{"id":252835,"date":"2023-07-13T06:44:34","date_gmt":"2023-07-12T22:44:34","guid":{"rendered":"\/\/m.iemloyee.com\/?p=252835"},"modified":"2023-07-12T23:35:35","modified_gmt":"2023-07-12T15:35:35","slug":"%e6%b5%8e%e5%8d%97%e5%a4%a7%e5%ad%a6%e5%be%90%e9%94%a1%e9%87%91-%e7%8e%8b%e6%99%93-chemical-engineering-journal%ef%bc%9asnpx-rgo%e7%9a%84p-n%e6%b0%94%e6%95%8f%e5%b1%9e%e6%80%a7%e8%bd%ac%e5%8f%98","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=252835","title":{"rendered":"\u6d4e\u5357\u5927\u5b66\u5f90\u9521\u91d1\/\u738b\u6653 Chem. Eng. J.\uff1aSnPx\/rGO\u7684p-n\u6c14\u654f\u5c5e\u6027\u8f6c\u53d8\u53caNH3\u6c14\u654f\u6027\u80fd\u7814\u7a76"},"content":{"rendered":"

0<\/b><\/strong>1 [\u5bfc\u8bfb<\/b><\/strong>]<\/b><\/strong><\/p>\n

SnPx<\/sub>\u5177\u6709\u5206\u5c42\u6676\u4f53\u7ed3\u6784\uff0c\u7531\u4ea4\u66ff\u6392\u5217\u7684Sn\u548cP\u5c42\u7ec4\u6210\uff0c\u4f7f\u5916\u90e8\u79bb\u5b50\u6613\u4e8e\u63d2\u5165\uff0c\u8fdb\u4e00\u6b65\u66b4\u9732\u66f4\u591a\u7684\u8868\u9762\u53cd\u5e94\u6d3b\u6027\u4f4d\u70b9\u3002\u6b64\u5916\uff0c\u7531\u4e8eP\u539f\u5b50\u6bd4\u91d1\u5c5e\u539f\u5b50\u7535\u8d1f\u6027\u9ad8\uff0c\u6240\u4ee5SnPx<\/sub>\u7684\u7535\u5b50\u4e91\u5bc6\u5ea6\u5206\u5e03\u53ef\u63a7\u3002\u91d1\u5c5e\u539f\u5b50\u7684\u7535\u5b50\u4e91\u5c06\u504f\u5411P\u539f\u5b50\uff0c\u4f7fP\u539f\u5b50\u5e26\u8d1f\u7535\u8377,\u4ece\u800c\u5438\u9644\u66f4\u591a\u7684\u6c27\u6c14\u5206\u5b50\u3002\u6b64\u5916\uff0cSnPx<\/sub>\u8fd8\u5177\u6709\u4e30\u5bcc\u7684\u9178\u6027P\u7a7a\u4f4d\u4f4d\u70b9\uff0c\u6709\u5229\u4e8e\u78b1\u6027\u6c14\u4f53\uff08\u5982NH3<\/sub>\uff09\u7684\u5438\u9644\u3002\u7136\u800c\uff0c\u5728\u4f20\u7edf\u5408\u6210\u5de5\u827a\u4e2d\uff0cSnPx<\/sub>\u7eb3\u7c73\u9897\u7c92\u7684\u901a\u5e38\u4f1a\u56e2\u805a\uff0c\u5bfc\u81f4\u5bfc\u7535\u6027\u548c\u8868\u9762\u6d3b\u6027\u4f4d\u70b9\u964d\u4f4e\uff0c\u4ece\u800c\u963b\u788d\u5176\u5728\u6c14\u4f53\u4f20\u611f\u5668\u4e2d\u7684\u5e94\u7528\u3002\u8fd8\u539f\u6c27\u5316\u77f3\u58a8\u70ef\uff08rGO\uff09\u4f5c\u4e3a\u4e00\u79cd\u5bfc\u7535\u6750\u6599\uff0c\u5177\u6709\u9ad8\u8f7d\u6d41\u5b50\u8fc1\u79fb\u7387\u548c\u6bd4\u8868\u9762\u79ef\u7684\u4f18\u70b9\u3002\u5728rGO\u4e0a\u4fee\u9970SnPx<\/sub>\u53ef\u4ee5\u6709\u6548\u6291\u5236\u4f53\u79ef\u81a8\u80c0\u548c\u9897\u7c92\u805a\u96c6\u3002\u6b64\u5916\uff0cSnPx<\/sub>\u548crGO\u4e4b\u95f4\u7684\u5f02\u8d28\u7ed3\u6784\u8fd8\u5c06\u63d0\u4f9b\u66f4\u591a\u7684\u8868\u9762\u5438\u9644\u4f4d\u70b9\u5e76\u4fc3\u8fdb\u7535\u8377\u8f6c\u79fb\uff0c\u4ece\u800c\u5e26\u6765\u66f4\u597d\u7684\u611f\u5e94\u6027\u80fd\u3002\u7136\u800c\uff0c\u5bf9SnPx<\/sub>\u6750\u6599\u7684\u8868\u9762\u6c14\u4f53\u5438\u9644\u60c5\u51b5\u53ca\u5176\u6c14\u654f\u6027\u80fd\u4e0e\u654f\u611f\u673a\u5236\u7684\u7814\u7a76\u5c1a\u4e0d\u5145\u5206\u3002<\/p>\n

