{"id":230737,"date":"2021-12-12T06:30:23","date_gmt":"2021-12-11T22:30:23","guid":{"rendered":"\/\/m.iemloyee.com\/?p=230737"},"modified":"2021-12-11T21:59:34","modified_gmt":"2021-12-11T13:59:34","slug":"%e5%ae%a1%e7%a8%bf%e7%96%91%e4%ba%91%e7%a4%be%e4%ba%a4%e5%aa%92%e4%bd%93%e9%a2%84%e5%8d%b0%e6%9c%ac%e8%b4%a8%e7%96%91-nature-catalysis%e6%92%a4%e7%a8%bf%ef%bc%81","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=230737","title":{"rendered":"\u5ba1\u7a3f\u7591\u4e91+\u793e\u4ea4\u5a92\u4f53+\u9884\u5370\u672c+\u8d28\u7591= Nature Catalysis\u64a4\u7a3f\uff01"},"content":{"rendered":"<p><strong>\u4e00\u3001\u5bfc\u8bfb<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-230738\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/1-13.png\" alt=\"\" width=\"600\" height=\"280\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/1-13.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/1-13-300x140.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u8fd1\u65e5\uff0c<em>Nature Catalysis<\/em>\u5ba3\u5e03\u64a4\u56de\u4e8e2021\u5e74\u521d\u53d1\u8868\u7684\u4e00\u7bc7\u6765\u81ea\u56fd\u5185\u67d0\u9ad8\u6821\u7684\u4e00\u9879\u6210\u679c\uff0c\u5e76\u520a\u53d1\u4e86\u6765\u81ea\u5308\u7259\u5229\u3001\u82f1\u56fd\u4ee5\u53ca\u7f8e\u56fd\u7b49\u540c\u884c\u7684\u4e09\u7bc7\u8d28\u7591\u6027\u6587\u7ae0\uff08Matters Arising\uff09\u3002\u540c\u65f6\uff0c\u7f16\u8f91\u90e8\u7279\u610f\u9488\u5bf9\u6b64\u6b21\u64a4\u7a3f\u4e8b\u4ef6\u520a\u53d1\u4e86\u4e00\u7bc7\u9898\u4e3a\u201cSelf-correcting science at work\u201d\u7684\u793e\u8bba\u3002\u4f5c\u4e3aNature\u7cfb\u5217\u671f\u520a\u7684\u4e00\u5458\uff0c\u8fd9\u662f\u5373\u5c06\u8d70\u5b8c\u7b2c\u56db\u4e2a\u5e74\u5934\u7684<em>Nature Catalysis<\/em>\u64a4\u56de\u7684\u7b2c\u4e8c\u7bc7\u6587\u7ae0\uff0c\u8ddd\u79bb\u4eca\u5e745\u6708\u7684\u9996\u6b21\u64a4\u7a3f\u8fd8\u4e0d\u5230\u4e00\u5e74\u3002<strong>\u00a0<\/strong><\/p>\n<p><strong>\u4e8c\u3001\u64a4\u7a3f\u8def\u7ebf\u56fe<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-230739\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/2-13.png\" alt=\"\" width=\"600\" height=\"235\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/2-13.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/2-13-300x118.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u4e0a\u56fe\u4e3a\u8fd9\u7bc7\u88ab\u64a4\u7a3f\u8bba\u6587\u7684\u6458\u8981\uff0c\u4ece\u4e2d\uff0c\u6211\u4eec\u53ef\u4ee5\u6355\u83b7\u5230\u4e24\u4e2a\u6700\u91cd\u8981\u8868\u8ff0\uff1a<strong>robust<\/strong><strong>\u3001catalysed by amines<\/strong>\uff0c\u8fd9\u662f\u8fd9\u7bc7\u8bba\u6587\u7684\u6838\u5fc3\u53d1\u73b0\u3002<\/p>\n<p>Suzuki-Miyaura\u53cd\u5e94\u662f\u4e00\u4e2a\u5f88\u7ecf\u5178\u7684\u6709\u673a\u5316\u5b66\u5076\u8054\u53cd\u5e94\uff0c\u5176\u53d1\u73b0\u8005Akira