{"id":30406,"date":"2016-08-02T17:00:23","date_gmt":"2016-08-02T09:00:23","guid":{"rendered":"\/\/m.iemloyee.com\/?p=30406"},"modified":"2016-08-17T20:50:44","modified_gmt":"2016-08-17T12:50:44","slug":"angew-chem-int-ed-%e9%98%b3%e7%a6%bb%e5%ad%90%e6%8f%92%e5%b1%82%e6%b0%a7%e5%8c%96%e9%94%b0%e7%ba%b3%e7%b1%b3%e7%89%87%e5%af%b9%e9%94%82%e9%92%a0%e5%82%a8%e8%83%bd%e7%94%b5%e6%b1%a0%e7%9a%84","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=30406","title":{"rendered":"Angew. Chem. Int. Ed. \u9633\u79bb\u5b50\u63d2\u5c42\u6c27\u5316\u9530\u7eb3\u7c73\u7247\u5bf9\u9502\/\u94a0\u50a8\u80fd\u7535\u6c60\u7684\u5f71\u54cd"},"content":{"rendered":"

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u4e8c\u7ef4\uff082D\uff09\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u7247\uff08\u5982MnO2\uff0cCo3O4\uff0cTiO2\uff0cWO3\u7b49\uff09\u5177\u6709\u5f88\u5927\u7684\u6bd4\u8868\u9762\u79ef\uff0c\u8868\u73b0\u51fa\u72ec\u7279\u7684\u7269\u7406\u5316\u5b66\u6027\u8d28\uff0c\u5728\u6676\u4f53\u7ba1\u3001\u50a8\u80fd\u88c5\u7f6e\u548c\u7535\u50ac\u5316\u7b49\u65b9\u9762\u5e94\u7528\u5e7f\u6cdb\uff0c\u5438\u5f15\u4e86\u5168\u4e16\u754c\u79d1\u7814\u8005\u7684\u5174\u8da3\u3002\u5728\u50a8\u80fd\u5e94\u7528\u65b9\u9762\uff0c\u5c42\u72b6\u8fc7\u6e21\u91d1\u5c5e\u6c27\u5316\u7269\uff08MO2\uff1bM=Ti\uff0cV\uff0cCr\uff0cMn\uff09\u88ab\u5e7f\u6cdb\u7528\u4f5c\u9502\/\u94a0\u7535\u6c60\u7684\u7535\u6781\u6750\u6599\u3002\u4f46\u5728\u7535\u6c60\u7684\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\uff0c\u968f\u7740\u78b1\u91d1\u5c5e\u79bb\u5b50\u9502\/\u94a0\u7684\u8131\u51fa\uff0c\u5176\u7ed3\u6784\u6613\u574d\u584c\uff0c\u81f4\u4f7f\u5bb9\u91cf\u8870\u51cf\u3002\u91d1\u5c5e\u5143\u7d20\u63ba\u6742\/\u66ff\u6362\u53ef\u4ee5\u63d0\u9ad8\u5176\u7ed3\u6784\u7a33\u5b9a\u6027\uff0c\u4f46\u5f88\u96be\u6784\u5efa\u4e00\u4e2a\u53ef\u8c03\u8282\u7684Li+\/ Na+\u901a\u9053\u3002\u5206\u5b50\u7ea7\u539a\u5ea6\u7684\u4e8c\u7ef4\u6c27\u5316\u9530\u7eb3\u7c73\u7247\u53ef\u901a\u8fc7\u754c\u9762\u5de5\u7a0b\u548c\u7ec4\u88c5\u6210\u4e09\u7ef4\u591a\u5b54\u9aa8\u67b6\u6765\u8c03\u6574\u5fae\u89c2\u7ed3\u6784\uff0c\u8fdb\u800c\u63d0\u9ad8\u50a8\u80fd\u5bb9\u91cf\u3002\u4f46\u662f\uff0c\u73b0\u4eca\u6240\u62a5\u9053\u7684\u65b9\u6cd5\u53d7\u9650\u4e8e\u591a\u6b65\u5265\u79bb\u548c\u91cd\u7ec4\u8fc7\u7a0b\u3002<\/p>\n

