{"id":255165,"date":"2023-10-18T06:33:13","date_gmt":"2023-10-17T22:33:13","guid":{"rendered":"\/\/m.iemloyee.com\/?p=255165"},"modified":"2023-10-17T17:11:30","modified_gmt":"2023-10-17T09:11:30","slug":"nano-energy-%e4%bb%8e%e7%a9%ba%e6%b0%94%e5%92%8c%e6%b0%b4%e4%b8%ad%e5%9b%ba%e6%b0%ae%e5%88%b6%e6%b0%a8%ef%bc%9a%e9%ab%98%e5%88%86%e6%95%a3%e9%93%9c%e9%93%81%e7%ba%b3%e7%b1%b3%e5%90%88%e9%87%91","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=255165","title":{"rendered":"Nano Energy\u2014\u4ece\u7a7a\u6c14\u548c\u6c34\u4e2d\u56fa\u6c2e\u5236\u6c28\uff1a\u9ad8\u5206\u6563\u94dc\u94c1\u7eb3\u7c73\u5408\u91d1\u589e\u5f3a\u7535\u50ac\u5316\u8fd8\u539f\u4e0e\u7b49\u79bb\u5b50\u6c27\u5316\u76f8\u8026\u5408"},"content":{"rendered":"

\u7b2c\u4e00\u4f5c\u8005\uff1a\u5218\u6d0b<\/p>\n

\u901a\u8baf\u4f5c\u8005\uff1a\u9ad8\u4e66\u71d5<\/p>\n

\u901a\u8baf\u5355\u4f4d\uff1a\u6cb3\u5357\u5e08\u8303\u5927\u5b66<\/p>\n

\u8bba\u6587DOI\uff1a10.1016\/j.nanoen.2023.108840<\/p>\n

\"\"<\/p>\n

\u3010\u5168\u6587\u901f\u89c8\u3011<\/p>\n

\u672c\u5de5\u4f5c\u521b\u65b0\u6027\u5730\u5f00\u53d1\u4e86\u4e00\u79cd\u9ad8\u5206\u6563\u94dc\u94c1\u7eb3\u7c73\u5408\u91d1\u589e\u5f3a\u7535\u50ac\u5316\u785d\u9178\u6839\u8fd8\u539f\u8f6c\u6c28\u8026\u5408\u7b49\u79bb\u5b50\u4f53\u6c2e\u6c14\u6c27\u5316\u7684\u65b0\u7b56\u7565\u3002\u91c7\u7528\u7684\u77ac\u65f6\u70ed\u51b2\u51fb\u7126\u8033\u70ed\u6cd5\u80fd\u591f\u6291\u5236\u94dc\u94c1\u7eb3\u7c73\u5408\u91d1\u7684\u76f8\u5206\u79bb\uff0c\u4ece\u800c\u6709\u6548\u5730\u8c03\u8282\u50ac\u5316\u4f4d\u70b9\u5438\u9644\u80fd\u3002\u5229\u7528\u539f\u5b50\u529b\u663e\u5fae\u955c\u548c\u5f00\u5c14\u6587\u63a2\u9488\u63a2\u7d22\u4e86\u4e0d\u540c\u50ac\u5316\u5242\u7684\u8868\u9762\u7535\u52bf\u5206\u5e03\u89c4\u5f8b\uff0c\u539f\u4f4d\u7535\u5316\u5b66\u62c9\u66fc\u5149\u8c31\u8fdb\u4e00\u6b65\u9610\u660e\u4e86\u785d\u9178\u6839\u8fd8\u539f\u8f6c\u6c28\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u8868\u9762\u7269\u79cd\u968f\u7535\u6781\u7535\u52bf\u7684\u53d8\u5316\u89c4\u5f8b\u3002\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\u8ba1\u7b97\u7ed3\u679c\u63ed\u793a\u4e86\u94c1\u539f\u5b50\u7684\u52a0\u5165\u5bf9\u94dc\u94c1\u5408\u91d1\u5438\u9644\u80fd\u548c\u7535\u5b50\u7ed3\u6784\u7684\u589e\u5f3a\u4f5c\u7528\u4e0e\u8c03\u8282\u673a\u5236\u3002<\/p>\n

