{"id":252620,"date":"2023-07-05T05:48:46","date_gmt":"2023-07-04T21:48:46","guid":{"rendered":"\/\/m.iemloyee.com\/?p=252620"},"modified":"2023-07-04T14:55:23","modified_gmt":"2023-07-04T06:55:23","slug":"j-chem-eng-%e9%ab%98%e4%ba%a7%e9%87%8f%e5%b9%b2%e6%b3%95%e5%88%b6%e5%a4%87%e9%ab%98%e6%80%a7%e8%83%bd%e9%94%82%e7%a6%bb%e5%ad%90%e7%94%b5%e6%b1%a0%e7%94%b5%e6%9e%81","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=252620","title":{"rendered":"J. Chem. Eng.: \u9ad8\u4ea7\u91cf\u5e72\u6cd5\u5236\u5907\u9ad8\u6027\u80fd\u9502\u79bb\u5b50\u7535\u6c60\u7535\u6781"},"content":{"rendered":"

\u7814\u7a76\u80cc\u666f<\/i><\/b><\/em><\/strong><\/p>\n

\u4e3a\u4e86\u66f4\u597d\u5730\u7f13\u89e3\u6c7d\u8f66\u4ea7\u751f\u7684\u78b3\u6392\u653e\uff0c\u9502\u79bb\u5b50\u7535\u6c60\u7535\u52a8\u6c7d\u8f66\u5df2\u5f62\u6210\u4e86\u4e00\u79cd\u8d8b\u52bf\u3002\u76ee\u524d\u9502\u79bb\u5b50\u7535\u6c60\u7535\u6781\u5747\u7531\u6e7f\u6cd5\u5236\u5907\uff0c\u56e0\u6b64\u4f1a\u5bfc\u81f4\u7c98\u5408\u5242\u8fc1\u79fb\u5e76\u4ea7\u751f\u4e00\u7cfb\u5217\u7535\u6781\u673a\u68b0\u6027\u80fd\u7535\u5316\u5b66\u6027\u80fd\u65b9\u9762\u7684\u95ee\u9898\uff0c\u4e0d\u80fd\u5f88\u597d\u5730\u6ee1\u8db3\u672a\u6765\u5927\u89c4\u6a21\u751f\u4ea7\u9ad8\u8d1f\u8f7d\u7535\u6781\u7684\u9700\u6c42\u3002 \u53e6\u5916\u6e7f\u6cd5\u5236\u5907\u7535\u6781\u8fc7\u7a0b\u5fc5\u4e0d\u53ef\u5c11\u7684\u6d46\u6599\u6d82\u5236\u548c\u70d8\u5e72\u5360\u751f\u4ea7\u6210\u672c\u7684\u8fd111.5%\u548c\u603b\u80fd\u91cf\u6d88\u8017\u768446%\u4ee5\u4e0a\u3002\u56e0\u6b64\uff0c\u5de5\u4e1a\u5c4a\u8feb\u5207\u9700\u8981\u7814\u53d1\u80fd\u591f\u5927\u89c4\u6a21\u751f\u4ea7\u9502\u7535\u7535\u6781\u7684\u65b0\u4e00\u4ee3\u5236\u5907\u65b9\u6cd5\uff0c\u79d1\u7814\u4eba\u5458\u5f00\u59cb\u8003\u8651\u548c\u63a2\u7d22\u9502\u7535\u7535\u6781\u5e72\u6cd5\u5236\u5907\u5de5\u827a\u3002<\/p>\n