\u8fd1\u65e5\uff0c\u5c71\u4e1c\u5927\u5b66\u5316\u5b66\u4e0e\u5316\u5de5\u5b66\u9662\u7684\u5f20\u8fdb\u6d9b\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u548c\u9a6c\u539a\u4e49\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba\u91c7\u7528\u4e86\u4e00\u79cd\u81ea\u4e0b\u800c\u4e0a\u7684\u7b56\u7565\uff0c\u5c06\u4e8c\u7ef4\u6c27\u5316\u9530\u7eb3\u7c73\u7247\u548c\u591a\u79cd\u91d1\u5c5e\u9633\u79bb\u5b50\u8fdb\u884c\u81ea\u7ec4\u88c5\uff0c\u5408\u6210\u4e86\u5c42\u95f4\u8ddd\u79bb\u53ef\u8c03\u3001\u5448\u201c\u4e09\u660e\u6cbb\u201d\u72b6\u7ed3\u6784\u3001\u9633\u79bb\u5b50\u63d2\u5c42\u7684\u4e09\u7ef4MxMnO2\uff08M=Li\uff0cNa\uff0cK\uff0cCo\u548cMg\uff09\u9634\u6781\u6750\u6599\u3002\u8fd9\u79cd\u5c42\u72b6MxMnO2\u7535\u6781\u6750\u6599\u5728\u9502\/\u94a0\u50a8\u80fd\u7535\u6c60\u4e2d\u8868\u73b0\u51fa\u4e0d\u540c\u7684\u50a8\u80fd\u5bb9\u91cf\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u7814\u7a76\u7ed3\u679c\u8868\u660e\u6539\u53d8\u91d1\u5c5e\u9633\u79bb\u5b50\u53ef\u4ee5\u6539\u53d8\u6c27\u5316\u9530\u7eb3\u7c73\u7247\u7684\u5c42\u95f4\u8ddd\u3002\u7814\u7a76\u8005\u53d1\u73b0\u91d1\u5c5e\u9633\u79bb\u5b50\u7684\u5927\u5c0f\u4ee5\u53ca\u5176\u4e0eLi+ \u6216 Na+\u7684\u76f8\u4e92\u4f5c\u7528\u5f71\u54cd\u7535\u6781\u6750\u6599\u7684\u5bb9\u91cf\u548c\u7a33\u5b9a\u6027\u3002\u8be5\u5de5\u4f5c\u4e3a\u4eca\u540e\u9502\/\u94a0\u7535\u6c60\u5148\u8fdb\u7535\u6781\u6750\u6599\u7684\u5408\u7406\u8bbe\u8ba1\u63d0\u4f9b\u4e86\u65b0\u65b9\u6cd5\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u6d41\u7a0b\u56fe1 \u4e09\u7ef4\u5c42\u72b6\u6c27\u5316\u9530\u9aa8\u67b6\u7684\u5236\u5907<\/strong><\/p>\n

\"S1-10.1002@anie\"<\/p>\n

\u4e09\u7ef4\u5c42\u72b6\u7ed3\u6784\u662f\u7531\u4e8c\u7ef4\u7eb3\u7c73\u6c27\u5316\u5c42\u91cd\u590d\u5806\u79ef\u800c\u6210\uff0c\u7eb3\u7c73\u7247\u81ea\u4e0b\u800c\u4e0a\u8fdb\u884c\u81ea\u7ec4\u88c5\uff0c\u53d7\u4f53\u91d1\u5c5e\u9633\u79bb\u5b50\u5728\u5c42\u95f4\u8d77\u5230\u5206\u79bb\u7684\u4f5c\u7528\u3002(Mn+= Li+\uff0cNa+\uff0cK+\uff0cMg2+\uff0c\u548cCo2+\uff0c\u4e0b\u540c)<\/p>\n