\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u6c28\u4f5c\u4e3a\u4e00\u79cd\u7406\u60f3\u7684\u6c22\u80fd\u6e90\u8f7d\u4f53\uff0c\u53d7\u5230\u4e86\u4e16\u754c\u5404\u56fd\u7684\u5173\u6ce8\u3002\u5de5\u4e1a\u4e0a\u5927\u89c4\u6a21\u5408\u6210\u6c28\u7684\u54c8\u4f2f\u5de5\u827a\u9700\u8981\u4e25\u82db\u7684\u9ad8\u6e29\u9ad8\u538b\u6761\u4ef6\uff0c\u4eba\u4eec\u8feb\u5207\u9700\u8981\u5f00\u53d1\u4e00\u79cd\u9ad8\u6548\u4fbf\u6377\u4e14\u80fd\u591f\u5728\u6e29\u548c\u73af\u5883\u6761\u4ef6\u4e0b\u5408\u6210\u6c28\u7684\u65b0\u9014\u5f84\uff0c\u8fd9\u5bf9\u4e8e\u5229\u7528\u504f\u8fdc\u5730\u533a\u4e2d\u4e30\u5bcc\u7684\u53ef\u518d\u751f\u80fd\u6e90\u548c\u5168\u7403\u7684\u4f4e\u78b3\u51cf\u6392\u5177\u6709\u91cd\u8981\u4ef7\u503c\u3002\u901a\u8fc7\u5c06\u7535\u50ac\u5316\u785d\u9178\u6839\u8fd8\u539f\u4e0e\u7b49\u79bb\u5b50\u4f53\u6c27\u5316\u8fc7\u7a0b\u76f8\u8026\u5408\uff0c\u53ef\u4ee5\u5728\u5e38\u6e29\u5e38\u538b\u4e0b\u5c06\u7a7a\u6c14\u4e2d\u6c2e\u6c14\u3001\u6c27\u6c14\u548c\u6c34\u4e2d\u6c22\u539f\u5b50\u8f6c\u5316\u6c28\uff0c\u5177\u6709\u6613\u542f\u505c\u548c\u6613\u642d\u5efa\u7684\u5236\u6c28\u4f18\u70b9\u3002\u7535\u50ac\u5316\u785d\u9178\u6839\u8fd8\u539f\u8fc7\u7a0b\u9762\u4e34\u53cd\u5e94\u901f\u7387\u4f4e\u548c\u9009\u62e9\u6027\u5dee\u7684\u74f6\u9888\u95ee\u9898\uff0c\u76ee\u524d\u91d1\u5c5e\u94dc\u662f\u6700\u5177\u6d3b\u6027\u548c\u9009\u62e9\u6027\u7684\u785d\u9178\u6839\u8fd8\u539f\u8f6c\u6c28\u7684\u50ac\u5316\u5242\u4e4b\u4e00\u00a0\uff0c\u51b3\u901f\u6b65\u9aa4\u4e3a\u785d\u9178\u6839\u5230\u4e9a\u785d\u9178\u6839\u8fc7\u7a0b\u3002\u7531\u963f\u4f26\u5c3c\u4e4c\u65af\u516c\u5f0f\u548cBEP\u7ebf\u6027\u5173\u7cfb\u53ef\u77e5\uff1a\u53cd\u5e94\u901f\u7387\u4e0e\u6d3b\u5316\u80fd\u6210\u6307\u6570\u5173\u7cfb\uff0c\u5438\u9644\u80fd\u4e0e\u6d3b\u5316\u80fd\u6210\u7ebf\u6027\u5173\u7cfb\u3002\u56e0\u6b64\uff0c\u63d0\u9ad8\u91d1\u5c5e\u94dc\u5bf9\u785d\u9178\u6839\u7684\u5438\u9644\u80fd\u662f\u964d\u4f4e\u51b3\u901f\u6b65\u9aa4\u53cd\u5e94\u6d3b\u5316\u80fd\u3001\u4fc3\u8fdb\u603b\u53cd\u5e94\u901f\u7387\u7684\u6709\u6548\u7b56\u7565\u3002\u5728\u6b64\u57fa\u7840\u4e0a\uff0c\u5f15\u5165\u5176\u4ed6\u91d1\u5c5e\u5f62\u6210\u5408\u91d1\u50ac\u5316\u5242\u662f\u63d0\u9ad8\u5438\u9644\u80fd\u7684\u53ef\u884c\u9014\u5f84\u3002<\/p>\n