\u7f8e\u56fdMaxwell Technologies\u516c\u53f8\u5f00\u53d1\u4e86Maxwell\u578b\u7684\u5e72\u6df7-\u6eda\u538b\u5236\u5907\u6cd5\uff0c\u663e\u73b0\u51fa\u6765\u5f88\u597d\u7684\u5de5\u4e1a\u5316\u524d\u666f\u3002\u5982\u56fe1\u6240\u793a,\u8be5\u65b9\u6cd5\u5305\u62ec\u4e863\u4e2a\u7b80\u5355\u6b65\u9aa4\uff1a\uff081\uff09\u5e72\u6df7\u7535\u6781\u539f\u6599\u5e76\u9884\u7ea4\u7ef4\u5316\u7279\u5bcc\u9f99(\u805a\u56db\u6c1f\u4e59\u70ef)\u7c98\u5408\u5242\uff1b\uff082\uff09\u5c06\u5e72\u6df7\u540e\u7684\u7c89\u4f53\u6df7\u5408\u7269\u6eda\u538b\u6210\u81ea\u652f\u6491\u7535\u6781\uff1b\uff083\uff09\u628a\u81ea\u652f\u6491\u7535\u6781\u538b\u5408\u5230\u96c6\u6d41\u4f53\u4e0a\u3002\u7531\u4e8e\u6448\u5f03\u4e86\u6eb6\u5242\u3001\u6d82\u6599\u673a\u548c\u9ad8\u6e29\u5e72\u71e5\uff0c\u8be5\u5e72\u6cd5\u5236\u5907\u5de5\u827a\u53ef\u4ee5\u5b9e\u73b0\u4f4e\u6210\u672c\u8282\u80fd\u7684\u9502\u7535\u751f\u4ea7\u3002\u4e0d\u4ec5\u5982\u6b64\uff0c\u8be5\u5236\u5907\u5de5\u827a\u8fd8\u53ef\u4ee5\u6709\u6548\u907f\u514d\u9ad8\u8d1f\u8f7d\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u7535\u6781\u4e2d\u666e\u904d\u5b58\u5728\u7684\u7c98\u5408\u5242\u8fc1\u79fb\u95ee\u9898\uff0c\u8fdb\u800c\u53ef\u5b9e\u73b0\u9ad8\u6027\u80fd\u9502\u7535\u6c60\u3002<\/p>\n

\u4f46\u662f\u79d1\u5b66\u754c\u672a\u80fd\u5bf9\u8be5\u5e72\u6cd5\u5236\u5907\u5de5\u827a\u76f8\u5173\u7684\u751f\u4ea7\u5236\u5907\u6280\u672f\u7ec6\u8282\u53ca\u5176\u5f71\u54cd\u8fdb\u884c\u5145\u5206\u7684\u7814\u7a76\u5206\u6790\uff0c\u4e3a\u4e86\u5f25\u8865\u8fd9\u65b9\u9762\u7684\u7406\u8bba\u7a7a\u767d\uff0c\u6a61\u6811\u5cad\u56fd\u5bb6\u5b9e\u9a8c\u5ba4\u7684\u9502\u7535\u6c60\u751f\u4ea7\u5236\u9020\u5b66\u4e13\u5bb6Jianlin Li\u535a\u58eb\u548c\u6750\u6599\u5316\u5b66\u4e13\u5bb6Runming Tao\u7b49\u591a\u4f4d\u79d1\u7814\u4eba\u5458\u5f00\u5c55\u4e86\u6df1\u5165\u7684\u7814\u7a76\uff0c\u521b\u65b0\u6027\u5730\u5bf9\u5e72\u6cd5\u5236\u5907\u7684\u7535\u6781\u7684\u7ed3\u6784\u3001\u7535\u5316\u5b66\u52a8\u529b\u5b66\u3001\u949d\u5316\u819c\u8fdb\u884c\u4e86\u7cfb\u7edf\u7684\u7814\u7a76\uff0c\u5e76\u5bf9\u6bd4\u4e86\u4f20\u7edf\u6e7f\u6cd5\u5236\u5907\u7684\u7535\u6781\u3002\u6210\u679c\u201cHigh-T<\/b><\/strong>h<\/b><\/strong>roughput and High-Performance Lithium-Ion Batteries via Dry Processing<\/b><\/strong>\u201d\u53d1\u8868\u5728\u56fd\u9645\u9876\u5c16\u5316\u5de5\u671f\u520aChemical Engineering Journal<\/i><\/em>\u4e0a\u3002<\/p>\n

