{"id":49002,"date":"2016-10-30T06:30:14","date_gmt":"2016-10-29T22:30:14","guid":{"rendered":"\/\/m.iemloyee.com\/?p=49002"},"modified":"2016-10-27T21:42:15","modified_gmt":"2016-10-27T13:42:15","slug":"angew-chem-int-ed-%e5%8d%8e%e4%b8%ad%e7%a7%91%e6%8a%80%e5%a4%a7%e5%ad%a6%e7%a0%94%e5%8f%91%e5%85%b7%e6%9c%89%e7%bb%93%e6%9e%84%e4%be%9d%e8%b5%96%e9%87%8a%e6%94%be%e8%a1%8c%e4%b8%ba%e7%9a%84","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=49002","title":{"rendered":"Angew. Chem. Int. Ed. \u534e\u4e2d\u79d1\u6280\u5927\u5b66\u7814\u53d1\u5177\u6709\u7ed3\u6784\u4f9d\u8d56\u91ca\u653e\u884c\u4e3a\u7684\u5d4c\u6bb5\u5171\u805a\u7269\u80f6\u56ca"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u805a\u5408\u7269\u80f6\u56ca\u6709\u5f88\u591a\u91cd\u8981\u5e94\u7528\uff0c\u5c24\u5176\u662f\u5728\u6076\u52a3\u7684\u73af\u5883\u4e2d\u4fdd\u62a4\u5b83\u6240\u5305\u88f9\u7684\u836f\u7269\u5e76\u5728\u9047\u5230\u5916\u89e6\u53d1\u5668\u65f6\u5c06\u5b83\u4eec\u91ca\u653e\u3002\u5236\u5907\u805a\u5408\u7269\u80f6\u56ca\u7684\u65b9\u6cd5\u6709\u5f88\u591a\uff0c\u5982\u4e73\u6ef4\u76f8\u5206\u79bb\u3001\u727a\u7272\u6a21\u677f\u6cd5\u3001\u5c42\u5c42\u81ea\u7ec4\u88c5\u3001\u5d4c\u6bb5\u5171\u805a\u7269\uff08BCPs\uff09\u5728\u9009\u62e9\u6eb6\u5242\u4e2d\u81ea\u7ec4\u88c5\u7b49\u7b49\u3002\u5bf9\u4e8eBCPs\u80f6\u56ca\u6765\u8bf4\uff0c\u5b83\u7684\u5f62\u6210\u8fc7\u7a0b\u8f83\u4e3a\u590d\u6742\uff0c\u9274\u4e8e\u5d4c\u6bb5\u95f4\u7684\u5fae\u76f8\u5206\u79bb\u4e0e\u957f\u94fe\u70f7\u70c3\u548c\u5d4c\u6bb5\u95f4\u7684\u5b8f\u89c2\u5206\u79bb\u540c\u65f6\u5b58\u5728\u3002\u76ee\u524d\uff0c\u60f3\u8981\u5236\u5907\u5177\u6709\u53ef\u8c03\u63a7\u58f3\u7ed3\u6784\u7684BCP\u80f6\u56ca\u4ecd\u662f\u4e00\u9879\u6311\u6218\u3002\u800c\u4e14\uff0c\u76f8\u5e94\u7684\u7ed3\u6784\u4f9d\u8d56\u91ca\u653e\u884c\u4e3a\u4e5f\u6ca1\u6709\u5f97\u5230\u5f88\u597d\u7684\u7814\u7a76\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u6700\u8fd1\uff0c\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u5316\u5b66\u4e0e\u5316\u5de5\u5b66\u9662\u6731\u9526\u6d9b\u6559\u6388\u4e0e\u540c\u6d4e\u533b\u5b66\u9662\u9676\u5a1f\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u8bfe\u9898\u7ec4<\/strong>\u901a\u8fc7\u8c03\u63a7\u805a\u5408\u7269-\u6eb6\u5242\u76f8\u4e92\u4f5c\u7528\u6765\u63a7\u5236\u76f8\u5206\u79bb\u987a\u5e8f\uff0c\u4ece\u800c\u5236\u5907\u4e86\u5177\u6709\u53ef\u8c03\u63a7\u58f3\u7ed3\u6784\u7684BCP\u80f6\u56ca\uff0c\u5e76\u4e14\u5bf9\u5176\u7ed3\u6784\u4f9d\u8d56\u91ca\u653e\u884c\u4e3a\u8fdb\u884c\u4e86\u9610\u8ff0\u3002\u8be5\u7814\u7a76\u56e2\u961f\u901a\u8fc7\u84b8\u53d1\u4e73\u6db2\u6eb6\u5242\u5236\u5907\u4e86\u4ee5\u5341\u516d\u70f7\uff08HD\uff09\u6216\u8005\u5341\u516b\u6c1f\u8f9b\u70f7\uff08PFO\uff09\u4e3a\u6db2\u6838\u7684\u805a\u82ef\u4e59\u70ef-\u805a(4-\u4e59\u70ef\u5421\u5576)\u5d4c\u6bb5\u5171\u805a\u7269\uff08PS-b-P4VP\uff09\u80f6\u56ca\u3002\u6db2\u6838\u7684\u6027\u8d28\u51b3\u5b9a\u4e86\u80f6\u56ca\u7684\u5f62\u6210\u673a\u5236\u4ee5\u53ca\u6700\u7ec8\u7684\u58f3\u7ed3\u6784\u3002\u5728\u7cbe\u786e\u63a7\u5236\u7ed3\u6784\u7684\u57fa\u7840\u4e0a\uff0c\u6210\u529f\u5236\u5907\u4e86\u7403\u5f62\u3001\u5706\u67f1\u5f62\u3001\u5c42\u72b6\u4e2d\u5b54\u7684\u80f6\u56ca\uff0c\u5e76\u63a2\u7a76\u4e86\u5b54\u7ed3\u6784\u4e0e\u91ca\u653e\u884c\u4e3a\u7684\u5173\u7cfb\u3002\u7ed3\u679c\u8868\u660e\u5177\u6709\u7403\u5f62\u5b54\u7684\u80f6\u56ca\u6e17\u900f\u6027\u6700\u597d\uff0c\u91ca\u653e\u901f\u5ea6\u6700\u5feb\uff0c\u800c\u5177\u6709\u5c42\u72b6\u5b54\u7684\u80f6\u56ca\u91ca\u653e\u901f\u5ea6\u6700\u6162\uff0c\u4f46\u5374\u662f\u9010\u6b65\u8fdb\u884c\u7684\u3002\u8be5\u9879\u7814\u7a76\u53ef\u7528\u4e8e\u5236\u5907\u4e0d\u540c\u7ed3\u6784\u80f6\u56ca\u7684\u57fa\u7840\u7814\u7a76\u4ee5\u53ca\u6d3b\u6027\u7269\u8d28\u7684\u53ef\u8bbe\u8ba1\u91ca\u653e\u3002<\/p>\n

