{"id":214764,"date":"2020-12-19T06:30:00","date_gmt":"2020-12-18T22:30:00","guid":{"rendered":"\/\/m.iemloyee.com\/?p=214764"},"modified":"2020-12-18T22:02:05","modified_gmt":"2020-12-18T14:02:05","slug":"%ef%bc%88%e5%b7%b2%e6%a0%a1%e7%a8%bf%e4%bb%b6%ef%bc%89%e5%8c%97%e5%a4%a7%e6%b8%85%e5%8d%8e-adv-mater-%ef%bc%9a%e8%bf%87%e6%b8%a1%e9%87%91%e5%b1%9e%e7%a1%ab%e5%8c%96%e7%89%a9%e8%96%84%e7%89%87","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=214764","title":{"rendered":"\u5317\u5927&#038;\u6e05\u534e Adv. Mater. \uff1a\u8fc7\u6e21\u91d1\u5c5e\u786b\u5316\u7269\u8584\u7247\u4e2d\u539f\u5b50\u7a7a\u4f4d\u5f15\u8d77\u7684\u5c40\u57df\u78c1\u77e9"},"content":{"rendered":"<p><strong>\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/p>\n<p>\u4e8c\u7ef4\uff082D\uff09\u6750\u6599\u662f\u6307\u7535\u5b50\u4ec5\u53ef\u5728\u4e24\u4e2a\u7ef4\u5ea6\u7684\u975e\u7eb3\u7c73\u5c3a\u5ea6\uff081-100 nm\uff09\u4e0a\u81ea\u7531\u8fd0\u52a8\uff08\u5e73\u9762\u8fd0\u52a8\uff09\u7684\u6750\u6599\u30022D\u6750\u6599\u7684\u51fa\u73b0\u63a8\u52a8\u4e86\u73b0\u4ee3\u51dd\u805a\u6001\u7269\u7406\u548c\u7535\u5b50\u5668\u4ef6\u7684\u53d1\u5c55\u3002 2D\u6750\u6599\u62e5\u6709\u4f17\u591a\u5947\u5f02\u7684\u7269\u7406\u7279\u6027\uff0c\u5176\u4e2d\uff0c2D\u78c1\u6027\u56e0\u5176\u5728\u81ea\u65cb\u7535\u5b50\u5b66\u4e2d\u663e\u793a\u51fa\u6f5c\u5728\u7684\u5e94\u7528\u524d\u666f\u800c\u6210\u4e3a\u6700\u53d7\u5173\u6ce8\u7684\u7814\u7a76\u524d\u6cbf\u4e4b\u4e00\u3002\u7136\u800c\uff0c\u672c\u5f81\u76842D\u78c1\u6027\u6750\u6599\u5728\u81ea\u7136\u754c\u4e2d\u5e76\u4e0d\u5e38\u89c1\uff0c\u800c\u4e14\u76ee\u524d\u5df2\u53d1\u73b0\u76842D\u78c1\u6027\u6750\u6599\u5927\u591a\u5728\u5927\u6c14\u4e2d\u4e0d\u7a33\u5b9a\uff0c\u5bf92D\u78c1\u6027\u6750\u6599\u7684\u6df1\u5165\u7814\u7a76\u548c\u5e94\u7528\u56e0\u6b64\u53d7\u5230\u4e86\u9650\u5236\u3002\u56e0\u6b64\uff0c\u5982\u4f55\u5728\u7a7a\u6c14\u4e2d\u7a33\u5b9a\u76842D\u6750\u6599\u4e2d\u8bf1\u5bfc\u78c1\u6027\u6210\u4e3a\u8be5\u7814\u7a76\u9886\u57df\u7684\u5173\u952e\u95ee\u9898\u4e4b\u4e00\u3002\u8fd1\u5e74\u6765\uff0c\u7814\u7a76\u8005\u63d0\u51fa\u4e86\u901a\u8fc7\u78c1\u6027\u6742\u8d28\u63ba\u6742\u3001\u90bb\u8fd1\u8026\u5408\u3001\u7f3a\u9677\u5de5\u7a0b\u7b49\u5728\u975e\u78c1\u60272D\u6750\u6599\u4e2d\u5f15\u5165\u78c1\u6027\u7684\u65b9\u6cd5\uff0c\u4e3a\u5728\u539f\u5b50\u6216\u5206\u5b50\u5c3a\u5ea6\u4e0a\u8c03\u63a7\u78c1\u6027\u63d0\u4f9b\u4e86\u65b0\u7684\u601d\u8def\uff0c\u5bf9\u4e8e\u81ea\u65cb\u7535\u5b50\u5b66\u548c\u91cf\u5b50\u4fe1\u606f\u5904\u7406\u7684\u672a\u6765\u5e94\u7528\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n<p><strong>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n<p>\u8fd1\u65e5\uff0c<strong>\u5317\u4eac\u5927\u5b66\u7684\u738b\u5065\u6559\u6388\u3001\u