{"id":248798,"date":"2023-04-03T05:46:49","date_gmt":"2023-04-02T21:46:49","guid":{"rendered":"\/\/m.iemloyee.com\/?p=248798"},"modified":"2023-03-31T15:47:03","modified_gmt":"2023-03-31T07:47:03","slug":"nat-commun%e7%94%a8%e4%ba%8e%e7%9b%b4%e6%8e%a5%e4%b9%99%e9%86%87%e7%87%83%e6%96%99%e7%94%b5%e6%b1%a0%e7%9a%84pd-conc%e7%9a%84%e7%95%8c%e9%9d%a2%e5%8d%8f%e5%90%8c%e4%bd%9c%e7%94%a8%e5%92%8c%e5%b7%a5","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=248798","title":{"rendered":"Nat.Commun:\u7528\u4e8e\u76f4\u63a5\u4e59\u9187\u71c3\u6599\u7535\u6c60\u7684Pd\/Co@NC\u7684\u754c\u9762\u534f\u540c\u4f5c\u7528\u548c\u5de5\u7a0b"},"content":{"rendered":"

\u4e00\u3001\u3010\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

\u00a0 \u00a0\u76f4\u63a5\u4e59\u9187\u71c3\u6599\u7535\u6c60\uff08DEFC\uff09\u4f5c\u4e3a\u65e0\u6bd2\u3001\u4f4e\u8150\u8680\u6027\u3001\u9ad8\u80fd\u91cf\u5bc6\u5ea6\u548c\u529f\u7387\u5bc6\u5ea6\u7684\u80fd\u91cf\u8f6c\u6362\u88c5\u7f6e\u5f97\u5230\u4e86\u5e7f\u6cdb\u7684\u7814\u7a76\u3002DEFC\u4e3b\u8981\u7531\u4e59\u9187\u6c27\u5316\u53cd\u5e94\uff08EOR\uff09\u548c\u6c27\u8fd8\u539f\u53cd\u5e94\uff08ORR\uff09\u7ec4\u6210\u3002\u94c2\uff08Pt\uff09\u65cf\u91d1\u5c5e\uff08PGM\uff09\u57fa\u50ac\u5316\u5242\u56e0\u5176\u6700\u4f73\u7535\u5b50\u7ed3\u6784\u800c\u88ab\u5e7f\u6cdb\u5f00\u53d1<\/a>\u7528\u4e8e<\/a>DEFC\u4e2d\u3002\u7136\u800c\uff0cPGM\u7684\u9ad8\u6210\u672c\u3001\u7a00\u6709\u6027\u3001\u53cd\u5e94\u52a8\u529b\u5b66\u7f13\u6162\u3001EOR\u4e0d\u5b8c\u5168\u548c\u50ac\u5316\u5242\u4e2d\u6bd2\u7b49\u56e0\u7d20\uff0c\u5bfc\u81f4DEFC\u7684\u5e7f\u6cdb\u5546\u4e1a\u5316\u53d7\u5230\u4e25\u91cd\u7684\u963b\u788d\u3002\u7814\u7a76\u53d1\u73b0\u94af\uff08Pd\uff09\u57fa\u50ac\u5316\u5242\u5728\u78b1\u6027\u4e2d\u5177\u6709\u548cPGM\u76f8\u5f53\u7684\u7535\u50ac\u5316EOR\u548cORR\u6d3b\u6027\u3002\u4f7f\u78b1\u6027DEFC\u5177\u6709\u53ef\u6269\u5c55\u7684\u5546\u4e1a\u5316\u524d\u666f\u3002\u7136\u800c\uff0cPd\u57fa\u50ac\u5316\u5242\u5728EOR\u4e2d\u901a\u8fc7\u4e0d\u5b8c\u5168\u7684C2-4e–<\/sup>\u9014\u5f84\u5c06\u4e59\u9187\u7535\u5316\u5b66\u8f6c\u5316\u6210\u918b\u9178\u76d0\uff0c\u8fd9\u4e25\u91cd\u7684\u5bfc\u81f4DEFC\u6027\u80fd\u4e0b\u964d\u3002\u56e0\u6b64\uff0c\u5408\u7406\u8bbe\u8ba1\u548c\u5f00\u53d1\u9ad8\u6d3b\u6027\u548c\u8010\u7528\u7684Pd\u57fa\u50ac\u5316\u5242\u4ee5\u5728\u9633\u6781\u8fdb\u884c\u5b8c\u5168\u7684\u4e59\u9187\u6c27\u5316\u53cd\u5e94\u548c\u5728\u9634\u6781\u8fdb\u884c\u52a0\u901f\u7684\u6c27\u8fd8\u539f\u53cd\u5e94\u4ecd\u7136\u5177\u6709\u6311\u6218\u6027\u3002<\/p>\n