\u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u56fe1 \u4ee5HD\u4e3a\u6db2\u6838\u7684BCP\u80f6\u56ca\u7684TEM\u7167\u7247<\/strong><\/p>\n

\"1\"<\/p>\n

a) PS22K-b-P4VP22K<\/p>\n

b) PS110K-b-P4VP107K<\/p>\n

c) PS17K-b-P4VP49K<\/p>\n

d) PS51K-b-P4VP18K<\/p>\n

e) P4VP4.5K-b-PS27K-b-P4VP4.5K<\/p>\n

f) P4VP4.5K-b-PS38K-b-P4VP4.5K<\/p>\n

\u6240\u6709\u6837\u54c1\u7684\u521d\u59cbBCP\/HD\u4f53\u79ef\u6bd4\u5747\u4e3a4:6\u3002\u5728\u505aTEM\u4e4b\u524d\u5148\u7528\u7898\u84b8\u6c14\u5bf9P4VP\u663e\u8272\u3002\u56fea\uff0cc\uff0ce\u901a\u8fc7\u52a8\u753b\u5bf9\u58f3\u7ed3\u6784\u8fdb\u884c\u4e86\u6a21\u62df\uff0c\u5176\u4e2d\u84dd\u8272\u548c\u9ec4\u8272\u90e8\u5206\u5206\u522b\u8868\u793aP4VP\u548cPS\u3002<\/p>\n