\u56fe1 \u4e0d\u540c\u91d1\u5c5e\u9633\u79bb\u5b50\u63d2\u5c42MnO2\u7684\u7814\u7a76<\/strong><\/p>\n

\"f1-10.1002@anie\"<\/p>\n

\uff08a\uff09\u6c27\u5316\u9530\u80f6\u4f53\u60ac\u6d6e\u6db2\u548cMxMnO2\u6837\u54c1\u7684\u6570\u7801\u7167\u7247\u3002\u6c27\u5316\u9530\u80f6\u4f53\u5206\u6563\u826f\u597d\uff0c\u56e0\u4e3a\u4e01\u8fbe\u5c14\u6548\u5e94\u800c\u5448\u73b0\u660e\u663e\u7684\u5149\u6563\u5c04\u3002\u6dfb\u52a0\u91d1\u5c5e\u9633\u79bb\u5b50\u540e\uff0c\u4e0e\u8868\u9762\u7535\u8377\u4e2d\u548c\uff0c\u6c27\u5316\u9530\u7eb3\u7c73\u7247\u53d1\u751f\u9759\u7535\u6c89\u6dc0\u3002
\n\uff08b\uff09\u6c27\u5316\u9530\u548cMxMnO2\u7684XRD\u56fe\u8c31\u3002\u7ed3\u679c\u8868\u660e\uff0c\u52a0\u5165\u91d1\u5c5e\u9633\u79bb\u5b50\u7684\u534a\u5f84\u589e\u5927\uff0c\u5c42\u95f4\u8ddd\u4e5f\u968f\u4e4b\u589e\u5927\u3002
\n\uff08c\uff09MxMnO2\u7684\u9ad8\u5206\u8fa8\u7387XPS\u56fe\u8c31\u3002<\/p>\n

\u56fe2 MnO2\u7eb3\u7c73\u7247\u548cNaMO\u7684\u8868\u5f81\u4e0e\u5206\u6790<\/strong><\/p>\n

\"f2-10.1002@anie\"<\/p>\n

\uff08a\uff09MnO2\u7eb3\u7c73\u7247\u7684TEM\u7167\u7247\uff1b\uff08b\uff09MnO2\u7eb3\u7c73\u7247\u7684AFM\u7167\u7247\u3002\u6c27\u5316\u9530\u7eb3\u7c73\u7247\u5728\u4e9a\u5fae\u7c73\u8303\u56f4\u5185\u5177\u6709\u6a2a\u5411\u5c3a\u5bf8\u7684\u9ad8\u4e8c\u7ef4\u5404\u5411\u5f02\u6027\uff0c\u539a\u5ea6\u7ea6\u4e3a0.8nm\u3002
\n\uff08c\uff0cd\uff09NaMO\u7684TEM\u7167\u7247\u3002
\n\uff08e\uff09NaMO\u7684SEM\u7167\u7247\u3002\u81ea\u7ec4\u88c5\u7eb3\u7c73\u5c42\u76f8\u4e92\u8fde\u63a5\uff0c\u5f62\u6210\u4e00\u4e2a\u5f00\u653e\u7684\u3001\u591a\u5b54\u7684\u4e09\u7ef4\u7ed3\u6784\u3002
\n\uff08f\uff09\u5143\u7d20\u6620\u5c04\u56fe\u50cf\u3002Na\u3001Mn\u548cO\u5747\u5300\u5206\u5e03\uff0c\u8868\u660e\u6837\u54c1\u4e2d\u542b\u6709Na\u3001Mn\u548cO\u3002<\/p>\n

\u56fe3 \u63d2\u5c42\u5bf9\u6750\u6599\u7535\u5316\u5b66\u6027\u80fd\u5f71\u54cd\u7684\u7814\u7a76<\/strong><\/p>\n