\u4e8c\u3001\u3010\u6210\u679c\u63a0\u5f71\u3011<\/strong><\/span><\/p>\n

\u00a0 \u00a0<\/strong>\u8fd1\u65e5\uff0c\u4e2d\u4f5b\u7f57\u91cc\u8fbe\u5927\u5b66\u6768\u9633\u6559\u6388\u56e2\u961f\u63d0\u51fa\u4e00\u79cd\u754c\u9762\u8c03\u8282\u7b56\u7565\u3002\u6210\u529f\u5408\u6210\u51faPd\/Co@NC\u50ac\u5316\u5242\u5b9e\u73b0Pb\u548cCo@NC\u4e4b\u95f4\u7684\u754c\u9762\u534f\u540c\u4f5c\u7528\u3002Pd\/Co@NC\u63d0\u9ad8\u78b1\u6027\u6761\u4ef6\u4e0bEOR\u7684C1-12e–<\/sup>\u7535\u5b50\u8f6c\u79fb\u8def\u5f84\u9009\u62e9\u6027\u4ee5\u53ca\u7535\u50ac\u5316\u6d3b\u6027\/\u8010\u4e45\u6027\u3002\u76f8\u5173\u7684\u7814\u7a76\u6210\u679c\u4ee5\u201cInterface synergism and engineering of Pd\/Co@N-C for direct ethanol fuel cells<\/em><\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728Nature Communications<\/em><\/strong>\u4e0a\u3002<\/p>\n

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\u4e09\u3001\u3010\u6838\u5fc3\u521b\u65b0\u70b9\u3011<\/strong><\/span><\/p>\n

\u00a0 1<\/strong>\u3001\u4f5c\u8005\u901a\u8fc7\u4e00\u79cd\u5de7\u5999\u7684\u7ed3\u6784\u8bbe\u8ba1\u51fa\u5177\u6709\u754c\u9762<\/strong>\u534f\u540c\u4f5c\u7528\u7684<\/strong>Pd\/Co@NC\u50ac\u5316\u5242\u3002<\/strong>Co\u4fc3\u8fdb\u65e0\u5b9a\u5f62\u78b3\u5411\u9ad8\u5ea6\u77f3\u58a8\u5316\u78b3\u7684\u8f6c\u53d8\uff0c\u6709\u52a9\u4e8e\u5b9e\u73b0\u7a7a\u95f4\u9650\u5236\u6548\u5e94\uff0c\u4ece\u800c\u9632\u6b62\u50ac\u5316\u5242\u7684\u7ed3\u6784\u964d\u89e3\u3002<\/strong>Pd\u548cCo@NC\u754c\u9762\u7684\u5f3a\u50ac\u5316\u5242\u8f7d\u4f53\u548c\u7535\u5b50\u6548\u5e94\u8d4b\u4e88<\/strong>Pd\u7f3a\u7535\u5b50\u72b6\u6001\uff0c\u4ece\u800c\u589e\u5f3a\u7535\u5b50\u8f6c\u79fb\u5e76\u63d0\u9ad8\u6d3b\u6027<\/strong>\/<\/strong>\u8010\u4e45\u6027\u3002<\/strong><\/p>\n

\u00a0 2<\/strong>\u3001<\/strong>Pd\/Co@N-C<\/strong>\u754c\u9762\u7684\u7535\u5b50\u6548\u5e94\u589e\u5f3a\u4e86\u7535\u5b50\u76f4\u63a5\u5411<\/strong>C1-12e–<\/sup> EOR<\/strong>\u8def\u5f84\u7684\u8f6c\u79fb\u3002\u5177\u6709\u754c\u9762\u534f\u540c\u4f5c\u7528\u548c\u6574\u4f53\u7ed3\u6784\u6548\u5e94\u7684<\/strong>Pd\/Co@N-C<\/strong>\u5728<\/strong>DEFC<\/strong>\u4e2d\u63d0\u4f9b\u4e86<\/strong>439 mW cm\u22122<\/sup><\/strong>\u7684\u6700\u5927\u529f\u7387\u5bc6\u5ea6\u548c\u8d85\u8fc7<\/strong>1000<\/strong>\u5c0f\u65f6\u7684\u5de5\u4f5c\u65f6\u95f4\uff0c\u8fdc\u8fdc\u8d85\u8fc7\u4e86\u6700\u5148\u8fdb\u7684\u50ac\u5316\u5242\u3002<\/strong><\/p>\n

