{"id":212501,"date":"2020-11-09T06:10:13","date_gmt":"2020-11-08T22:10:13","guid":{"rendered":"\/\/m.iemloyee.com\/?p=212501"},"modified":"2020-11-08T11:10:21","modified_gmt":"2020-11-08T03:10:21","slug":"%e8%b7%9f%e7%9d%80%e9%a1%b6%e5%88%8a%e5%ad%a6%e6%b5%8b%e8%af%95%ef%bd%9c%e7%be%8e%e5%9b%bd%e8%a5%bf%e5%8c%97%e5%a4%a7%e5%ad%a6jacs%ef%bc%9a%e9%80%8f%e5%b0%84%e7%94%b5%e9%95%9c%e8%a7%82%e5%af%9fmofs","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=212501","title":{"rendered":"\u8ddf\u7740\u9876\u520a\u5b66\u6d4b\u8bd5\uff5c\u7f8e\u56fd\u897f\u5317\u5927\u5b66JACS\uff1a\u900f\u5c04\u7535\u955c\u89c2\u5bdfMOFs\u7684\u7ed3\u6784\u548c\u52a8\u529b\u5b66"},"content":{"rendered":"<p>MOF\u548c\u7c7bMOF\u6750\u6599\u7684\u8868\u5f81\u5e38\u7528\u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c(SEM)\u3001\u7c89\u672bX\u5c04\u7ebf\u884d\u5c04(PXRD)\u3001\u5355\u6676X\u5c04\u7ebf\u884d\u5c04(SXRD)\u3001\u6c14\u4f53\u5438\u9644(\u5982\u8868\u9762\u79ef\u3001\u5b54\u5f84)\u3001\u70ed\u91cd\u5206\u6790(TGA)\u3001\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c(TEM)\u7b49\u3002\u4e0e\u8bb8\u591a\u53ea\u80fd\u5e94\u7528\u4e8e\u5927\u5757\u6837\u54c1\u7684\u66f4\u4f20\u7edf\u7684\u8868\u5f81\u6280\u672f\u76f8\u6bd4\uff0cTEM\u7684\u72ec\u7279\u4e4b\u5904\u5728\u4e8e\u5b83\u53ef\u4ee5\u76f4\u63a5\u83b7\u5f97\u5355\u4e2aMOF\u7ed3\u6676\u7684\u7ed3\u6784\u548c\u52a8\u6001\u4fe1\u606f\u3002\u7136\u800c\uff0c\u7531\u4e8eMOFs\u5bf9\u9ad8\u80fd\u7535\u5b50\u7684\u654f\u611f\u6027\uff0cMOF\u6750\u6599\u7684TEM\u4ecd\u7136\u5177\u6709\u6311\u6218\u6027\uff0c\u8fd9\u9650\u5236\u4e86\u7535\u5b50\u5242\u91cf\u6761\u4ef6\u3001\u53ef\u83b7\u5f97\u7684\u56fe\u50cf\u5206\u8fa8\u7387\u548c\u7528\u4e8e\u5408\u7406\u7ed3\u6784\u548c\u52a8\u6001\u8868\u5f81\u7684\u4fe1\u566a\u6bd4\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-212502 size-full\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-1-2.png\" alt=\"\" width=\"600\" height=\"205\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-1-2.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-1-2-300x103.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u8fd1\u65e5\uff0c\u7f8e\u56fd\u897f\u5317\u5927\u5b66Nathan C. Gianneschi\u6559\u6388\u8bfe\u9898\u7ec4\u548c\u52a0\u5dde\u5927\u5b66\u5723\u5730\u4e9a\u54e5\u5206\u6821Seth M. Cohen\u7814\u7a76\u56e2\u961f\u5408\u4f5c\u4ee5\u201cInsights into the Structure and Dynamics of Metal\u2013Organic Frameworks via Transmission Electron Microscopy\u201d\u4e3a\u9898\u5728<em><i>J. Am. Chem. 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<\/b><\/strong><strong><b>(a) TEM\u548cSTEM\u6a21\u5f0f\u4e0b\u7684\u7535\u5b50\u675f\u8def\u5f84\u793a\u610f\u56fe\u3002(b)\u7535\u5b50-\u8bd5\u6837\u76f8\u4e92\u4f5c\u7528\u548c\u5149\u675f\u635f\u4f24\u3002EELS\u3001EDS\u3001CL\u3001SE\u548cBSE\u5206\u522b\u662f\u7535\u5b50\u80fd\u91cf\u635f\u5931\u5149\u8c31\u3001\u80fd\u91cf\u8272\u6563x\u5c04\u7ebf\u5149\u8c31\u3001\u9634\u6781\u53d1\u5149\u3001\u4e8c\u6b21\u7535\u5b50\u548c\u80cc\u6563\u5c04\u7535\u5b50\u3002(c)\u5728\u6b64\u89c2\u70b9\u4e2d\u8ba8\u8bba\u7684MOF\u6676\u4f53\u7ed3\u6784<\/b><\/strong><strong><b>\u3002<\/b><\/strong><\/p>\n<p><strong><b><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-212503 size-full\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-6-3.png\" alt=\"\" width=\"600\" height=\"395\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-6-3.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-6-3-300x198.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" 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height=\"560\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-7.png 515w, \/\/m.iemloyee.com\/wp-content\/uploads\/2020\/11\/\u56fe\u7247-7-276x300.png 276w\" sizes=\"(max-width: 515px) 100vw, 515px\" 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