{"id":247821,"date":"2023-03-10T06:16:43","date_gmt":"2023-03-09T22:16:43","guid":{"rendered":"\/\/m.iemloyee.com\/?p=247821"},"modified":"2023-03-07T13:47:12","modified_gmt":"2023-03-07T05:47:12","slug":"%e5%a4%a9%e6%b4%a5%e5%a4%a7%e5%ad%a6acs-nano%e5%8f%8c%e6%b4%bb%e6%80%a7%e4%bd%8d%e7%82%b9%e5%af%bc%e7%94%b5mof%e7%94%a8%e4%ba%8e%e6%b0%b4%e7%b3%bb%e9%94%8c%e7%94%b5","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=247821","title":{"rendered":"\u5929\u6d25\u5927\u5b66ACS Nano:\u53cc\u6d3b\u6027\u4f4d\u70b9\u5bfc\u7535MOF\u7528\u4e8e\u6c34\u7cfb\u950c\u7535"},"content":{"rendered":"

1.<\/strong>\u3010\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u76f8\u6bd4\u6709\u673a\u7535\u89e3\u6db2\u4f53\u7cfb\u7684\u4e8c\u6b21\u7535\u6c60\uff0c\u6c34\u6027\u950c\u79bb\u5b50\u7535\u6c60\u5177\u6709\u5b89\u5168\u6027\u9ad8\u3001\u6210\u672c\u4f4e\u3001\u73af\u5883\u53cb\u597d\u7b49\u4f18\u52bf\u3002\u7136\u800c\uff0c\u7531\u4e8e\u7f3a\u4e4f\u5408\u9002\u7684\u9ad8\u5bb9\u91cf\u3001\u957f\u5faa\u73af\u3001\u9ad8\u500d\u7387\u7684\u6b63\u6781\u6750\u6599\uff0c\u6c34\u7cfb\u950c\u79bb\u5b50\u7535\u6c60\u7684\u5b9e\u9645\u5e94\u7528\u53d7\u5230\u9650\u5236\u3002\u5178\u578b\u7684\u950c\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u6750\u6599\u5305\u62ec\u5c42\u72b6\u65e0\u673a\u6750\u6599\uff08\u5982MnO2<\/sub>\u3001V2<\/sub>O5<\/sub>\u7b49\uff09\u3001\u5c0f\u5206\u5b50\u6709\u673a\u6750\u6599\uff08\u5982\u7fb0\u57fa\u5316\u5408\u7269\u3001\u4e9a\u80fa\u5316\u5408\u7269\u7b49\uff09\u548c\u666e\u9c81\u58eb\u84dd\u7c7b\u4f3c\u7269\u3002\u5bf9\u4e8e\u5c42\u72b6\u65e0\u673a\u6750\u6599\uff0c\u950c\u79bb\u5b50\u5d4c\u5165\/\u8131\u51fa\u65f6\u4f53\u79ef\u53d8\u5316\u5927\uff0c\u4e25\u91cd\u9650\u5236\u4e86\u5176\u5faa\u73af\u5bff\u547d\u3002\u76f8\u6bd4\u4e4b\u4e0b\uff0c\u6709\u673a\u6b63\u6781\u4e2d\u7684\u950c\u79bb\u5b50\u7684\u5b58\u50a8\u4e3b\u8981\u662f\u901a\u8fc7\u6709\u673a\u5206\u5b50\u4e2d\u5316\u5b66\u952e\u7684\u91cd\u6392\u6765\u5b9e\u73b0\uff0c\u867d\u7136\u53ef\u4ee5\u6709\u6548\u5730\u907f\u514d\u6750\u6599\u7684\u4f53\u79ef\u81a8\u80c0\/\u7c89\u788e\uff0c\u4f46\u662f\u8fd9\u4e9b\u5e38\u89c1\u7684\u5c0f\u5206\u5b50\u6709\u673a\u6b63\u6781\u6750\u6599\u5f80\u5f80\u5bb9\u6613\u6eb6\u89e3\u5230\u6c34\u7cfb\u7535\u89e3\u6db2\u4e2d\uff0c\u540c\u6837\u4e0d\u5229\u4e8e\u5176\u5faa\u73af\u7a33\u5b9a\u6027\uff1b\u6b64\u5916\uff0c\u4e0a\u8ff0\u4f20\u7edf\u6b63\u6781\u6750\u6599\u8f83\u4f4e\u7684\u7535\u5b50\/\u79bb\u5b50\u5bfc\u901a\u80fd\u529b\u8fdb\u4e00\u6b65\u9650\u5236\u4e86\u7535\u6c60\u500d\u7387\u6027\u80fd\u7684\u63d0\u9ad8\u3002\u91d1\u5c5e<\/strong>–<\/strong>\u6709\u673a\u6846\u67b6\uff08<\/strong>MOF<\/strong>\uff09\u6750\u6599\u4e2d\u91d1\u5c5e\u79bb\u5b50\u4e0e\u6709\u673a\u914d\u4f53\u7ed3\u5408\u7684\u7a33\u5b9a\u914d\u4f4d\u7ed3\u6784\uff0c\u53ef\u4ee5\u6709\u6548\u6291\u5236\u6709\u673a\u914d\u4f53\u7684\u6eb6\u89e3\uff0c\u4ece\u800c\u63d0\u9ad8\u5176\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u503c\u5f97\u6ce8\u610f\u7684\u662f\uff0c\u5bfc\u7535<\/strong>MOFs<\/strong>\uff08<\/strong>c-MOFs<\/strong>\uff09\u4e0e\u4f20\u7edf<\/strong>MOFs<\/strong>\u76f8\u6bd4\uff0c\u4e0d\u4ec5\u5177\u6709\u591a\u5b54\u7ed3\u6784\u548c\u9ad8\u6bd4\u8868\u9762\u79ef\uff0c\u800c\u4e14\u517c\u5177\u4f18\u5f02\u7684\u5bfc\u7535\u6027<\/strong>\u3002\u56e0\u6b64\uff0c\u5bfc\u7535MOF\u6750\u6599\u88ab\u5e94\u7528\u4e8e\u4e86\u9502\u79bb\u5b50\u548c\u94a0\u79bb\u5b50\u7535\u6c60\uff0c\u5728\u6c34\u7cfb\u950c\u79bb\u5b50\u7535\u6c60\u4e2d\u4e5f\u5177\u6709\u6f5c\u5728\u9002\u7528\u6027\u3002<\/p>\n

