{"id":209420,"date":"2020-09-16T06:51:58","date_gmt":"2020-09-15T22:51:58","guid":{"rendered":"\/\/m.iemloyee.com\/?p=209420"},"modified":"2020-09-15T21:52:27","modified_gmt":"2020-09-15T13:52:27","slug":"adv-mater-%e5%b7%a5%e4%b8%9a%e6%b8%a9%e5%ba%a6%e4%b8%8b%e7%9a%84%e9%87%8d%e6%9e%84%e5%8c%96%e5%ad%a6%e5%8f%8a%e7%a2%b1%e6%80%a7%e7%94%b5%e8%a7%a3%e6%b0%b4%e6%80%a7%e8%83%bd%e8%af%84%e4%bc%b0","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=209420","title":{"rendered":"Adv. Mater.:\u5de5\u4e1a\u6e29\u5ea6\u4e0b\u7684\u91cd\u6784\u5316\u5b66\u53ca\u78b1\u6027\u7535\u89e3\u6c34\u6027\u80fd\u8bc4\u4f30"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u7535\u89e3\u6c34\u5236\u6c22\u6280\u672f\u53ef\u5b9e\u73b0\u4e8c\u6c27\u5316\u78b3\u7684\u96f6\u6392\u653e\uff0c\u662f\u672a\u6765\u53ef\u6301\u7eed\u80fd\u6e90\u7cfb\u7edf\u7684\u5173\u952e\u7ec4\u6210\u90e8\u5206\u3002\u8be5\u6280\u672f\u4ec5\u5360\u5f53\u524d\u6c22\u6c14\u603b\u4ea7\u80fd\u76844\uff05\uff0c\u8fd9\u4e3b\u8981\u662f\u7531\u4e8e\u4e0e\u5176\u4ed6\u65b9\u6cd5\uff08\u4f8b\u5982\u5929\u7136\u5316\u77f3\u71c3\u6599\u7684\u8f6c\u5316\uff09\u76f8\u6bd4\uff0c\u5176\u6210\u672c\u8f83\u9ad8\u3002\u5f53\u524d\u7684\u7535\u89e3\u6c34\u7cfb\u7edf\u4e3b\u8981\u5229\u7528\u7684\u662f\u6602\u8d35\u7684Ir\/Ru\/Pt\u57fa\u9ad8\u50ac\u5316\u6d3b\u6027\u4f46\u7a33\u5b9a\u6027\u8f83\u5dee\u7684\u50ac\u5316\u5242\uff0c\u6216\u8005\u4f7f\u7528\u7ecf\u6d4e\u5b9e\u7528\u4f46\u6d3b\u6027\u4e0d\u9ad8\u7684\u954d\u7f51\u6216\u4e0d\u9508\u94a2\u7f51\uff1b\u5176\u7535\u89e3\u6c34\u5236\u6c22\u80fd\u91cf\u8f6c\u5316\u6548\u7387\u957f\u671f\u572850-70%\u4e4b\u95f4\uff0c\u662f\u7535\u89e3\u6c34\u6210\u672c\u5c45\u9ad8\u4e0d\u4e0b\u7684\u5173\u952e\u56e0\u7d20\u4e4b\u4e00\u3002\u56e0\u6b64\uff0c\u5fc5\u987b\u5f00\u53d1\u5177\u6709\u826f\u597d\u7a33\u5b9a\u6027\u7684\u9ad8\u6d3b\u6027\u548c\u9ad8\u6210\u672c\u6548\u76ca\u7684\u50ac\u5316\u5242\u3002\u5c3d\u7ba1\u6700\u8fd1\u5728\u7814\u7a76\u7528\u4e8eOER\u548cHER\u7684\u9ad8\u6548\u8fc7\u6e21\u91d1\u5c5e\u57fa\u50ac\u5316\u5242\u65b9\u9762\u53d6\u5f97\u4e86\u91cd\u8981\u7a81\u7834\uff0c\u4f46\u662f\u6d4b\u8bd5\u6761\u4ef6\u4e0e\u5b9e\u9645\u5e94\u7528\u4e4b\u95f4\u4ecd\u7136\u5b58\u5728\u4e00\u5b9a\u5dee\u8ddd\u3002\u5728\u5ba4\u6e29\u4e0b\u8fdb\u884c\u6d4b\u8bd5\u65f6\uff0c\u8fc7\u6e21\u91d1\u5c5e\u57fa\u50ac\u5316\u5242\u901a\u5e38\u5b58\u5728\u6709\u9650\u7684\u8868\u9762\u91cd\u6784\uff08\u91cd\u6784\u5c42\u539a\u5ea6\u901a\u5e38<10 nm\uff09\u3002\u7136\u800c\uff0c\u5728\u9ad8\u6e2950-80\u00b0C\u65f6\u5219\u53ef\u80fd\u4f1a\u4fc3\u8fdb\u548c\u52a0\u6df1\u50ac\u5316\u5242\u7684\u8868\u9762\u7ed3\u6784\u91cd\u6784\u3002\u56e0\u6b64\uff0c\u5e38\u89c4\u6d4b\u8bd5\u548c\u5de5\u4e1a\u6d4b\u8bd5\u4e4b\u95f4\u7684\u5b9e\u9645\u50ac\u5316\u7269\u79cd\u548c\u91cd\u6784\/\u50ac\u5316\u673a\u7406\u53ef\u80fd\u6709\u6240\u4e0d\u540c\uff1b\u5f00\u5c55\u5e38\u89c4\u6d4b\u8bd5\u6761\u4ef6\u4e0e\u5de5\u4e1a\u53c2\u6570\u4e0b\u524d\u50ac\u5316\u5242\u7684\u91cd\u6784\u673a\u5236\u5dee\u5f02\u6027\u63a2\u7d22\u548c\u6027\u80fd\u8bc4\u4f30\uff0c\u4e5f\u5c06\u8fdb\u4e00\u6b65\u4fc3\u8fdb\u50ac\u5316\u5242\u8fc8\u5411\u4ea7\u4e1a\u5316\u8fdb\u7a0b\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6b66\u6c49\u7406\u5de5\u5927\u5b66\u9ea6\u7acb\u5f3a\u6559\u6388\u3001\u5434\u52b2\u677e\u6559\u6388\uff0c\u4e2d\u56fd\u79d1\u5b66\u6280\u672f\u5927\u5b66\u502a\u5803\u535a\u58eb\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u7b49\u4eba\u6bd4\u8f83\u4e86\u6790\u6c27\u524d\u50ac\u5316\u5242\u5728\u5e38\u6e29\u548c\u5de5\u4e1a\u6e29\u5ea6\u4e0b\u91cd\u6784\u8fc7\u7a0b\u3001\u91cd\u6784\u7ed3\u679c\u7684\u5dee\u5f02\u6027\uff0c\u53d1\u73b0\u4e86\u91cd\u6784\u7a0b\u5ea6\u4e0e\u91cd\u6784\u5c42\u5fae\u7ed3\u6784\u4e4b\u95f4\u7684\u5185\u5728\u8054\u7cfb\uff0c\u63d0\u51fa\u4e86\u70ed\u81f4\u5168\u91cd\u6784\u673a\u5236\u53ca\u6676\u754c-\u6c27\u7a7a\u4f4d\u5171\u540c\u63d0\u5347OER\u52a8\u529b\u5b66\u673a\u5236\uff0c\u5e76\u5f3a\u8c03\u4e86\u5de5\u4e1a\u53c2\u6570\u4e0b\u8bc4\u4f30\u50ac\u5316\u6027\u80fd\u548c\u63ed\u793a\u50ac\u5316\u673a\u5236\u7684\u91cd\u8981\u6027\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u201cReconstruction-Determined Alkaline Water Electrolysis at Industrial Temperatures<\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728Advanced Materials<\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00\u3001<\/strong>\u6e29\u5ea6\u8c03\u63a7\u7684\u91cd\u6784\u5de5\u7a0b<\/strong><\/p>\n