BCP\u7684\u5206\u5b50\u91cf\uff0819800-217000Da\uff09\u3001\u5d4c\u6bb5\u6bd4\u4f8b\uff08\u5bf9\u79f0\u6216\u4e0d\u5bf9\u79f0\uff09\u3001\u94fe\u7ed3\u6784\uff08AB\u4e24\u5d4c\u6bb5\u6216ABA\u4e09\u5d4c\u6bb5\uff09\u5bf9\u58f3\u7ed3\u6784\u5747\u65e0\u592a\u5927\u5f71\u54cd\u3002\u4f46\u662f\uff0c\u4ec5\u4ec5\u89c2\u5bdf\u5230\u4e86\u7403\u5f62\u7684P4VP\u3002<\/p>\n

\u56fe2 \u4ee5PFO\u4e3a\u6db2\u6838\u7684BCP\u80f6\u56ca\u7684TEM\u7167\u7247<\/strong><\/p>\n

\"2\"<\/p>\n

a) PS9.8K-b-P4VP10K<\/p>\n

b) PS51K-b-P4VP18K<\/p>\n

c) P4VP4.5K-b-PS38K-b-P4VP4.5K<\/p>\n

d) P4VP4.5K-b-PS27K-b-P4VP4.5K<\/p>\n

\u4ee5PFO\u4f5c\u4e3a\u6db2\u6838\u65f6\uff0c\u89c2\u5bdf\u5230\u5bf9\u79f0\u7684PS9.8K-b-P4VP10K\u80f6\u56ca\u5177\u6709\u5c42\u72b6\u58f3\u7ed3\u6784\uff0c\u800c\u4e0d\u662f\u7403\u5f62\u58f3\u7ed3\u6784\u3002\u5e76\u4e14\u901a\u8fc7\u6539\u53d8\u5d4c\u6bb5\u6bd4\u4f8b\u53ef\u4ee5\u5f88\u5bb9\u6613\u5730\u6539\u53d8BCP\u80f6\u56ca\u7684\u58f3\u7ed3\u6784\u3002\u542b\u6709\u8f83\u5c11P4VP\u5d4c\u6bb5\uff0824.3vol%\uff09\u7684\u975e\u5bf9\u79f0PS51K-b-P4VP18K\u80f6\u56ca\u5177\u6709\u7403\u5f62P4VP\u3002\u53e6\u5916\uff0c\u8fd9\u9879\u6280\u672f\u4e5f\u53ef\u4ee5\u7528\u4e8e\u5236\u5907ABA\u4e09\u5d4c\u6bb5\u5171\u805a\u7269\u80f6\u56ca\uff08\u56fe2c\u3001d\uff09\u3002<\/p>\n

\u56fe3 \u542b\u6709PS-b-P4VP\u548c3-\u5341\u4e94\u70f7\u57fa\u82ef\u915a\uff08PDP\uff09\u7684\u8d85\u5206\u5b50\u7684TEM\u7167\u7247<\/strong><\/p>\n

\"3\"<\/p>\n

a-c) P4VP4.5K-b-PS38K-b-P4VP4.5K(PDP)x\u80f6\u56ca\u7684TEM\u56fe\uff0c\u5176\u4e2dx\u5206\u522b\u4e3aa)0.25\uff0cb)0.50\uff0cc)1.0.<\/p>\n

d-f) \u4ecb\u5b54P4VP4.5K-b-PS38K-b-P4VP4.5K(PDP)x\u80f6\u56ca\u7684TEM\u56fe\u53ca\u793a\u610f\u56fe\uff0c\u5176\u4e2dx\u5206\u522b\u4e3ad)0\uff0ce)0.25\uff0cf)1.0. \u84dd\u8272\u3001\u9ec4\u8272\u548c\u7eff\u8272\u90e8\u5206\u5206\u522b\u4ee3\u8868P4VP\u3001PS\u548c\u4e2d\u5b54\u3002<\/p>\n

