{"id":27623,"date":"2016-07-20T08:00:04","date_gmt":"2016-07-20T00:00:04","guid":{"rendered":"\/\/m.iemloyee.com\/?p=27623"},"modified":"2016-07-19T21:15:00","modified_gmt":"2016-07-19T13:15:00","slug":"jacs%ef%bc%9a%e6%89%93%e7%a0%b4%e4%bc%a0%e7%bb%9f%e8%a7%82%e5%bf%b5%ef%bc%81%e9%95%81%e7%a6%bb%e5%ad%90%e7%94%b5%e6%b1%a0%e4%b8%admgpf62%e5%9f%ba%e7%94%b5%e8%a7%a3%e8%b4%a8%e4%bd%93%e7%b3%bb","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=27623","title":{"rendered":"JACS\uff1a\u6253\u7834\u4f20\u7edf\u89c2\u5ff5\uff01\u9541\u79bb\u5b50\u7535\u6c60\u4e2dMg(PF6)2\u57fa\u7535\u89e3\u8d28\u4f53\u7cfb\u4e0e\u7535\u6781\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\u7684\u63a2\u7a76"},"content":{"rendered":"

\u3010\u5f15\u8bed\u3011\u9541\u79bb\u5b50\u7535\u6c60\u76f8\u6bd4\u4e8e\u4f20\u7edf\u7684\u9502\u79bb\u5b50\u7535\u6c60\u66f4\u4e3a\u5b89\u5168\u3001\u6210\u672c\u66f4\u4f4e\u3002\u4e14\u66f4\u4e3a\u91cd\u8981\u7684\u662f\u7531\u4e8e\u4e00\u4e2aMg2+<\/sup>\u53ef\u4ee5\u643a\u5e26\u4e24\u4e2a\u7535\u5b50\u7684\u5173\u7cfb\uff0c\u5176\u8d1f\u6781\u6750\u6599\u7684\u7406\u8bba\u5bb9\u91cf\u53ef\u8fbe\u52303833 mAh\u2219cm-3<\/sup>\uff0c\u8fd9\u4e00\u6570\u503c\u63a5\u8fd1\u9502\u91d1\u5c5e\u7cfb\u7edf\uff082062 mAh\u2219cm-3<\/sup>\uff09\u7684\u4e24\u500d\u3002\u7136\u800c\uff0c\u53d1\u5c55\u5177\u6709\u7ade\u4e89\u529b\u7684\u9541\u79bb\u5b50\u7535\u6c60\u7684\u4e00\u4e2a\u4e3b\u8981\u7684\u9650\u5236\u56e0\u7d20\u662f\uff0c\u7f3a\u4e4f\u65e2\u53ef\u4ee5\u5728\u5bbd\u7535\u538b\u8303\u56f4\u5185\u4fdd\u6301\u7a33\u5b9a\u53c8\u80fd\u591f\u4e0e\u591a\u79cd\u6b63\u3001\u8d1f\u7535\u6781\u76f8\u517c\u5bb9\u7684\u7535\u89e3\u6db2\u3002\u8fd1\u65e5\uff0c\u5251\u6865\u5927\u5b66<\/span><\/strong>\u7684Dominic S. Wright\u6559<\/strong>\u6388<\/span>\u548cClare P. Grey\u6559\u6388<\/strong><\/span>\u7b49\u4eba\u8054\u5408\u5728JACS<\/em><\/strong>\u4e0a\u53d1\u6587\uff0c\u9898\u4e3a\u201cMg(PF6<\/sub>)2<\/sub>-Based Electrolyte Systems: Understanding Electrolyte-Electrode Interactions for the Development of Mg-Ion Batteries<\/em><\/strong>\u201d\u3002\"\u65e0\u6807\u9898a\"<\/p>\n