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Figure 1 a) Chronopotentiometric measurements of NiMoO4<\/sub> pre-catalyst and nickel foam (NF) at 10 mA cm-2<\/sup> in 1 M KOH with solution temperatures of T. In detail, the initial 0-12 h stage was tested at 25.0 \u2103, and the next 12-48 h stage was tested at T \u2103 (T = 25.0, 32.4, 39.6, 51.9), and the final 48-60 h stage was tested at 25.0 \u2103. The finally obtained catalysts are denoted as cat.-T for subsequent performance evaluation. For NF-T sample, T is 51.9. b) Schematic diagram for the temperature-dependent potential curve, which associates with the thermal-induced reconstruction results. The reduced potential \u0394V is based on the difference value of potentials at 60 and 12 h in (a). c-e) LSV curves, the corresponding overpotentials, and Tafel values of cat.-T tested at 25.0 \u2103, respectively.<\/p>\n

\u56fe\u4e8c\u3001\u975e\u539f\u4f4d\u7269\u76f8<\/strong>\/<\/strong>\u5fae\u7ed3\u6784\u8868\u5f81\u53ca\u539f\u4f4d\u9ad8\u4f4e\u6e29\u62c9\u66fc\u8868\u5f81<\/strong><\/p>\n

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Figure 2 a-d) HRTEM and e-h) HAADF-STEM images and the corresponding elemental mappings of cat.-T (T = 25.0, 32.4, 39.6, 51.9). The white dotted lines in (a-c) represent the obviously observed reconstruction boundary. i) In situ low-temperature Raman spectra and the corresponding chronopotentiometric curve of NiMoO4<\/sub> pre-catalyst with the interval time of 200 s in 1 M KOH at 25.0 \u2103. j) In situ high-temperature Raman spectra and the corresponding chronopotentiometric curve of NiMoO4<\/sub> pre-catalyst with the interval time of 80 s in 1 M KOH at 52.0 \u2103.<\/p>\n

