{"id":243875,"date":"2022-11-05T09:24:56","date_gmt":"2022-11-05T01:24:56","guid":{"rendered":"\/\/m.iemloyee.com\/?p=243875"},"modified":"2022-11-05T09:24:56","modified_gmt":"2022-11-05T01:24:56","slug":"%e9%a6%99%e6%b8%af%e5%9f%8e%e5%b8%82%e5%a4%a7%e5%ad%a6-%e9%ba%bb%e7%9c%81%e7%90%86%e5%b7%a5%e5%ad%a6%e9%99%a2%ef%bc%8c%e6%9c%80%e6%96%b0nature-protocols","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=243875","title":{"rendered":"\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\/\u9ebb\u7701\u7406\u5de5\u5b66\u9662\uff0c\u6700\u65b0Nature Protocols"},"content":{"rendered":"

\u3010\u5bfc\u8bfb\u3011<\/strong><\/p>\n

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\u3010\u6210\u679c\u63a0\u5f71\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\uff08CityU\uff09\u66fe\u5fd7\u8fdc\u6559\u6388\uff0c\u9ebb\u7701\u7406\u5de5\u5b66\u9662\u674e\u5de8\u6559\u6388\u7b49\u4eba<\/strong>\uff0c\u62a5\u9053\u4e86\u4f7f\u7528\u7eb3\u7c73\u5236\u9020\u6280\u672f\uff08\u5149\u523b\u6280\u672f\uff09\u5236\u5907\u539f\u4f4d\u6db2\u76f8TEM\u6838\u5fc3\u90e8\u4ef6-\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u3002\u6b64\u5916\uff0c\u4f5c\u8005\u8fd8\u4ecb\u7ecd\u4e86\u4f7f\u7528\u5236\u5907\u7684\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u8fdb\u884c\u539f\u4f4dTEM\u89c2\u5bdf\u7684\u5177\u4f53\u64cd\u4f5c\u3002\u968f\u540e\uff0c\u4f5c\u8005\u5c55\u793a\u4e86\u4f7f\u7528\u5236\u5907\u7684\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u8fdb\u884c\u539f\u4f4dTEM\u89c2\u5bdf\u7684\u5e94\u7528\u4e3e\u4f8b\u3002\u8be5\u5de5\u4f5c\u4ee5\u9898\u4e3a\u201c<\/strong>Fabrication of Liquid Cell for In-Situ Transmission Electron Microscopy of Electrochemical Processes<\/strong>\u201d<\/strong>\u53d1\u8868\u5728\u77e5\u540d\u671f\u520aNature Protocols<\/strong>\u4e0a\uff0c\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\u4e3a\u7b2c\u4e00\u5355\u4f4d\u3002\u6b64\u5916\u8be5\u5de5\u4f5c\u5f97\u5230\u9ebb\u7701\u7406\u5de5\u5b66\u9662\uff0c\u53a6\u95e8\u5927\u5b66\uff0c\u4ee5\u53ca\u897f\u5b89\u4ea4\u901a\u5927\u5b66\u7684\u534f\u52a9\u3002<\/p>\n

\u3010\u6838\u5fc3\u521b\u65b0\u3011<\/strong><\/p>\n

\u5f00\u53d1\u4e86\u4e00\u79cd\u5236\u5907\u539f\u4f4d\u6db2\u76f8TEM\u6838\u5fc3\u90e8\u4ef6-\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u7684\u6280\u672f\uff08\u5149\u523b\u6280\u672f\uff09\u3002\u5e76\u4e14\u516c\u5e03\u4e86\u5236\u5907\u7ec6\u8282\u3002\u6240\u5236\u5907\u7684\u6db2\u4f53\u6c60\u53ef\u7528\u4e8e\u539f\u4f4dTEM\u89c2\u5bdf\u591a\u79cd\u6db2\u76f8\u53cd\u5e94\uff0c\u5982\u7535\u89e3\u6db2\u4e2d\u7684\u7535\u5316\u5b66\u53cd\u5e94\uff0c\u6676\u4f53\u6210\u6838\u548c\u751f\u957f\u7b49\u3002<\/p>\n

\u3010\u6570\u636e\u6982\u89c8\u3011<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe1\uff1a\u539f\u4f4dTEM\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u793a\u610f\u56fe @2022 Springer Nature<\/p>\n

(a)\u6db2\u4f53\u6c60\u6570\u7801\u7167\u7247\uff083 mm \u00b4 3mm\uff09<\/p>\n

(b)\u6db2\u4f53\u6c60\u793a\u610f\u56fe\u3002\u7d2b\u8272\uff1a\u7845\u7247\uff1b\u7070\u8272\uff1a\u73af\u6c27\u6811\u8102\u3002<\/p>\n