0<\/b><\/strong>2 [\u6210\u679c\u63a0\u5f71<\/b><\/strong>]<\/b><\/strong><\/p>\n

\u672c\u6587\u5236\u5907\u4e86SnPx<\/sub>\/rGO\u590d\u5408\u6750\u6599\uff0c\u7528\u4e8e\u5ba4\u6e29\u4e0bNH3<\/sub>\u6c14\u4f53\u4f20\u611f\u3002\u7ed3\u6784\u8868\u5f81\u8868\u660e\uff0c\u5728rGO\u8868\u9762\u5747\u5300\u5206\u5e03\u4e86\u5c0f\u5c3a\u5bf8\u7684SnPx<\/sub>\uff0c\u4e14\u5b58\u5728\u4e30\u5bcc\u7684\u9178\u6027P\u7a7a\u4f4d\u4f4d\u70b9\u3002\u6c14\u4f53\u4f20\u611f\u7ed3\u679c\u663e\u793a\uff0cSnPx<\/sub>\/rGO\u590d\u5408\u6750\u6599\u7684\u54cd\u5e94\u503c\u5728\u78f7\u5316\u6bd4\u4e3a1:5\uff08SG-5\uff09\u65f6\uff0c\u5bf940 ppm\u7684NH3<\/sub>\u7684\u54cd\u5e94\u503c\u53ef\u8fbe117.5%\u3002SG-5\u8fd8\u5bf9\u4f4e\u6d53\u5ea6\u7684NH3<\/sub>\u6c14\u4f53\uff08\u54cd\u5e94\u503c\uff1a500 ppb NH3<\/sub>\u4e0b\u54cd\u5e943%\uff09\u8868\u73b0\u51fa\u9ad8\u54cd\u5e94\u6027\u548c43.6 ppb\u7684LOD\u3002\u6b64\u5916\uff0c\u901a\u8fc7NH3<\/sub>-TPD\u548c\u539f\u4f4dDRIFTs\u5206\u6790\uff0c\u7814\u7a76\u4e86NH3<\/sub>\u5206\u5b50\u5728\u6750\u6599\u8868\u9762\u7684\u7269\u7406\u5438\u9644\u548c\u8131\u9644\u60c5\u51b5\u3002\u66f4\u6709\u8da3\u7684\u662f\uff0c\u7531\u4e8e\u4e0d\u540c\u7684\u5438\u9644\u4f4d\u70b9\u548c\u5bfc\u7535\u901a\u9053\uff0cSnPx\/rGO\u590d\u5408\u6750\u6599\u5728\u66b4\u9732\u4e8e\u8fd8\u539f\u6c14\u4f53\u548c\u6c27\u5316\u6c14\u4f53\u65f6\u8868\u73b0\u51fa\u4e0d\u540c\u7684\u6c14\u654f\u4f20\u611f\u7c7b\u578b\u3002\u5728\u4e0d\u540c\u80cc\u666f\u6c14\u6c1b\u4e0b\u7684\u4f20\u611f\u54cd\u5e94\u53caDFT\u8ba1\u7b97\u7ed3\u679c\u8868\u660e\uff0cNH3<\/sub>\u6c14\u4f53\u4e3b\u8981\u88ab\u5438\u9644\u5728\u5f02\u8d28\u7ed3\u4e0a\u4e0e\u8868\u9762\u5438\u9644\u6c27\u53cd\u5e94\uff0c\u8868\u73b0\u51fan\u578b\u6c14\u654f\u4f20\u611f\u6027\u80fd\u3002\u7136\u800c\uff0cNO2<\/sub>\u6c14\u4f53\u4e3b\u8981\u88ab\u5438\u9644\u5728rGO\u8868\u9762\u5438\u5f15\u7535\u5b50\uff0c\u8868\u73b0\u51fap\u578b\u4f20\u611f\u884c\u4e3a\u3002\u8be5\u9879\u5de5\u4f5c\u4ee5\u6807\u9898\u4e3a\u201d\u00a0<\/b><\/strong>Investigation of p-n sensing transition and related highly sensitive NH<\/b><\/strong>3<\/b><\/sub><\/strong>\u00a0gas sensing behavior of SnP<\/b><\/strong>x<\/b><\/sub><\/strong>\/rGO composites\u201d,<\/b><\/strong>\u53d1\u8868\u5728\u671f\u520aChemical Engineering Journal\u4e0a\u3002<\/p>\n

