{"id":235563,"date":"2022-04-07T06:45:30","date_gmt":"2022-04-06T22:45:30","guid":{"rendered":"\/\/m.iemloyee.com\/?p=235563"},"modified":"2022-04-06T21:52:46","modified_gmt":"2022-04-06T13:52:46","slug":"%e7%86%8a%e5%ae%87%e6%9d%b0%e9%be%99%e5%86%89%e7%ad%89-adv-sci-%ef%bc%9acu2o%e8%b6%85%e5%be%ae%e7%b2%92%e9%ab%98%e9%80%89%e6%8b%a9%e6%80%a7%e7%94%b5%e5%82%ac%e5%8c%96co2%e8%bf%98%e5%8e%9f","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=235563","title":{"rendered":"\u718a\u5b87\u6770&\u9f99\u5189\u7b49 Adv. Sci.\uff1aCu2O\u8d85\u5fae\u7c92\u9ad8\u9009\u62e9\u6027\u7535\u50ac\u5316CO2\u8fd8\u539f\u4e3aC2+\u4ea7\u7269"},"content":{"rendered":"

\u4e00\u3001\u3010\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u7535\u50ac\u5316CO2<\/sub>\u8fd8\u539f\u53cd\u5e94\uff08CO2 reduction reaction, CO2<\/sub>RR\uff09<\/strong><\/span>\u751f\u4ea7\u6709\u4ef7\u503c\u7684C2+<\/sub>\u4ea7\u7269\u662f\u4e00\u79cd\u975e\u5e38\u6709\u524d\u9014\u7684\u7b56\u7565\uff0c\u6765\u89e3\u51b3\u4e0e\u5316\u77f3\u71c3\u6599\u6301\u7eed\u6d88\u8017\u6709\u5173\u7684\u80fd\u6e90\u548c\u73af\u5883\u95ee\u9898\u3002\u5176\u4e2d\uff0c\u94dc\uff08Cu\uff09\u57fa\u50ac\u5316\u5242\u662f\u6700\u6709\u5e0c\u671b\u7684\u91d1\u5c5e\u50ac\u5316\u5242\uff0c\u7531\u4e8e\u5176\u4e0e*CO\u4e2d\u95f4\u4f53\u7684\u4e2d\u7b49\u7ed3\u5408\u80fd\uff0c\u80fd\u4ee5\u53ef\u89c2\u7684\u4ea7\u7387\u4ea7\u751fC2+<\/sub>\u4ea7\u7269\u3002\u7136\u800c\uff0c\u5408\u7406\u8bbe\u8ba1Cu\u57fa\u50ac\u5316\u5242\u5e76\u4e0d\u5bb9\u6613\uff0c\u56e0\u4e3a\u5728\u7535\u5316\u5b66CO2<\/sub>\u8fd8\u539f\u7535\u4f4d\u4e0b\u4e0d\u53ef\u907f\u514d\u7684\u53d1\u751f\u7ed3\u6784\u91cd\u6784\u3002\u7814\u7a76\u53d1\u73b0\uff0cCu\u7eb3\u7c73\u9897\u7c92\u53ef\u901a\u8fc7\u7535\u5316\u5b66\u7eb3\u7c73\u6676\u4f53\u6270\u4e71\u4ea7\u751f\u65e0\u5e8f\u7ed3\u6784\uff0c\u5bf9\u4f4e\u8fc7\u7535\u4f4dC2+<\/sub>\u7684\u5f62\u6210\u5177\u6709\u5185\u5728\u7684\u6d3b\u6027\uff0c\u4f46\u7ed3\u6784\u91cd\u5efa\u5bf9CO2<\/sub>RR\u6027\u80fd\u4ecd\u6709\u5f88\u5927\u7684\u4e0d\u786e\u5b9a\u6027\u3002\u5728\u67d0\u4e9b\u60c5\u51b5\u4e0b\uff0cCu\u57fa\u50ac\u5316\u5242\u5728\u7ed3\u6784\u91cd\u5efa\u8fc7\u7a0b\u4e2d\u53ef\u80fd\u4f1a\u5931\u53bb\u7535\u50ac\u5316\u6d3b\u6027\u548c\u9009\u62e9\u6027\uff0c\u4f7f\u5f97\u5408\u7406\u8bbe\u8ba1Cu\u57fa\u50ac\u5316\u5242\u5177\u6709\u6311\u6218\u6027\u3002\u56e0\u6b64\uff0cCu\u57fa\u9884\u50ac\u5316\u5242\u7684\u5408\u7406\u9009\u62e9\u548c\u5bf9\u5176\u7ed3\u6784\u6f14\u5316\u7684\u6df1\u523b\u7406\u89e3\u662f\u5b9e\u73b0\u9ad8\u6027\u80fd\u751f\u6210C2+<\/sub>\u4ea7\u7269\u7684\u5173\u952e\u3002<\/p>\n