\u6b64\u6b21\u7814\u7a76\u6210\u679c\u4e3b\u8981<\/strong><\/span>\u662f\uff1a \u8be5\u7814\u7a76\u5c0f\u7ec4\u5408\u6210\u4e86\u590d\u6742\u7684Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u5e76\u63a2\u7a76\u4e86\u8fd9\u79cd\u7535\u89e3\u8d28\u6eb6\u6db2\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002\u7814\u7a76\u53d1\u73b0Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u5728CH3<\/sub>CN \u548cCH3<\/sub>CN\/THF\u7684\u6df7\u5408\u7269\u4e2d\u8868\u73b0\u51fa\u9ad8\u4f20\u5bfc\u7387\uff08\u8fbe\u523028 mS\u00b7cm\u20131\uff09\u53ca\u4f18\u5f02\u7684\u7535\u5316\u5b66\u7a33\u5b9a\u6027\uff08\u5728Al\u7535\u6781\u4e0a\u53ef\u627f\u53d7\u7684\u7a33\u5b9a\u7535\u538b\u81f3\u5c11\u8fbe\u52304V vs Mg\uff09\u3002\u6700\u4e3a\u91cd\u8981\u7684\u662f\u8be5\u7814\u7a76\u6210\u679c\u6253\u7834\u4e86\u5bf9\u4e8eMg\uff08PF6<\/sub>\uff092<\/sub>\u57fa\u7535\u89e3\u8d28\u7684\u4f20\u7edf\u89c2\u5ff5\uff0c\u5177\u6709\u5f00\u521b\u6027\u610f\u4e49\u3002<\/p>\n

\"\u65e0\u6807\u9898b\"<\/p>\n

\u6210\u679c\u7b80\u4ecb\uff1a<\/span><\/strong>\u5728\u9541\u79bb\u5b50\u7535\u6c60\u7684\u7814\u7a76\u4e2dMg\uff08PF6<\/sub>\uff092<\/sub>\u57fa\u7535\u89e3\u8d28\u5e76\u4e0d\u5982\u7c7b\u4f3c\u7684LiPF6<\/sub>\u57fa\u7535\u89e3\u8d28\u5728\u9502\u79bb\u5b50\u7535\u6c60\u4e2d\u53d7\u91cd\u89c6\uff0c\u8fd9\u662f\u7531\u4e8e\u6709\u89c2\u70b9\u8ba4\u4e3aPF6\u2013<\/sup>\u9634\u79bb\u5b50\u5c06\u4f1a\u4f7f\u5f97Mg\u7535\u6781\u5206\u89e3\u548c\u949d\u5316\u3002\u540c\u65f6\u5148\u524d\u5e76\u6ca1\u6709Mg\uff08PF6<\/sub>\uff092<\/sub>\u76d0\u7684\u5408\u6210\u62a5\u9053\uff0c\u66f4\u6ca1\u6709\u76f8\u5173\u7684\u7535\u5316\u5b66\u7814\u7a76\u3002\u8be5\u7814\u7a76\u5c0f\u7ec4\u5408\u6210\u5e76\u7814\u7a76\u4e86Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u6eb6\u6db2\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002\u53d1\u73b0Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u5728CH3<\/sub>CN \u548cCH3<\/sub>CN\/THF\u7684\u6df7\u5408\u7269\u4e2d\u8868\u73b0\u51fa\u9ad8\u4f20\u5bfc\u7387\uff08\u8fbe\u523028 mS\u00b7cm\u20131\uff09\u53ca\u4f18\u5f02\u7684\u7535\u5316\u5b66\u7a33\u5b9a\u6027\uff08\u5728Al\u7535\u6781\u4e0a\u53ef\u627f\u53d7\u7684\u7a33\u5b9a\u7535\u538b\u81f3\u5c11\u8fbe\u52304V vs Mg\uff09\u3002\u4e0e\u4f20\u7edf\u89c2\u5ff5\u76f8\u53cd\u7684\u662f\uff0c\u5728\u5faa\u73af\u8fc7\u7a0b\u4e2dMg\u7535\u6781\u80fd\u5728\u8fd9\u79cdMg(PF6)2\u57fa\u7535\u89e3\u8d28\u4e2d\u4fdd\u6301\u7535\u5316\u5b66\u6d3b\u6027\uff0c\u5e76\u4e14\u4e0d\u4f1a\u6709\u65e0\u6c1f\u5316\u7269\uff08\u4f8b\u5982MgF2<\/sub>\uff09\u5f62\u6210\u5728Mg\u8868\u9762\u3002\u53e6\u4e00\u65b9\u9762\uff0c\u8be5\u5c0f\u7ec4\u4e5f\u7814\u7a76\u53d1\u73b0\u5728\u5faa\u73af\u8fc7\u7a0b\u4e2d\u4e0d\u9508\u94a2\u7535\u6781\u4f1a\u88abMg(PF6)2\u57fa\u7535\u89e3\u8d28\u8150\u8680\uff0c\u800cAl\u7535\u6781\u5219\u4f1a\u88ab\u949d\u5316\u3002\u540c\u65f6\uff0c\u8fd9\u79cd\u7535\u89e3\u6db2\u5df2\u7ecf\u88ab\u7528\u4e8eMo3<\/sub>S4<\/sub>\u4e3a\u6b63\u6781\uff0cMg\u4e3a\u9634\u6781\u7684\u539f\u578b\u9541\u7535\u6c60\u4e2d\u4e86\u3002\u8be5\u6210\u679c\u201c\u98a0\u8986\u201d\u4e86\u4eba\u4eec\u5bf9\u4e8eMg\uff08PF6<\/sub>\uff092<\/sub>\u57fa\u7535\u89e3\u8d28\u7684\u4f20\u7edf\u89c2\u5ff5\uff0c\u662f\u5177\u6709\u5f00\u521b\u6027\u610f\u4e49\u7684\u7814\u7a76\u3002<\/p>\n