\u3010\u672c\u6587\u4eae\u70b9\u3011<\/strong><\/p>\n

\uff081\uff09\u91c7\u7528\u7126\u8033\u52a0\u70ed\u6cd5\uff0c\u6210\u529f\u5236\u5907\u4e86\u78b3\u7ea4\u7ef4\u7eb8\u4e0a\u9ad8\u5ea6\u5206\u6563\u7684\u94dc\u94c1\u7eb3\u7c73\u5408\u91d1\u3002<\/p>\n

\uff082\uff09\u5229\u7528\u5f00\u5c14\u6587\u63a2\u9488\u5206\u6790\u4e86\u94c1\u539f\u5b50\u5728\u8c03\u8282\u7535\u6781\u8868\u9762\u7535\u4f4d\u5206\u5e03\u4e2d\u8d77\u5230\u7684\u4f5c\u7528\u3002<\/p>\n

\uff083\uff09\u5229\u7528\u539f\u4f4d\u7535\u5316\u5b66\u62c9\u66fc\u5149\u8c31\u5206\u6790\u4e86\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u4e2d\u95f4\u7269\u79cd\u968f\u7535\u4f4d\u7684\u53d8\u5316\u3002<\/p>\n

\uff084\uff09 DFT\u8ba1\u7b97\u8bc1\u660e\u4e86\u9ad8d\u5e26\u4e2d\u5fc3\u7684\u94c1\u539f\u5b50\u80fd\u591f\u589e\u5f3a\u5438\u9644\u80fd\u7684\u672c\u5f81\u7535\u5b50\u8c03\u63a7\u673a\u5236\u3002<\/p>\n

\u3010\u56fe\u6587\u89e3\u6790\u3011<\/strong><\/p>\n

A.\u53cd\u5e94\u8fc7\u7a0b\u4e0e\u6750\u6599\u5408\u6210\u6d41\u7a0b\u793a\u610f\u56fe<\/b><\/strong><\/p>\n

\u5728\u7b49\u79bb\u5b50\u4f53\u7684\u4f5c\u7528\u4e0b\uff0c\u7a7a\u6c14\u4e2d\u7684N2<\/sub>\u548cO2<\/sub>\u88ab\u6c27\u5316\u4e3a\u6c2e\u6c27\u5316\u7269\uff08NOx<\/sub>–<\/sup>\uff09\uff0c\u5176\u4e2d\u5927\u90e8\u5206\u662f\u785d\u9178\u6839\uff0c\u968f\u540e\u785d\u9178\u6839\u5728\u50ac\u5316\u5242\u7684\u4f5c\u7528\u4e0b\u88ab\u8fd8\u539f\u4e3a\u6c28\u3002<\/p>\n

\u5c06\u7a7a\u767d\u78b3\u7eb8\u6d78\u6da6\u5728\u91d1\u5c5e\u76d0\u524d\u9a71\u4f53\u6eb6\u6db2\u4e2d\uff0c\u5f85\u5b8c\u5168\u6d78\u6da6\u540e\u7528\u7ea2\u5916\u70e4\u706f\u5b8c\u5168\u70e4\u5e72\uff0c\u968f\u540e\u653e\u5165\u7126\u8033\u70ed\u5408\u6210\u8bbe\u5907\u4e2d\uff0c\u5728\u9ad8\u6e29\u6761\u4ef6\u4e0bCu2+<\/sup>\u548cFe3+<\/sup>\u88ab\u8fd8\u539f\u4e3a\u94dc\u94c1\u5408\u91d1\u3002<\/p>\n

\"\"<\/p>\n

Scheme 1. Schematic illustration of (a) plasma oxidation coupled with NRA and (b) thesynthesis of Cux<\/sub>Fey<\/sub>-CFP nanoalloys using the Joule heating method.<\/p>\n

B.\u7b49\u79bb\u5b50\u4f53\u6c27\u5316\u4e0e\u53cd\u5e94\u673a\u7406<\/b><\/strong><\/p>\n