2.<\/strong>\u3010\u6210\u679c\u63a0\u5f71\u3011<\/strong><\/p>\n

\u57fa\u4e8e\u4ee5\u4e0a\u7814\u7a76\u80cc\u666f\uff0c\u5929\u6d25\u5927\u5b66\u6881\u9aa5\u6559\u6388\u3001\u4faf\u5cf0\u526f\u6559\u6388<\/strong>\uff08\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba\u901a\u8fc7\u5c06\u8d85\u5c0f\u76841, 2, 4, 5-\u56db\u6c28\u57fa\u82ef\uff08BTA\uff09\u914d\u4f53\u4e0e\u94dc\u79bb\u5b50\u914d\u4f4d\uff0c\u63d0\u51fa\u4e86\u4e00\u79cd\u9ad8\u7ed3\u6676\u7684\u4e00\u7ef4<\/strong>\u03c0 – d<\/strong>\u5171\u8f6d\u5bfc\u7535\u91d1\u5c5e<\/strong>–<\/strong>\u6709\u673a\u6846\u67b6\uff08<\/strong>Cu-BTA-H<\/strong>\uff09\uff0c\u4f5c\u4e3a\u950c\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u3002<\/strong>Cu-BTA-H<\/strong>\u5177\u6709\u8f83\u9ad8\u7684\u6d3b\u6027\u4f4d\u70b9\u6bd4\u4f8b\u548c\u53cc\u91cd\u6c27\u5316\u8fd8\u539f\u673a\u5236<\/strong>\uff0c\u5305\u62ec\u94dc\u79bb\u5b50\u4e0a\u7684\u5355\u7535\u5b50\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\uff08Cu2+<\/sup>\/Cu+<\/sup>\uff09\u548c\u6709\u673a\u914d\u4f53\u4e0a\u7684\u53cc\u7535\u5b50\u6c27\u5316\u8fd8\u539f\u53cd\u5e94\uff08C=N\/C\u2212N\uff09\uff0c\u6709\u6548\u5730\u589e\u5f3a\u4e86\u5176\u53ef\u9006\u53cd\u5e94\u80fd\u529b\uff0c\u5b9e\u73b0\u4e86\u6c34\u7cfb\u950c\u79bb\u5b50\u7535\u6c60\u7684\u9ad8\u500d\u7387\u4e0e\u957f\u5faa\u73af\u6027\u80fd\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u4ee5\u201cMetal-Organic Framework with Dual Redox Active Sites for High-Capacity and Durable Cathodes for Aqueous Zinc Batteries\u201d\u4e3a\u9898\u53d1\u8868\u5728ACS Nano<\/em><\/strong>\u671f\u520a\u4e0a\u3002<\/p>\n

