{"id":246786,"date":"2023-02-15T12:10:23","date_gmt":"2023-02-15T04:10:23","guid":{"rendered":"\/\/m.iemloyee.com\/?p=246786"},"modified":"2023-02-21T11:00:58","modified_gmt":"2023-02-21T03:00:58","slug":"%e3%80%90%e6%96%b0%e8%83%bd%e6%ba%90%e5%89%8d%e7%ba%bf%e3%80%91appl-catal-b%ef%bc%9a%e6%97%a0%e8%86%9c%e6%97%a0%e7%bc%93%e5%86%b2%e6%b5%b7%e6%b0%b4%e7%94%b5%e8%a7%a3%e4%ba%a7%e9%ab%98%e7%ba%af","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=246786","title":{"rendered":"Appl. Catal. B\uff1a\u65e0\u819c\u65e0\u7f13\u51b2\u6d77\u6c34\u7535\u89e3\u4ea7\u9ad8\u7eaf\u6c22\u6c14"},"content":{"rendered":"

\u4e00\u3001<\/strong>\u3010\u5bfc\u8bfb\u3011<\/strong><\/span><\/p>\n

\u00a0 \u00a0\u8fd1\u5e74\u6765\uff0c\u6d77\u6c34\u7535\u89e3\u5236\u6c22\u88ab\u8ba4\u4e3a\u662f\u80fd\u6e90\u8f6c\u578b\u7684\u5173\u952e\u6280\u672f\uff0c\u7136\u800c\u4ee5\u5f80\u7684\u7814\u7a76\u4e3b\u8981\u5173\u6ce8\u7684\u662f\u78b1\u6027\u6d77\u6c34\u3002\u5176\u4e2d\uff0c\u819c\uff08\u5206\u79bbH2<\/sub>\u548cO2<\/sub>\uff09\u548c\u8150\u8680\u6027 KOH (\u63d0\u9ad8\u6790\u6c27\u53cd\u5e94\u7684\u9009\u62e9\u6027) \u7684\u4f7f\u7528\u663e\u8457\u589e\u52a0\u4e86H2<\/sub>\u7684\u751f\u4ea7\u6210\u672c\u3002\u4e3a\u4e86\u964d\u4f4e\u6c22\u6c14\u7684\u6210\u672c\u4ee5\u53ca\u5b9e\u73b0\u6d77\u4e0a\u5feb\u901f\u8fd0\u8f93\uff0c\u76f4\u63a5\u6d77\u6c34\u7535\u89e3\u7814\u7a76\u5f15\u8d77\u4e86\u5e7f\u6cdb\u7684\u5173\u6ce8\u3002\u76f4\u63a5\u6d77\u6c34\u7535\u89e3\u5bf9\u7535\u6781\u7684\u9009\u62e9\u6027\u8981\u6c42\u5341\u5206\u4e25\u683c\u3002\u8fd9\u5f52\u56e0\u4e8e\u9633\u6781\u7684\u6790\u6c27\u53cd\u5e94\uff08OER\uff09\u548c\u6c2f\u6c27\u5316\u53cd\u5e94\uff08ClOR\uff09\u7684\u7ade\u4e89\uff0c\u4ee5\u53ca\u9634\u6781\u7684\u6c2f\u8fd8\u539f\u53cd\u5e94\uff08ClRR\uff0c\u6765\u81ea\u4e8e\u9633\u6781\u4ea7\u751f\u7684HClO\/ClO–<\/sup>\uff09\u548c\u6790\u6c22\u53cd\u5e94\uff08HER\uff09\u7684\u7ade\u4e89\u3002ClOR\u548cClRR\u7684\u53c2\u4e0e\u6781\u5927\u9650\u5236O2<\/sub>\u548cH2<\/sub>\u7684\u751f\u4ea7\u6548\u7387\u3002\u56e0\u6b64\u8981\u60f3\u5b9e\u73b0\u76f4\u63a5\u6d77\u6c34\u7535\u89e3\u5fc5\u987b\u5f00\u53d1\u51fa\u9ad8\u9009\u62e9\u6027\u548c\u7a33\u5b9a\u6027\u7684\u7535\u50ac\u5316\u5242\u3002<\/p>\n

