{"id":259407,"date":"2024-04-15T06:26:43","date_gmt":"2024-04-14T22:26:43","guid":{"rendered":"\/\/m.iemloyee.com\/?p=259407"},"modified":"2024-04-14T20:26:51","modified_gmt":"2024-04-14T12:26:51","slug":"nature-energy%ef%bc%9a%e6%89%93%e7%a0%b4%e4%b8%9a%e5%86%85%e5%85%b1%e8%af%86%ef%bc%8c%e6%97%a0%e6%b0%9f%e5%90%ab%e6%b0%a7%e7%94%b5%e8%a7%a3%e6%b6%b2%e4%b8%ba%e9%94%82%e7%94%b5%e4%ba%a7%e4%b8%9a","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=259407","title":{"rendered":"Nature Energy\uff1a\u6253\u7834\u4e1a\u5185\u5171\u8bc6\uff0c\u65e0\u6c1f\u542b\u6c27\u7535\u89e3\u6db2\u4e3a\u9502\u7535\u4ea7\u4e1a\u8d4b\u80fd"},"content":{"rendered":"

\u4e00\u3001\u3010\u79d1\u5b66\u80cc\u666f\u3011<\/strong>\u00a0 <\/strong><\/p>\n

\u5728\u9502\u91d1\u5c5e\u7535\u6c60\u4e2d\uff0c\u56fa\u4f53\u7535\u89e3\u8d28\u754c\u9762\u5c42\uff08SEI\uff09\u5728\u7a33\u5b9a\u9502\u91d1\u5c5e\u8d1f\u6781\u548c\u963b\u6b62\u754c\u9762\u526f\u53cd\u5e94\u65b9\u9762\u8d77\u7740\u5173\u952e\u7684\u4f5c\u7528\u3002\u901a\u5e38\u8ba4\u4e3aSEI\u5305\u62ec\u65e0\u673a\u76f8\u548c\u6709\u673a\u76f8\uff0c\u65e0\u673a\u76f8\u4e3b\u8981\u6709\u6c1f\u5316\u9502(LiF)\u3001\u6c27\u5316\u9502(Li2<\/sub>O)\u3001\u78b3\u9178\u9502(Li2<\/sub>CO3<\/sub>)\u548c\u6c2e\u5316\u9502(Li3<\/sub>N),\u53d6\u51b3\u4e8e\u76d0\uff1b\u6709\u673a\u76f8\u4e3b\u8981\u5305\u62ec\u6709\u673a\u76d0\u548c\u805a\/\u4f4e\u805a\u7269\uff0c\u53d6\u51b3\u4e8e\u6eb6\u5242\u3002<\/p>\n

LiF\u88ab\u8ba4\u4e3a\u662fSEI\u7684\u5173\u952e\u7ec4\u5206\uff0c\u6709\u52a9\u4e8e\u5b9e\u73b0\u9ad8\u5e93\u4f26\u6548\u7387\uff0c\u5bfc\u81f4\u5b9e\u73b0\u9502\u91d1\u5c5e\u754c\u9762\u6c1f\u5316\u6210\u4e3a\u4e3b\u8981\u7684\u7535\u89e3\u8d28\u8bbe\u8ba1\u7b56\u7565\u3002LiF\u5177\u6709\u5316\u5b66\u60f0\u6027\u3001\u9ad8\u673a\u68b0\u5f3a\u5ea6\u3001\u4f4e\u7535\u5b50\u7535\u5bfc\u7387\u548c\u9ad8\u754c\u9762\u80fd\uff0c\u56e0\u6b64\u88ab\u8ba4\u4e3a\u662f\u7406\u60f3\u7684SEI\u76f8\u3002\u7136\u800c\uff0cLiF\u4e5f\u662fLi+<\/sup>\u4f20\u8f93\u7684\u8f83\u9ad8\u7535\u963b\u76f8\u4e4b\u4e00\u3002\u6b64\u5916\uff0c\u8d8a\u6765\u8d8a\u591a\u7684\u8bc1\u636e\u8d28\u7591LiF\u5728SEI\u4e2d\u662f\u5426\u5177\u6709\u660e\u663e\u7684\u5316\u5b66\u4f18\u52bf\uff0c\u8fd9\u4fc3\u4f7f\u4eba\u4eec\u66f4\u6df1\u5165\u5730\u7814\u7a76\u54ea\u4e9b\u76f8\u63d0\u4f9b\u4e86\u4e3b\u8981\u7684SEI\u529f\u80fd\u3002<\/p>\n