\"\"<\/p>\n

3.<\/strong>\u3010\u6838\u5fc3\u521b\u65b0\u70b9\u3011<\/strong><\/p>\n

    \n
  1. \u5408\u6210\u4e86\u4e00\u79cd\u03c0-d\u5171\u8f6d\u7684\u3001\u5177\u6709\u53cc\u6c27\u5316\u8fd8\u539f\u6d3b\u6027\u4f4d\u70b9\u7684\u4e00\u7ef4\u5bfc\u7535MOF\u6750\u6599Cu-BTA-H\uff0c\u4f5c\u4e3a\u950c\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u3002<\/li>\n
  2. Cu-BTA-H\u5177\u6709\u9ad8\u53ef\u9006\u5bb9\u91cf\uff0c\u4f18\u5f02\u7684\u500d\u7387\u6027\u80fd\u548c\u957f\u5faa\u73af\u7a33\u5b9a\u6027\uff0c2.0 A g-1<\/sup>\u7535\u6d41\u5bc6\u5ea6\u4e0b\u5faa\u73af500\u6b21\u540e\u4ecd\u5177\u6709106.1 mAh g-1<\/sup>\u7684\u9ad8\u6bd4\u5bb9\u91cf\u3002<\/li>\n<\/ol>\n

    4.<\/strong>\u3010\u6570\u636e\u6982\u89c8\u3011<\/strong><\/p>\n

    \"\"<\/strong><\/p>\n

    \u56fe<\/strong>1. <\/strong>\u00a9 2023 American Chemical Society<\/p>\n

    \uff08a\uff09\u5bfc\u7535Cu-BTA\u7684\u5408\u6210\u8fc7\u7a0b\u793a\u610f\u56fe\u3002<\/p>\n

    \uff08b\uff09\u4fef\u89c6\u89d2\u5ea6\u7684\u5e73\u9762\u4e00\u7ef4\u5171\u8f6dCu-BTA\u5206\u5b50\u7ed3\u6784\u3002<\/p>\n

    \uff08c\uff09Cu-BTA-H\/L\u548c Ni-BTA-H \u7c89\u672b\u7684XRD\u8c31\u56fe\u3002<\/p>\n

    \uff08d-f\uff09Cu-BTA-H\/L\u548c Ni-BTA-H \u7c89\u672b\u7684TEM\u56fe\u50cf\u3002<\/p>\n

    \uff08g-i\uff09Cu-BTA-H \u548cd Ni-BTA-H\u7684XPS\u5168\u8c31\u3001\u9ad8\u5206\u8fa8N 1s\u8c31\u3001Cu 2p\u8c31\u548cNi 2p\u8c31\u3002<\/p>\n

    \uff08j-l\uff09Cu-BTA-H \u548cd Ni-BTA-H\u7684EPR\u8c31\u3001\u62c9\u66fc\u5149\u8c31\u548c\u7ea2\u5916\u5149\u8c31\u3002<\/p>\n

    \"\"<\/p>\n

    \u56fe<\/strong>2. <\/strong>\u7535\u5316\u5b66\u6027\u80fd\u6d4b\u8bd5<\/strong>\u3002<\/strong>\u00a9 2023 American Chemical Society<\/p>\n

    \uff08a\uff09Cu-BTA-H\u548c\uff08b\uff09Ni-BTA-H\u57280.1 mV s-1<\/sup>\u4e0b\u7684\u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf\u3002<\/p>\n

    \uff08c\uff09Cu-BTA-H\/Ni-BTA-H \u57280.2 A g-1<\/sup>\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

    \uff08d\uff09Cu-BTA-H\/L\u548cNi-BTAH \u7684\u500d\u7387\u6027\u80fd\u548c\uff08e\uff092.0 A g-1<\/sup>\u4e0b\u7684\u5faa\u73af\u6027\u80fd\u3002<\/p>\n