\u901a\u8fc74VP\u5355\u5143\u548cPDP\u4e4b\u95f4\u7684\u6c22\u952e\u8fde\u63a5\uff0c\u5f97\u5230\u542b\u6709PS-b-P4VP\u548cPDP\u7684\u8d85\u5206\u5b50\uff0c\u8fd9\u662f\u53e6\u4e00\u79cd\u8c03\u63a7\u58f3\u7ed3\u6784\u7684\u65b9\u6cd5\u3002\u4f46\u662f\uff0c\u4ee5HD\u505a\u6db2\u6838\u65f6\uff0c\u5e76\u4e0d\u80fd\u5f97\u5230PS-b-P4VP(PDP)x\uff08\u5176\u4e2dx\u4e3aPDP\u4e0e4VP\u7684\u6469\u5c14\u6bd4\uff09\u80f6\u56ca\uff0c\u539f\u56e0\u662fHD\u548cPDP\u4e4b\u95f4\u7684\u4f5c\u7528\u8f83\u5f3a\u3002\u800c\u4ee5PFO\u4e3a\u6db2\u6838\u65f6\u5219\u53ef\u4ee5\u5f97\u5230\u76f8\u5e94\u7684\u80f6\u56ca\uff0c\u56e0\u4e3aPFO\u4e0eP4VP(PDP)\u4e0d\u80fd\u76f8\u4e92\u6df7\u5408\u3002\u4ee5P4VP4.5K-b-PS38K-b-P4VP4.5K(PDP)x\u80f6\u56ca\u4e3a\u4f8b\uff0c\u5b83\u7684\u58f3\u7ed3\u6784\u968f\u7740PDP\u542b\u91cf\u7684\u589e\u52a0\u800c\u6539\u53d8\uff0cx=0\u65f6\uff0c\u4e3a\u7403\u5f62\uff08\u56fe2c\uff09\uff1bx=0.25\u65f6\uff0c\u4e3a\u5706\u67f1\u5f62\uff1bx=0.5\u65f6\uff0c\u4e3a\u7f51\u72b6\uff1bx=1.0\u65f6\uff0c\u4e3a\u5c42\u72b6\uff08\u56fe3a-c\uff09\u3002<\/p>\n

\u56fe4 \u4e0d\u540c\u58f3\u7ed3\u6784\u80f6\u56ca\u7684\u91ca\u653e\u884c\u4e3a\u53ca\u5bf9\u9ed1\u8272\u7d20\u7624\u7ec6\u80de\u51cb\u4ea1\u7684\u5f71\u54cd<\/strong><\/p>\n

\"4\"<\/p>\n

a) \u5de6\u56fe\uff1a\u4e0d\u540c\u58f3\u7ed3\u6784\u80f6\u56ca\u5728\u4e0d\u540cpH\u4e0b\u5bf9\u7f57\u4e39\u660e6G\uff08R6G\uff09\u7684\u91ca\u653e\u884c\u4e3a\uff1b\u53f3\u56fe\uff1a\u5c42\u72b6\u80f6\u56ca\u5728pH\u4e3a4.0\u65f6\u5bf9R6G\u7684\u9010\u6b65\u91ca\u653e\u56fe\uff0c\u5176\u4e2d\u7bad\u5934\u8868\u793a\u91ca\u653e\u8fc7\u7a0b\u76843\u4e2a\u9636\u6bb5\u3002pH=4.0\u65f6\uff0c\u91ca\u653e\u901f\u7387\u4e3aRS>RC>RL\u3002\u9274\u4e8e\u58f3\u539a\u5ea6\u4e00\u81f4\uff0c\u91ca\u653e\u901f\u7387\u7684\u4e0d\u540c\u53ef\u80fd\u4e0e\u4eb2\u6c34\u6027\u90e8\u5206\u7684\u5f62\u72b6\u548c\u5206\u5e03\u6709\u5173\u3002\u53e6\u5916\uff0c\u5c42\u72b6\u7ed3\u6784\u7684\u80f6\u56ca\u8868\u73b0\u51fa\u9010\u6b65\u91ca\u653e\u884c\u4e3a\uff0c\u8fd9\u662f\u56e0\u4e3a\u58f3\u58c1\u4e0a\u7684\u540c\u5fc3PS\u5c42\u8d77\u5230\u4e86\u9010\u6b65\u91ca\u653e\u836f\u7269\u7684\u4f5c\u7528\u3002<\/p>\n