Li2<\/sub>O\u662fSEI\u7684\u6240\u6709\u6a21\u578b\u63cf\u8ff0\u4e2d\u51fa\u73b0\u7684\u7b2c\u4e8c\u4e2a\u4e3b\u8981\u76f8\u7ec4\u5206\u3002\u7136\u800c\uff0c\u5728\u9502\u91d1\u5c5e\u7535\u6c60\u4e2d\uff0cLi2<\/sub>O\u53d7\u5230\u7684\u5173\u6ce8\u8f83\u5c11\uff0c\u5c24\u5176\u662f\u4e0eLiF\u76f8\u6bd4\u3002\u4f5c\u8005\u4e4b\u524d\u89c2\u5bdf\u5230\uff0c\u5728\u9502\u7b94\u4e0a\u751f\u957f\u7684\u5168Li2<\/sub>O SEI\u7684Li+<\/sup>\u7535\u5bfc\u7387\u6bd4\u5168LiF SEI\u9ad8\u7ea6\u4e24\u500d\uff0c\u56e0\u6b64\u652f\u6301\u76f8\u5bf9\u66f4\u5747\u5300\u7684Li+<\/sup>\u901a\u91cf\uff0c\u56e0\u6b64Li2<\/sub>O\u66f4\u6709\u5229\u4e8eLi+<\/sup>\u5728SEI\u4e2d\u7684\u4f20\u8f93\u3002<\/p>\n

\u4e8c\u3001\u3010\u521b\u65b0\u6210\u679c\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u9ebb\u7701\u7406\u5de5\u5b66\u9662\u7814\u7a76\u4eba\u5458\u8fdb\u4e00\u6b65\u8bc1\u660e\u4e86Li2<\/sub>O\u5728SEI\u4e2d\u8d77\u5230\u4e86\u5173\u952e\u4f5c\u7528\uff0c\u6709\u52a9\u4e8e\u5b9e\u73b0\u9502\u91d1\u5c5e\u7535\u6c60\u7684\u9ad8\u5e93\u4f26\u6548\u7387\u3002\u7814\u7a76\u4eba\u5458\u53d1\u73b0Li2<\/sub>O\u4e0e\u9ad8\u5e93\u4ed1\u6548\u7387\u4e4b\u95f4\u5b58\u5728\u5f3a\u70c8\u7684\u6b63\u76f8\u5173\u5173\u7cfb\uff0c\u6bd4LiF\u7684\u76f8\u5173\u6027\u66f4\u5f3a\uff1b\u5e76\u5229\u7528Li2<\/sub>O\u7684\u6709\u76ca\u4f5c\u7528\uff0c\u6210\u529f\u521b\u9020\u4e86\u5b8c\u5168\u65e0\u6c1f\u7684\u7535\u89e3\u6db2\uff0c\u5b9e\u73b0\u4e86\u8d85\u8fc799%\u7684\u5e93\u4ed1\u6548\u7387\uff0c\u4e3a\u7535\u89e3\u6db2\u8bbe\u8ba1\u63d0\u4f9b\u4e86\u65b0\u7684\u7b56\u7565\u3002\u6b64\u5916\uff0cCryo-HRTEM\u8868\u5f81\u7ed3\u679c\u8868\u660e\uff0cLi2<\/sub>O\u5728SEI\u4e2d\u7684\u5206\u5e03\u548c\u5f62\u6001\u5bf9\u9502\u91d1\u5c5e\u8d1f\u6781\u7684\u6027\u80fd\u6709\u91cd\u8981\u5f71\u54cd\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>1<\/strong>\uff08<\/strong>a<\/strong>\uff09\u4e0d\u540c\u7535\u89e3\u6db2\u7684\u5e93\u4ed1\u6548\u7387\u3002\uff08<\/strong>b<\/strong>\uff09\u4e0d\u540c\u7535\u89e3\u6db2\u4e2d\u7684\u6eb6\u5242\u7269\u79cd\u548c\u76d0\u7684\u793a\u4f8b\u3002\uff08<\/strong>c<\/strong>\uff09\u4e0d\u540c\u7535\u89e3\u6db2\u4e2d<\/strong>SEI\/Li0<\/sup><\/strong>\u6b8b\u7559\u7269\u7684\u5f52\u4e00\u5316\u6d4b\u91cf\u503c\u3002\uff08<\/strong>d<\/strong>\uff09\u4e0d\u540c\u7535\u89e3\u6db2\u4e2d<\/strong>SEI\/Li0<\/sup><\/strong>\u6b8b\u7559\u7269\u5f52\u4e00\u5316\u6d4b\u91cf\u503c\u7684\u7d2f\u79ef\u8868\u793a\u3002<\/strong>\u00a9 2023 Springer Nature<\/strong><\/p>\n