\"f3-10.1002@anie\"<\/p>\n

\uff08a\uff0cb\uff09MxMnO2\u7684\u6bd4\u5bb9\u91cf\uff1aa)\u94a0\u7535\u6c60 b)\u9502\u7535\u6c60\u3002\u7535\u6d41\u5bc6\u5ea6\u4e3a30 mAg-1\uff0c\u6570\u636e\u662f\u81f3\u5c11\u4e09\u6b21\u72ec\u7acb\u8bd5\u9a8c\u7684\u5e73\u5747\u503c\u3002\u534a\u5f84\u4e0d\u540c\u7684\u91d1\u5c5e\u9633\u79bb\u5b50\u63d2\u5c42\u8868\u73b0\u51fa\u4e0d\u540c\u7684\u5bb9\u91cf\u3002
\n\uff08c\uff09\u4e0d\u540c\u7535\u538b\u4e0b\u7684v1\/2\u548ci\/ v1\/2\u7684\u66f2\u7ebf\u3002v(mVs-1)\u548ci(mA)\u5206\u522b\u4e3a\u4e0d\u540c\u7535\u538b\u4e0b\u7684\u626b\u63cf\u901f\u5ea6\u548c\u7535\u6d41\u3002
\n\uff08d\uff09\u4e0d\u540c\u6761\u4ef6\u4e0b\uff0c\u63d2\u5c42\u5bb9\u91cf\u8d21\u732e\u7387\uff0c\u8303\u56f4\u4e3a59%-82%\u3002\u8fd9\u8bf4\u660e\u5728\u80fd\u91cf\u50a8\u5b58\u8fc7\u7a0b\u4e2d\uff0c\u9633\u79bb\u5b50\u63d2\u5c42\u8d77\u4e3b\u5bfc\u4f5c\u7528\u3002
\n\uff08e\uff09\u5145\u653e\u7535\u66f2\u7ebf\u3002
\n\uff08f\uff0cg\uff09\u7b2c\u4e00\u6b21\u5faa\u73af\u65f6\u4e0d\u540c\u5145\u653e\u7535\u72b6\u6001\u4e0b\u7684EDX\u5149\u8c31\u548cKMO\u4e2dNa\u5143\u7d20\u6620\u5c04\u56fe\u8c31\u3002\u653e\u7535\u8fc7\u7a0b\u4e2d\uff0cNa+\u7684\u6d53\u5ea6\u9010\u6e10\u589e\u52a0\u5230\u6700\u5927\u503c\uff0c\u5145\u7535\u8fc7\u7a0b\u4e0e\u4e4b\u76f8\u53cd\u3002<\/p>\n

\u56fe4 \u500d\u7387\u6027\u80fd\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u7684\u7814\u7a76<\/strong><\/p>\n

\"f4-10.1002@anie\"<\/p>\n

\uff08a\uff0cb\uff09MxMnO2\u7535\u6c60\u7684\u500d\u7387\u6027\u80fd\uff1a\uff08a\uff09\u94a0\u7535\u6c60\uff0c\uff08b\uff09\u9502\u7535\u6c60\u3002\u5728\u4e0d\u540c\u7684\u500d\u7387\u4e0b\uff0cKMO\u548cNaMO\u5747\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u5bb9\u91cf\u4fdd\u5b58\u7387\u3002
\n\uff08c\uff0cd\uff09MxMnO2\u7535\u6c60\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff1a\uff08a\uff09\u94a0\u7535\u6c60\uff0c\uff08b\uff09\u9502\u7535\u6c60\uff0c\u7535\u6d41\u5bc6\u5ea6\u4e3a80mAg-1\u3002\u81ea\u7ec4\u88c5\u5408\u6210\u7684MxMnO2\u7535\u6781\u6750\u6599\u8868\u73b0\u51fa\u8f83\u4e3a\u957f\u4e45\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff0c\u7535\u6c60\u5bb9\u91cf\u7531\u9633\u79bb\u5b50\u51b3\u5b9a\u3002<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/p>\n