\u80f6\u4f53\u8d85\u5fae\u7c92\uff08colloidal superparticles\uff09<\/span><\/strong>\u7531\u5c3a\u5bf8\u548c\u5f62\u72b6\u53ef\u63a7\u7684\u7eb3\u7c73\u9897\u7c92\u81ea\u7ec4\u88c5\u800c\u6210\uff0c\u662f\u4e00\u7c7b\u5177\u6709\u590d\u6742\u7ed3\u6784\u7684\u6750\u6599\uff0c\u5728\u5149\u50ac\u5316\u3001\u5149\u5b50\u5668\u4ef6\u7b49\u9886\u57df\u5747\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u6027\u80fd\u3002\u5f53Cu\u57fa\u8d85\u5fae\u7c92\u4f5c\u4e3a\u7535\u5316\u5b66CO2<\/sub>\u8fd8\u539f\u7684\u9884\u50ac\u5316\u5242\u65f6\uff0c\u7194\u5408\u80fd\u8bf1\u5bfc\u6676\u754c\u7684\u5f62\u6210\uff0c\u5206\u79bb\u80fd\u4ea7\u751f\u7eb3\u7c73\u95f4\u9699\u9650\u5236OH–<\/sup>\u7269\u79cd\uff0c\u7ef4\u6301\u8f83\u9ad8\u7684pH\u503c\uff0c\u4e24\u8005\u90fd\u662f\u52a0\u901fC-C\u8026\u5408\u7684\u91cd\u8981\u56e0\u7d20\u3002\u56e0\u6b64\uff0cCu\u57fa\u8d85\u5fae\u7c92\u662f\u751f\u6210C2+<\/sub>\u4ea7\u7269\u7684\u9ad8\u6548\u91cd\u6784\u7ed3\u6784\u7684\u6f5c\u5728\u9884\u50ac\u5316\u5242\uff0c\u4f46\u5728\u7535\u5316\u5b66CO2<\/sub>\u8fd8\u539f\u7535\u4f4d\u4e0b\uff0c\u8d85\u7c92\u5b50\u7684\u7ed3\u6784\u53d8\u5316\u4ecd\u6709\u5f85\u63a2\u7d22\u3002
\n \"\"
\n \u4e8c\u3001\u3010\u6210\u679c\u63a0\u5f71\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u4e2d\u56fd\u79d1\u5b66\u6280\u672f\u5927\u5b66\u718a\u5b87\u6770\u6559\u6388\u548c\u9f99\u5189\u6559\u6388\u3001\u65b0\u52a0\u5761\u79d1\u6280\u7814\u7a76\u5c40\u6750\u6599\u7814\u7a76\u4e0e\u5de5\u7a0b\u7814\u7a76\u6240Enyi Ye\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba<\/strong>\u62a5\u9053\u4e86\u5229\u7528\u7b80\u5355\u65b9\u6cd5\u5408\u6210\u7684Cu2<\/sub>O\u8d85\u5fae\u7c92\u4f5c\u4e3a\u7535\u5316\u5b66CO2<\/sub>RR\u7684\u6a21\u578b\u9884\u50ac\u5316\u5242\uff0c\u5728\u7535\u5316\u5b66\u8fd8\u539f\u6761\u4ef6\u4e0bCu2<\/sub>O\u8d85\u5fae\u7c92\u4f1a\u7ecf\u5386\u590d\u6742\u7684\u7ed3\u6784\u6f14\u5316\uff0c\u4ece\u800c\u5728\u7535\u50ac\u5316\u4e2d\u5b9e\u73b0\u9ad8\u9009\u62e9\u6027\u7684\u50ac\u5316CO2<\/sub>\u8f6c\u5316\u4e3aC2+<\/sub>\u4ea7\u7269\u3002\u7535\u5b50\u663e\u5fae\u955c\u8868\u5f81\u4ee5\u53ca\u539f\u4f4dX\u5c04\u7ebf\u5438\u6536\u5149\u8c31\uff08XAS\uff09\u548c\u62c9\u66fc\u5149\u8c31\u53d1\u73b0\uff0c\u8d85\u5fae\u7c92\u5185\u90e8\u7684\u6784\u4ef6\u878d\u5408\u4ea7\u751f\u5927\u91cf\u6676\u754c\uff0c\u800c\u5916\u58f3\u4e2d\u7684\u6784\u4ef6\u5206\u79bb\u5f62\u6210\u7eb3\u7c73\u95f4\u9699\u7ed3\u6784\uff0c\u53ef\u4ee5\u6709\u6548\u5730\u9650\u5236OH–<\/sup>\u4ee5\u8bf1\u5bfc\u9ad8\u5c40\u90e8pH\u503c\u3002\u8fd9\u79cd\u72ec\u7279\u7684\u7ed3\u6784\u7279\u5f81\u4e0e\u5c40\u90e8\u53cd\u5e94\u73af\u5883\u7684\u7ed3\u5408\uff0c\u4e3a\u4fc3\u8fdbC-C\u5076\u8054\u63d0\u4f9b\u4e86\u4e24\u4e2a\u91cd\u8981\u56e0\u7d20\u3002\u56e0\u6b64\uff0cCu2<\/sub>O\u8d85\u5fae\u7c92\u884d\u751f\u50ac\u5316\u5242\u5bf9\u7535\u50ac\u5316CO2<\/sub>\u8f6c\u5316\u4e3a\u4e59\u70ef\uff08C2<\/sub>H4<\/sub>\uff09\u548cC2+<\/sub>\u4ea7\u7269\u7684\u6cd5\u62c9\u7b2c\u6548\u7387\uff08FE\uff09\u5206\u522b\u4e3a53.2%\u548c74.2%\uff0c\u8d85\u8fc7\u4e86\u51e0\u4f55\u4e0a\u66f4\u7b80\u5355\u7684Cu2<\/sub>O\u7acb\u65b9\u4f53\u884d\u751f\u50ac\u5316\u5242\uff0c\u4ee5\u53ca\u5728\u76f8\u540c\u6761\u4ef6\u4e0b\u5927\u591a\u6570\u5df2\u62a5\u9053\u7684Cu\u57fa\u7535\u50ac\u5316\u5242\u7684\u6027\u80fd\u3002\u8be5\u5de5\u4f5c\u4e3a\u901a\u8fc7\u63a7\u5236\u7ed3\u6784\u91cd\u6784\u5408\u7406\u8bbe\u8ba1\u9ad8\u9009\u62e9\u6027CO2<\/sub>\u8fd8\u539f\u7535\u50ac\u5316\u5242\u63d0\u4f9b\u4e86\u89c1\u89e3\u3002\u7814\u7a76\u6210\u679c\u4ee5\u9898\u4e3a\u201cStructural Reconstruction of Cu2<\/sub>O Superparticles toward Electrocatalytic CO2<\/sub> Reduction with High C2+<\/sub> Products Selectivity\u201d<\/strong>\u53d1\u5e03\u5728\u56fd\u9645\u8457\u540d\u671f\u520aAdv. Sci.<\/em><\/strong>\u4e0a\u3002<\/p>\n

