{"id":50788,"date":"2016-11-13T14:00:08","date_gmt":"2016-11-13T06:00:08","guid":{"rendered":"\/\/m.iemloyee.com\/?p=50788"},"modified":"2017-03-18T20:48:59","modified_gmt":"2017-03-18T12:48:59","slug":"energy-environ-sci-%e5%a4%a7%e8%bf%9e%e5%8c%96%e7%89%a9%e6%89%80%e5%8c%85%e4%bf%a1%e5%92%8c%e9%99%a2%e5%a3%ab%e5%85%b3%e4%ba%8e%e9%94%8c%e7%a9%ba%e6%b0%94%e7%94%b5%e6%b1%a0%e6%b0%a7%e8%bf%98%e5%8e%9f","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=50788","title":{"rendered":"Energy Environ. Sci.\u5927\u8fde\u5316\u7269\u6240\u5305\u4fe1\u548c\u9662\u58eb\u5173\u4e8e\u950c\u7a7a\u6c14\u7535\u6c60\u6c27\u8fd8\u539f\u6548\u7387\u7684\u63d0\u9ad8\u65b0\u8fdb\u5c55"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u91d1\u5c5e\u7a7a\u6c14\u7535\u6c60\u548c\u9502\u786b\u7535\u6c60\u7531\u4e8e\u9ad8\u7684\u7406\u8bba\u529f\u7387\u5bc6\u5ea6\u548c\u73af\u5883\u53cb\u597d\u7684\u7279\u6027\u6210\u4e3a\u4fbf\u643a\u5f0f\u8fd0\u8f93\u52a8\u529b\u80fd\u6e90\u7684\u6709\u529b\u5019\u9009\u3002\u91d1\u5c5e\u7a7a\u6c14\u7535\u6c60\u8f93\u51fa\u80fd\u91cf\u7684\u80fd\u529b\u5f88\u5927\u7a0b\u5ea6\u51b3\u5b9a\u4e8e\u9634\u6781\u6c27\u8fd8\u539f\u53cd\u5e94\u7684\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\uff1b\u5c3d\u7ba1\u6709\u4e86\u91cd\u5927\u8fdb\u5c55\uff0c\u91d1\u5c5e\u548c\u91d1\u5c5e\u6c27\u5316\u7269\u50ac\u5316\u5242\u4ecd\u7136\u662f\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\u4e0d\u8db3\uff0c\u8d28\u91cf\u4f20\u8f93\u6027\u80fd\u5dee\uff1b\u56e0\u6b64\uff0c\u9ad8\u6548\u6c27\u8fd8\u539f\u50ac\u5316\u5242\u7684\u53d1\u5c55\u8fd8\u662f\u8feb\u5207\u5730\u3002\u94dc\u91d1\u5c5e\u9176\u53ef\u4ee5\u5728\u4f4e\u8fc7\u7535\u538b\u4e0b\u9ad8\u6548\u50ac\u5316\u6c27\u8fd8\u539f\u53cd\u5e94\uff0c\u56e0\u6b64\u9971\u548c\u7684Cu-N\u4e2d\u5fc3\u6eb6\u6db2\u53ef\u4ee5\u4f5c\u4e3a\u6d3b\u6027\u4f4d\u70b9\uff0c\u5468\u56f4\u7684\u914d\u4f53\u53ef\u4ee5\u63d0\u4f9b\u7a33\u5b9a\u7684\u6d3b\u6027\u4f4d\u70b9\u7ed3\u6784\uff0c\u5728\u6b64\u53d1\u73b0\u540e\uff0c\u5404\u79cd\u7c7b\u4f3c\u4e8eCu-N\u6709\u673a\u91d1\u5c5e\u590d\u5408\u7269\u7c7b\u578b\u7684\u7ed3\u6784\u88ab\u5408\u6210\uff0c\u4f46\u4e5f\u5b58\u5728\u95ee\u9898\uff0c\u7535\u6781\u7684\u6d3b\u6027\u4f4d\u70b9\u5bc6\u5ea6\u4f4e\uff0c\u6709\u673a\u914d\u4f53\u6291\u5236\u4e86\u6d3b\u6027\u4f4d\u70b9\u548c\u57fa\u5730\u95f4\u7684\u7535\u5b50\u4f20\u8f93\u3002\u57fa\u4e8e\u4ee5\u4e0a\uff0c\u6b64\u6b21\u62a5\u9053\u7684\u5de5\u4f5c\u901a\u8fc7\u8bbe\u8ba1\u548c\u5408\u6210\u5148\u8fdb\u7684Cu-N\u50ac\u5316\u5242\u6765\u514b\u670d\u8fd9\u4e9b\u7f3a\u70b9\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u671f\uff0c\u4e2d\u79d1\u9662\u5927\u8fde\u5316\u7269\u6240\u5305\u4fe1\u548c\u9662\u58eb\u548c\u6c6a\u56fd\u96c4\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u8bfe\u9898\u7ec4<\/strong>\u5229\u7528CuPc\u548c\u53cc\u6c30\u80fa\u4f5c\u4e3a\u5171\u540c\u524d\u9a71\u4f53\uff0c\u5236\u5907\u5d4c\u5165\u77f3\u58a8\u70ef\u4e2d\u8d1f\u8f7d\u8d85\u8fc78.5 wt %\u9ad8\u5bc6\u5ea6\u7684\u6d3b\u6027\u4f4d\u70b9\u3002\u5b64\u7acb\u7684\u6d3b\u6027\u4f4d\u70b9\u901a\u8fc7\u9ad8\u89d2\u5ea6\u73af\u5f62\u6697\u573a\u626b\u63cf\u6295\u5c04\u663e\u5fae\u955c\uff0c\u626b\u63cf\u6295\u5c04\u663e\u5fae\u955c\uff0cX\u5c04\u7ebf\u5438\u6536\u7cbe\u7ec6\u7ed3\u6784\u5149\u8c31\u7b49\u6d4b\u8bd5\u6765\u8bc1\u5b9e\u3002\u66b4\u9732\u7684\u4f4d\u70b9\u6570\u91cf\u53ef\u4ee5\u901a\u8fc7\u8c03\u63a7\u53cc\u6c30\u80fa\u7684\u6bd4\u7387\u63a7\u5236\uff0c\u5728\u78b1\u6027\u4ecb\u8d28\u4e2d\u7684\u6c27\u8fd8\u539f\u53cd\u5e94\uff0c\u6700\u4f73\u7684Cu-N@C\u6676\u4f53\u663e\u793a\u51fa\u5f88\u9ad8\u7684\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\u3002<\/p>\n