\u56db\u3001\u3010\u6570\u636e\u6982\u89c8\u3011<\/strong><\/span><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>1<\/strong> Pd\/Co@NC \u7684\u5408\u6210\u8fc7\u7a0b\u793a\u610f\u56fe\u3002(a)\u5408\u6210\u4e86\u6838\u58f3\u7ed3\u6784\u7684ZIF-67@ZIF-8\uff0c\u7ecf\u8fc7\u70ed\u89e3\u548c\u9178\u6d17\uff0c\u5f97\u5230\u4e86\u5177\u6709\u7a7a\u95f4\u9650\u57df\u6548\u5e94\u7684Co@NC\u3002\u901a\u8fc7\u539f\u4f4d\u5fae\u6ce2\u8fd8\u539f\u65b9\u6cd5\u5c06Pd \u8d1f\u8f7d\u5728Co@NC\u4e0a\uff0c\u5728Co@NC\u548cPd\u4e4b\u95f4\u5f62\u6210\u5f3a\u5927\u7684\u754c\u9762\u6548\u5e94\u3002(\u00a0b\u00a0) Co@NC \u548c (c) NC \u7684 TEM \u56fe\u50cf\u3002Co@NC \u548c NC \u7684\uff08d\uff09\u62c9\u66fc\u5149\u8c31\u548c\uff08e\uff09XRD\u56fe\u3002\uff08f\uff09 (BF)-STEM \u56fe\u50cf\u3002\uff08f\uff09\u91cc\u7684\u63d2\u56fe\u663e\u793a\u4e86 Pd\u7684\u653e\u5927STEM\u56fe\u50cf\u3002\uff08g\uff09\u00a0HAADF-STEM \u548c Pd\u3001Co \u548c N \u7684\u76f8\u5e94 EDS \u5143\u7d20\u6620\u5c04\u3002\uff08h\uff09Pd+Co@NC \u7684 HR-TEM\u3001HAADF-STEM \u548c\u76f8\u5e94\u7684 Pd \u548c Co \u7684 EDS \u5143\u7d20\u6620\u5c04\u3002\u00a92023 The Author(s)<\/p>\n

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\u56fe<\/strong>2<\/strong> Pd\u548cCo@NC\u4e4b\u95f4\u7684\u5f3a\u7535\u5b50\u6548\u5e94\u3002\uff08a\uff09\u00a0Pd 3d\u00a0XPS \u5149\u8c31\u3002\uff08b\uff09\u00a0Pd\/C\u3001Pd\/NC\u3001Pd\/Co@NC\u3001\u7269\u7406\u6df7\u5408 Pd+Co@NC\u548cCo@NC\u7684WF (\u0278)\u3002\uff08c\uff09Pd\u548cCo@NC\u4e4b\u95f4\u53d1\u751f\u7684\u7535\u5b50\u754c\u9762\u76f8\u4e92\u4f5c\u7528\u7684\u793a\u610f\u56fe\u3002\uff08d\uff09\u4e0d\u540c\u6837\u54c1\u57280.8 V\u00a0RHE\u4e0b\u7684\u4eb2\u6c27\u7279\u6027\u3002\uff08e\uff09\u542b\u6709 grapN\u3001pydN \u548c p-pydN \u7684\u6c2e\u63ba\u6742\u77f3\u58a8\u70ef\u5c42\u7684\u539f\u5b50\u7ed3\u6784\u3002\uff08f\uff09\u5341\u4e09\u539f\u5b50 Pd\u00a013\u7c07\u7684\u4f18\u5316\u539f\u5b50\u7ed3\u6784\u5438\u9644\u5728\u6c2e\u63ba\u6742\u77f3\u58a8\u70ef\u5c42\u7684\u4e0d\u540c N \u4f4d\u70b9\u4e0a\u3002\u00a92023 The Author(s)<\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>3<\/strong> Pd\/Co@NC \u5bf9\u7535\u50ac\u5316EOR\u6027\u80fd\u7684\u754c\u9762\u534f\u540c\u6548\u5e94\u3002\uff08a\uff09\u4e0d\u540c\u6837\u54c1\u4e0a\u7684 CO\u6c27\u5316\u5cf0\u3002\uff08b\uff09\u5f52\u4e00\u5316\u4e3a Pd\/C\u3001Pd\/NC\u3001Pd\/Co@NC \u548c Pd+Co@NC \u7684Pd\u8d1f\u8f7d\uff08\u5de6\uff09\u548c ECSA\uff08\u53f3\uff09\u7684\u5cf0\u7535\u6d41\u5bc6\u5ea6 (J\u00a0)\u00a0\u3002\uff08c\uff09\u00a0J\u4f5c\u4e3a\u626b\u63cf\u901f\u7387(v1\/2<\/sup>)\u7684\u5e73\u65b9\u6839\u7684\u51fd\u6570\u3002\uff08d\uff09\u4e0d\u540c\u6837\u54c1\u5728 0.6 V\u00a0RHE\u65f6\u7684\u7cfb\u7edf\u7535\u963b\uff08Rs<\/sub>\uff0c\u5de6\uff09\u548c\u7535\u8377\u8f6c\u79fb\u7535\u963b\uff08RCT<\/sub>\uff0c\u53f3\uff09\u3002\uff08e\uff09\u5de6\u8f74\uff1a500\u4e2a\u5faa\u73afAST\u4e4b\u524d\uff08\u5b9e\u7ebf\uff09\u548c\u4e4b\u540e\uff08\u865a\u7ebf\uff09\u7684EOR\u8d28\u91cf\u6d3b\u6027\u3002\u53f3\u8f74\uff1a Jafter<\/sub>\uff08AST\u540e\u7684\u8d28\u91cf\u6d3b\u5ea6\uff09\u5230 Jinitial<\/sub>\uff08AST \u524d\u7684\u521d\u59cb\u8d28\u91cf\u6d3b\u5ea6\uff09\u7684\u767e\u5206\u6bd4\u3002(f) \u5728\u4e0d\u540c\u7535\u52bf\u4e0bCO2<\/sub>\u7684\u6cd5\u62c9\u7b2c\u6548\u7387 (FE)\u00a0\u3002\u00a92023 The Author(s)<\/p>\n