Suzuki\u662f2010\u5e74\u8bfa\u8d1d\u5c14\u5316\u5b66\u5956\u5f97\u4e3b\u3002\u8fd9\u4e2a\u53cd\u5e94<strong>\u539f\u672c\u662f\u91c7\u7528\u91d1\u5c5e\u94af\u7684\u914d\u5408\u7269<\/strong>\u8fdb\u884c\u50ac\u5316\uff0c\u4ece\u800c\u5b9e\u73b0C-C\u952e\u7684\u5076\u8054\uff0c\u4f46\u6602\u8d35\u7684\u91d1\u5c5e\u7684\u5b58\u5728\u52bf\u5fc5\u5bfc\u81f4\u4ea7\u7269\u4e2d\u53ef\u80fd\u7684\u91d1\u5c5e\u6742\u8d28\uff0c\u4ee5\u53ca\u8f83\u9ad8\u7684\u6210\u672c\uff0c\u56e0\u6b64\uff0c\u5c3d\u7ba1\u8fd9\u4e00\u53cd\u5e94\u7528\u9014\u5e7f\u6cdb\uff0c\u4f46\u8fd9\u4e00\u5173\u952e\u77ed\u677f\u5c1a\u672a\u5f97\u5230\u89e3\u51b3\u3002\u56e0\u6b64\uff0c\u4e0a\u8ff0\u8bba\u6587\u91c7\u7528\u4e86\u65e0\u91d1\u5c5e\u7684\u80fa\u6765\u50ac\u5316\u53cd\u5e94\uff0c\u90a3\u4e48\uff0c\u663e\u7136\u7684\u4f18\u52bf\u5c31\u4f53\u73b0\u51fa\u6765\u4e86\uff1a\u91d1\u5c5e\u7684\u5f0a\u7aef\u6ca1\u6709\u4e86\uff01\u5e76\u4e14\u5728\u8bba\u6587\u4e2d\u8fd8\u5b9e\u73b0\u4e86\u514b\u7ea7\u7684\u4ea7\u7269\u5236\u5907\uff0c\u8fd9\u6837\u7684\u60ca\u8273\u7ed3\u679c\u53d1\u8868\u5728<em>Nature<\/em>\u7cfb\u5217\u671f\u520a\u662f\u8db3\u591f\u7684\u3002<\/p>\n<p>\u4e0d\u8fc7\uff0c\u5c31\u5728\u8bba\u6587\u521a\u521a\u53d1\u8868\u4e0d\u4e45\uff0c\u5c31\u5728\u793e\u4ea4\u5a92\u4f53\u5f97\u5230\u4e86\u5173\u6ce8\uff1a<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-230746\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/3-13.png\" alt=\"\" width=\"584\" height=\"120\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/3-13.png 584w, \/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/3-13-300x62.png 300w\" sizes=\"(max-width: 584px) 100vw, 584px\" \/><\/p>\n<p>\u540c\u884c\u91cd\u590d\u5b9e\u9a8c\u7684\u65f6\u5019\u53d1\u73b0\uff0c\u6548\u679c\u6bd4\u8bba\u6587\u62a5\u9053\u7684\u4f4e\u4e86\u4e0d\u5c11\uff0c\u56e0\u6b64\uff0c\u5f15\u53d1\u4e86\u4e00\u7cfb\u5217\u8d28\u7591\u3002<\/p>\n<p>\u5f53\u6211\u4eec\u67e5\u9605\u8bba\u6587\u65f6\uff0c\u5728\u652f\u6491\u6750\u6599\u90e8\u5206\u7684\u5b9e\u9a8c\u8fc7\u7a0b\u4e2d\uff0c\u770b\u5230\u4e86\u5982\u4e0b\u7684\u7ec6\u8282\uff1a<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-230741\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/4-12.png\" alt=\"\" width=\"600\" height=\"261\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/4-12.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/4-12-300x131.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u4f5c\u8005\u5728\u5236\u5907\u80fa\u50ac\u5316\u5242\u65f6\uff0c\u91c7\u7528\u4e86Pd\uff0c\u90a3\u4e48\uff0c\u4f1a\u4e0d\u4f1a\u5b58\u5728\u6781\u5fae\u91cf\u7684\u91d1\u5c5e\u6b8b\u7559\uff0c\u4ece\u800c\u50ac\u5316\u4e86\u8fd9\u4e2a\u53cd\u5e94\uff1f<\/p>\n<p>\u5728\u8bba\u6587\u4e2d\uff0c\u4f5c\u8005\u4e5f\u7814\u7a76\u4e86\u91d1\u5c5e\u4f1a\u4e0d\u4f1a\u5f71\u54cd\u50ac\u5316\u53cd\u5e94\uff1a<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-230742\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/5-11.png\" alt=\"\" width=\"600\" height=\"368\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/5-11.