\"\"<\/p>\n

03 [\u6838\u5fc3\u521b\u65b0\u70b9<\/b><\/strong>]<\/b><\/strong><\/p>\n

1. \u7531\u4e8eNH3<\/sub>\u4e0eNO2<\/sub>\u5728SnPx<\/sub>\/rGO\u8868\u9762\u7684\u5438\u9644\u80fd\u53ca\u5bfc\u7535\u901a\u9053\u4e0d\u540c\uff0c\u4f20\u611f\u5668\u5bf9\u8fd8\u539f\u6027\u53ca\u6c27\u5316\u6027\u6c14\u4f53\u8868\u73b0\u51fa\u4e0d\u540c\u7684p-n\u54cd\u5e94\u5c5e\u6027\u3002<\/p>\n

2.NH3<\/sub>-TPD\u548cDRIFTs\u5206\u6790\u7ed3\u679c\u63ed\u793a\u4e86NH3<\/sub>\u6c14\u4f53\u5728SnPx<\/sub>\/rGO\u8868\u9762\u7684\u5438\u9644\u4e3a\u7269\u7406\u5438\u9644\uff0c\u4e14\u5728\u5ba4\u6e29\u4e0b\u53ef\u4ee5\u5b8c\u5168\u7684\u8131\u9644\u3002<\/p>\n

3.SG-5\u5bf9\u4f4e\u6d53\u5ea6\u7684NH3<\/sub>\u6c14\u4f53\u8868\u73b0\u51fa\u9ad8\u54cd\u5e94\u6027\uff08\u54cd\u5e94\u503c\uff1a500 ppb NH3<\/sub>\u4e0b\u54cd\u5e943%\uff09\u548c\u8f83\u4f4e\u7684\u68c0\u6d4b\u6781\u9650\uff08LOD\uff1a43.6 ppb\uff09\u3002<\/p>\n

04 <\/b><\/strong>[<\/b><\/strong>\u6570\u636e\u6982\u89c8<\/b><\/strong>]<\/b><\/strong><\/p>\n

\"\"<\/p>\n

\u56fe1.\u00a0SG-5 (a)\u3001SG-10 (b)\u548cSG-15 (c)\u4f20\u611f\u5668\u5728\u5ba4\u6e29\u4e0b\u5bf9NH3<\/sub>\u7684\u52a8\u6001\u4f20\u611f\u6027\u80fd\u3002\u4f20\u611f\u54cd\u5e94\u968fNH3<\/sub>\u6d53\u5ea6\u7684\u53d8\u5316(d)(\u9644\u56fe\u4e3a\u5bf9\u4f4e\u6d53\u5ea6NH3<\/sub>\u6c14\u4f53\u7684\u54cd\u5e94)\u3002SG-5\u5bf910 ppm NH3<\/sub>\u6c14\u4f53(e)\u548c10 ppm NO2<\/sub>\u6c14\u4f53(f)\u5728RT\u4e0b\u7684\u54cd\u5e94-\u6062\u590d\u8fc7\u7a0b\u3002\u00a0<\/p>\n

\"\"<\/p>\n

\u56fe2.SnPx<\/sub>\/rGO\u7684\u6c14\u654f\u54cd\u5e94\u673a\u5236(a)\u53ca\u80fd\u5e26\u7ed3\u6784(b-d)<\/p>\n

\"\"<\/p>\n

\u56fe3.\u00a0\u7a7a\u6c14\u3001O2<\/sub>\u548cN2<\/sub>\u80cc\u666f\u4e0bSG-5\u5bf910 ppm NH3<\/sub>\u00a0(a-c)\u548c10 ppm NO2<\/sub>\u00a0(d-f)\u7684\u54cd\u5e94\u5faa\u73af\u66f2\u7ebf\u3002<\/p>\n

0<\/b><\/strong>5 [\u6210\u679c\u542f\u793a<\/b><\/strong>]<\/b><\/strong><\/p>\n