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\u56fe<\/strong>4<\/strong> \u57fa\u4e8e\u539f\u4f4d ATR-SEIRAS \u6d4b\u91cf\u7684EOR\u53cd\u5e94\u9014\u5f84\u7684\u673a\u7406\u7814\u7a76\u3002\u57280.1 M KOH + 1.0 M EtOH\u6c34\u6eb6\u6db2\u4e2d\uff0c\uff08a\uff09\u00a0Pd\/C\u3001\uff08b\uff09\u00a0Pd\/NC\u3001\uff08c\u00a0\uff09Pd\/Co@NC \u548c\uff08d\uff09\u00a0Pd+Co@NC\u5728\u4e0d\u540c\u7535\u4f4d\u4e0b\u6d4b\u91cf\u7684\u539f\u4f4d ATR-SEIRA \u5149\u8c31\u3002\uff08e\uff09\u00a0Pd\/C\uff08\u6216 Pt\/C\u3001Pd\/NC\u3001Pd+Co@NC\uff09\u548c\uff08f\u00a0\uff09Pd\/Co@NC \u5728\u78b1\u6027\u6eb6\u6db2\u4e2d\u7684EOR\u673a\u5236\u3002\u00a92023 The Author(s)<\/p>\n

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\u56fe<\/strong>5<\/strong> Pd\/Co@NC\u5bf9\u7535\u50ac\u5316 ORR \u6027\u80fd\u7684\u754c\u9762\u534f\u540c\u6548\u5e94\u3002\uff08a\uff09\u4e0d\u540c\u6837\u54c1\u7684ORR\u534a\u6ce2\u7535\u4f4d(E\u00a01\/2 )\u3002\uff08b\uff09\u901a\u8fc7 RRDE \u6d4b\u8bd5\u7684\u7535\u5b50\u8f6c\u79fb\u6570\uff08n\uff0c\u5de6\uff09\u548c H2<\/sub>O2<\/sub>\u4ea7\u751f\u6548\u7387\uff08\u53f3\uff09\u3002\uff08c\uff09\u00a0\u57280.9 V\u00a0RHE\u65f6\u7684ORR\u8d28\u91cf\u6d3b\u6027\u3002\uff08d\uff09\u00a0Pd\/Co@NC \u5728AST\u524d\u540e15k\u548c30k\u5faa\u73af\u7684ORR\u6781\u5316\u66f2\u7ebf\u3002\uff08e\uff09\u5f52\u4e00\u5316\u7684ORR\u521d\u59cb\u8d28\u91cf\u6d3b\u6027\uff0c\u4ee5\u53ca\u200b\u200b15k\u548c30k\u5faa\u73af\u540e\u7684AST\u3002\uff08f\uff09\u5177\u6709\u4e0d\u540cOH\u8986\u76d6\u7387\u7684Pd(111)\u4e0aORR\u7684\u706b\u5c71\u56fe\u3002\u00a92023 The Author(s)<\/p>\n