\u56fe\u6587\u5bfc\u8bfb\uff1a<\/strong><\/span><\/p>\n

\u56fe1\uff1aMg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u7684X\u5c04\u7ebf\u6676\u4f53\u7ed3\u6784<\/strong><\/p>\n

\"\u65e0\u6807\u9898c\"<\/p>\n

Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u7684X\u5c04\u7ebf\u6676\u4f53\u7ed3\u6784\uff0c\u70ed\u692d\u7403\u4f53\u7684\u7279\u5b9a\u6982\u7387\u4e3a50%\uff0c\u4e14\u63d0\u9ad8\u4e3a\u4e86\u6e05\u6670\u5ea6\u76f8\u5173\u8d28\u5b50\u548c\u969c\u788d\u5df2\u88ab\u6e05\u9664\uff08Mg\uff1a\u7eff\u8272\uff0cP\uff1a\u6a59\u8272\uff0cF\uff1a\u9ec4\u8272\uff0cN\uff1a\u84dd\u8272\uff0cC\uff1a\u7070\u8272\uff09\u3002<\/p>\n

\u56fe2\uff1a\u5faa\u73af\u4f0f\u5b89\u7279\u6027\u66f2\u7ebf<\/strong><\/p>\n

\"\u65e0\u6807\u9898d\"<\/p>\n

\u6240\u6709\u5b9e\u9a8c\u5747\u572825\u00b0C\u8fdb\u884c<\/p>\n

\uff08a\uff09\u7ecf\u6311\u9009\u7684\u4e09\u7535\u6781\u7535\u6c60\u5faa\u73af\u4f0f\u5b89\u7279\u6027\u66f2\u7ebf\u56fe\uff0c\u5176\u4e2d\u7535\u89e3\u6db2\u4e3a0.12 M Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u4e0eTHF-CH3<\/sub>CN \u6bd4\u4f8b\u4e3a1 : 1\uff0c\u5de5\u4f5c\u7535\u6781\u4e3a\u73bb\u7483\u78b3\uff08GC\uff09 \uff0c\u4ee5\u53caMg\u53c2\u6bd4\u7535\u6781\u548c\u5bf9\u7535\u6781\u3002\u5faa\u73af\u901f\u7387\u4e3a25 mV\u2219s-1<\/sup>\u3002<\/p>\n

