684\u7535\u5316\u5b66\u8868\u5f81<\/strong><\/p>\n

\"fig4\"<\/p>\n

(a)\u5e73\u677fTP\/EG-MSCs\u7684\u9876\u89c6\u793a\u610f\u56fe\uff1b<\/p>\n

(b)\u7535\u8377\u72b6\u6001\u7684\u4fa7\u89c6\u793a\u610f\u56fe\uff1b<\/p>\n

(c)\u57280.1 V\/s\u81f31000 V\/s\u8303\u56f4\u5185\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u83b7\u5f97\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

(d)\u9762\u79ef\u6bd4\u5bb9\u91cf\u548c\u4f53\u79ef\u6bd4\u5bb9\u91cf\u4e0e\u626b\u63cf\u901f\u7387\u7684\u51fd\u6570\u5173\u7cfb\u66f2\u7ebf\uff1b<\/p>\n

(e)\u5e73\u94fa\u72b6\u548c\u5f2f\u66f2\u72b6TP\/EG-MSCs\u5728\u626b\u63cf\u901f\u7387\u4e3a1 V\/s\u7684\u6761\u4ef6\u4e0b\u83b7\u5f97\u7684CV\u66f2\u7ebf\uff0c\u63d2\u56fe\u662f\u5e73\u94fa\u72b6\u548c\u5f2f\u66f2\u72b6TP\/EG-MSCs\u7684\u7167\u7247\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u4e0e\u5c55\u671b\u3011<\/strong><\/p>\n

\u4f5c\u8005\u6240\u5728\u7814\u7a76\u56e2\u961f\u5236\u9020\u4e86\u4ee5\u8d85\u8584TP\u548cEG\u7eb3\u7c73\u7247\u5806\u53e0\u5c42\u5f02\u8d28\u7ed3\u819c\u4e3a\u7535\u6781\u7684\u5168\u56fa\u6001\u8d5d\u7535\u5bb9\u5668\u548c\u5fae\u578b\u8d85\u7ea7\u7535\u5bb9\u5668,\u5e76\u8bc1\u5b9e\u6b64\u7c7b\u7535\u5bb9\u5668\u5177\u6709\u9ad8\u4f53\u79ef\u6bd4\u7535\u5bb9,\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u3001\u9ad8\u529f\u7387\u5bc6\u5ea6\u548c\u8d85\u67d4\u6027\u3002\u5728\u8fd9\u91cc\u6709\u7406\u7531\u76f8\u4fe1\uff0c\u8fd9\u79cd\u5806\u53e0\u5c42\u5f02\u8d28\u7ed3\u819c\u5728\u8d85\u7ea7\u7535\u5bb9\u5668\u4e2d\u4f7f\u7528\u80fd\u591f\u4e3a\u8bf8\u5982\u4e8c\u7ef4\u77f3\u58a8\u70ef\u7b49\u65b0\u6982\u5ff5\u8584\u819c\u5728\u50a8\u80fd\u8bbe\u5907\u4e2d\u7684\u5e94\u7528\u6253\u5f00\u4e00\u6247\u65b0\u7684\u5927\u95e8\u3002<\/p>\n

\u6587\u732e\u8fde\u63a5<\/strong>\uff1aStacked-Layer Heterostructure Films of 2D Thiophene Nanosheets and Graphene for High-Rate All-Solid-State Pseudocapacitors with Enhanced Volumetric Capacitance<\/a>\uff08Adv. Mater. 2016, DOI:10.1002\/adma.201602960\uff09<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u5b66\u672f\u5c0f\u7ec4\u9ec4M\u5409\u6574\u7406\u3002<\/p>\n

\u6750\u6599\u725b\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u8fd9\u91cc\u6c47\u96c6\u4e86\u5404\u5927\u9ad8\u6821\u7855\u535a\u751f\u3001\u4e00\u7ebf\u79d1\u7814\u4eba\u5458\u4ee5\u53ca\u884c\u4e1a\u4ece\u4e1a\u8005\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u6750\u6599\u4eba\u7f16<\/a>\u8f91\u90e8<\/a>\u3002<\/p>\n

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\u6750\u6599\u6d4b\u8bd5\uff0c\u6570\u636e\u5206\u6790\uff0c\u4e0a<\/strong>\u6d4b\u8bd5\u8c37<\/strong><\/a>\uff01<\/strong><\/p>\n

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