\u3010\u56fe\u6587\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u00a0\u56fe\u4e00\uff1a<\/strong>Cu-N@C-60<\/strong>\u7684\u5f62\u6001\u548c\u7ed3\u6784<\/strong><\/p>\n

\"1-1\"<\/p>\n

a) TEM\u56fe\u50cf\uff1b<\/p>\n

b) HAADF-STEM\u56fe\u50cf\uff1b<\/p>\n

c)\u00a0\u76f8\u5173\u7684\u539f\u5b50Cu\u3001N\u3001C\u7684\u5143\u7d20mapping\uff1b<\/p>\n

d-e)STM\u3001STM\u6a21\u62df\u56fe\u50cf\u3002<\/p>\n

\u4ece\u56fe\u4e2d\u53ef\u4ee5\u770b\u51fa\uff0c\u6837\u54c1\u8868\u9762\u5747\u4e00\u7684\u5206\u5e03\u7740Cu\u3001N\u3001C\u5143\u7d20\uff0c\u7ed3\u5408TEM\u56fe\u8bf4\u660e\u5927\u91cf\u7684Cu\u539f\u5b50\u5d4c\u5165\u5728\u77f3\u58a8\u70ef\u77e9\u9635\u4e2d\uff1b\u56fed\u7684STM\u56fe\u50cf\u5c55\u793a\u4e86Cu-N\u4f4d\u70b9\u5d4c\u5165\u77f3\u58a8\u70ef\u77e9\u9635\u4e4b\u4e2d\u3002<\/p>\n

\u56fe\u4e8c\uff1a<\/strong>Cu-N@C<\/strong>\u50ac\u5316\u5242\u7684\u7279\u5f81<\/strong><\/p>\n

