{"id":232901,"date":"2022-02-12T06:25:11","date_gmt":"2022-02-11T22:25:11","guid":{"rendered":"\/\/m.iemloyee.com\/?p=232901"},"modified":"2022-02-11T21:25:18","modified_gmt":"2022-02-11T13:25:18","slug":"%e9%9f%a9%e5%9b%bd%e6%88%90%e5%9d%87%e9%a6%86%e5%a4%a7%e5%ad%a6aem%ef%bc%9a%e4%ba%8c%e7%bb%b4%e6%89%ad%e6%9b%b2%e8%81%9a%e5%90%88%e7%89%a9%e9%9d%9e%e6%99%b6%e5%8c%96%e9%87%91%e5%b1%9e%e7%ba%b3","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=232901","title":{"rendered":"\u97e9\u56fd\u6210\u5747\u9986\u5927\u5b66AEM\uff1a\u4e8c\u7ef4\u626d\u66f2\u805a\u5408\u7269\u975e\u6676\u5316\u91d1\u5c5e\u7eb3\u7c73\u7c92\u5b50\u53ca\u5176\u5728\u6790\u6c22\u53cd\u5e94\u4e2d\u7684\u5e94\u7528"},"content":{"rendered":"

\u4e00\u3001\u80cc\u666f\u4ecb\u7ecd<\/strong><\/p>\n

\u5728\u78b1\u6027\u6eb6\u6db2\u4e2d\u7535\u89e3\u6c34\u5236\u6c22\u662f\u4e00\u79cd\u5f88\u6709\u524d\u666f\u7684\u6e05\u6d01\u6c22\u80fd\u6280\u672f\u3002\u7136\u800c\uff0c\u4f20\u7edf\u7684\u94c2\u57fa\u50ac\u5316\u5242\u7531\u4e8e\u6210\u672c\u9ad8\u3001\u7a33\u5b9a\u6027\u5dee\u7b49\u56e0\u7d20\u9650\u5236\u4e86\u5176\u5728\u8be5\u9886\u57df\u7684\u5e94\u7528\u3002\u7814\u7a76\u8005\u53d1\u73b0\u4e00\u4e9b\u65e0\u5b9a\u5f62\u6750\u6599\uff0c\u5982\u91d1\u5c5e\u78f7\u5316\u7269\u3001\u91d1\u5c5e\u786b\u5316\u7269\u548c\u91d1\u5c5e\u6c27\u5316\u7269\uff0c\u6bd4\u5904\u4e8e\u7ed3\u6676\u72b6\u6001\u7684\u76f8\u540c\u6750\u6599\u8868\u73b0\u51fa\u66f4\u597d\u7684\u7535\u50ac\u5316\u6027\u80fd\u3002\u7136\u800c\uff0c\u7531\u4e8e\u5728\u9ad8\u6e29\u4e0b\u5b58\u5728\u5f3a\u539f\u5b50\u95f4\u91d1\u5c5e\u952e\uff0c\u56e0\u6b64\u96be\u4ee5\u5408\u6210\u975e\u6676\u6001\u91d1\u5c5eNPs\u6216NCs\u63ba\u6742\u7684\u78b3\u6750\u6599\uff0c\u8bbe\u8ba1\u975e\u6676\u91d1\u5c5e\u6750\u6599\u4ecd\u7136\u5177\u6709\u6311\u6218\u6027\u3002<\/p>\n