\u4e8c\u3001\u3010<\/strong>\u6210\u679c\u63a0\u5f71\u3011<\/strong><\/span><\/p>\n

\u00a0 \u00a0<\/strong>\u8fd1\u65e5\uff0c\u97e9\u56fd\u5e86\u5317\u5927\u5b66Hyunwoong\u00a0Park\u6559\u6388\u548c\u5361\u5854\u5c14\u5927\u5b66DongSuk Han\u6559\u6388\u7b49\u4eba\u63d0\u51fa\u5e76\u5b9e\u73b0\u4e86\u4e00\u79cd\u65e0\u819c\u65e0\u7f13\u51b2\u6d77\u6c34\u4ea7\u9ad8\u7eaf\u6c22\u6c14\u7684\u65b9\u6848\uff0c\u8be5\u65b9\u6848\u662f\u7531\u9ad8ClOR\u9009\u62e9\u6027\u9633\u6781\u548c\u9ad8ClRR\u6291\u5236\u6027\u9634\u6781\u7ec4\u6210\uff0c\u5b8c\u5168\u5b9e\u73b0\u4e86\u6291\u5236O2<\/sub>\u7684\u751f\u6210\uff0c\u540c\u65f6\u4f7f\u9634\u6781\u751f\u4ea7H2<\/sub>\u6700\u5927\u5316\u3002\u76f8\u5173\u7684\u7814\u7a76\u6210\u679c\u4ee5\u201cMembraneless unbuffered seawater electrolysis for pure hydrogen production using PtRuTiOx anode and MnOx cathode pairs<\/em><\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728Applied Catalysis B: Environmental<\/em><\/strong>\u4e0a\u3002\u97e9\u56fd\u5e86\u5317\u5927\u5b66\u80fd\u6e90\u5de5\u7a0b\u5b66\u9662\u535a\u58eb\u6881\u6960\u6960\u4e3a\u7b2c\u4e00\u4f5c\u8005\uff0cHyunwoong\u00a0Park\u6559\u6388\u4e3a\u7b2c\u4e00\u901a\u8baf\u4f5c\u8005\u3002<\/p>\n

<\/p>\n

\u4e09\u3001\u3010<\/strong>\u6838\u5fc3\u521b\u65b0\u70b9\u3011<\/strong><\/span><\/p>\n

1<\/strong>\u3001\u8be5\u5de5\u4f5c\u5f00\u53d1\u51fa\u4e00\u79cd\u6700\u4f4e<\/strong>Pt<\/strong>\u6c34\u5e73\u7684\u4e09\u5143<\/strong>Pt<\/strong>\u3001<\/strong> Ru <\/strong>\u548c<\/strong> Ti (PRT<\/strong>\uff0c<\/strong>Pt 0.06<\/sub>Ru 0.24<\/sub>Ti0.7<\/sub>Ox<\/sub>)<\/strong>\u7535\u50ac\u5316\u5242\uff0c\u53ef\u4ee5\u5728\u76d0\u6c34\u4e2d\u5b9e\u73b0\u9ad8<\/strong>ClOR<\/strong>\u9009\u62e9\u6027\uff0c\u6cd5\u62c9\u7b2c\u6548\u7387<\/strong>(FE) ~100%<\/strong>\u3002\u5e76\u4e14\u5728\u5de5\u4e1a\u7ea7\u7535\u6d41\u5bc6\u5ea6\uff08<\/strong>800 mA cm-2<\/sup><\/strong>\uff09\u4e0b\uff0c\u8be5\u7535\u6781\u4fdd\u6301\u7740\u5de5\u4e1a\u7ea7\u7a33\u5b9a\u6027\u548c\u6052\u5b9a\u7684<\/strong>ClOR<\/strong>\u6d3b\u6027\uff1b<\/strong><\/p>\n