\u4f5c\u8005\u7814\u7a76\u4e86\u4e0d\u540c\u7684\u7535\u89e3\u6db2\u4f53\u7cfb\u7684\u5e93\u4f26\u6548\u7387\uff0c\u5e93\u4f26\u6548\u7387\u8f83\u9ad8\uff08\u901a\u5e38\u5927\u4e8e 90%\uff09\u7684\u7535\u89e3\u8d28\u4e2d\uff0cSEI\u7531Li2<\/sub>O\u4e3b\u5bfc\u3002<\/p>\n

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\u56fe<\/strong>2<\/strong>\uff08<\/strong>a<\/strong>\uff09\u7535\u89e3\u6db2\u4e2d\u7535\u9540\u9502\u6c89\u79ef\u5f62\u6001\u7684\u4f4e\u500d\u7387\u56fe\u50cf\u3002\uff08<\/strong>b<\/strong>\uff09\u653e\u5927\u7684\u754c\u9762\u56fe\u50cf\u3002\uff08<\/strong>c<\/strong>\uff09\u63a5\u8fd1\u754c\u9762\u7684\u9009\u533a\u7535\u5b50\u884d\u5c04\uff08<\/strong>SAED<\/strong>\uff09\u6d4b\u91cf\u3002\uff08<\/strong>d<\/strong>\uff09<\/strong>SEI<\/strong>\u5185\u6676\u4f53\u7ed3\u6784\u7684<\/strong>HRTEM<\/strong>\u56fe\u50cf\u3002\uff08<\/strong>e<\/strong>\uff09\u5728<\/strong>1.37M LiFSI 7TTE\/3DMC LHCE<\/strong>\u7535\u89e3\u6db2\u4e2d\u7684\u9502\u6c89\u79ef\u7684\u4f4e\u500d\u7387\u56fe\u50cf\u3002\uff08<\/strong>f<\/strong>\uff09<\/strong>SEI<\/strong>\u7684<\/strong>SAED<\/strong>\u3002\uff08<\/strong>g<\/strong>\uff09<\/strong>SEI<\/strong>\u4e2d\u7684\u6676\u4f53\u76f8\u7684<\/strong>HRTEM<\/strong>\u56fe\u50cf\u3002\uff08<\/strong>h<\/strong>\uff09\u6240\u793a\u767d\u8272\u533a\u57df\u7684\u5085\u91cc\u53f6\u53d8\u6362\u3002\uff08<\/strong>i<\/strong>\uff09\u9540\u9502\u7535\u6781\u4e2d<\/strong>-SO2<\/sub>F<\/strong>\u548c<\/strong>LiF<\/strong>\u7684<\/strong>19<\/sup><\/strong>F-NMR<\/strong>\u6d4b\u91cf\u3002<\/strong>\u00a9 2023 Springer Nature<\/strong><\/p>\n