\u7814\u7a76\u8005\u901a\u8fc7\u4e8c\u7ef4\u6c27\u5316\u9530\u7eb3\u7c73\u7247\u7684\u81ea\u7ec4\u88c5\u8fc7\u7a0b\u5408\u6210\u4e86\u591a\u5b54\u7684\u4e09\u7ef4\u6c27\u5316\u9530\u7ed3\u6784\u3002\u4e0d\u540c\u91d1\u5c5e\u9633\u79bb\u5b50\u7684\u63d2\u5c42\u53ef\u4ee5\u6539\u53d8\u5c42\u95f4\u8ddd\uff0c\u8fdb\u800c\u6539\u53d8\u7535\u5316\u5b66\u6027\u80fd\u3002\u4e00\u4ef7\u9633\u79bb\u5b50\u548c\u4e8c\u4ef7\u9633\u79bb\u5b50\u63d2\u5c42\u8868\u73b0\u51fa\u7684\u5bb9\u91cf\u4e0d\u540c\uff1a\u5bf9\u4e8e\u4e00\u4ef7\u9633\u79bb\u5b50\u6765\u8bf4\uff0c\u5c42\u95f4\u8ddd\u589e\u5927\u53ef\u4ee5\u63d0\u9ad8\u7535\u6c60\u5bb9\u91cf\uff0c\u4e8c\u4ef7\u9633\u79bb\u5b50\uff08\u5982Co2+\uff09\u867d\u53ef\u4ee5\u589e\u5927\u5c42\u95f4\u8ddd\uff0c\u4f46\u662f\u4e0d\u80fd\u63d0\u9ad8\u5bb9\u91cf\u3002\u7814\u7a76\u7ed3\u679c\u8bf4\u660e\u5c42\u95f4\u8ddd\u548c\u9633\u79bb\u5b50\u95f4\u7684\u6f5c\u5728\u5e93\u4f26\u6392\u65a5\u529b\u5f71\u54cd\u7740\u4e8c\u7ef4\u6c27\u5316\u9530\u7684\u5bb9\u91cf\u548c\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u8be5\u7814\u7a76\u4e3a\u5229\u7528\u5df2\u77e5\u7684\u4e8c\u7ef4\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u7247\u5408\u7406\u8bbe\u8ba1\u5148\u8fdb\u9502\/\u94a0\u7535\u6c60\u7684\u7535\u6781\u6750\u6599\u63d0\u4f9b\u4e86\u65b0\u57fa\u7840\u3002<\/p>\n

\u5f20\u8fdb\u6d9b\u6559\u6388\u7b80\u4ecb\uff1a<\/strong><\/p>\n

2012\u5e74\u5728\u65b0\u52a0\u5761\u56fd\u7acb\u5927\u5b66\u83b7\u535a\u58eb\u5b66\u4f4d\uff1b2012\u81f32015\u5e74\u5728\u5357\u6d0b\u7406\u5de5\u5927\u5b66\uff08\u65b0\u52a0\u5761\uff09\u548c\u51ef\u65af\u897f\u50a8\u5927\u5b66\uff08\u7f8e\u56fd\uff09\u8fdb\u884c\u535a\u58eb\u540e\u7814\u7a76\uff1b2015\u5e748\u6708\u88ab\u8058\u4e3a\u5c71\u4e1c\u5927\u5b66\u5316\u5b66\u4e0e\u5316\u5de5\u5b66\u9662\u6559\u6388\u3001\u535a\u58eb\u751f\u5bfc\u5e08\u3002\u81f4\u529b\u4e8e\u5f00\u53d1\u9ad8\u6027\u80fd\u7684\u65b0\u578b\u7535\u6781\u6750\u6599\u7528\u4e8e\u6784\u5efa\u6027\u80fd\u4f18\u5f02\u7684\u7535\u5316\u5b66\u80fd\u6e90\u5b58\u50a8\u4e0e\u8f6c\u5316\u5668\u4ef6\u3002\u81f3\u4eca\u5df2\u5728Nature Nanotechnology\u3001Angew. Chem. Int. Ed.\u3001Science Advances\u3001Energy & Environmental Science\u3001Journal Materials Chemistry\u7b49\u56fd\u9645\u671f\u520a\u53d1\u8868SCI\u8bba\u658720\u4f59\u7bc7\uff0c\u88ab\u5f15\u75282300\u4f59\u6b21 \uff08H-index \u4e3a21\uff09\u3002\uff08\u901a\u8baf\u4f5c\u8005\u4fe1\u606f\u6765\u6e90\u4e8e\u5c71\u4e1c\u5927\u5b66\u5316\u5b66\u4e0e\u5316\u5de5\u5b66\u9662\u7f51\u7ad9<\/a>\uff09<\/p>\n