\u4e8c\u3001\u6210\u679c\u7b80\u4ecb<\/strong><\/p>\n

\u97e9\u56fd\u6210\u5747\u9986\u5927\u5b66\u57fa\u7840\u79d1\u5b66\u7814\u7a76\u6240<\/strong>(IBS)<\/strong>\u7efc\u5408\u7eb3\u7c73\u7ed3\u6784\u7269\u7406\u4e2d\u5fc3<\/strong>(CINAP)<\/strong>\u6559\u6388Young Hee Lee<\/strong>\u548c\u4ed6\u7684\u7814\u7a76\u4eba\u5458\u4f7f\u7528\u626d\u66f2\u7684\u5171\u4ef7\u6709\u673a\u7f51\u7edc(CON)\u6210\u529f\u5408\u6210\u4e86\u4e00\u7cfb\u5217\u65e0\u5b9a\u5f62\u8fc7\u6e21\u91d1\u5c5e\u7eb3\u7c73\u7c92\u5b50(NPs)\u3002\u4f4e\u8d1f\u8f7d\u91cf\u7684RuCl3<\/sub>\u4f1a\u4ea7\u751f\u65e0\u5b9a\u5f62Ru\u7eb3\u7c73\u56e2\u7c07(NCs)\uff0c\u800c\u9ad8\u8d1f\u8f7d\u7684RuCl3<\/sub>\u4f1a\u5f62\u6210\u6676\u4f53\u5360\u4e3b\u5bfc\u5730\u4f4d\u7684Ru NPs\u3002\u7814\u7a76\u53d1\u73b0\uff0c\u4e0e\u6df7\u5408\u76f8Ru-CON\u6750\u6599\u76f8\u6bd4\uff0c\u7eaf\u975e\u6676\u6001Ru-CON\u8868\u73b0\u51fa\u66f4\u597d\u7684\u8d28\u91cf\u6d3b\u6027\u548c\u66f4\u9ad8\u7684\u7a33\u5b9a\u6027\u3002\u4f7f\u7528\u76f8\u4f3c\u7684\u5408\u6210\u7b56\u7565\uff0c\u4f5c\u8005\u6210\u529f\u5730\u5236\u5907\u4e86\u65e0\u5b9a\u5f62\u7ed3\u6784\u7684Fe NPs\u548cIr NPs\u5e76\u7528\u4e8eHER\u6d4b\u8bd5\u3002\u76f8\u5173\u8bba\u6587\u4ee5\u9898\u4e3a \u201cAmorphization of Metal Nanoparticles by 2D Twisted Polymer for Super Hydrogen Evolution Reaction<\/em>\u201d\u53d1\u8868\u5728 Adv. Energy Mater<\/i>.<\/strong>\u4e0a\u3002<\/p>\n

\u4e09\u3001\u56fe\u6587\u89e3\u6790<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>1<\/strong> Ru-CON\u7684\u5408\u6210\u548c\u7ed3\u6784\u793a\u610f\u56fe \u00a92022 Wiley<\/span><\/p>\n

\u5982\u56fe<\/strong>1<\/strong>\u6240\u793a\uff0cRuCl3<\/sub>\u4f5c\u4e3a\u50ac\u5316\u5242\u548c\u948c\u6e90\uff0cTAPB\u548cTPA\u53d1\u751f\u7f29\u5408\u53cd\u5e94\uff0c\u5408\u6210\u4e86Ru-CON\u6750\u6599\u3002\u9000\u706b\u540e\uff0c\u7531CON\u884d\u751f\u7684\u591a\u5b54\u7c7b\u77f3\u58a8\u4e8c\u7ef4\u78b3\u6750\u6599\u53ef\u4ee5\u6709\u6548\u63a7\u5236Ru NPs\u7684\u7c92\u5f84\uff0c\u9632\u6b62Ru\u5728\u78b1\u6027\u73af\u5883\u4e2d\u6cc4\u6f0f\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>2 <\/strong>Ru-CON\u50ac\u5316\u5242\u7684\u7ed3\u6784\u8868\u5f81\u548c\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c(TEM)\u5206\u6790 \u00a92022 Wiley<\/span><\/p>\n