\u00a0<\/strong><\/p>\n

\u4f5c\u8005\u5229\u7528Cryo-HRTEM\u6280\u672f\u5bf9\u4e0d\u540c\u7535\u89e3\u6db2\u4e2d\u5f62\u6210\u7684SEI\u4e2d\u7684Li2<\/sub>O\u7684\u5fae\u89c2\u7ed3\u6784\u8fdb\u884c\u4e86\u8be6\u7ec6\u7684\u8868\u5f81\u3002\u901a\u8fc7\u5728\u4f4e\u6e29\u6761\u4ef6\u4e0b\u5bf9\u6837\u54c1\u8fdb\u884c\u6210\u50cf\uff0cCryo-HRTEM\u80fd\u591f\u63d0\u4f9bSEI\u4e2dLi2<\/sub>O\u9897\u7c92\u7684\u7a7a\u95f4\u5206\u5e03\u548c\u6676\u4f53\u7ed3\u6784\u4fe1\u606f\u3002\u4f5c\u8005\u63ed\u793a\u4e86Li2<\/sub>O\u5728\u9ad8\u9ad8\u5e93\u4f26\u6548\u7387\u7535\u89e3\u6db2\u4e2d\u5f62\u6210\u7684\u5747\u5300\u4e14\u6709\u5e8f\u7684\u7eb3\u7c73\u7ed3\u6784\uff0c\u53d1\u73b0\u4e86\u5747\u5300\u7684\u7ea65-10 nm Li2<\/sub>O\u5c42\uff0c\u5176\u65b9\u5411\u4e0eSEI\u8868\u9762\u5e73\u884c\uff0c\u8fd9\u5bf9\u4e8e\u7406\u89e3\u5176\u5728\u63d0\u9ad8\u7535\u6c60\u6027\u80fd\u4e2d\u7684\u4f5c\u7528\u81f3\u5173\u91cd\u8981\u3002<\/p>\n

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\u56fe<\/strong>3<\/strong>\uff08<\/strong>a<\/strong>\uff09<\/strong>0.5 M<\/strong>\u548c<\/strong>1.37 M LiFSI TTE\/ DMC<\/strong>\u4e2d\u6240\u6709\u7535\u89e3\u6db2\u6210\u5206\u7684\u6269\u6563\u6027\uff0c\u63ed\u793a\u4e86<\/strong>DMC-Li+<\/sup>-FSI\u2212<\/sup><\/strong>\u914d\u4f4d\u58f3\u5c42\u7684\u5f62\u6210\u3002\uff08<\/strong>b<\/strong>\uff09\u5728<\/strong>LiFSI 7TTE\/3DMC<\/strong>\uff08<\/strong>TTE\/DMC (v\/v:7\/3)<\/strong>\uff09\u7535\u89e3\u6db2\u4e2d\uff0c\u968f\u7740\u76d0\u6d53\u5ea6\u4ece<\/strong>0.5 M<\/strong>\u589e\u52a0\u5230<\/strong>1.37 M<\/strong>\uff0c\u7b2c\u4e00\u5468\u671f\u5bb9\u91cf\u635f\u5931\u548c\u5e93\u4f26\u6548\u7387\u3002\uff08<\/strong>c<\/strong>\uff09\u76d0\u884d\u751f<\/strong>SEI<\/strong>\u76f8\u548c\u6eb6\u5242\u884d\u751f<\/strong>SEI<\/strong>\u76f8\u7684\u91cf\u3002\uff08<\/strong>d<\/strong>\uff09\u5728<\/strong>0.5 M<\/strong>\u548c<\/strong>1.37 M<\/strong>\u7535\u89e3\u6db2\u4e2d\uff0c\u7535\u6781\u6b8b\u7559\u7269\u6eb6\u89e3\u5728<\/strong>H2<\/sub>O<\/strong>\u540e\u7684<\/strong>19<\/sup><\/strong>F-NMR<\/strong>\u3002<\/strong>\u00a9 2023 Springer Nature<\/strong><\/p>\n

\u00a0\"\"<\/strong><\/p>\n

\u56fe<\/strong>4<\/strong>\u65e0\u6c1f\u9ad8\u5e93\u4f26\u6548\u7387\u7535\u89e3\u6db2\u7684\u8bbe\u8ba1\u3002\uff08<\/strong>a<\/strong>\uff09\u5e93\u4f26\u6548\u7387\u6d4b\u8bd5\u3002\uff08<\/strong>b<\/strong>\uff09\u603b\u7ed3\u4e86<\/strong>LiBF4<\/sub><\/strong>\u3001<\/strong>LiPF6<\/sub><\/strong>\u3001<\/strong>LiClO4<\/sub><\/strong>\u548c<\/strong>LiNO3<\/sub><\/strong>\u4f5c\u4e3a\u76d0\u7684<\/strong>LHCE<\/strong>\u7684\u5e93\u4f26\u6548\u7387\u3002\uff08<\/strong>c<\/strong>\uff09\u9009\u5b9a\u7535\u89e3\u6db2\u4e2d<\/strong>Li2<\/sub>O<\/strong>\u6216<\/strong>LiF<\/strong>\u7684\u5f52\u4e00\u5316\u542b\u91cf\u3002<\/strong>\u00a9 2023 Springer Nature<\/strong><\/p>\n