5f20\u8273\u950b\u6559\u6388\u548c\u6e05\u534e\u5927\u5b66\u7684\u6bb5\u6587\u6656\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09\u7b49\u4eba<\/strong>\u901a\u8fc7\u7cfb\u7edf\u7684\u8f93\u8fd0\u6d4b\u91cf\uff0c\u63ed\u793a\u4e86\u5316\u5b66\u6c14\u76f8\u6c89\u79ef\uff08CVD\uff09\u5408\u6210\u7684\u7b2c\u4e8c\u7c7b\u72c4\u62c9\u514b\u534a\u91d1\u5c5ePtSe<sub>2<\/sub>\u8584\u7247\u4e2d\u7531Pt\u539f\u5b50\u7a7a\u4f4d\u8bf1\u5bfc\u7684\u5c40\u57df\u78c1\u77e9\u3002\u7814\u7a76\u4eba\u5458\u901a\u8fc7\u7cfb\u7edf\u8868\u5f81\u53d1\u73b0\uff0c\u6240\u751f\u957f\u7684PtSe<sub>2<\/sub>\u6837\u54c1\u5177\u6709\u8f83\u9ad8\u7684\u7ed3\u6676\u8d28\u91cf\uff0c\u5e76\u4e14\u672a\u53d1\u73b0\u78c1\u6027\u6742\u8d28\u3002\u6709\u8da3\u7684\u662f\uff0c \u7814\u7a76\u4eba\u5458\u5728PtSe<sub>2<\/sub>\u8584\u7247\u4e2d\u89c2\u6d4b\u5230\u4e86\u968f\u6e29\u5ea6\u964d\u4f4e\u5bf9\u6570\u589e\u5927\u7684\u7eb5\u5411\u7535\u963b\u4ee5\u53ca\u9762\u5185\u5404\u5411\u540c\u6027\u7684\u8d1f\u78c1\u963b\uff08NMR\uff09\u3002\u8fdb\u4e00\u6b65\u7684\u5206\u6790\u8868\u660e\uff0c\u968f\u6e29\u5ea6\u964d\u4f4e\u5bf9\u6570\u589e\u5927\u7684\u7eb5\u5411\u7535\u963b\u4ee5\u53ca\u9762\u5185\u5404\u5411\u540c\u6027\u7684NMR\u6765\u6e90\u4e8ePt\u7a7a\u4f4d\u5f15\u8d77\u7684\u5c40\u57df\u78c1\u77e9\u5bfc\u81f4\u7684Kondo\u6548\u5e94\u3002\u91cd\u8981\u7684\u662f\uff0cPt\u7a7a\u4f4d\u8bf1\u5bfc\u7684\u5c40\u57df\u78c1\u77e9\u548cKondo\u6e29\u5ea6\u663e\u793a\u51fa\u539a\u5ea6\u4f9d\u8d56\u7684\u7279\u5f81\uff0c\u66f4\u8584\u7684PtSe<sub>2<\/sub>\u8584\u7247\u5177\u6709\u66f4\u5927\u7684\u5c40\u57df\u78c1\u77e9\u548c\u66f4\u4f4e\u7684Kondo\u6e29\u5ea6\u3002\u4f5c\u8005\u901a\u8fc7\u7406\u8bba\u8ba1\u7b97\u63ed\u793a\u4e86Pt\u539f\u5b50\u7a7a\u4f4d\u5c40\u57df\u78c1\u77e9\u8f83\u5c0f\u7684\u78c1\u6676\u5404\u5411\u5f02\u6027\uff08MCA\uff09\uff0c\u8868\u660e\u4e0d\u5b58\u5728\u957f\u7a0b\u78c1\u5e8f\uff0c\u8fdb\u4e00\u6b65\u652f\u6301\u4e86\u5b9e\u9a8c\u7ed3\u679c\u3002\u603b\u4e4b\uff0c\u8be5\u7814\u7a76\u7ed3\u679c\u4e3a\u63a2\u7d22\u975e\u78c1\u60272D\u8fc7\u6e21\u91d1\u5c5e\u786b\u5316\u7269\uff08TMDCs\uff09\u4e2d\u7684\u78c1\u6027\u63d0\u4f9b\u4e86\u65b0\u7684\u601d\u8def\uff0c\u5e76\u4e14\u53ef\u80fd\u4f1a\u6fc0\u53d1\u66f4\u591a\u5173\u4e8e\u65b0\u578b2D\u6750\u6599\u4e2d\u7f3a\u9677\u8bf1\u5bfc\u78c1\u6027\u7684\u6df1\u5165\u7814\u7a76\u3002\u8be5\u5de5\u4f5c\u6210\u679c\u4ee5<strong> \u201cMagnetic Moments Induced by Atomic Vacancies in Transition Metal Dichalcogenide Flakes\u201d<\/strong>\u4e3a\u9898\u53d1\u8868\u5728\u8457\u540d\u671f\u520a<strong>Adv. Mater.