b) \u8f7d\u6709\u963f\u9709\u7d20\uff08DOX\uff09\u7684\u7403\u5f62\u80f6\u56ca\u7528\u4e8e\u6cbb\u7597A375\u9ed1\u8272\u7d20\u7624\u7ec6\u80de\u7684\u5171\u805a\u7126\u6fc0\u5149\u626b\u63cf\u663e\u5fae\u955c\u7167\u7247\uff08CLSM\uff09\u3002\u6700\u540e\u4e00\u5f20\u56fe\u7247\u4e2d\u7684\u6bd4\u4f8b\u5c3a\u540c\u6837\u9002\u7528\u4e8e\u5176\u4ed6\u56fe\u7247\u3002\u5728A375\u9ed1\u8272\u7d20\u7624\u7ec6\u80de\u5185\u7814\u7a76\u4e86\u8f7dDOX\u80f6\u56ca\u7684\u7ec6\u80de\u6444\u53d6\u884c\u4e3a\u548c\u5728\u7ec6\u80de\u5185\u7684\u5206\u5e03\u60c5\u51b5\uff0c\u57f9\u517b4\u5c0f\u65f6\u540e\uff0cA375\u7ec6\u80de\u5185\u7684DOX\u8367\u5149\u5f3a\u5ea6\u663e\u8457\u589e\u5927\uff0c\u8868\u660e\u8be5\u80f6\u56ca\u80fd\u591f\u6709\u6548\u5730\u5b9e\u73b0\u7ec6\u80de\u6444\u53d6\u3002<\/p>\n

c) \u4e0d\u540c\u58f3\u7ed3\u6784\u7684\u8f7dDOX\u80f6\u56ca\u7ecf\u8fc712\u5c0f\u65f6\u621624\u5c0f\u65f6\u5bfc\u81f4A375\u7ec6\u80de\u51cb\u4ea1\u7684\u767e\u5206\u6bd4\u3002\u57f9\u517b12h\u540e\uff0c\u7531\u7403\u5f62\uff08S\uff09-DOX\u3001\u5706\u67f1\u5f62\uff08C\uff09-DOX\u548c\u5c42\u72b6\uff08L\uff09-DOX\u8bf1\u5bfc\u7684A375\u7ec6\u80de\u51cb\u4ea1\u7684\u767e\u5206\u6bd4\u5206\u522b\u4e3a21.7%\u300117.8%\u548c16.6%\u3002\u57f9\u517b24h\u5177\u6709\u76f8\u540c\u7684\u8d8b\u52bf\uff0c\u51cb\u4ea1\u6bd4\u5206\u522b\u4e3a38.2%\u300132.8%\u548c22.1%\u3002<\/p>\n

d) \u8f7dDOX\u80f6\u56ca\u5bf9A375\u7ec6\u80de\u7684\u7ec6\u80de\u6bd2\u6027\u3002\u4e0d\u8f7d\u836f\u7684\u7403\u5f62\u80f6\u56ca\u548cPBS\u4e3a\u5bf9\u7167\u7ec4\u3002\u57f9\u517b24h\u540e\uff0cS-DOX\u3001C-DOX\u548cL-DOX\u5bf9\u5e94\u7684\u7ec6\u80de\u6d3b\u6027\u5206\u522b\u4e3a49.7\u00b11.2%\uff0c61.3\u00b16.3%\u548c72.3\u00b13.8%\u3002\u764c\u7ec6\u80de\u5185\u7684pH\u503c\u968f\u7740\u80de\u541e\u9014\u5f84\u9010\u6e10\u964d\u4f4e\uff0c\u7531\u6838\u5185\u4f53\u4e2d\u7684\u5927\u7ea66.0-6.5\u964d\u5230\u6eb6\u9176\u4f53\u4e2d\u76844.5-5.0\u3002\u5728\u9178\u6027\u73af\u5883\u4e2d\uff0cP4VP\u4f1a\u53d1\u751f\u6eb6\u80c0\u800c\u4f7f\u5404\u79cd\u5f62\u72b6\u7684\u4e2d\u5b54\u589e\u52a0\uff0c\u5bfc\u81f4DOX\u7684\u91ca\u653e\u901f\u7387\u548c\u764c\u7ec6\u80de\u7684\u51cb\u4ea1\u6bd4\u4f8b\u6709\u6240\u4e0d\u540c\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Block Copolymer Capsules with Structure-Dependent Release Behavior<\/a>\u00a0\uff08Angew. Chem. Int. Ed.\uff0c2016\uff0cDOI: 10.1002\/anie.201607982\uff09<\/p>\n

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