(c)\u6db2\u4f53\u6c60\u6210\u50cf\u7a97\u53e3\u5904\u7684\u622a\u9762\u56fe\uff0c\u663e\u793a\u4e86\u6db2\u4f53\u6c60\u5185\u90e8\u7ec4\u6210\u548c\u7ed3\u6784\u3002\u4ece\u4e0a\u5230\u4e0b\uff0c\u5176\u7ec4\u6210\u5143\u7d20\u4f9d\u6b21\u662f\u7845\u6676\u7247\u3001SiNx<\/sub>\u3001\u7535\u89e3\u8d28\u3001\u7535\u6781\u3001SiNx<\/sub>\u548c\u7845\u6676\u7247\u3002\u5e95\u90e8\u56fe\u663e\u793a\u4e86\u7531\u7535\u5b50\u675f\u7167\u5c04\u7684\u533a\u57df\u7684\u653e\u5927\u56fe\uff0c\u793a\u610f\u4e86\u8981\u89c2\u5bdf\u7684\u7535\u5316\u5b66\u53cd\u5e94\uff08\u4f8b\u5982\uff0c\u91d1\u5c5e\u679d\u6676\u7684\u5f62\u6210\uff09\u3002<\/p>\n

\"\"<\/p>\n

\u56fe2\uff1a\u5149\u523b\u6280\u672f\u5236\u5907\u539f\u4f4dTEM\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u8fc7\u7a0b\u4e2d\u82af\u7247\u7684\u6f14\u53d8 @2022 Springer Nature<\/p>\n

\"\"<\/p>\n

\u56fe3\uff1a\u5149\u523b\u6280\u672f\u5236\u5907\u539f\u4f4dTEM\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u8fc7\u7a0b\u4e2d\u82af\u7247\u6f14\u53d8\u7684\u4fa7\u89c6\u56fe @2022 Springer Nature<\/p>\n

\"\"<\/p>\n

\u56fe4\uff1a\u539f\u4f4dTEM\u89c2\u5bdf\u548c\u540e\u539f\u4f4d\u8868\u5f81\uff08HAADF-STEM, EDS, 4D-STEM\uff09\u793a\u610f\u56fe @2022 Springer Nature<\/p>\n

\"\"<\/p>\n

\u56fe5\uff1a\u5e94\u7528\u4e3e\u4f8b\uff1aMoS2<\/sub>\u7eb3\u7c73\u7247\u9502\u5316\u548c\u8131\u9502\u7684\u539f\u4f4dTEM\u89c2\u5bdf @2022 Springer Nature<\/p>\n

\"\"<\/p>\n

\u56fe6\uff1a\u5e94\u7528\u4e3e\u4f8b\uff1aTi\u5e73\u9762\u4e0aNa\u7535\u6c89\u79ef\u7684\u539f\u4f4dTEM\u89c2\u5bdf @2022 Springer Nature<\/p>\n

\"\"<\/p>\n

\u56fe7\uff1a\u5e94\u7528\u4e3e\u4f8b\uff1aTi\u9633\u6781\u4e0a\u56fa\u4f53\u7535\u89e3\u8d28\u754c\u9762\u819c\uff08SEI\uff09\u7684\u540e\u539f\u4f4d\u8868\u5f81\uff08HADDF, EDS\uff09@2022 Springer Nature<\/p>\n

\u3010\u6210\u679c\u542f\u793a\u3011<\/strong><\/p>\n

\u603b\u4e4b\uff0c\u4f5c\u8005\u5f00\u53d1\u4e86\u4e00\u79cd\u5236\u5907\u539f\u4f4d\u6db2\u76f8TEM\u6838\u5fc3\u90e8\u4ef6-\u6db2\u4f53\u6c60\uff08liquid cell\uff09\u7684\u6280\u672f\u3002\u5e76\u4e14\u516c\u5e03\u4e86\u5236\u5907\u7ec6\u8282\u3002\u6240\u5236\u5907\u7684\u6db2\u4f53\u6c60\u53ef\u7528\u4e8e\u539f\u4f4dTEM\u89c2\u5bdf\u591a\u79cd\u6db2\u76f8\u53cd\u5e94\uff0c\u5982\u7535\u89e3\u6db2\u4e2d\u7684\u7535\u5316\u5b66\u53cd\u5e94\uff0c\u6676\u4f53\u6210\u6838\u548c\u751f\u957f\u7b49\u3002\u6b64\u5916\uff0c\u63d0\u51fa\u7684\u5236\u9020\u65b9\u6848\u4e5f\u4e3a\u5f00\u53d1TEM\u4ee5\u5916\u7684\u5176\u4ed6\u539f\u4f4d\u6c60\uff08\u4f8b\u5982\uff0cX-ray absorption spectroscopy\u6db2\u4f53\u6c60, X-ray diffraction\u6db2\u4f53\u6c60\u7b49\uff09\u63d0\u4f9b\u4e86\u542f\u53d1\u548c\u6307\u5bfc\u3002<\/p>\n

\u8bba\u6587\u5730\u5740\uff1ahttps:\/\/www.nature.com\/articles\/s41596-022-00762-y<\/p>\n","protected":false},"excerpt":{"rendered":"

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