<\/strong>\u4e0a\u3002<\/p>\n<p>\u672c\u6587\u5171\u540c\u7b2c\u4e00\u4f5c\u8005\uff1a\u845b\u519b\u3001\u7f57\u5929\u521b\u3001\u6797\u7956\u6da8\u3001\u53f2\u5efa\u5e73\u3002<\/p>\n<p><strong>\u3010\u56fe\u6587\u89e3\u8bfb\u3011<\/strong><\/p>\n<p><strong>\u56fe\u4e00\u3001CVD\u5408\u6210\u7684PtSe<sub>2<\/sub>\u8584\u7247\u7684\u539f\u5b50\u7ed3\u6784\u8868\u5f81<\/strong><br \/>\n <img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-214765\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/1-23.jpg\" alt=\"\" width=\"800\" height=\"539\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/1-23.jpg 800w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/1-23-300x202.jpg 300w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/1-23-768x517.jpg 768w\" sizes=\"(max-width: 800px) 100vw, 800px\" \/>\uff08a\uff09\u5c11\u5c42PtSe<sub>2<\/sub>\u8584\u7247\u7684\u4f4e\u500dTEM\u56fe\u50cf\uff1b<\/p>\n<p>\uff08b\uff09\u4ece\uff08a\uff09\u4e2d\u6807\u6709\u6570\u5b571-9\u7684\u533a\u57df\u91c7\u96c6\u7684SAED\u56fe\u50cf\uff1b<\/p>\n<p>\uff08c-d\uff09\u5728\u5ba4\u6e29\u4e0b\u83b7\u5f97\u7684\u5c11\u5c42PtSe<sub>2<\/sub>\u8584\u7247\u7684\u539f\u5b50\u5206\u8fa8TEM\u56fe\u50cf\u548c\u76f8\u5e94\u7684FFT\u7ed3\u679c\uff1b<\/p>\n<p>\uff08e-f\uff09\u4f4e\u6e29\uff08\u224890 K\uff09\u65f6\u83b7\u5f97\u7684\u5c11\u5c42PtSe<sub>2<\/sub>\u8584\u7247\u7684\u539f\u5b50\u5206\u8fa8TEM\u56fe\u50cf\u548c\u76f8\u5e94\u7684FFT\u7ed3\u679c\uff1b<\/p>\n<p>\uff08g\uff09\u5c11\u5c42PtSe<sub>2<\/sub>\u8584\u7247\u7684\u539f\u5b50\u5206\u8fa8HAADF-STEM\u56fe\u50cf\uff1b<\/p>\n<p>\uff08h\uff09\u5c11\u5c42PtSe<sub>2<\/sub>\u8584\u7247\u7684\u539f\u5b50\u5206\u8fa8HAADF-STEM\u56fe\u50cf\uff0c\u663e\u793a\u51fa1T\u76f8\u7279\u5f81\u548cA-A\u5806\u53e0\u6784\u578b\uff1b<\/p>\n<p>\uff08i\uff09\u4ece1T-PtSe<sub>2<\/sub>\u8584\u7247\u7684\u8fb9\u7f18\u91c7\u96c6\u7684\u539f\u5b50\u5206\u8fa8HAADF-STEM\u56fe\u50cf\u3002<\/p>\n<p><strong>\u56fe\u4e8c\u3001PtSe<sub>2<\/sub>\u8584\u7247\u7684\u8f93\u8fd0\u7279\u6027<\/strong><br \/>\n <img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-214766\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/2-25.jpg\" alt=\"\" width=\"800\" height=\"665\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/2-25.jpg 800w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/2-25-300x249.jpg 300w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/2-25-768x638.jpg 768w\" sizes=\"(max-width: 800px) 100vw, 800px\" \/>\uff08a\uff09s3\u7684\u7eb5\u5411\u7535\u963b\u968f\u6e29\u5ea6\u7684\u53d8\u5316\u66f2\u7ebf(\u6a2a\u8f74\u6e29\u5ea6\u5750\u6807\u4e3a\u5bf9\u6570\u5f62\u5f0f)\uff1b<\/p>\n<p>\uff08b\uff09\u5728PtSe<sub>2<\/sub>\u8584\u7247s3\u7684<em>ab<\/em>\u5e73\u9762\u65bd\u52a0\u78c1\u573a\u65f6\u6d4b\u5f97\u7684\u5404\u5411\u540c\u6027\u8d1f\u78c1\u963b(NMR)\uff1b<\/p>\n<p>\uff08c-d\uff09\u5728s1\u548cs5\u7684<em>ab<\/em>\u5e73\u9762\u65bd\u52a0\u78c1\u573a\u65f6\u6d4b\u5f97\u7684\u5404\u5411\u540c\u6027NMR\uff1b<\/p