\u4e09\u3001\u3010\u6838\u5fc3\u521b\u65b0\u70b9\u3011<\/strong><\/p>\n

1\u3001Cu2<\/sub>O\u8d85\u5fae\u7c92\u4f5c\u4e3a\u7535\u5316\u5b66CO2<\/sub>RR\u7684\u6a21\u578b\u9884\u50ac\u5316\u5242\uff0c\u5b9e\u73b0\u9ad8\u9009\u62e9\u6027\u7684\u50ac\u5316CO2<\/sub>\u8f6c\u5316\u4e3aC2+<\/sub>\u4ea7\u7269\u3002<\/p>\n

2\u3001Cu2<\/sub>O\u8d85\u5fae\u7c92\u884d\u751f\u50ac\u5316\u5242\u5bf9\u4e59\u70ef\uff08C2<\/sub>H4<\/sub>\uff09\u548cC2+<\/sub>\u4ea7\u7269\u7684\u6cd5\u62c9\u7b2c\u6548\u7387\uff08FE\uff09\u5206\u522b\u4e3a53.2%\u548c74.2%\uff0c\u8d85\u8fc7\u4e86Cu2<\/sub>O\u7acb\u65b9\u4f53\u884d\u751f\u50ac\u5316\u5242\u548c\u5927\u591a\u6570\u5df2\u62a5\u9053\u7684Cu\u57fa\u7535\u50ac\u5316\u5242\u7684\u6027\u80fd\u3002<\/p>\n

\u56db\u3001\u3010\u6570\u636e\u6982\u89c8\u3011<\/strong><\/p>\n

\u56fe\u4e00\u3001\u7535\u5316\u5b66\u8fd8\u539f\u6761\u4ef6\u4e0b\u8d85\u5fae\u7c92\u53ef\u80fd\u7684\u7ed3\u6784\u91cd\u6784\u8fc7\u7a0b\u793a\u610f\u56fe \u00a9 2022 The Authors<\/span><\/strong><\/p>\n

\"\"<\/p>\n

\u56fe\u4e8c\u3001Cu2<\/sub>O\u9884\u50ac\u5316\u5242\u7684\u5408\u6210\u4e0e\u8868\u5f81\u00a0\u00a9 2022 The Authors<\/span><\/strong>
\n \"\"\uff08a\uff09\u9884\u7535\u5316\u5b66\u8fd8\u539f\u540e\uff0cCu2<\/sub>O\u8d85\u5fae\u7c92\u7684\u7ed3\u6784\u6f14\u53d8\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b\uff09Ketjen\u70ad\u9ed1\u4e0a\u7684Cu2<\/sub>O\u8d85\u5fae\u7c92\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

\uff08c\uff09Cu2<\/sub>O\u8d85\u5fae\u7c92\u7684TEM\u56fe\u50cf\u548c\u76f8\u5e94\u7684SAED\u56fe\u6848\uff1b<\/p>\n

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\uff08h\uff09Cu2<\/sub>O\u8d85\u5fae\u7c92-CP3\u4e2d\u5c0f\u7684\u5206\u79bb\u7684Cu\u7eb3\u7c73\u9897\u7c92\u7684HRTEM\u56fe\u50cf\uff1b<\/p>\n

\uff08i\uff09\u9884\u7535\u5316\u5b66\u8fd8\u539f\u540e\uff0cCu2<\/sub>O\u7acb\u65b9\u4f53\u7684\u7ed3\u6784\u6f14\u53d8\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08j\uff09Ketjen\u70ad\u9ed1\u4e0aCu2<\/sub>O\u7acb\u65b9\u4f53\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

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\uff08l-m\uff09\u901a\u8fc7CP\uff08Cu2<\/sub>O\u7acb\u65b9\u4f53-CP3\uff09\u4eceCu2<\/sub>O\u7acb\u65b9\u4f53\u884d\u751f\u7684Cu\u50ac\u5316\u5242\u7684SEM\u548cHRTEM\u56fe\u50cf\u3002<\/p>\n