\uff08b\uff09\u7ebf\u6027\u4f0f\u5b89\u626b\u63cf\u56fe\uff0c\u5176\u4e2d\u7535\u89e3\u6db2\u4e3a0.12 M Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u4e0eTHF-CH3CN \u6bd4\u4f8b\u4e3a1 : 1\uff0c\u626b\u63cf\u901f\u7387\u4e3a25 mV\u2219s-1<\/sup>\uff0c\u5de5\u4f5c\u7535\u6781\u5206\u522b\u4e3a Pt\u3001ss-316\u3001GC\u3001Al\u3002\uff08\u63d2\u56fe\uff1a\u6269\u5c55\u533a\u57df\u663e\u793a\u7535\u6d41\u5bc6\u5ea6\u7531Al\u7535\u6781\u6240\u4ea7\u751f\u7684\uff09\u3002<\/p>\n

\uff08c\uff09\u7ecf\u6311\u9009\u7684Mg|Mg|Mg\u5bf9\u79f0\u4e09\u7535\u6781\u7535\u6c60\u7684\u5faa\u73af\u4f0f\u5b89\u7279\u6027\u66f2\u7ebf\u56fe\uff08\u63d2\u56fe\uff1a\u6269\u5c55\u533a\u57df\u663e\u793a\u4e3aMg \u7535\u9540\uff09\uff0c\u5176\u4e2d\u7535\u89e3\u6db2\u4e3a0.12 M Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u4e0eTHF-CH3CN \u6bd4\u4f8b\u4e3a1 : 1\uff0c\u626b\u63cf\u901f\u7387\u4e3a50 mV\u2219s-1\u3002<\/p>\n

\uff08d\uff09\u7ecf\u6311\u9009\u7684Mg|Mg|Mg\u5bf9\u79f0\u4e09\u7535\u6781\u7535\u6c60\u7684\u5faa\u73af\u4f0f\u5b89\u7279\u6027\u66f2\u7ebf\u56fe\uff0c\u5176\u4e2d\u7535\u89e3\u6db2\u4e3a0.71 M Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u4e0eTHF-CH3CN \u6bd4\u4f8b\u4e3a1 : 1\uff0c\u626b\u63cf\u901f\u7387\u4e3a50 mV\u2219s-1\u3002<\/p>\n

\u8bf4\u660e\uff1a<\/span><\/strong>\u4e09\u7535\u6781\u5305\u62ec\u5de5\u4f5c\u7535\u6781\u3001\u53c2\u6bd4\u7535\u6781\u548c\u5bf9\u7535\u6781\u3002\u53c2\u6bd4\u7535\u6781\u4e3a\u4e00\u4e2a\u7535\u4f4d\u7a33\u5b9a\u7684,\u548c\u5de5\u4f5c\u7535\u6781\u76f8\u8fde,\u80fd\u591f\u8f83\u4e3a\u51c6\u786e\u7684\u6d4b\u5f97\u5de5\u4f5c\u7535\u6781\u7684\u7535\u4f4d\u53ca\u7535\u4f4d\u53d8\u5316\u7684\u7535\u6781\u3002<\/p>\n

\u7535\u5316\u5b66\u6d4b\u91cf\u4e3a\u4f55\u4e00\u822c\u91c7\u7528\u4e09\u7535\u6781\u4f53\u7cfb?<\/span><\/strong><\/p>\n