\"\"<\/p>\n

Figure 1. Schematic demonstration of the dry processing based on dry-powder mixing and rolling\/calendering.<\/p>\n

\u7814\u7a76\u4eae\u70b9<\/i><\/b><\/em><\/strong><\/p>\n

1.\u5e72\u6cd5\u5236\u5907\u5de5\u827a\u5bf9\u7535\u6781\u7ed3\u6784\u7684\u5f71\u54cd<\/p>\n

2.\u7814\u7a76\u5e72\u6cd5\u5236\u5907\u7684\u7535\u6781\u7684\u7535\u5316\u5b66\u52a8\u529b\u5b66<\/p>\n

3.\u9996\u6b21\u8fdb\u884c\u4e86\u5168\u7535\u6c60\u7814\u7a76\uff08\u6b63\u8d1f\u6781\u5747\u4e3a\u5e72\u6cd5\u5236\u5907\u7684\u7535\u6781\uff09<\/p>\n

4.\u5206\u6790\u5e72\u6cd5\u5236\u5907\u7684\u7535\u6781\u4e0a\u7684\u949d\u5316\u819c\u5316\u5b66\u7ec4\u5206<\/p>\n

5.\u5e72\u6cd5\u5236\u5907\u5de5\u827a\u5728\u6750\u6599\u548c\u751f\u4ea7\u8bbe\u5907\u65b9\u9762\u7684\u666e\u9002\u6027\u63a2\u7a76<\/p>\n

\u56fe\u6587\u5bfc\u8bfb<\/i><\/b><\/em><\/strong><\/p>\n

\"\"\u200d<\/i><\/b><\/em><\/strong><\/p>\n

Figure 2. SEM images of DP- Gr and NMC622 electrodes. (a-d). Low- and high-magnification top view and cross-sectional view of Gr electrode, respectively. (e-h). Low- and high-magnification top view and cross-sectional view of NMC622 electrode, respectively.<\/p>\n

\u56fe2\u5c55\u793a\u4e86\u5e72\u6cd5\u5236\u5907\u7684\u77f3\u58a8\uff08DP-Gr\uff09\u8d1f\u6781\u548cNMC622\uff08DP-NMC622\uff09\u6b63\u6781\u7684\u8868\u9762\u548c\u6a2a\u622a\u9762\u626b\u63cf\u7535\u955c\u56fe\u7247\u3002\u901a\u8fc7\u56fe\u7247\uff0c\u53ef\u4ee5\u5f88\u6e05\u695a\u7684\u770b\u5230\u5728DP-Gr\u8d1f\u6781\u7684\u8868\u9762\u548c\u6a2a\u622a\u9762\u5747\u6709\u4e30\u5bcc\u7684\u805a\u56db\u6c1f\u4e59\u70ef\u7ea4\u7ef4\u3002DP-NMC622\u6b63\u6781\u8868\u9762\u4e0aNMC622\u4e8c\u7ea7\u9897\u7c92\u5747\u57fa\u672c\u7834\u788e\u6210\u4e3a\u9996\u7ea7\u9897\u7c92\uff0c\u5176\u8868\u9762\u6ca1\u6709\u592a\u591a\u805a\u56db\u6c1f\u4e59\u70ef\u7ea4\u7ef4\uff0c\u76f8\u53cd\u5176\u7535\u6781\u5185\u90e8\u5374\u8fd8\u662f\u6709\u7740\u5927\u91cf\u7684\u805a\u56db\u6c1f\u4e59\u70ef\u7ea4\u7ef4\u3002\u53e6\u5916\u6a2a\u622a\u9762\u626b\u63cf\u7535\u955c\u56fe\u7247\u8868\u660eDP-Gr\u8d1f\u6781\u548cDP-NMC622\u6b63\u6781\u7684\u539a\u5ea6\u5206\u522b\u4e3a154\u5fae\u7c73\u548c115\u5fae\u7c73\u3002<\/p>\n