\u5982\u56fe<\/strong>2<\/strong>\u6240\u793a\uff0c\u901a\u8fc7\u5085\u91cc\u53f6\u53d8\u6362\u7ea2\u5916\u5149\u8c31(FTIR)\u6765\u68c0\u6d4b\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u632f\u52a8\u5cf0\u7684\u53d8\u5316\u3002\u7f29\u5408\u53cd\u5e94\u540e\uff0c\u2013C=O\u548c\u2013NH2\u7684\u5178\u578b\u7279\u5f81\u5cf0\u51e0\u4e4e\u6d88\u5931\uff0c\u8868\u660e\u53cd\u5e94\u8fdb\u884c\u5b8c\u5168\u3002XRD\u8868\u5f81\u663e\u793a\u968f\u7740RuCl3<\/sub>\u542b\u91cf\u7684\u589e\u52a0\uff0c\u6676\u4f53Ru NPs\u5cf0\u9010\u6e10\u51fa\u73b0\uff0c\u8fd9\u8868\u660e\u7ed3\u6676Ru NPs\u7684\u6570\u91cf\u968f\u7740RuCl3<\/sub>\u7684\u589e\u52a0\u800c\u589e\u52a0\u3002\u901a\u8fc7TEM\u89c2\u6d4bRu-CON 30 mg\u7684\u5fae\u89c2\u7ed3\u6784\u53d1\u73b0\u5ba4\u6e29\u4e0b\u5176\u7ed3\u6784\u4e3a\u4ea4\u9519\u5c42\u7ed3\u6784\u3002\u9000\u706b\u540e\uff0c\u626d\u66f2\u5c42\u7ed3\u6784\u51e0\u4e4e\u6ca1\u6709\u53d8\u5316\uff0c\u8fd9\u8bf4\u660eRu-CON\u5177\u6709\u4f18\u5f02\u7684\u70ed\u7a33\u5b9a\u6027\u3002\u66f4\u91cd\u8981\u7684\u662f\uff0c\u9000\u706b\u540eRu-CON 30 mg\u7684EDS\u5149\u8c31\u6e05\u695a\u5730\u8868\u660e\u5b58\u5728\u78b3(C)\u3001\u6c2e(N)\u548c\u948c(Ru)\u5143\u7d20\u3002\u8fd9\u8868\u660e\u65e0\u5b9a\u5f62Ru NCs\u5747\u5300\u5206\u6563\u5728CON\u6846\u67b6\u7684\u591a\u5b54\u7ed3\u6784\u4e2d\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>3 <\/strong>Ru-CON\u50ac\u5316\u5242\u7684\u9ad8\u5206\u8fa8\u7387\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c(TEM)\u5206\u6790 \u00a92022 Wiley<\/span><\/p>\n

\u56fe<\/strong>3<\/strong>\u91c7\u7528HAADF STEM\u8fdb\u4e00\u6b65\u7814\u7a76Ru-CON 30 mg\u4e2dRu\u7684\u771f\u5b9e\u7ed3\u6784\uff0c\u53ef\u4ee5\u89c2\u5bdf\u5230\u5ba4\u6e29\u4e0bRu-CON 30 mg\u4e2d\u542b\u6709\u9ad8\u6d53\u5ea6\u7684Ru\u5355\u539f\u5b50\u548cNC\uff0c\u8868\u660eCON\u4e2d\u6709\u5145\u8db3\u7684\u6c2e\u4f4d\u70b9\u4e0eRu\u539f\u5b50\u914d\u4f4d\uff0c\u963b\u6b62\u4e86Ru\u7684\u805a\u96c6\u3002\u9000\u706b\u540e\uff0cRu-CON 30 mg\u4e2dRu NC\u7684\u5e73\u5747\u76f4\u5f84\u7ea6\u4e3a1.5 nm\u3002\u5f53RuCl3<\/sub>\u91cf\u589e\u52a0\u523080 mg\u65f6\uff0cRu-CON 80 mg\u4e2d\u7684Ru NPs\u7684\u5c3a\u5bf8\u7565\u6709\u589e\u52a0(\u5927\u7ea63 nm)\uff0c\u540c\u65f6\u89c2\u5bdf\u5230\u5177\u6709\u76f8\u4f3c\u5c3a\u5bf8\u7684\u65e0\u5e8f\u548c\u6709\u5e8fRu NPs\u3002\u5f53RuCl3<\/sub>\u91cf\u8fdb\u4e00\u6b65\u589e\u52a0\u5230150 mg\uff0cCON\u8868\u9762\u4e0a\u7684Ru NPs\u5747\u5300\u4e14\u9ad8\u5ea6\u5206\u6563\u3002\u6240\u6709TEM\u7ed3\u679c\u8868\u660e\uff0c\u591a\u5b54CON\u805a\u5408\u7269\u662f\u6355\u83b7Ru\u539f\u5b50\u548c\u63a7\u5236Ru NPs\u5c3a\u5bf8\u7684\u7edd\u4f73\u5019\u9009\u8005\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>4<\/strong> Ru-CON \u6750\u6599\u7684XPS\u3001XANES\u548cXAFS \u00a92022 Wiley<\/span><\/p>\n