\u7ed3\u679c\u8868\u660e\uff0cSG-5\u590d\u5408\u6750\u6599\u5728RT\u4e0b\u5bf940 ppm NH3<\/sub>\u5177\u6709\u6700\u5927\u7684\u4f20\u611f\u54cd\u5e94(117.5%)\uff0cLOD\u4e3a44.6 ppb\u3002\u901a\u8fc7TPD\u548c\u539f\u4f4dDRIFT\u8bc1\u5b9e\u4e86NH3<\/sub>\u6c14\u4f53\u5728\u6750\u6599\u8868\u9762\u7684\u7269\u7406\u5438\u9644\u3002\u6b64\u5916\uff0c\u7531\u4e8e\u5438\u9644\u4f4d\u70b9\u548c\u5bfc\u7535\u901a\u9053\u7684\u4e0d\u540c\uff0c\u8be5\u4f20\u611f\u6750\u6599\u5bf9\u8fd8\u539f\u6027\u548c\u6c27\u5316\u6027\u6c14\u4f53\u4e5f\u663e\u793a\u51fa\u76f8\u53cd\u7684\u4f20\u611f\u7c7b\u578b\u3002\u4e0d\u540c\u80cc\u666f\u6c14\u4f53\u6c14\u6c1b\u4e0b\u7684\u6c14\u654f\u7ed3\u679c\u7ed3DFT\u8ba1\u7b97\u8868\u660e\uff0cNH3<\/sub>\u4e3b\u8981\u5438\u9644\u5728\u5f02\u8d28\u7ed3\u4e0a\uff0c\u5e76\u4e0e\u8868\u9762\u5438\u9644\u7684\u6c27\u53d1\u751f\u53cd\u5e94\u3002NO2<\/sub>\u4e3b\u8981\u5438\u9644\u5728\u8fd8\u539f\u6c27\u5316\u77f3\u58a8\u70ef\u8868\u9762\u4ee5\u5438\u5f15\u7535\u5b50\u3002<\/p>\n

\u539f\u6587\u8be6\u60c5\uff1aYao Fu, Tongkai Wang, Xiao Wang*, Xixi Li, Yuli Zhao, Feifei Li, Gang Zhao, Xijin Xu* \uff0cInvestigation of p-n sensing transition and related highly sensitive NH3<\/sub>\u00a0gas sensing behavior of SnPx\/rGO composites\uff0cChemical Engineering Journal 471 (2023) 144499<\/p>\n

DOI: https:\/\/doi.org\/10.1016\/j.cej.2023.144499<\/p>\n

\u56e2\u961f\u4ecb\u7ecd<\/p>\n

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\n 1.Xixi Li, Xiao Wang<\/strong>*, Yuli Zhao, Tongkai Wang, Yao Fu, Feifei Li, Gang Zhao, Xijin Xu<\/b><\/strong>*\uff0cCoP decorated SnS2<\/sub>nanosheets with synergistic electronic and electrocatalysis sensitization for enhanced room temperature NO2<\/sub>\u00a0sensing, Sensors & Actuators: B. Chemical 389 (2023) 133883 \u00a0
\n 2.Tongkai Wang, Xiaojuan Li, Chuanlin Li, Na Li, Xiao Wang<\/strong>*,\u00a0Xijin Xu<\/b><\/strong>*, Multifunctional SnPx\/GO composites for fully integrated and self-powered gas sensing system for NO2<\/sub>\u00a0detection, Sensors & Actuators: B. Chemical 382 (2023) 133507.
\n 3.Xiao Wang<\/strong>*, Wenjing Liu, Tongkai Wang, Yuli Zhao, Gang Zhao, Shouwei Zhang, Jinzhao Huang, Xijin Xu<\/b><\/strong>*, Synthesis of multishelled SnOx<\/sub>\/Co3<\/sub>O4<\/sub>amorphous\/crystalline heterophase with galvanic replacement reaction for superior HCHO sensing, Sensors and Actuators: B. Chemical, 2022, 350, 130876<\/p>\n","protected":false},"excerpt":{"rendered":"

01 [\u5bfc\u8bfb] SnPx\u5177\u6709\u5206\u5c42\u6676\u4f53\u7ed3\u6784\uff0c\u7531\u4ea4\u66ff\u6392\u5217\u7684Sn\u548cP\u5c42\u7ec4\u6210\uff0c\u4f7f\u5916\u90e8\u79bb\u5b50\u6613\u4e8e\u63d2\u5165\uff0c\u8fdb\u4e00\u6b65\u66b4\u9732\u66f4\u591a\u7684\u8868\u9762\u53cd\u5e94\u6d3b\u6027\u4f4d\u70b9\u3002\u6b64\u5916\uff0c\u7531\u4e8eP\u539f\u5b50\u6bd4\u91d1\u5c5e\u539f\u5b50\u7535\u8d1f\u6027\u9ad8\uff0c…<\/p>\n","protected":false},"author":2,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[215],"tags":[],"class_list":["post-252835","post","type-post","status-publish","format-standard","hentry","category-jiedu"],"_links":{"self":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/252835"}],"collection":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/users\/2"}],"replies":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=252835"}],"version-history":[{"count":4,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/252835\/revisions"}],"predecessor-version":[{"id":252845,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/252835\/revisions\/252845"}],"wp:attachment":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=252835"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=252835"},{"taxonomy":"post_tag","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=252835"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}