\u56fe\u4e09\u3001\u50ac\u5316\u5242\u91cd\u6784\u5c42\u7279\u5f81<\/strong>–<\/strong>\u91cd\u6784\u7a0b\u5ea6\u4e4b\u95f4\u7684\u5173\u7cfb<\/strong><\/p>\n

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Figure 3 a) HAADF-STEM image of NiMoO4<\/sub> pre-catalyst after chronopotentiometric measurement at 10 mA cm-2<\/sup> at 25.0 \u2103 for 12 h. b) HAADF-STEM image of NiMoO4<\/sub> pre-catalyst after chronopotentiometric measurement at 10 mA cm-2<\/sup> at 25.0 \u2103 for 12 h and then rising to 51.9 \u2103. c) HAADF-STEM image and the corresponding elemental mappings of sample in (b), showing the dissolution of Mo species on the surface. d) Schematic diagram for the two reconstruction results of NiMoO4<\/sub> pre-catalyst under low-\/high-temperature electro-oxidation conditions.<\/p>\n

\u56fe\u56db\u3001\u91cd\u6784\u987a\u5e8f\u5de5\u7a0b\u53ca\u6676\u754c<\/strong>–<\/strong>\u6c27\u7a7a\u4f4d\u5171\u540c\u4f5c\u7528<\/strong><\/p>\n

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Figure 4 a) Chronopotentiometric measurements at 10 mA cm-2<\/sup> in 1 M KOH. For in situ reconstruction, the NiMoO4<\/sub> pre-catalyst was firstly measured at 51.9 \u2103 and then at 25.0 \u2103, and the obtained catalyst is called as in situ catalyst. For ex situ reconstruction, the NiMoO4<\/sub> was firstly soaked in 1 M KOH at 51.9 \u2103 and then measured at 25.0 \u2103, and the obtained catalyst is called as ex situ catalyst. b-e) HRTEM images and the corresponding fast Fourier transform patterns of (b,c) in situ catalyst and (d,e) ex situ catalyst. f) O 1s XPS spectra of in\/ex situ catalysts. g) Model of NiOOH (011)-NiOOH (011) twin boundary structure with O vacancy, showing the O vacancy site in the boundary region. h-j) DFT-calculated models with the optimal structures for intermediate products. k) Free energy of each reaction step on six different models, considering the effects of boundary, O\/OH vacancies on OER. l) PDOS calculation of d band of Ni-2 atom near the O vacancy site in the boundary region in boundary with VO<\/sub> model. Inset: the partial charge density drawn from -7 to -6.8 eV with iso-surface value of 0.025 e–<\/sup> bohr-3<\/sup>, corresponding to the PDOS peak at -6.9 eV.<\/p>\n

\u00a0<\/strong>\u56fe\u4e94\u3001\u5168\u91cd\u6784\u50ac\u5316\u5242\u7684<\/strong>OER\/<\/strong>\u7535\u89e3\u6c34\u6027\u80fd\u8bc4\u4f30<\/strong><\/p>\n

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Figure 5 a,b) Chronopotentiometric measurement of cat.-51.9 and NiFe-LDH catalysts tested at 10 mA cm-2<\/sup> in 1 M KOH at (a) 25.0 and (b) 51.9 \u2103. c) Schematic diagram of NPs-interconnected structure with open 3D pores. d-g) Representative HAADF-STEM images via electron tomography of single cat.-51.9 nanowire after long-term stability measurement in (b). h) The conventional condition (almost at room temperature) has a certain gap with the industrial one (at 50-80 \u2103). i) Schematic diagram of MoO2<\/sub>-Ni arrays on the nickel foam. j) Chronopotentiometric measurement of MoO2<\/sub>-Ni heterostructured nanowire arrays at 10 mA cm-2<\/sup> in 1 M KOH at 51.9 \u2103. k) Durability evaluation of high-temperature water electrolysis based on cat.-51.9 (anode) and MoO2<\/sub>-Ni (cathode) array system at 10 mA cm-2<\/sup> in 1 M KOH at 51.9 \u2103.<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a\u201c<\/strong>Reconstruction-Determined Alkaline Water Electrolysis\u00a0 at Industrial Temperatures<\/strong><\/a>\u201d<\/strong>(DOI: 10.1002\/adma.202001136)<\/strong><\/p>\n

\u672c\u6587\u7531\u5fae\u89c2\u4e16\u754c\u7f16\u8bd1\u4f9b\u7a3f\u3002<\/p>\n

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\u3010\u56e2\u961f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

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