\u56fe<\/strong>4<\/strong>\u9996\u5148\u901a\u8fc7XPS\u8868\u5f81\u4e86Ru-CON\u4e2d\u5143\u7d20\u7684\u5316\u5b66\u6210\u5206\u548c\u72b6\u6001\u3002\u7531\u4e8eRu\u539f\u5b50\u7684\u8f7b\u5fae\u805a\u96c6\u548c\u4e00\u4e9b\u6709\u5e8f\u7684\u5b58\u5728\uff0c\u9000\u706b\u540eRu-CON\u4e2d\u7684\u6240\u6709Ru 3p1\/2\u548cRu 3p3\/2\u5cf0\u90fd\u8f6c\u79fb\u5230\u8f83\u4f4e\u7684\u80fd\u91cfRu NPs\u3002\u5bf9\u4e8eRu-CON 150 mg\uff0c\u7ed3\u5408\u80fd\u6574\u4f53\u53d1\u751f\u4e86\u964d\u4f4e\uff0c\u8fd9\u8bf4\u660e\u5f62\u6210\u4e86\u66f4\u6709\u5e8f\u7684 Ru NPs\u3002\u800cRu-CON 30 mg\u7ed3\u5408\u80fd\u53ea\u964d\u4f4e\u4e86\u5f88\u5c11\uff0c\u518d\u6b21\u8bc1\u660e\u4e86\u65e0\u5e8fRu\u539f\u5b50\u7684\u5b58\u5728\u3002X\u5c04\u7ebf\u5438\u6536\u8fd1\u8fb9\u7ed3\u6784(XANES)\u5149\u8c31\u663e\u793a\u4e86Ru-CON 150 mg\u4e2d\u7684Ru\u4ef7\u6001\u4ecd\u9ad8\u4e8eRu\u7b94\uff0c\u8868\u660e\u5b58\u5728\u76f8\u5f53\u6570\u91cf\u7684\u65e0\u5e8fRu-N\u3002\u5085\u91cc\u53f6\u53d8\u6362\u6269\u5c55X\u5c04\u7ebf\u5438\u6536\u7cbe\u7ec6\u7ed3\u6784(EXAFS)\u5149\u8c31\u53d1\u73b0Ru\u7b94\u7684EXAFS\u5149\u8c31\u4e2d\u4f4d\u4e8e2.39 \u00c5\u7684\u4e3b\u5cf0\u5bf9\u5e94\u4e8e\u5e73\u5747\u6700\u8fd1\u7684Ru-Ru\u952e\u957f\uff0c\u4e0eRu\u7b94\u76f8\u6bd4\uff0cRu-CON 30 mg\u548cRu-CON 150 mg\u7684Ru-Ru\u5cf0\u79fb\u52a8\u5230\u66f4\u5927\u7684\u8ddd\u79bb\u3002\u8fd9\u5f52\u56e0\u4e8e\u65e0\u5e8fRu NPs\u7684\u5b58\u5728\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>5 <\/strong>\u4e0d\u540c\u6761\u4ef6\u4e0bRu-CON\u50ac\u5316\u5242\u5728\u78b1\u6027\u4ecb\u8d28\u4e2d\u7684HER\u6027\u80fd \u00a92022 Wiley<\/span><\/p>\n