\"2-1\"<\/p>\n

a) XRD\u56fe\u8c31\uff1b<\/p>\n

b)\u00a0Cu\u76842p\u9ad8\u5206\u8fa8\u7387XPS\u66f2\u7ebf\uff1b<\/p>\n

c) XANES\u56fe\u8c31\uff1b<\/p>\n

d) Cu\u7b94(\u9ed1\u8272)\u3001CuPc(\u84dd\u8272)\u3001Cu-N@C-0(\u7eff\u8272)\u548cCu-N@C-60(\u7ea2\u8272)\u7684EXAFS\u8f6c\u79fb\u56fe\u8c31\u3002<\/p>\n

XRD\u56fe\u8c31\u4e2d\u663e\u793a\u7684\u5cf0\u4f4d\u7f6e43\u00b0\u300150\u00b0\u300174\u00b0\u4f9d\u6b21\u5bf9\u5e94Cu\u7684(111)\u3001(200)\u3001(220)\u6676\u9762\u3002XPS\u56fe\u8c31\u4e2dCu-N@C-0\u663e\u793a\u51fa\u7684\u4e3b\u8981\u4fe1\u53f7\u5728932.4eV\u548c952.2eV\u5904\uff0c\u662f\u7531\u4e8eCu0<\/sup>\u7269\u76f8\u7684\u5b58\u5728\uff0c\u800c\u5176\u4ed6\u50ac\u5316\u5242\u4e3b\u8981\u5cf0\u7684\u4f4d\u7f6e\u5728932eV\u548c951.8eV\u5904\uff0c\u6307\u51fa\u4e86Cu+<\/sup>\u7269\u76f8\u7684\u5b58\u5728\u3002<\/p>\n

\u56fe\u4e09\uff1a\u4e0d\u540c\u50ac\u5316\u5242\u7684\u7535\u50ac\u5316\u6027\u80fd<\/strong><\/p>\n

\"3-1\"<\/p>\n

a) Cu-N@C-X\u7684\u6c27\u8fd8\u539f\u53cd\u5e94\u6781\u5316\u66f2\u7ebf\uff1b<\/p>\n

b) \u7535\u5b50\u8fc1\u79fb\u6570\u548c\u5728RRDE\u6d4b\u8bd5\u4e2dCu-N@C-X\u7684 H2<\/sub>O2<\/sub>\u4ea7\u91cf\uff0c\u6d4b\u8bd5\u6761\u4ef6\uff1a\u57281M KOH\u7684O2<\/sub>\u9971\u548c\u6eb6\u6db2\u4e2d\uff0c\u65cb\u8f6c\u901f\u5ea62500rpm\uff0c\u626b\u63cf\u901f\u5ea610mV s-1<\/sup>\u3002\u8d1f\u8f7d\u5728\u77f3\u58a8\u70ef\u4e0a\u7684\u50ac\u5316\u5242\u542b\u91cf\u6709286.7\u03bcg cm -2\uff1b<\/sup><\/p>\n

c) Cu-N@C-60\u5728\u6c27\u8fd8\u539f\u53cd\u5e94\u4e2d\u7684\u6781\u8c31\u7535\u6d41\u65f6\u95f4\u66f2\u7ebf\u6cd5\uff1b<\/p>\n

d) Cu-N@C-60\u3001\u785d\u9178\u5904\u7406\u540e\u7684Cu-N@C-60\u3001CuPc\u4e09\u8005\u7684\u6c27\u8fd8\u539f\u53cd\u5e94\u6781\u5316\u66f2\u7ebf\u5bf9\u6bd4\u3002<\/p>\n

\u4e0d\u540c\u7684Cu-N@C\u50ac\u5316\u5242\u663e\u793a\u51fa\u4e86\u4e0d\u540c\u7684\u6d3b\u6027\uff0c\u5176\u4e2d\uff0cCu-N@C-60\u548cCu-N@C-120 \u663e\u793a\u51fa\u4e86\u6700\u9ad8\u7684\u6c27\u8fd8\u539f\u53cd\u5e94\u6d3b\u6027\uff0c\u6bd4Ag\u548cwt% Pt\/C\u50ac\u5316\u5242\u7684\u6d3b\u6027\u8fd8\u6709\u9ad8\uff0cCu-N@C-0\u663e\u793a\u51fa\u4e86\u6700\u5dee\u7684\u6d3b\u6027\uff0c\u8bf4\u660e\u6c27\u8fd8\u539f\u53cd\u5e94\u4e2d\u6ca1\u6709Cu\u7eb3\u7c73\u9897\u7c92\u7684\u53c2\u4e0e\uff0cCu-N\u4f4d\u70b9\u624d\u6709\u53ef\u80fd\u662f\u5728\u50ac\u5316\u5242\u4e2d\u4f5c\u4e3a\u6d3b\u6027\u4f4d\u70b9\u50ac\u5316\u6c27\u8fd8\u539f\u53cd\u5e94\u3002<\/p>\n