\"\"<\/p>\n

Figure 3. (a and b). EIS Nyquist plots of the prepared Gr and NMC622 electrodes, respectively. The R<\/i><\/em>t<\/i><\/sub><\/em>\u00a0value is obtained from the interception point of the red-color extrapolation in the low-frequency region and the horizontal axis. (c and d). Bar graphs of the porosity and tortuosity of the obtained various electrodes, respectively.<\/p>\n

\u968f\u540e\u79d1\u7814\u4eba\u5458\u5229\u7528\u5bf9\u79f0\u7535\u6c60\u8bc4\u4f30\u4e86DP-Gr\u8d1f\u6781\u548cDP-NMC622\u6b63\u6781\u7684\u5b54\u7387\u548c\u5f2f\u66f2\u7387\u3002\u7814\u7a76\u8868\u660e\u5728\u76f8\u540c\u8d1f\u8f7d\u91cf\uff08Gr\u7535\u6781\u548cNMC622\u7535\u6781\u7684\u8d1f\u8f7d\u91cf\u5206\u522b\u4e3a6.6 mAh cm-2<\/sup>\u548c6.0 mAh cm-2<\/sup>\uff09\u548c\u76f8\u540c\u7535\u6781\u539a\u5ea6\u7684\u60c5\u51b5\u4e0b\uff0c\u5e72\u6cd5\u5236\u5907\u7684\u6b63\u8d1f\u6781\u5747\u6bd4\u4f20\u7edf\u6e7f\u6cd5\u5236\u5907\u7684\u6b63\u8d1f\u6781\uff08C-Gr\u548cC-NMC622\uff09\u6709\u7740\u660e\u663e\u8f83\u5c0f\u7684\u5f2f\u66f2\u7387\u3002\u8be5\u7ed3\u679c\u610f\u5473\u7740\u5e72\u6cd5\u5236\u5907\u7684\u7535\u6781\u6709\u7740\u66f4\u901a\u7545\u7684\u7535\u5316\u5b66\u52a8\u529b\u5b66\u6027\u80fd\u3002<\/p>\n

\"\"<\/p>\n

Figure 4. Electrochemical performance of the DP-Gr anode and DP-NMC622 cathode in half-cells. (a). DP-Gr discharge\/charge profile at a current density of 0.1 C. (b). Rate performance of DP-Gr and C-Gr. (c). DP-Gr and C-Gr cyclic performance at 0.2 C. (d). DP-NMC622 charge\/discharge profile at a current density of 0.1 C. (e). Rate performance of DP-NMC622 and C-NMC622. (f). DP-NMC622 and C-NMC622 cyclic performance at 0.2 C.<\/p>\n

\u5982\u56fe4a\u6240\u793a\uff0cDP\u2014Gr\u7535\u6781\u7684\u9996\u5708\u5e93\u4f26\u6548\u7387\u5e76\u4e0d\u662f\u5f88\u7406\u60f3\u3002\u8fd9\u4e3b\u8981\u662f\u7531\u805a\u56db\u6c1f\u4e59\u70ef\u5728\u4f4e\u7535\u52bf\u4e0b\u7684\u526f\u53cd\u5e94\u6240\u9020\u6210\u7684\u3002\u56fe4b\u548c4c\u8868\u660eDP\u2014Gr\u6709\u7740\u53ef\u4ee5\u5ab2\u7f8eC-Gr\u7684\u7535\u5316\u5b66\u6027\u80fd\uff0c\u800c\u57fa\u4e8e\u805a\u56db\u6c1f\u4e59\u70ef\u7684DP\u2014NMC622\u5219\u6709\u7740\u5f88\u597d\u7684\u9996\u5708\u5e93\u4f26\u6548\u7387\uff08\u56fe4d\uff09\u3002\u53e6\u5916\uff0c\u5982\u56fe4e\u6240\u793a\uff0cDP\u2014NMC622\u6bd4\u8d77C\u2014NMC622\u6709\u7740\u66f4\u9ad8\u7684\u500d\u7387\u6027\u80fd\uff0c\u7279\u522b\u662f\u57280.5C\u548c1C\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\u3002\u56fe4f\u5219\u663e\u793a\u4e86DP\u2014NMC622\u548cC\u2014NMC622\u4e00\u6837\u6709\u7740\u826f\u597d\u7684\u5faa\u73af\u6027\u3002<\/p>\n