2<\/strong>\u3001\u8be5\u5de5\u4f5c\u540c\u65f6\u4e5f\u63d0\u51fa\u5e76\u5b9e\u73b0\u4e00\u79cd\u65e0\u5e72\u6270\u3001\u65e0\u819c\u3001\u65e0\u7f13\u51b2\u6d77\u6c34\u4ea7\u9ad8\u7eaf<\/strong>H2<\/sub><\/strong>\u65b9\u6848\u3002\u8be5\u65b9\u6848\u4ee5<\/strong>PRT <\/strong>\u9633\u6781<\/strong>\/MnOx<\/strong>\u9634\u6781\u4f5c\u4e3a\u7535\u6781\u5bf9\uff0c\u5728\u65e0\u819c\u7535\u89e3\u6c60\u3001<\/strong>pH 8.2<\/strong>\u7684\u6d77\u6c34\u4e2d\u7535\u89e3\u8d85<\/strong>100<\/strong>\u5c0f\u65f6<\/strong>, HER<\/strong>\u548c<\/strong>ClOR<\/strong>\u4ee5<\/strong>~100%<\/strong>\u7684<\/strong>FE<\/strong>\u9a71\u52a8\uff0c\u6ca1\u6709<\/strong>O2<\/sub><\/strong>\u751f\u6210\u3002<\/strong><\/p>\n

\u56db\u3001<\/strong>\u3010\u6570\u636e\u6982\u89c8\u3011<\/strong><\/span><\/p>\n

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\u65b9\u68481<\/strong>\u00a0 \u5728\u65e0\u819c\u5355\u5ba4\u7535\u6c60\u4e2d\u4f7f\u7528 PtRuTiOx\u00a0(PRT) \u9633\u6781\u548c MnOx\u9634\u6781\u5bf9\u8fdb\u884c\u6d77\u6c34\u7535\u89e3\u7684\u793a\u610f\u56fe\u3002\u4f20\u7edf\u7684\u6d77\u6c34\u7535\u89e3\u5728\u78b1\u6027\u6761\u4ef6\u4e0b\u8fdb\u884c(pH>13)\u4ee5\u786e\u4fddOER\u5bf9ClOR\u7684\u9009\u62e9\u6027\u3002\u6b64\u5916\uff0c\u5b83\u901a\u5e38\u9700\u8981\u819c\u6765\u6291\u5236ClRR \u548c HER\uff0c\u540c\u65f6\u5c06 H2<\/sub>\u4e0eO2<\/sub>\u5206\u79bb\u3002\u7136\u800c\uff0c\u5982\u679c\u7535\u89e3\u4ea7\u7269\u53ea\u6709\u6eb6\u6db2\u4e2d\u7684 HClO\uff08\u548c\/\u6216 ClO\u00a0–<\/sup>\uff09\u548c\u9876\u90e8\u7a7a\u95f4\u4e2d\u7684H\u00a02<\/sub>\uff0cClOR \u548c HER \u7684\u6cd5\u62c9\u7b2c\u6548\u7387\u5206\u522b\u4e3a ~100%\uff0c\u5219\u5206\u79bb\u6c14\u4f53\uff08H2<\/sub>\u548cO2<\/sub>) \u548c\u6291\u5236\u9634\u6781\u6c2f\u8fd8\u539f\u5c31\u6ca1\u6709\u5fc5\u8981\u3002\u00a9 2022 Elsevier B.V.<\/p>\n

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\u56fe<\/strong>1<\/strong> \u00a0\u5728500 \u00b0C \u4e0b\u9000\u706b\u7684\u5408\u6210\u4e8c\u5143 PR (Pt0.2<\/sub>Ru0.8<\/sub>Oy<\/sub> ) \u548c\u4e09\u5143 PRT (Pt0.06<\/sub>Ru0.24<\/sub>Ti0.7<\/sub>Oy<\/sub> ) \u9897\u7c92\u7684\u8868\u5f81\u3002(a) XRD \u5149\u8c31\u3002(b-d) XPS \u5149\u8c31\uff08b\uff1aRu 3d\uff0cc\uff1aPt 4f\uff0cd\uff1aTi 2p \u548c O 1s\uff09 \u00a9 2022 Elsevier B.V.<\/strong><\/p>\n