>\n<p>\uff08e-g\uff09\u5f53\u9762\u5185\u78c1\u573a\u5206\u522b\u5782\u76f4\u4e8es3\u4e2d\u7684\u7535\u6d41\u548c\u5e73\u884c\u4e8es1\u3001s5\u4e2d\u7684\u7535\u6d41\u65f6\uff0cs3\u3001s1\u3001s5\u5728\u4e0d\u540c\u6e29\u5ea6\u4e0b\u7684\u78c1\u963b\u66f2\u7ebf\uff1b<\/p>\n<p>\uff08h-i\uff09s3\u548cs5\u4e2dNMR\u7684\u7406\u8bba\u62df\u5408\u3002<\/p>\n<p><strong>\u56fe\u4e09\u3001PtSe<sub>2<\/sub>\u8584\u7247\u7684\u5c40\u57df\u78c1\u77e9\u6027\u8d28\u548c\u7535\u5b50\u6027\u8d28<\/strong><br \/>\n <img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-214767\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/3-24.jpg\" alt=\"\" width=\"800\" height=\"650\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/3-24.jpg 800w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/3-24-300x244.jpg 300w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/12\/3-24-768x624.jpg 768w\" sizes=\"(max-width: 800px) 100vw, 800px\" \/>\uff08a\uff09\u516d\u5c42PtSe<sub>2<\/sub>\u8584\u7247\u7684\u7535\u5b50\u7ed3\u6784\uff1b<\/p>\n<p>\uff08b\uff09\u516d\u5c42PtSe<sub>2<\/sub>\u8584\u7247\u7684\u5c40\u57df\u78c1\u77e9\u7684\u793a\u610f\u56fe\uff1b<\/p>\n<p>\uff08c\uff09Pt\u7a7a\u4f4d\u7684\u4e09\u4e2a\u76f8\u90bbSe\u539f\u5b50<em>p<\/em>\u8f68\u9053\u7684\u7535\u5b50\u6001\u5bc6\u5ea6\uff1b<\/p>\n<p>\uff08d\uff09\u4e0d\u540c\u78c1\u6784\u578b\u7684\u80fd\u91cf\uff0c\u5176\u4e2d\u80fd\u91cf\u4e3a\u96f6\u5bf9\u5e94\u4e8e\u78c1\u77e9\u671d\u5411\u9762\u5916\u7684\u78c1\u6784\u578b\u3002<\/p>\n<p><strong>\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n<p>\u7efc\u4e0a\u6240\u8ff0\uff0c\u4f5c\u8005\u6210\u529f\u5730\u8bc1\u660e\u4e86\u7a7a\u6c14\u7a33\u5b9a\u7684PtSe<sub>2<\/sub>\u8584\u7247\u4e2d\u5b58\u5728\u7531Pt\u7a7a\u4f4d\u7f3a\u9677\u5f15\u8d77\u7684\u8fd1\u4f3c\u539a\u5ea6\u4f9d\u8d56\u7684\u5c40\u57df\u78c1\u77e9\u3002\u968f\u6e29\u5ea6\u964d\u4f4e\u5bf9\u6570\u589e\u5927\u7684\u7535\u963b\u548c\u9762\u5185\u5404\u5411\u540c\u6027\u7684\u8d1f\u78c1\u963b\u8bc1\u660e\u4e86\u7531\u5c40\u57df\u78c1\u77e9\u5bfc\u81f4\u7684Kondo\u6548\u5e94\u7684\u5b58\u5728\u3002\u8be5\u5de5\u4f5c\u63d0\u4f9b\u4e86\u4e00\u79cd\u5728\u975e\u78c1\u6027\u6750\u6599\u4e2d\u8bf1\u5bfc\u78c1\u6027\u7684\u7b80\u5355\u65b9\u6cd5\uff0c\u5e76\u4e14\u4e3a\u8c03\u5236TMDCs\u4e2d\u7684\u78c1\u6027\u5f00\u8f9f\u4e86\u4e00\u6761\u65b0\u9014\u5f84\u3002<\/p>\n<p><strong>\u6587\u732e\u94fe\u63a5\uff1a<a href=\"https:\/\/onlinelibrary.wiley.com\/doi\/10.1002\/adma.202005465\" target=\"_blank\" rel=\"noopener\">Magnetic Moments Induced by Atomic Vacancies in Transition Metal Dichalcogenide Flakes<\/a><\/strong>.\uff08<em>Adv. Mater.<\/em>, <strong>2020<\/strong>, DOI: 10.1002\/adma.202005465\uff09<\/p>\n<p style=\"text-align: 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