\"\"<\/p>\n

Figure 5. HRXPS spectra of the cycled DP-Gr and DP-NMC622 electrodes. (a-c). C-1s, F-1s and P-2p HRXPS spectra of the cycled DP-Gr anode. (d-f). C-1s, F-1s and P-2p HRXPS spectra of the cycled DP-NMC622 cathode.<\/p>\n

\u56fe5\u663e\u793a\u4e86DP-Gr\u7535\u6781\u548cDP-NMC622\u7535\u6781\u7684SEI\u548cCEI\u949d\u5316\u819c\u7ec4\u5206\u3002HRXPS\u5206\u6790\u7ed3\u679c\u8868\u660e\u5e72\u6cd5\u5236\u5907\u7684\u7535\u6781\u548c\u4f20\u7edf\u6e7f\u6cd5\u5236\u5907\u7684\u7535\u6781\u5728\u949d\u5316\u819c\u6210\u5206\u65b9\u9762\u6709\u7740\u660e\u663e\u533a\u522b\u3002<\/p>\n

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Figure 6. DP electrode electrochemical performance studies in full-cells. (a). Charge\/discharge profile at a current density of 0.1 C. (b-c). rate capability test and cyclic performance study of the full-cells after aging at a current density of 0.1 C for three cycles, respectively.<\/p>\n

\u56fe6\u5c55\u793a\u4e86\u7531DP-Gr\u4e0eDP-NMC622\u7ec4\u6210\u7684\u5168\u7535\u6c60\u7684\u6027\u80fd\u3002\u57280.2C\u00a0(1 C = 180 mA g-1<\/sup>)\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff08\u56fe6a\uff09\uff0c\u7535\u6c60\u8d21\u732e\u4e86108.2 mAh g-1<\/sup>\u7684\u6bd4\u5bb9\u91cf\uff0c\u53e6\u5916\u6240\u5f97\u7684\u7535\u538b\u5e73\u53f0\u57283.7 V\u3002\u8fd9\u610f\u5473\u7740\u8be5\u5168\u7535\u6c60\u5728\u7535\u6781\u5c3a\u5ea6\u6709\u7740227.2 Wh\/kg\u7684\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u3002\u5982\u56fe6b\u6240\u793a\uff0c\u57280.33 C\u30010.5 C\u30011 C\u30012 C\u30013 C \u7684\u9ad8\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0c\u6240\u68c0\u6d4b\u5230\u7684\u5e73\u5747\u653e\u7535\u6bd4\u5bb9\u91cf\u5206\u522b\u4e3a\u00a095.9 mAh g-1<\/sup>\u300171.0 mAh g-1<\/sup>\u300128.0 mAh g-1<\/sup>\u30015.1 mAh g-1<\/sup>\u30013.2 mAh g-1<\/sup>\u3002\u56fe6c\u5c55\u73b0\u4e86\u57fa\u4e8e\u5e72\u6cd5\u5236\u5907\u7535\u6781\u7684\u5168\u7535\u6c60\u57280.2 C\u7535\u6d41\u5bc6\u5ea6\u7684\u957f\u6548\u5faa\u73af\u6027\uff0c\u5728\u7b2c400\u5708\u548c\u7b2c800\u5708\u8be5\u5168\u7535\u6c60\u7cfb\u7edf\u5206\u522b\u6709\u774074.1 %\u548c63.6 % \u7684\u5bb9\u91cf\u4fdd\u6301\u7387\u3002<\/p>\n