\u9a6c\u539a\u4e49\u6559\u6388\u7b80\u4ecb\uff1a<\/strong><\/p>\n

1998\u5e74\u5728\u5c71\u4e1c\u5927\u5b66\u83b7\u535a\u58eb\u5b66\u4f4d\uff1b2000\u5e74\u81f32001\u5e74\u5728\u52a0\u62ff\u5927\u963f\u5c14\u4f2f\u5854\u5927\u5b66\u5316\u5de5\u4e0e\u6750\u6599\u5de5\u7a0b\u7cfb\u4ece\u4e8b\u535a\u58eb\u540e\u5de5\u4f5c\u3002\u73b0\u4efb\u5c71\u4e1c\u5927\u5b66\u5316\u5b66\u4e0e\u5316\u5de5\u5b66\u9662\u6559\u6388\uff0c\u535a\u58eb\u751f\u5bfc\u5e08\u3002\u5df2\u4ece\u4e8b\u7535\u5316\u5b66\u9886\u57df\u7684\u7814\u7a76\u5de5\u4f5c\u5c06\u8fd1\u4e8c\u5341\u5e74\uff0c\u8bfe\u9898\u7ec4\u5728\u91d1\u5c5e\u7eb3\u7c73\u7c92\u5b50\u7684\u7535\u5316\u5b66\u5408\u6210\u3001\u7eb3\u7c73\u7ed3\u6784\u7535\u6781\u7684\u8bbe\u8ba1\u5236\u4f5c\u53ca\u5176\u7535\u50ac\u5316\u6027\u80fd\u8868\u5f81\u3001\u7535\u5316\u5b66\u963b\u6297\u8c31\u7406\u8bba\u4e0e\u5e94\u7528\u3001\u81ea\u7ec4\u88c5\u7f13\u8680\u529f\u80fd\u5206\u5b50\u819c\u6280\u672f\u3001\u73af\u5883\u53cb\u597d\u578b\u8010\u8150\u8680\u6d82\u5c42\u7684\u7814\u53d1\u7b49\u65b9\u9762\u4e3a\u56fd\u5185\u5916\u540c\u884c\u6240\u5173\u6ce8\uff0c\u622a\u6b62\u52302014\u5e7411\u6708\u5e95\uff0c\u5df2\u7ecf\u53d1\u8868SCI\u8bba\u6587115\u7bc7\uff0c\u88ab\u5f153100\u4f59\u6b21\u3002\uff08\u901a\u8baf\u4f5c\u8005\u4fe1\u606f\u6765\u6e90\u4e8e\u5c71\u4e1c\u5927\u5b66\u5316\u5b66\u4e0e\u5316\u5de5\u5b66\u9662\u7f51\u7ad9<\/a>\uff09<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Cation Intercalation in Manganese Oxide Nanosheets: Effects on Lithium and Sodium Storage<\/a>\u00a0(Angew. Chem. Int. Ed., 2016, DOI: 10.1002\/anie.201605102\uff09<\/p>\n

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