\u7b49\u79bb\u5b50\u4f53\u653e\u7535\u7684\u5b9e\u7269\u56fe\uff0c\u653e\u7535\u5c16\u7aef\u4e0e\u6c34\u9762\u8ddd\u79bb\u7ea61.3 cm\uff0c\u572830 kV\u7684\u7535\u538b\u4e0b\u5206\u522b\u53cd\u5e9410\u300120\u300130\u300140 min\uff1b\u603b\u4f53\u4e0aNO2<\/sub>–<\/sup>\u4e0eNO3<\/sub>–<\/sup>\u7684\u4ea7\u91cf\u4e0e\u4ea7\u7387\u4e4b\u6bd4\u4ecb\u4e8e1\uff1a3\u52301\uff1a5\u4e4b\u95f4\uff0c\u4ece\u7a7a\u6c14\u5230NOx<\/sub>–<\/sup>\u7684\u53cd\u5e94\u8def\u5f84\u56fe\u8868\u660eN2<\/sub>\u548cO2<\/sub>\u4f1a\u5728\u4f4e\u6e29\u7b49\u79bb\u5b50\u4f53\u8fc7\u7a0b\u4e2d\u8f6c\u5316\u4e3aNO2<\/sub>–<\/sup>\u548cNO3<\/sub>–<\/sup>\u3002<\/p>\n

\"\"<\/p>\n

Fig. 1. <\/b><\/strong>(a) Photo of plasma oxidation reactor. (b) NOx<\/sub>\u2012<\/sup>\u00a0production and (c) NOx<\/sub>\u2012<\/sup>\u00a0yield rate achieved by the plasma oxidation process. (d) Multiple reaction pathways from air to NO3<\/sub>\u2012<\/sup>.<\/p>\n

C.\u94dc\u94c1\u5408\u91d1\u7684\u8868\u5f81\u7ed3\u679c<\/b><\/strong><\/p>\n

\u901a\u8fc7SEM\uff0cTEM\uff0c\u5143\u7d20mapping\u7b49\u8bc1\u5b9e\u4e86\u9ad8\u5ea6\u5206\u6563\u7684\u7403\u5f62\u94dc\u94c1\u7eb3\u7c73\u5408\u91d1\u5df2\u88ab\u6210\u529f\u5236\u5907\uff0c\u94dc\u94c1\u5143\u7d20\u5206\u5e03\u5747\u5300\uff1bXRD\u548cXPS\u63ed\u793a\u4e86\u5408\u91d1\u7684\u6676\u76f8\u4fe1\u606f\u548c\u5143\u7d20\u5206\u5e03\uff1b\u5229\u7528\u5f00\u5c14\u6587\u63a2\u9488\u68c0\u6d4b\u4e0d\u540c\u50ac\u5316\u5242\u8868\u9762\u7684\u7535\u52bf\u5206\u5e03\uff0cCu10<\/sub>Fe1<\/sub>-CFP\u4e2d\u50ac\u5316\u4f4d\u70b9\u7684\u8868\u9762\u7535\u52bf\u6bd4Cu-CFP\u7684\u8981\u4f4e\uff0c\u8bf4\u660eFe\u539f\u5b50\u7684\u52a0\u5165\u4f7f\u5f97\u5408\u91d1\u7684\u5438\u9644\u80fd\u589e\u5f3a\uff0c\u6709\u5229\u4e8e\u785d\u9178\u6839\u5230\u4e9a\u785d\u9178\u6839\u8fc7\u7a0b\u7684\u8f6c\u5316\u3002<\/p>\n

\"\"<\/p>\n

Fig. 2. <\/b><\/strong>(a,b) SEM images, (e)TEM image and (f) HRTEM image of Cu10<\/sub>Fe1<\/sub>-CFP. (c, d, h) EDS element mapping images and (g) HAADF image of Cu10<\/sub>Fe1<\/sub>-CFP. (i) The XRD spectra of Cux<\/sub>Fey<\/sub>-CFP. (j) Cu 2p and (k) Fe 2p XPS spectra of Cux<\/sub>Fey<\/sub>-CFP. (l-n) AFM images, (p-r) KPFM images and (o) corresponding 3D reconstruction pictures of Cu-CFP, Cu10<\/sub>Fe1<\/sub>-CFP\u00a0and Fe-CFP. (s) The surface potential distribution on the selected red lines.<\/p>\n

D.\u539f\u4f4d\u7535\u5316\u5b66\u62c9\u66fc\u5149\u8c31\u63a2\u5bfb\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u95f4\u7269\u79cd\u7684\u6f14\u53d8<\/b><\/strong><\/p>\n