\u7531\u4e8e\u4f53\u7cfb\u4e2d\u6709\u7535\u6d41\u901a\u8fc7,\u4ea7\u751f\u4e86\u6eb6\u6db2\u7535\u538b\u964d\u548c\u5bf9\u7535\u6781\u7684\u6781\u5316,\u56e0\u6b64\u5de5\u4f5c\u7535\u6781\u7684\u7535\u4f4d\u96be\u4ee5\u51c6\u786e\u6d4b\u5b9a,\u7531\u6b64\u5f15\u5165\u53c2\u6bd4\u7535\u6781.\u53c2\u6bd4\u7535\u6781\u6709\u7740\u975e\u5e38\u7a33\u5b9a\u7684\u7535\u4f4d,\u4e14\u7535\u6d41\u4e0d\u7ecf\u8fc7\u53c2\u6bd4\u7535\u6781\u4e0d\u4f1a\u5f15\u8d77\u6781\u5316,\u4ece\u800c\u5de5\u4f5c\u7535\u6781\u7684\u7535\u4f4d\u53ef\u4ee5\u7531\u53c2\u6bd4\u7535\u6781\u5f97\u5230,\u800c\u7535\u6d41\u7531\u5de5\u4f5c\u7535\u6781-\u8f85\u52a9\u7535\u6781\u56de\u8def\u5f97\u5230.
\n\u5f53\u4f53\u7cfb\u4e2d\u6ca1\u6709\u7535\u6d41\u901a\u8fc7,\u5de5\u4f5c\u7535\u6781\u7684\u7535\u4f4d\u53ef\u4ee5\u7531\u5bf9\u7535\u6781\u76f4\u63a5\u51c6\u786e\u6d4b\u5b9a,\u56e0\u6b64\u53ef\u4ee5\u7528\u53cc\u7535\u6781\u4f53\u7cfb.\u7531\u6b64\u53ef\u5f97,\u5982\u679c\u4f53\u7cfb\u4e2d\u6ca1\u6709\u7535\u6d41\u901a\u8fc7,\u90fd\u53ef\u4ee5\u7528\u53cc\u7535\u6781\u4f53\u7cfb.\u4e00\u65e6\u6709\u7535\u6d41\u901a\u8fc7,\u8981\u91c7\u7528\u4e09\u7535\u6781\u4f53\u7cfb,\u4ee5\u540c\u65f6\u6d4b\u5f97\u5de5\u4f5c\u7535\u6781\u7684\u7535\u4f4d\u548c\u7535\u6d41.<\/p>\n

\u56fe3\uff1a\u7535\u89e3\u6db2\u5bf9ss-316 \u7535\u6781\u7684\u8150\u8680\u60c5\u51b5\u63a2\u7a76<\/strong><\/p>\n

\"\u65e0\u6807\u9898e\"<\/p>\n

0.71 M Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u4e0eTHF-CH3CN \u6bd4\u4f8b\u4e3a1 : 1\u7684\u7535\u89e3\u6db2\u5728\u5faa\u73af\u8fc7\u7a0b\u4e2d\u5bf9ss-316 \u7535\u6781\u7684\u8150\u8680<\/p>\n

\uff08a\uff09\u5bf9\u4e8ess-316\u5de5\u4f5c\u7535\u6781\u7684\u7ebf\u6027\u4f0f\u5b89\u626b\u63cf\uff0c\u626b\u63cf\u901f\u7387\u4e3a25 mV\u2219s-1<\/sup>\u3002<\/p>\n

\uff08b\uff09\u548c\uff08d\uff09\u5206\u522b\u4e3a\u539f\u59cb\u72b6\u6001\u4e0bss-316\u96c6\u6d41\u4f53\u53ca\u5176\u653e\u59275000\u500d\u540e\u7684\u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff09\u56fe\u3002<\/p>\n

\uff08c\uff09\u4e3a\u53d7\u8150\u8680\u540ess-316\u96c6\u6d41\u4f53\u7684\u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff09\u56fe\u3002<\/p>\n

\uff08e\uff09\u4e3ass-316\u96c6\u6d41\u4f53\u53d7\u8150\u8680\u533a\u57df\u653e\u59274109\u500d\u540e\u7684\u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff09\u56fe\u3002<\/p>\n

\u56fe4\uff1a\u7535\u6781\u53d7\u8150\u8680\u524d\u540e\u7684\u8868\u9762\u5206\u6790<\/strong><\/p>\n

\"\u65e0\u6807\u9898f\"<\/p>\n

Mg\u7535\u6781\u53d70.71 M Mg(PF6<\/sub>)2<\/sub>(CH3<\/sub>CN)6<\/sub>\u4e0eTHF-CH3CN \u6bd4\u4f8b\u4e3a1 : 1\u7684\u7535\u89e3\u6db2\u8150\u8680\u524d\u540e\u7684\u8868\u9762\u5206\u6790<\/p>\n

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\u539f\u6587\u94fe\u63a5\uff1aMg(PF6<\/sub>)2<\/sub>-Based Electrolyte Systems: Understanding Electrolyte-Electrode Interactions for the Development of Mg-Ion Batteries<\/strong>\uff08JACS,2016\uff0cDOI:\u00a0<\/strong>10.1021\/jacs.6b04319\uff09<\/a><\/p>\n

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