\u603b\u7ed3\u4e0e\u5c55\u671b<\/i><\/b><\/em><\/strong><\/p>\n

\u6839\u636e\u4ee5\u4e0a\u6240\u5f97\u7ed3\u679c\u4e0e\u5206\u6790\uff0c\u8be5\u7814\u7a76\u9996\u6b21\u8bc1\u660e\u9502\u7535\u7535\u6781\u5e72\u6cd5\u5236\u5907\u5de5\u827a\u8f83\u6e7f\u6cd5\u5236\u5907\u5de5\u827a\u800c\u8a00\u5728\u591a\u65b9\u9762\u6709\u7740\u5f88\u660e\u663e\u7684\u4f18\u52bf\u3002\u9996\u5148\u5e72\u6cd5\u5236\u5907\u5de5\u827a\u5bf9\u751f\u4ea7\u8bbe\u5907\u548c\u539f\u6599\u6709\u7740\u826f\u597d\u7684\u666e\u9002\u6027\uff1b\u5176\u6b21\uff0c\u53ef\u4ee5\u5927\u5e45\u51cf\u5c11\u9502\u7535\u7535\u6781\u751f\u4ea7\u6210\u672c\u548c\u80fd\u91cf\u6d88\u8017\uff1b\u7b2c\u4e09\uff0c\u7531\u4e8e\u805a\u56db\u6c1f\u4e59\u70ef\u7c98\u5408\u5242\u7684\u7ea4\u7ef4\u5316\u52a0\u4e0a\u907f\u514d\u4e86\u6eb6\u5242\u7684\u4f7f\u7528\uff0c\u5e72\u6cd5\u5236\u5907\u7684\u7535\u6781\u6709\u7740\u5f88\u597d\u7684\u673a\u68b0\u6027\u80fd\u548c\u66f4\u4e3a\u5747\u4e00\u81f4\u5bc6\u7684\u5185\u90e8\u7ed3\u6784\uff0c\u4ece\u800c\u5b9e\u73b0\u4e86\u4f18\u826f\u7684\u7535\u6c60\u6027\u80fd\u3002\u4f46\u662f\uff0c\u805a\u56db\u6c1f\u4e59\u70ef\u4f5c\u4e3a\u7c98\u5408\u5242\u5728\u77f3\u58a8\u8d1f\u6781\u65b9\u9762\u8fd8\u5b58\u5728\u660e\u663e\u7684\u77ed\u677f\uff0c\u8fd9\u4e5f\u63d0\u51fa\u4e86\u5bf9\u7814\u53d1\u65b0\u7c98\u5408\u5242\u7684\u9700\u6c42\u3002\u7efc\u4e0a\u6240\u8ff0\uff0c\u8be5\u7814\u7a76\u4e0d\u4ec5\u521b\u65b0\u6027\u5730\u63d0\u51fa\u4e86\u4e00\u79cd\u9ad8\u6548\u7535\u6781\u5236\u5907\u7684\u65b9\u6cd5\uff0c\u800c\u4e14\u8fd8\u5efa\u7acb\u4e86\u5bf9\u805a\u56db\u6c1f\u4e59\u70ef\u7c98\u5408\u5242\u526f\u53cd\u5e94\u548c\u949d\u5316\u819c\u7684\u7406\u8bba\u8ba4\u77e5\u3002<\/p>\n

\u6587\u732e\u4fe1\u606f<\/p>\n

High-Throughput and High-Performance Lithium-Ion Batteries via Dry Processing. Chem. Eng. J. <\/em>2023<\/strong>, 144300<\/p>\n

DOI\uff1a10.1016\/j.cej.2023.144300<\/p>\n

\u539f\u6587\u94fe\u63a5\uff1ahttps:\/\/doi.org\/10.1016\/j.cej.2023.144300<\/p>\n","protected":false},"excerpt":{"rendered":"

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