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\u56fe<\/strong>2<\/strong> (a\u548cb)\u5206\u522b\u662f\u5408\u6210\u7684PR\u548cPRT\u9897\u7c92\u7684SEM\u56fe\u3002(c)\u5408\u6210Pt\u3001RuO2<\/sub>\u3001PR\u548cPRT\u6837\u54c1\u7684N2<\/sub>\u5438\u9644-\u89e3\u5438\u7b49\u6e29\u7ebf\u66f2\u7ebf\u3002\u63d2\u56fe\u663e\u793aBET\u8868\u9762\u79ef\u3002(d\u548ce) PRT\u6837\u54c1\u7684HR-TEM\u56fe\u50cf\u548cSAED\u6a21\u5f0f\u3002(f-j) PRT\u6837\u54c1\u7684EDS\u548c\u5143\u7d20\u6620\u5c04 \u00a9 2022 Elsevier B.V.<\/strong><\/p>\n

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\u56fe<\/strong>3<\/strong> \u00a0(a) Pt, Ru, PR\u548cPRT\u7535\u6781\u57280.5 M NaCl\u6eb6\u6db2(pH 6)\u4e2d\u7684LSV\u3002\u4f5c\u4e3a\u6bd4\u8f83\uff0c\u4e5f\u4f7f\u75280.137 M NaCl\u62160.5 M NaClO4<\/sub> (pH 6)\u3002PRT(1\/4)\u662f\u6307\u8d1f\u8f7d\u8d28\u91cf\u4e3a0.83 mg cm\u22122<\/sup>\u7684PRT\u3002\u63d2\u56fe\u663e\u793a\u4e86PRT\u7535\u6781\u57280.5 M NaCl\u3001<\/strong>J<\/em> = 80 mA cm\u22122<\/sup>\u4e0b\u7684O2<\/sub>\u6790\u51fa\u53caFE\u3002(b) J<\/em> = 80 mA cm\u22122<\/sup>\u65f6ClOR\u7684FE\u503c\u3002\u63d2\u56fe\u663e\u793a\u4e86\u5728J = 80 mA cm\u22122<\/sup>\u65f6\u81ea\u7531\u6c2f\u7684\u4ea7\u751f\u3002(c) Cdl<\/sub>\u548cRct<\/sub>\u503c\u3002(d)\u5728J <\/em>= 800 mA cm\u22122<\/sup>\u6761\u4ef6\u4e0b\uff0c\u57280.941 M NaCl\u6eb6\u6db2\u4e2d\uff0c\u5bf9\u55b7\u6d82\u540e\u548c\u9000\u706b\u540e\u7684PRT\u9633\u6781\u8fdb\u884c\u957f\u65f6\u95f4\u7535\u89e3\u3002\u63d2\u56fe\u663e\u793a\u4e86\u57280.5 M NaCl\u6eb6\u6db2\u4e2d\u55b7\u6d82\u3001\u9000\u706b\u548c500 h\u4f7f\u7528\u7684PRT\u7535\u6781\u7684\u4f0f\u5b89\u56fe\u548cFE\u503c(J<\/em> = 80 mA cm\u22122<\/sup>)\u3002\u8fd8\u663e\u793a\u4e86XRD\u5149\u8c31\u548cSEM\u56fe\u50cf(\u5de6:\u9000\u706b\u65f6\uff0c\u53f3:\u4f7f\u7528500 h) \u00a9 2022 Elsevier B.V.<\/strong><\/p>\n