\u56fe\u4e09\u3001CO2<\/sub>\u7535\u8fd8\u539f\u6027\u80fd\u00a0\u00a9 2022 The Authors<\/span><\/strong>
\n \"\"\uff08a-b\uff09\u4e09\u79cd\u50ac\u5316\u5242\u7684C2<\/sub>H4<\/sub>\u548cC2+<\/sub>\u4ea7\u7269\u7684\u6cd5\u62c9\u7b2c\u6548\u7387\uff08FE\uff09\uff1b<\/p>\n

\uff08c\uff09\u4e09\u79cd\u50ac\u5316\u5242\u5728-1.15 V vs HE\u4e0b\u7684C2+<\/sub>\/C1<\/sub>\u6cd5\u62c9\u7b2c\u6548\u7387\uff08FE\uff09\u6bd4\uff1b<\/p>\n

\uff08d\uff09\u4e09\u79cd\u50ac\u5316\u5242\u5728\u6d4b\u8bd5\u7535\u4f4d\u4e0b\u7684\u603b\u7535\u6d41\u5bc6\u5ea6\u4ee5\u53caC2<\/sub>H4<\/sub>\u548cC2+<\/sub>\u4ea7\u7269\u7684\u5c40\u90e8\u7535\u6d41\u5bc6\u5ea6\uff1b<\/p>\n

\uff08f\uff09Cu2<\/sub>O\u8d85\u5fae\u7c92-CP3\u5728-40 mA cm-2<\/sup>\u4e0b\u7684\u7a33\u5b9a\u6027\u6d4b\u8bd5\u3002<\/p>\n

\u56fe\u56db\u3001\u539f\u4f4d\u8868\u5f81 \u00a0\u00a9 2022 The Authors<\/span><\/strong>
\n \"\"\uff08a\uff09Cu2<\/sub>O\u8d85\u5fae\u7c92-CP3\u548cCu2<\/sub>O\u7acb\u65b9\u4f53-CP3\u7684\u539f\u4f4dCu K<\/em>-edge XANES\u5149\u8c31\uff1b<\/p>\n

\uff08b\uff09\u76f8\u5e94\u7684FT-EXAFS\u5149\u8c31\uff1b<\/p>\n

\uff08c-d\uff09Cu2<\/sub>O\u8d85\u5fae\u7c92-CP3\u548cCu2<\/sub>O\u7acb\u65b9\u4f53-CP3\u5728-1.15 V vs RHE\u7684R\u7a7a\u95f4\u4e2d\u7684EXAFS\u62df\u5408\u66f2\u7ebf\u3002<\/p>\n

\u56fe\u4e94\u3001\u673a\u7406\u7814\u7a76 \u00a0\u00a9 2022 The Authors<\/span><\/strong>
\n \"\"\uff08a-b\uff09Cu2<\/sub>O\u8d85\u5fae\u7c92-CP3\u548cCu2<\/sub>O\u7acb\u65b9\u4f53-CP3\u5728CO2<\/sub>RR\u8fc7\u7a0b\u4e2d\u7684\u539f\u4f4d\u62c9\u66fc\u5149\u8c31\uff1b<\/p>\n

\uff08c\uff09lead\u7684\u6b20\u7535\u4f4d\u6c89\u79ef\uff1aPb\u5355\u5c42\u5265\u79bb\u5cf0\uff1b<\/p>\n

\uff08d\uff09\u57280.1 M KOH\u6eb6\u6db2\u4e2d\u6536\u96c6\u7684OHads<\/sub>\u5cf0\u7684\u4f0f\u5b89\u56fe\uff1b<\/p>\n

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\u4e94\u3001\u3010\u6210\u679c\u542f\u793a\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1aStructural Reconstruction of Cu2<\/sub>O Superparticles toward Electrocatalytic CO2<\/sub> Reduction with High C2+<\/sub> Products Selectivity<\/a><\/strong>. Adv. Sci.<\/em>, 2022<\/strong>, DOI: 10.1002\/advs.202105292.<\/p>\n

\u672c\u6587\u7531CQR\u7f16\u8bd1\u3002<\/p>\n

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