    \uff08f, g\uff09Cu-BTA-H\u548c Ni-BTA-H\u7535\u8377\u5b58\u50a8\u7684\u7535\u5bb9\u4e0e\u6269\u6563\u8d21\u732e\u6bd4\u3002<\/p>\n

    \uff08h\uff09Cu-BTA-H\u4e0e\u5176\u5b83\u950c\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u6750\u6599\u6bd4\u8f83\u3002<\/p>\n

    \"\"<\/p>\n

    \u56fe<\/strong>3. <\/strong>\u7535\u5316\u5b66\u5b58\u50a8\u673a\u7406\u3002<\/strong>\u00a9 2023 American Chemical Society<\/p>\n

    \uff08a\uff09Cu-BTA-H\u5728200 mA g-1<\/sup>\u7535\u538b\u8303\u56f4 0.3-1.6 V\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

    \uff08b, c\uff09\u5145\u653e\u7535\u4e0d\u540c\u7535\u538b\u9636\u6bb5Cu-BTA-H\u7684\u975e\u539f\u4f4dN 1s\u3001C 1s\u548cCu 2p XPS\u5149\u8c31\uff0cNi-BTA-H\u7684Ni 2p XPS\u5149\u8c31\u3002<\/p>\n

    \uff08d\uff09Cu-BTA-H \u548cNi-BTA-H\u53ef\u80fd\u7684\u53cd\u5e94\u673a\u7406\u3002<\/p>\n

    \"\"<\/p>\n

    \u56fe<\/strong>4. Zn<\/strong>\u5b58\u50a8\u7684<\/strong>DFT<\/strong>\u8ba1\u7b97\u3002<\/strong>\u00a9 2023 American Chemical Society<\/p>\n

    \uff08a, b\uff09Cu-BTA\u548cNi-BTA\u4e0d\u540c\u91cd\u590d\u5355\u5143\u805a\u5408\u7269\u94fe\u7684\u6784\u578b\u548c\u524d\u7ebf\u5206\u5b50\u8f68\u9053\u3002<\/p>\n

    \uff08c\uff09\u8ba1\u7b97\u5f97\u5230\u7684Cu-BTA\/Ni-BTA MESP\u5206\u5e03\u3002<\/p>\n

    \uff08d\uff09Cu-BTA\/Ni-BTA\u63a5\u53d7\u4e0d\u540c\u6570\u91cfZn\u79bb\u5b50\u524d\u540e\u7684\u987a\u5e8f\u7ed3\u5408\u80fd\uff08\u0394E\uff09\u3002<\/p>\n

    \uff08e\uff09Cu-BTA\u548cNi-BTA\u5728\u5438\u96443\u548c2\u4e2aZn\u79bb\u5b50\u524d\u540e\u7684\u4f18\u5316\u6784\u578b\u3002<\/p>\n

    \uff08f\uff09Cu-BTA\u653e\u7535\u8fc7\u7a0b\u4e2d\u7ed3\u6784\u6f14\u5316\u548c\u8d28\u5b50\u5316\u8def\u5f84\u7684\u8ba1\u7b97\u7ed3\u679c\u3002<\/p>\n

    \"\"<\/p>\n

    \u56fe<\/strong>5. Cu-BTA-H<\/strong>\u81ea\u5145\u7535\u6027\u80fd\u3002<\/strong>\u00a9 2023 American Chemical Society<\/p>\n

    \uff08a\uff09Cu-BTA-H\u5728\u6263\u5f0f\u7535\u6c60\u4e2d\u9759\u7f6e24 h\u540e\u5728500 mA g-1<\/sup>\u4e0b\u7684\u81ea\u5145\u7535\u6027\u80fd\u3002<\/p>\n

    \uff08b\uff09\u6263\u5f0f\u7535\u6c60\u4e2d\u653e\u7535\u81f30.3 V\u540e\u7684\u7535\u538b-\u65f6\u95f4\u66f2\u7ebf\u3002<\/p>\n

    \uff08c\uff09\u5f00\u5b54\u7535\u6c60\u4e2d\u653e\u7535\u81f30.3 V\u540e\u7684\u7535\u538b-\u65f6\u95f4\u66f2\u7ebf\u3002<\/p>\n

    \uff08d\uff09\u5f00\u5b54\u7535\u6c60\u4e2d\u4e0d\u540c\u6c27\u5316\u65f6\u95f4\u65f6\u7535\u6c60\u76f8\u5e94\u7684\u4e8c\u6b21\u653e\u7535\u80fd\u529b\uff0c\u3002<\/p>\n