\u56fe\u56db\uff1a<\/strong>Cu<\/strong>\u539f\u5b50\u4e0d\u540c\u5316\u5408\u4ef7\u7ed3\u6784\u7684\u5bf9\u6bd4<\/strong><\/p>\n

\"4-1\"<\/p>\n

a) Cu\u539f\u5b50\u5728\u4e0d\u540c\u5316\u5408\u4ef7\u65f6\u7684\u4e0d\u540c\u7ed3\u6784\uff1aCu3<\/sub>-N\u3001Cu-N@C\u3001Cu-N2<\/sub>\u3001Cu-N3<\/sub>\u3001Cu-N4<\/sub>\u8fd8\u6709CuPc\u5206\u5b50\uff1b<\/p>\n

b) \u6c27\u8fd8\u539f\u53cd\u5e94\u548c\u2206E0<\/sub>\u4e4b\u95f4\u7684\u706b\u5c71\u66f2\u7ebf\uff1b<\/p>\n

c) Cu-N2<\/sub>\u3001Cu-N3<\/sub>\u3001Cu-N4<\/sub>\u3001CuPc\u7684Total DOS(\u9ed1\u8272)\u548c\u9884\u671f\u7684Cu\u539f\u5b50\u7684DOS(\u7ea2\u8272)\uff1b<\/p>\n

d) \u5438\u9644\u6c27\u540e\u7684Cu-N2<\/sub>-O\u3001Cu-N3<\/sub>-O\u3001Cu-N4<\/sub>-O\u3001CuPc-O \u7684Total DOS(\u9ed1\u8272)\u3001\u9884\u671f\u7684Cu\u539f\u5b50\u7684DOS(\u7ea2\u8272)\u548cO\u539f\u5b50\u7684DOS(\u7eff\u8272)\uff1b<\/p>\n

e) Cu-N2<\/sub>\u7ed3\u6784\u4e2d\u6c27\u8fd8\u539f\u53cd\u5e94\u8fc7\u7a0b\u3002<\/p>\n

\u56fe\u4e94\uff1a<\/strong>Cu-N@C-60<\/strong>\u4ee5\u5176\u4ed6\u50ac\u5316\u5242\u7535\u6027\u80fd\u5bf9\u6bd4<\/strong><\/p>\n

\"5-1\"<\/p>\n

a) Cu-N@C-60\u3001Ni\u7c89\u672b\u3001Ag\u7c89\u672b\u300140wt% Pt\/C\u56db\u8005\u7684\u6c27\u8fd8\u539f\u53cd\u5e94\u6781\u5316\u66f2\u7ebf\u5bf9\u6bd4\uff1b<\/p>\n

b) Cu-N@C-60\u3001Ni\u7c89\u672b\u3001Ag\u7c89\u672b\u300140wt% Pt\/C\u4f5c\u4e3a\u950c\u7a7a\u6c14\u7535\u6c60\u7535\u6781\u50ac\u5316\u5242\u7684\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

c)\u57280V\u4e0b\u7535\u6d41\u5bc6\u5ea6\u7684\u53d8\u5316\u548c\u950c\u7a7a\u6c14\u7535\u6c60\u5728\u4e00\u4e2a\u7279\u5b9aCu-N@C\u50ac\u5316\u5242\u6bd4\u8868\u9762\u79ef\u7684\u5cf0\u503c\u529f\u7387\u5bc6\u5ea6\uff1b<\/p>\n

d) Cu-N@C-60\u950c\u7a7a\u6c14\u7535\u6c60\u5728\u6052\u5b9a\u7535\u6d41\u5bc6\u5ea620mA cm-2<\/sup>\u4e0b\u6781\u8c31\u7535\u6d41\u65f6\u95f4\u66f2\u7ebf\u6d4b\u8bd5100h\u3002<\/p>\n