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/5-11-300x184.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>Moreover, to exclude any major effect from residual traces of the transition-metal species, we studied the reaction kinetics in the presence\/absence of additional metal species. After <strong>adding 10 ppb\u221210 ppm Pd, 100 ppm Fe and 10 ppm Ni, the reaction rate did not change significantly<\/strong>.<\/p>\n<p>\u901a\u8fc7\u6dfb\u52a0\u91d1\u5c5e\u7269\u79cd\uff0c\u53d1\u73b0\u53cd\u5e94\u901f\u7387\u6ca1\u6709\u53d1\u751f\u5f88\u5927\u7684\u53d8\u5316\uff0c\u56e0\u6b64\uff0c\u8be5\u53cd\u5e94\u662f\u7531\u80fa\u50ac\u5316\u5bfc\u81f4\u7684\u3002<\/p>\n<p>\u5728\u8fd9\u7bc7\u8bba\u6587\u53d1\u8868\u540e\uff0c\u56fd\u5916\u6709\u5b66\u8005\u5728\u5316\u5b66\u9884\u5370\u672cChemRxiv\u53d1\u5e03\u4e86\u4e00\u7bc7\u62a5\u544a\uff1a<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-230743\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/6-7.png\" alt=\"\" width=\"600\" height=\"108\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/6-7.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2021\/12\/6-7-300x54.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u7814\u7a76\u8868\u660e\uff0c\u6b8b\u5b58\u7684Pd\u548cP\u89e6\u53d1\u4e86\u50ac\u5316\u53cd\u5e94\uff0c\u800c\u975e\u80fa\u8bf1\u5bfc\u3002\u901a\u8fc7\u5b9e\u9a8c\u76f4\u63a5\u786e\u8ba4\u4e86\u4e0a\u8ff0\u8bba\u6587\u7684\u6838\u5fc3\u7ed3\u679c\u662f\u201c\u65e0\u6548\u7684\u201d\u3002<\/p>\n<p>\u968f\u540e\uff0c\u5c31\u6709\u4e86\u672c\u6b21\u64a4\u7a3f\u4e8b\u4ef6\u3002<\/p>\n<p><strong>\u4e09\u3001\u53cd\u601d<\/strong><\/p>\n<p>\u672c\u6b21\u64a4\u7a3f\u4e8b\u4ef6\u4e2d\uff0c<em>Nature Catalysis<\/em>\u7684\u793e\u8bba\u4e2d\u8fd8\u6307\u51fa\uff0c\u5728\u540c\u884c\u8bc4\u8bae\u8fc7\u7a0b\u4e2d\uff0c\u5ba1\u7a3f\u4eba\u5176\u5b9e\u5c31\u6307\u51fa\u4e86\u76f8\u5173\u7591\u8651\uff0c\u4e0d\u8fc7\uff0c\u8bba\u6587\u6700\u7ec8\u8fd8\u662f\u5f97\u4ee5\u53d1\u8868\u3002\u76ee\u524d\uff0c\u6ca1\u6709\u516c\u5e03\u5ba1\u7a3f\u76f8\u5173\u7684\u7ec6\u8282\u4fe1\u606f\uff0c\u6211\u4eec\u65e0\u4ece\u5f97\u77e5\u5177\u4f53\u7684\u60c5\u5f62\u3002<\/p>\n<p>\u4e0d\u8fc7\uff0c\u5176\u5b9e\u65e9\u57282003\u5e74\uff0cLeadbeater\u7b49\u4eba\u5c31\u8fdb\u884c\u4e86\u76f8\u5173\u7684\u5b9e\u9a8c\uff0c\u7814\u7a76\u8bc1\u660e\u201c<strong>\u5373\u4f7f\u5b58\u5728<\/strong><strong> ppb<\/strong><strong>\u7ea7\u522b\u7684Pd<\/strong><strong>\uff0c\u4e5f\u80fd\u5b9e\u73b0\u50ac\u5316\u53cd\u5e94<\/strong>\u201d\uff0c\u800c\u8fd9\u7bc7\u8bba\u6587\u4e5f\u88ab\u8fd9\u7bc7\u64a4\u7a3f\u8bba\u6587\u5f15\u7528\uff0c\u6587\u7ae0\u4e2d\u6307\u51fa\uff0c\u201cthe