\u6700\u540e\uff0c\u4f5c\u8005\u8bbe\u8ba1\u4e86\u5b8c\u5168\u65e0\u6c1f\u3001\u5bcc\u6c27\u7684\u7535\u89e3\u6db2\uff0c\u8bc1\u660e\u4e86\u53ef\u4ee5\u4ea7\u751f\u5bcc\u542bLi2<\/sub>O\u3001\u4e0d\u542bLiF\u7684SEI\u7684\u7535\u89e3\u6db2\uff081 M LiClO4<\/sub> DOL\/DME+3 wt% LiNO3<\/sub>\u4f53\u7cfb\u53ef\u4ee5\u5b9e\u73b099.1%\u7684\u5e93\u4f26\u6548\u7387\uff09\u662f\u57fa\u4e8eLiFSI\u7684\u5c40\u90e8\u9ad8\u6d53\u5ea6\u7535\u89e3\u6db2\uff08LHCE\uff09\u7684\u4e00\u79cd\u6709\u524d\u9014\u7684\u66ff\u4ee3\u54c1\uff1b\u867d\u7136LiFSI\u57fa\u7535\u89e3\u6db2\u7684\u53ef\u4ee5\u5b9e\u73b099.3%\u7684\u5e93\u4f26\u6548\u7387\uff0c\u4f46\u662f\u7531\u4e8e\u5176\u9ad8\u6c1f\u542b\u91cf\uff0c\u901a\u5e38\u5177\u6709\u8150\u8680\u6027\u548c\u6bd2\u6027\u3002\u7531\u4e8e\u975e\u6c1f\u5316\u919a\u5728\u6b63\u6781\u7535\u4f4d\u4e0b\u7684\u4e0d\u7a33\u5b9a\u6027\u3001\u4e0eLiClO4<\/sub>\u7b49\u5f3a\u6c27\u5316\u6027\u76d0\u76f8\u5173\u7684\u5b89\u5168\u95ee\u9898\u4ee5\u53ca\u6eb6\u5242\u7c98\u5ea6\u5bfc\u81f4\u7684\u6709\u9650\u9ad8\u500d\u7387\u6027\u80fd\uff0c\u672c\u6587\u62a5\u544a\u7684\u7279\u5b9a\u7535\u89e3\u6db2\u6df7\u5408\u7269\u5bf9\u5168\u7535\u6c60\u800c\u8a00\u5e76\u4e0d\u7406\u60f3\uff0c\u8fd9\u4e9b\u6311\u6218\u4fc3\u4f7f\u5bf9\u975e\u6c1f\u5316\u4f46\u6b63\u6781\u7a33\u5b9a\u7684\u76d0\u548c\u6eb6\u5242\u8fdb\u884c\u8fdb\u4e00\u6b65\u7814\u7a76\u3002<\/p>\n

\u8be5\u7814\u7a76\u5b9e\u73b0\u4e86\u4e00\u79cd\u9ad8\u5e93\u4f26\u6548\u7387\u7684\u9502\u91d1\u5c5e\u7535\u6c60\uff0c\u4ee5\u201cHigh lithium oxide prevalence in the lithium solid\u2013electrolyte interphase for high Coulombic efficiency<\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728\u56fd\u9645\u9876\u7ea7\u671f\u520aNature Energy<\/strong>\u4e0a\uff0c\u5f15\u8d77\u4e86\u76f8\u5173\u9886\u57df\u7814\u7a76\u4eba\u5458\u70ed\u8bae\u3002<\/p>\n

\"\"<\/p>\n

\u4e09\u3001\u3010\u79d1\u5b66\u542f\u8fea\u3011<\/strong><\/p>\n

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\u539f\u6587\u8be6\u60c5<\/strong>\uff1aHobold, G.M., Wang, C., Steinberg, K. et al. High lithium oxide prevalence in the lithium solid\u2013electrolyte interphase for high Coulombic efficiency. Nat Energy (2024). https:\/\/doi.org\/10.1038\/s41560-024-01494-x<\/p>\n

 <\/p>\n

\u672c\u6587\u7531\u666f\u884c\u64b0\u7a3f<\/strong><\/p>\n

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