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\u56fe<\/strong>4<\/strong> \u5728\u4e0d\u540c\u6e29\u5ea6(200-500\u00b0C)\u4e0b\u9000\u706b\u7684MnOx\u7535\u6781(\u6c89\u79ef\u5728\u949b\u677f\u4e0a)\u7684\u8868\u5f81\u548c\u7535\u5316\u5b66\u5206\u6790\u3002\u9664\u975e\u53e6\u6709\u8bf4\u660e\uff0cMnOx\u4ee3\u8868MnOx-400(400\u00b0C\u9000\u706b)\u3002(a) XRD\u5149\u8c31\uff0c(b) HR-TEM\u548cSEM\u56fe\u50cf(\u5206\u522b\u4e3a\u9876\u90e8\u548c\u5e95\u90e8)\uff0c(c\u548cd) XPS\u5149\u8c31(\u5206\u522b\u4e3aMn 2p\u548cMn 3s)\uff0c (e) Cdl<\/sub>\u548cRct<\/sub>\u3002\u7535\u89e3100 h\u540e\uff0c\u7528XRD\u3001SEM\u3001XPS\u5bf9MnOx\u6837\u54c1\u8fdb\u884c\u4e86\u8868\u5f81 \u00a9 2022 Elsevier B.V.<\/strong><\/p>\n

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\u56fe<\/strong>5<\/strong> \u00a0\u4f7f\u7528 Pt\u3001Ti \u548c MnOx\u7535\u6781\u5728pH 6\u7684 0.5 M NaCl\u30010.5 M NaCl \u548c 5 mM NaClO \u6216 0.4 M NaCl \u548c 0.1 M NaClO\u6eb6\u6db2\u4e2d\u5bf9ClRR \u548c HER \u7684\u7535\u5316\u5b66\u884c\u4e3a\u548c\u6d3b\u6027\u8fdb\u884c\u7814\u7a76\u3002\u9664\u975e\u53e6\u6709\u8bf4\u660e\uff0cMnOx\u4ee3\u8868MnOx-400(400\u00b0C\u9000\u706b)\u3002(a)LSV\u3002(b)\u7528CEM\u5206\u9694\u7684\u53cc\u5ba4\u7535\u6c60\uff0c\u57280.5 M NaCl\u548c5 mM NaClO\u3001<\/strong>J<\/em>=\u221210 mA cm\u22122<\/sup>\u4e0b\uff0c\u4e0d\u540c\u7535\u6781\u7684\u6c2f\u79bb\u5b50\u6d53\u5ea6(Ct<\/sub> \/ C0<\/sub>)\u53d8\u5316\u3002\u63d2\u56fe\u663e\u793a30\u5206\u949f\u5185\u7684ClRR-FE\u503c(c) ClRR-FE\u503c\u4f5c\u4e3aJ<\/em>\u548cNaOCl\u6d53\u5ea6\u7684\u51fd\u6570\u3002(d)\u57280.5 M NaCl\u548c5 mM NaClO\u3001<\/strong>J<\/em>=\u221210 mA cm\u22122<\/sup>\u4e0b\uff0cHER-FE\u7684\u53d8\u5316 \u00a9 2022 Elsevier B.V.<\/strong><\/p>\n