    \uff08e\uff09\u5f00\u5b54\u7535\u6c60\u4e2d\u4e0d\u540c\u6c27\u5316\u65f6\u95f4\u65f6\u7535\u6c60\u76f8\u5e94\u7684\u6062\u590d\u5bb9\u91cf\u4e0e\u6052\u6d41\u653e\u7535\u5bb9\u91cf\u4e4b\u6bd4\u3002<\/p>\n

    \uff08f\uff09\u5145\u7535\u5b8c\u6210\u540eCu-BTA-H\u7535\u6781\u5f00\u5b54\u7535\u6c60\u4e2d\u6c27\u531624 h\u540e\u7684\u975e\u539f\u4f4dN 1s\u548cCu 2p XPS\u5149\u8c31\u3002<\/p>\n

    \uff08g\uff09\u63d0\u51fa\u7684Cu-BTA\u81ea\u5145\u7535\u673a\u7406\u3002<\/p>\n

    5.<\/strong>\u3010\u6210\u679c\u542f\u793a\u3011<\/strong><\/p>\n

    \u672c\u7814\u7a76\u4e2d\uff0c\u4f5c\u8005\u5229\u75281, 2, 4, 5-\u56db\u6c28\u57fa\u82ef\uff08BTA\uff09\u914d\u4f53\u4e0e\u591a\u4ef7Cu\u79bb\u5b50\u914d\u4f4d\uff0c\u5236\u5907\u4e86\u4e00\u7ef4\u5bfc\u7535MOF\uff08Cu-BTA\uff09\u3002\u5c0f\u5206\u5b50\u914d\u4f53BTA\u7684\u91c7\u7528\u6709\u6548\u5730\u6700\u5927\u5316\u4e86\u5bfc\u7535MOF\u4e2d\u7684\u6c27\u5316\u8fd8\u539f\u6d3b\u6027\u7ec4\u5206\uff08-C=N-\uff09\u7684\u542b\u91cf\uff0c\u6700\u5c0f\u5316\u4e86\u975e\u6d3b\u6027\u7ec4\u5206\uff08\u82ef\u57fa\uff09\u542b\u91cf\uff1b\u591a\u4ef7\u6001Cu\u79bb\u5b50\u63d0\u4f9b\u4e86Cu2+<\/sup>\/Cu+<\/sup>\u7684\u7b2c\u4e8c\u4e2a\u6c27\u5316\u8fd8\u539f\u4f4d\u70b9\uff0c\u589e\u52a0\u4e86\u989d\u5916\u7684Zn\u79bb\u5b50\u5b58\u50a8\u3002\u6b64\u5916\uff0cCu-BTA\u7684\u9ad8\u7ed3\u6676\u5ea6\u3001\u9ad8\u79bb\u5b50\/\u7535\u5b50\u7535\u5bfc\u7387\u548c\u7a33\u5b9a\u7684\u914d\u4f4d\u7ed3\u6784\uff0c\u63d0\u9ad8\u4e86\u950c\u79bb\u5b50\u7535\u6c60\u5faa\u73af\u7a33\u5b9a\u6027\u548c\u500d\u7387\u6027\u80fd\u3002\u672c\u5de5\u4f5c\u4e3a\u6784\u5efa\u5177\u6709\u53cc\u6c27\u5316\u8fd8\u539f\u6d3b\u6027\u4f4d\u70b9\u7684\u5bfc\u7535MOF\uff0c\u5e76\u7528\u4e8e\u9ad8\u6027\u80fd\u950c\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u6750\u6599\u63d0\u4f9b\u4e86\u7814\u7a76\u501f\u9274\u3002<\/p>\n

    \u539f\u6587\u8be6\u60c5<\/strong>\uff1a Sang Z, Liu J, Zhang X, et al. One-Dimensional \u03c0\u2013d Conjugated Conductive Metal\u2013Organic Framework with Dual Redox-Active Sites for High-Capacity and Durable Cathodes for Aqueous Zinc Batteries[J]. ACS nano, 2023. https:\/\/doi.org\/10.1021\/acsnano.2c11974\u3002<\/p>\n

    \u672c\u6587\u7531famous\u7a0b\u4f9b\u7a3f\u3002<\/p>\n","protected":false},"excerpt":{"rendered":"

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