\u3010\u5c55\u671b\u3011<\/strong><\/p>\n

\u62a5\u9053\u4e5f\u63d0\u4f9b\u4e86\u4e00\u79cd\u53d1\u5c55\u9ad8\u6d3b\u6027\u548c\u6301\u4e45\u6c27\u8fd8\u539f\u53cd\u5e94\u50ac\u5316\u6c27\u8fd8\u539f\u53cd\u5e94\u7684\u50ac\u5316\u5242\u7684\u65b9\u6cd5\uff0c\u5728\u77f3\u58a8\u70ef\u4e2d\u9ad8\u63ba\u6742\u548c\u88f8\u9732\u7684\u53ef\u4ee5\u901a\u8fc7\u70ed\u89e3CuPc\u548c\u53cc\u6c30\u80fa\u5408\u6210\uff0c\u901a\u8fc7\u4e00\u7cfb\u5217\u6d4b\u8bd5\u8bc1\u5b9e\u4e86Cu-N@C\u50ac\u5316\u5242\u4e2d\u5b64\u7acb\u7684Cu(I)-N\u4f4d\u70b9\u7684\u5b58\u5728\uff0c\u76f8\u6bd4\u4e8e\u5176\u4ed6\u5316\u5408\u4ef7\u7684Cu\uff0c\u8be5\u50ac\u5316\u5242\u663e\u793a\u4e86\u9ad8\u7684\u6c27\u8fd8\u539f\u53cd\u5e94\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Highly doped and exposed Cu(I)\u2013N active sites\u00a0within graphene towards efficient oxygen\u00a0reduction for zinc\u2013air batteries<\/a>. (Energy Environ. Sci\uff0c2016\uff0cDOI:\u00a010.1039\/C6EE01867J)<\/span><\/p>\n

\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb<\/strong><\/p>\n

\u5305\u4fe1\u548c\uff0c\u7406\u5b66\u535a\u58eb\uff0c\u7814\u7a76\u5458\uff0c\u535a\u58eb\u751f\u5bfc\u5e08\u3001\u4e2d\u79d1\u9662\u9662\u58eb\u3001\u7269\u7406\u5316\u5b66\u5bb6\uff0c\u4e2d\u56fd\u79d1\u5b66\u9662\u5927\u8fde\u5316\u5b66\u7269\u7406\u7814\u7a76\u6240\u7814\u7a76\u5458\uff0c1995\u5e74\u5e94\u8058\u56de\u56fd\u5148\u540e\u4efb\u4e2d\u79d1\u9662\u5927\u8fde\u5316\u5b66\u7269\u7406\u7814\u7a76\u6240\u50ac\u5316\u57fa\u7840\u56fd\u5bb6\u91cd\u70b9\u5b9e\u9a8c\u5ba4\u7814\u7a76\u5458\u3001\u535a\u58eb\u751f\u5bfc\u5e08\u3001\u6240\u957f\u52a9\u7406\u3001\u526f\u6240\u957f\uff0c2000\u5e748\u6708\u62c5\u4efb\u5927\u8fde\u5316\u7269\u6240\u6240\u957f\u3002<\/p>\n

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\u53c2\u8003\u6587\u732e\uff1a<\/strong><\/p>\n

1. G. Li, X. L.Wang and Z. W. Chen .\u00a0Pomegranate-Inspired Design of Highly Active and Durable Bifunctional Electrocatalysts for Rechargeable Metal\u2013Air Batteries<\/a>\u00a0.\u00a0Angew. Chem., Int. Ed., 2016, 55, 4977\u20134982.
\n2 .J. S. Lee, S. T. Kim\u00a0and J. Cho .\u00a0Metal\u2013Air Batteries with High Energy Density: Li\u2013Air versus Zn\u2013Air<\/a>\u00a0.\u00a0Adv. Energy Mater., 2011, 1, 34\u201350.
\n3. Y. G. Li and H. J. Dai .\u00a0Recent advances in zinc\u2013air batteries<\/a>\u00a0.\u00a0Chem. Soc. Rev., 2014, 43, 5257\u20135275.
\n4. M. Armand and J. M. Tarascon .\u00a0Building better batteries<\/a>\u00a0.\u00a0Nature, 2008, 451, 652\u2013657.<\/p>\n

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