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\u56fe<\/strong> 6<\/strong> \u5728\u5355\u5ba4\u7535\u6c60\u4e2d\u4f7f\u7528 PRT \u9633\u6781\u548c MnOx\u9634\u6781 (PRT\/MnO x ) \u5bf9\u8fdb\u884c\u6d77\u6c34\u7535\u89e3\u3002(a) \u6bcf\u4e2a\u7535\u6781\u5728 0.5 M NaCl \u548c\u6d77\u6c34\u6eb6\u6db2\uff08\u76d0\u5ea6 36 g L-1<\/sup>\uff09\u4e2d\u7684LSV\u3002(b) \u6c2f\u7684\u751f\u4ea7\u548cClOR-FE\uff0c\u5728Jcell<\/sub><\/em> = 80 mA cm-2<\/sup>\u7684\u6d77\u6c34\u6eb6\u6db2\u4e2d\uff0c\u4f7f\u7528 PRT\/Ti \u548c PRT\/MnOx\u3002 (c) H2<\/sub>\u7684\u751f\u4ea7\u548c HER-FE\uff0c\u5728Jcell<\/sub><\/em> = 80 mA cm-2<\/sup>\u7684\u6d77\u6c34\u6eb6\u6db2\u4e2d\uff0c\u4f7f\u7528 PRT\/Ti \u548c PRT\/MnOx\u3002(d) \u4f7f\u7528 PRT\/MnOx\u7535\u6781\u5bf9\uff0cJcell<\/sub><\/em> = 80 mA cm-2<\/sup>\u7684\u6d77\u6c34\u6eb6\u6db2\u4e2d\u8fdb\u884c\u957f\u65f6\u95f4\u7535\u89e3\u3002\u653e\u51fa\u7684 H2<\/sub>\u548c O2<\/sub>\u6c14\u4f53\u5728\u539f\u4f4d\u5b9e\u65f6\u6d4b\u91cf\uff0c\u540c\u65f6\u5bf9\u6c2f\u8fdb\u884c\u95f4\u6b47\u6027\u5206\u6790 \u00a9 2022 Elsevier B.V.<\/strong><\/p>\n

\u4e94\u3001<\/strong>\u3010\u6210\u679c\u542f\u793a\u3011<\/strong><\/p>\n

\u00a0 \u00a0\u5728\u8be5\u5de5\u4f5c\u4e2d\uff0c\u4f5c\u8005\u9996\u5148\u5f00\u53d1\u51fa\u4e00\u79cd\u4f18\u5f02\u7684ClOR\u9009\u62e9\u6027\u50ac\u5316\u5242\uff0c\u5e76\u5b9e\u73b0\u5de5\u4e1a\u7ea7\u7684\u7a33\u5b9a\u548c\u50ac\u5316\u6d3b\u6027\u3002\u8fd9\u4e3a\u6c2f\u78b1\u5de5\u4e1a\uff0c\u6c2f\u9178\u76d0\u5de5\u4e1a\u4ee5\u53ca\u6c34\u5904\u7406\u5de5\u4e1a\u63d0\u4f9b\u66f4\u9ad8\u6548\u7684\u9633\u6781\u9009\u62e9\u6027\u50ac\u5316\u5242\u3002\u540c\u65f6\u63d0\u51fa\u4e00\u79cd\u65b0\u9896\u7684\u76f4\u63a5\u6d77\u6c34\u7535\u89e3\u5236\u6c22\u7684\u7b56\u7565\uff0c\u5c06ClOR\u9009\u62e9\u6027\u9633\u6781\u548cHER\u9009\u62e9\u6027\u9634\u6781\u76f8\u7ed3\u5408\u5b9e\u73b0\u65e0\u819c\u65e0\u7f13\u51b2\u6d77\u6c34\u7535\u89e3\u4ea7\u9ad8\u7eaf\u6c22\u6c14\u3002\u8fd9\u79cd\u7b56\u7565\u4e3a\u5de5\u4e1a\u7535\u89e3\u5236\u6c22\u63d0\u4f9b\u65b0\u9896\u7684\u601d\u8def\uff0c\u540c\u65f6\u4e5f\u8fdb\u4e00\u6b65\u52a0\u5feb\u5b9e\u73b0\u6d77\u4e0a\u5236\u6c22\u548c\u6d77\u4e0aH2<\/sub>\u5feb\u901f\u8fd0\u8f93\u7684\u6b65\u4f10\u3002<\/p>\n

 <\/p>\n

\u539f\u6587\u8be6\u60c5\uff1a<\/strong>https:\/\/doi.org\/10.1016\/j.apcatb.2022.122275<\/p>\n

\u672c\u6587\u7531K . L\u64b0\u7a3f\u3002<\/p>\n

 <\/p>\n","protected":false},"excerpt":{"rendered":"

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