\u56fe5<\/strong>\u4e2d\uff0c\u4f5c\u8005\u4ee5Hg\/HgO\u4f5c\u4e3a\u53c2\u6bd4\u7535\u6781\uff0c\u4f7f\u7528\u7ebf\u6027\u626b\u63cf\u4f0f\u5b89\u6cd5\u57281 m KOH\u6eb6\u6db2\u4e2d\u63a2\u7d22\u4e86\u4e00\u7cfb\u5217Ru-CON\u50ac\u5316\u5242\u7684HER\u6027\u80fd\u3002\u5728\u76f8\u540c\u6761\u4ef6\u4e0b\u6d4b\u91cf\u4e86\u5546\u4e1a20 wt% Pt\/C\u50ac\u5316\u5242\u548cCON\u4f5c\u4e3a\u53c2\u7167\u3002Ru-CON 150 mg \u663e\u793a\u51fa\u6bd4\u5546\u4e1a20 wt% Pt\/C\u66f4\u597d\u7684\u7535\u50ac\u5316\u6d3b\u6027\u3002\u4f5c\u8005\u8fdb\u4e00\u6b65\u5408\u6210\u4e86Ru-CON 150 mg (700 \u00b0C, 2 h)\u7528\u4e8e\u7814\u7a76\u9000\u706b\u6e29\u5ea6\u7684\u5f71\u54cd\u3002Ru-CON-150 mg-700 \u00b0C\u7684HER\u6d3b\u6027\u4f4e\u4e8e800 \u00b0C\u65f6\u7684HER\u6d3b\u6027\u3002\u62c9\u66fc\u6d4b\u8bd5\u7ed3\u679c\u8868\u660eRu-CON 150 mg-800 \u00b0C\u6709\u66f4\u9ad8\u7684ID\/IG\u6bd4\u503c\uff0c\u8fd9\u610f\u5473\u5728\u9ad8\u6e29\u4e0b\u5bb9\u6613\u5f62\u6210\u66f4\u591a\u7684\u7f3a\u9677\u78b3\u5c42\uff0c\u53ef\u80fd\u6709\u76ca\u4e8e\u589e\u52a0HER\u6d3b\u6027\u3002\u4f5c\u8005\u6bd4\u8f83\u4e86\u76f8\u540c\u6761\u4ef6\u4e0b\u4e0d\u540cRu\u542b\u91cf\u7684Ru-CON\u7684HER\u6d3b\u6027\uff0c\u53d1\u73b0\u968f\u7740Ru\u542b\u91cf\u7684\u589e\u52a0\uff0cRu-CON\u6750\u6599\u7684HER\u6027\u80fd\u9010\u6e10\u63d0\u9ad8\uff0c\u603b\u4e4b\uff0cRu-CON\u6837\u54c1\u7684\u6790\u6c22\u52a8\u529b\u5b66\u603b\u4f53\u901f\u5ea6\u76f8\u8f83\u4e8e\u5546\u4e1aPt\/C\u50ac\u5316\u5242\u66f4\u5feb\u3002<\/p>\n

\"\"<\/p>\n

\u56fe<\/strong>6<\/strong> \u6709\u5e8f\u548c\u65e0\u5e8fS-Ru-CON\u50ac\u5316\u5242\u7684DFT\u8ba1\u7b97\u7814\u7a76 \u00a92022 Wiley<\/span><\/p>\n

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\u56fe<\/strong>7<\/strong> \u5236\u5907\u7684\u91d1\u5c5e-CON\u6750\u6599\u7684\u5806\u53e0\u65b9\u5f0f\u548cIr\/Fe-CON\u7684HER\u6027\u80fd\u6d4b\u8bd5 \u00a92022 Wiley<\/span><\/p>\n

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\u6587\u732e\u94fe\u63a5: Amorphization of Metal Nanoparticles by 2D Twisted Polymer for Super Hydrogen Evolution Reaction. 2022, Advanced Energy Materials, https:\/\/doi.org\/10.1002\/aenm.202102257.<\/p>\n","protected":false},"excerpt":{"rendered":"

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