\u901a\u8fc7\u539f\u4f4d\u7535\u5316\u5b66\u62c9\u66fc\u5149\u8c31\u7814\u7a76\u4e86Cu-CFP\u548cCu10<\/sub>Fe1<\/sub>-CFP\u57280.1 M KNO3<\/sub>\u6eb6\u6db2\u4e2d\u7684\u785d\u9178\u6839\u8fd8\u539f\u8f6c\u6c28\u8fc7\u7a0b\u3002\u7ed3\u679c\u8868\u660e\uff0cFe\u539f\u5b50\u7684\u52a0\u5165\u589e\u5f3a\u4e86Cu-N\u952e\u548c\u5438\u9644\u6001NO3<\/sub>–<\/sup>\u7684\u5f3a\u5ea6\uff0c E\/F\u5cf0\u6bd4\u503c\u6709\u660e\u663e\u63d0\u5347\u3002\u7531\u6b64\u53ef\u4ee5\u63a8\u65ad\uff0cFe\u539f\u5b50\u7684\u52a0\u5165\u53ef\u4ee5\u52a0\u901fNO3<\/sub>–<\/sup>\u8f6c\u5316\u4e3aNO2<\/sub>–<\/sup>\u8fd9\u4e00\u51b3\u901f\u6b65\u9aa4\uff0c\u4ece\u800c\u63d0\u9ad8\u603b\u53cd\u5e94\u901f\u7387\u3002<\/p>\n

\"\"<\/p>\n

Fig. 4. <\/b><\/strong>In situ electrochemical Raman spectra of Cu-CFP (a) and Cu10<\/sub>Fe1<\/sub>-CFP (b) from open circuit potential (OCP) to \u20120.45 V. (c) Schematic diagram of the vibration model of the adsorbed species and corresponding peaks. (d) Comparison of reaction rate of the rate-determining step between Cu-CFP and Cu10<\/sub>Fe1<\/sub>-CFP.<\/p>\n

\u901a\u8fc7\u7406\u8bba\u8ba1\u7b97\u5206\u6790\u94dc\u94c1\u5408\u91d1\u50ac\u5316\u6d3b\u6027\u589e\u5f3a\u7684\u539f\u56e0<\/b><\/strong><\/p>\n

\u968f\u7740\u94dc\u57fa\u5e95\u8868\u9762Fe\u539f\u5b50\u7684\u52a0\u5165\uff0c\u50ac\u5316\u5242\u8868\u9762\u5bf9NO3<\/sub>–<\/sup>\u3001 H\u539f\u5b50\u548cNH3<\/sub>\u7684\u5438\u9644\u80fd\u9010\u6e10\u589e\u5927\uff0c\u5dee\u5206\u7535\u8377\u8ba1\u7b97\u8868\u660eFe\u539f\u5b50\u5bf9NO3<\/sub>–<\/sup>\u4e2dO\u539f\u5b50\u7684\u5438\u9644\u66f4\u5f3a\uff1b\u7535\u5b50\u6001\u5bc6\u5ea6\u7684\u8ba1\u7b97\u8868\u660e\u968f\u7740Fe\u539f\u5b50\u7684\u52a0\u5165\uff0cNO3<\/sub>–<\/sup>\u53cd\u952e\u8f68\u9053\u7684\u586b\u5145\u7535\u5b50\u9010\u6e10\u589e\u52a0\uff0cN-O\u952e\u7684\u7a33\u5b9a\u6027\u964d\u4f4e\uff0c\u8fd9\u6709\u5229\u4e8e\u4fc3\u8fdbNO3<\/sub>–<\/sup>\u53ca\u5176\u540e\u7eed\u6b65\u9aa4\u4e2dN-O\u952e\u7684\u65ad\u88c2\uff0c\u52a0\u5feb\u51b3\u901f\u6b65\u9aa4\u53cd\u5e94\u901f\u7387\u3002<\/p>\n

\"\"<\/p>\n

Fig. 5. <\/b><\/strong>(a) The absorption energy of NO3<\/sub>\u2012<\/sup>, H atom and NH3<\/sub>\u00a0over different simulated CuFe substrates in the form of radar map. (b) The charge density difference of NO3<\/sub>\u2012<\/sup>\u00a0adsorbed on different simulated CuFe substrates, the yellow, steel blue, red and bright blue spheres represent atoms of Cu, Fe, O and N, respectively. (c) The PDOS of absorbed NO3<\/sub>\u2012<\/sup>\u00a02p orbitals. (d) The integral area of PDOS under\/above the Fermi level.<\/p>\n

5.\u603b\u7ed3\u4e0e\u5c55\u671b<\/p>\n

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