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\u56fe<\/strong>6<\/strong> Pd\/Co@NC\u5bf9DEFC\u6027\u80fd\u7684\u754c\u9762\u534f\u540c\u6548\u5e94\u3002\uff08a\uff09\u4f7f\u7528\u4e0d\u540c\u50ac\u5316\u5242\u7684\u7a33\u6001 DEFC\u6781\u5316\u548c\u529f\u7387\u5bc6\u5ea6\u66f2\u7ebf\u3002\uff08b\uff09\u4f7f\u7528\u4e0d\u540cPd\u8d1f\u8f7d\u7684Pd\/Co@NC \u5728MEA\u4e0a\u7684\u7a33\u6001DEFC\u6781\u5316\u548c\u529f\u7387\u5bc6\u5ea6\u66f2\u7ebf\u3002\uff08c\uff09\u4f7f\u7528\u4e0d\u540c\u50ac\u5316\u5242\u7684\u7a33\u6001DEFC\u6781\u5316\u548c\u529f\u7387\u5bc6\u5ea6\u66f2\u7ebf\u3002\uff08d\uff09\u4f7f\u7528\u4e0d\u540c\u50ac\u5316\u5242\u7684DEFC\u7684\u6700\u5927\u529f\u7387\u5bc6\u5ea6\u3002\uff08e\uff09\u5728 0.6-0.9 V \u8303\u56f4\u5185\u7535\u538b\u5faa\u73af10k\u300120k \u548c30k\u5faa\u73afAST\uff0cPd\/Co@NC \u7684\u7a33\u6001DEFC\u6781\u5316\u548c\u529f\u7387\u5bc6\u5ea6\u66f2\u7ebf\u3002\uff08f\uff0910k\u300120k \u548c30k\u5faa\u73af AST \u540e0.8 A cm-2<\/sup>\u65f6\u7684\u7535\u538b\u635f\u5931\uff08\u5de6\uff09\u548c 0.6 V \u65f6\u7684\u7535\u6d41\u5bc6\u5ea6\u635f\u5931\uff08\u53f3\uff09\u3002\uff08g\uff09\u4f7f\u7528 Pd\/Co@NC \u4f5c\u4e3a\u9633\u6781\u548c\u9634\u6781\u50ac\u5316\u5242\u7684DEFC\u5728 0.5 V \u4e0b\u7684 1000 \u5c0f\u65f6\u7a33\u5b9a\u6027\u3002\u00a92023 The Author(s)<\/p>\n

\u4e94\u3001\u3010\u6210\u679c\u542f\u793a\u3011<\/strong><\/span><\/p>\n

\u00a0 \u7efc\u4e0a\u6240\u8ff0\uff0c\u8fd9\u9879\u5de5\u4f5c\u5c55\u793a\u51fa\u4e86\u4e00\u79cd\u5f88\u6709\u524d\u9014\u7684\u5177\u6709\u754c\u9762\u534f\u540c\u4f5c\u7528\u548c\u6574\u4f53\u7ed3\u6784\u6548\u5e94\u7684 Pd\/Co@NC\u50ac\u5316\u5242\u3002Pd\/Co@NC\u4e0d\u4ec5\u6539\u53d8EOR\u7684\u7535\u5b50\u8f6c\u79fb\u8def\u5f84\uff0c\u540c\u65f6\u4e5f\u6539\u5584\u4f20\u7edf\u50ac\u5316\u5242\u5728EOR\u548cORR\u4e2d\u7684\u5b8c\u6574\u6027\/\u7a33\u5b9a\u6027\u548c\u6d3b\u6027\/\u9009\u62e9\u6027\u3002\u56e0\u6b64\uff0c\u8fd9\u9879\u5de5\u4f5c\u4e3a\u57fa\u4e8e\u534f\u540c\u754c\u9762\u6982\u5ff5\u7684 DEFC \u9ad8\u6548\u50ac\u5316\u5242\u7684\u5408\u7406\u8bbe\u8ba1\u5f00\u8f9f\u4e86\u4e00\u79cd\u9009\u62e9\u9053\u8def\uff0c\u8fd9\u5c06\u4fc3\u8fdb\u71c3\u6599\u7535\u6c60\u548c\u5176\u4ed6\u53ef\u6301\u7eed\u80fd\u6e90\u76f8\u5173\u6280\u672f\u7684\u53d1\u5c55\u3002<\/strong><\/p>\n

\u539f\u6587\u8be6\u60c5\uff1a<\/strong>https:\/\/doi.org\/10.1038\/s41467-023-37011-z<\/p>\n

\u672c\u6587\u7531K . L\u64b0\u7a3f\u3002<\/p>\n","protected":false},"excerpt":{"rendered":"

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