concentration of several commonly used transition metals (Mn, Co, Ni, Cu, Ru, Pd, Ir) in the reaction mixture, as well as that of Pd or Ni in the catalyst, is less than 1 parts per 10<sup>9<\/sup> (ppb) (Supplementary Tables 3 and 4), which is considerably lower than the requisite amount of related catalysts\u201d\uff0c\u56e0\u6b64\uff0c\u4f5c\u8005\u57fa\u4e8e\u524d\u4eba\u7684\u62a5\u9053\uff0c\u5f97\u51fa\u81ea\u5df1\u7684\u5b9e\u9a8c\u7ed3\u679c\u6765\u81ea\u4e8e\u80fa\uff0c\u800c\u975e\u91d1\u5c5e\uff0c\u4f46\u4f5c\u8005\u6ca1\u6df1\u601d\u7684\u662f\uff0c\u91d1\u5c5e\u542b\u91cf\u7a76\u7adf\u4f4e\u5230\u51e0\u4e2appb\u624d\u4e0d\u4f1a\u89e6\u53d1\u53cd\u5e94\uff1f<\/p>\n<p>\u4ece\u6574\u4e2a\u4e8b\u4ef6\u6765\u770b\uff0c\u4f5c\u8005\u6ca1\u6709\u4e3b\u89c2\u6545\u610f\u7684\u5b66\u672f\u4e0d\u5f53\uff0c\u4f46\u4e3a\u4f55\u4ecd\u51fa\u73b0\u4e86\u201c\u4e4c\u9f99\u201d\uff1f\u8fd9\u662f\u6211\u4eec\u9700\u8981\u6df1\u601d\u7684\uff0c\u5176\u5b9e\uff0c\u5728\u50ac\u5316\u5242\u7684\u5408\u6210\u4e2d\uff0cPd\u7684\u5b58\u5728\u5c31\u6ce8\u5b9a\u57cb\u4e0b\u4e86\u9690\u60a3\uff0c\u800c\u6211\u4eec\u901a\u5e38\u975e\u5e38\u76f8\u4fe1\u4eea\u5668\u7684\u6d4b\u8bd5\u7ed3\u679c\uff0c\u4f46\uff0c\u5373\u4f7f\u662fICP-MS\u8fd9\u6837\u7684\u8bbe\u5907\u4e5f\u5b58\u5728\u4e00\u4e2a\u201c<strong>\u68c0\u6d4b\u9650<\/strong>\u201d\uff0c\u6211\u4eec\u4e0d\u80fd\u8ba4\u4e3a\uff0c<strong>\u5b9e\u9a8c\u6570\u636e\u6ca1\u6709\u663e\u73b0\u51fa\u7684\u53ef\u80fd\u6027\u5c31\u7b49\u4e8e\u8be5\u53ef\u80fd\u6027\u4e00\u5b9a\u4e0d\u5b58\u5728<\/strong>\uff0c\u8fd9\u4e00\u601d\u7ef4\u9677\u9631\u5728\u5b66\u672f\u8bba\u6587\u4e2d\u51e0\u4e4e\u975e\u5e38\u666e\u904d\u3002<\/p>\n<p>\u524d\u4e00\u6bb5\u65f6\u95f4\uff0c\u56fd\u5185\u67d0\u5927\u578b\u5b66\u672f\u4f1a\u8bae\u5728\u7ebf\u4e3e\u529e\uff0c\u7b14\u8005\u89c2\u6469\u4e00\u573a\u62a5\u544a\u540e\uff0c\u9690\u7ea6\u89c9\u5f97\u62a5\u544a\u4eba\u63d0\u4f9b\u7684\u4e00\u5f20\u5df2\u53d1\u8868\u8bba\u6587\u7684\u5149\u8c31\u56fe\u53ef\u80fd\u6709\u95ee\u9898\uff0c\u6709\u4e9b\u5cf0\u6709\u5f02\u5e38\uff0c\u968f\u540e\uff0c\u5728\u63d0\u95ee\u73af\u8282\u63d0\u4e86\u51fa\u6765\uff0c\u4f5c\u8005\u7acb\u523b\u642a\u585e\u4e86\u8fc7\u53bb\uff0c\u7b14\u8005\u4e5f\u6ca1\u6709\u7ee7\u7eed\u8ffd\u95ee\u3002\u540e\u6765\uff0c\u4e0b\u8f7d\u4e86\u90a3\u7bc7\u8bba\u6587\uff0c\u53d1\u73b0\u786e\u5b9e\u6709\u5176\u4ed6\u7684\u53ef\u80fd\u89e3\u91ca\uff0c\u6570\u636e\u4e0d\u80fd\u5b8c\u5168\u652f\u6301\u8bba\u6587\u7684\u7ed3\u679c\u3002<\/p>\n<p>\u56e0\u6b64\uff0c\u8fd9\u7bc7<em>Narure<\/em>\u5b50\u520a\u8bba\u6587\u7684\u64a4\u7a3f\uff0c\u5176\u5b9e\u5e26\u7ed9\u6211\u4eec<strong>\u4e24\u4e2a<\/strong>\u5173\u952e\u79d1\u7814\u4fe1\u6761\uff1a<\/p>\n<p>1. 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