{"id":208143,"date":"2020-08-26T12:00:53","date_gmt":"2020-08-26T04:00:53","guid":{"rendered":"\/\/m.iemloyee.com\/?p=208143"},"modified":"2020-08-26T09:37:07","modified_gmt":"2020-08-26T01:37:07","slug":"%e9%9d%92%e5%b2%9b%e8%83%bd%e6%ba%90%e6%89%80angew%ef%bc%9a%e9%98%b4%e7%a6%bb%e5%ad%90%e6%ba%b6%e5%89%82%e5%8c%96%e7%bb%93%e6%9e%84%e9%87%8d%e6%9e%84%e5%8a%a9%e5%8a%9b%e9%ab%98%e7%94%b5%e5%8e%8b","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=208143","title":{"rendered":"\u9752\u5c9b\u80fd\u6e90\u6240Angew\uff1a\u9634\u79bb\u5b50\u6eb6\u5242\u5316\u7ed3\u6784\u91cd\u6784\u52a9\u529b\u9ad8\u7535\u538b\u78b3\u9178\u916f\u7c7b\u7535\u89e3\u8d28\u7528\u4e8e\u957f\u5bff\u547d\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u4f4e\u6210\u672c\u3001\u957f\u5bff\u547d\u7684\u4e8c\u6b21\u7535\u6c60\u662f\u5b9e\u73b0\u7535\u7f51\u89c4\u6a21\u50a8\u80fd\u6765\u5229\u7528\u95f4\u6b47\u6027\u53ef\u518d\u751f\u80fd\u6e90\u53d1\u7535\u7684\u6709\u6548\u9014\u5f84\u4e4b\u4e00\u3002\u77f3\u58a8\u6b63\u6781\u5177\u6709\u6210\u672c\u4f4e\u3001\u73af\u5883\u53cb\u597d\u7684\u7279\u6027\uff0c\u800c\u950c\u8d1f\u6781\u5177\u6709\u4f53\u79ef\u80fd\u91cf\u5bc6\u5ea6\u9ad8\u3001\u50a8\u91cf\u4e30\u5bcc\u3001\u950c\u6c89\u79ef\/\u6eb6\u89e3\u8fc7\u7535\u4f4d\u4f4e\u7b49\u4f18\u70b9\uff0c\u56e0\u6b64\u7ed3\u5408\u950c\u8d1f\u6781\u4e0e\u77f3\u58a8\u6b63\u6781\u5404\u81ea\u4f18\u70b9\u7684\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u5728\u89c4\u6a21\u50a8\u80fd\u6ce8\u91cd\u7684\u6210\u672c\u6548\u76ca\u65b9\u9762\u6781\u5177\u7ade\u4e89\u529b\u3002\u7531\u4e8e\u9634\u79bb\u5b50\u5d4c\u5165\/\u8131\u51fa\u77f3\u58a8\u7684\u7535\u4f4d\u8f83\u9ad8\uff0c\u9ad8\u7535\u538b\u7535\u89e3\u8d28\u4f53\u7cfb\u662f\u5173\u952e\u3002\u7136\u800c\uff0c\u76ee\u524d\u5e38\u7528\u7684\u79bb\u5b50\u6db2\u4f53\u3001\u9ad8\u6d53\u76d0\u4ee5\u53ca\u6df7\u5408\u79bb\u5b50\u7535\u89e3\u6db2\u4f53\u7cfb\u5747\u5b58\u5728\u6210\u672c\u53ca\u7269\u5316\u6027\u8d28\u4e0a\u7684\u4e0d\u8db3\u3002\u4f20\u7edf\u9502\u79bb\u5b50\u7535\u6c60\u7535\u89e3\u8d28\u4e2d\u7684\u78b3\u9178\u916f\u7c7b\u6eb6\u5242\u4f53\u7cfb\u53ef\u4ee5\u5f25\u8865\u4e0a\u8ff0\u95ee\u9898\u3002\u66f4\u5173\u952e\u7684\u662f\uff0c\u5982\u78b3\u9178\u7532\u4e59\u916f\uff08EMC\uff09\u7684\u78b3\u9178\u916f\u5206\u5b50\u81ea\u8eab\u7684\u6c27\u5316\u7a33\u5b9a\u6027\uff082.7 V vs.<\/em> Zn\/Zn2+<\/sup>\uff09\uff0c\u7406\u8bba\u4e0a\u53ef\u4ee5\u652f\u6301\u9ad8\u7535\u538b\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u5316\u5b66\u7684\u53cd\u5e94\u3002\u4f46\u662f\u5d4c\u5165\/\u8131\u51fa\u77f3\u58a8\u6b63\u6781\u7684\u542b\u6c1f\u9634\u79bb\u5b50\uff08PF6<\/sub>\u2212<\/sup>\u3001TFSI\u2212<\/sup>\u3001BF4<\/sub>\u2212<\/sup>\uff09\u53ef\u4ee5\u4e0e\u78b3\u9178\u916f\u53d1\u751f\u7edc\u5408\uff0c\u5728\u9ad8\u7535\u4f4d\u4e0b\u5bb9\u6613\u53d1\u751f\u78b3\u9178\u916f\u4e2d\u7532\u57fa\u8131\u6c22\u4e0e\u9634\u79bb\u5b50\u8131\u6c1f\u7684\u5206\u89e3\u53cd\u5e94\uff0c\u964d\u4f4e\u4e86\u78b3\u9178\u916f\u56fa\u6709\u7684\u6c27\u5316\u7a33\u5b9a\u6027\u3002\u56e0\u6b64\uff0c\u8c03\u53d8\u9634\u79bb\u5b50\u7684\u6eb6\u5242\u5316\u7ed3\u6784\uff0c\u4f7f\u78b3\u9178\u916f\u5206\u5b50\u4e0e\u542b\u6c1f\u9634\u79bb\u5b50\u201c\u89e3\u8026\u201d\uff0c\u662f\u63d0\u5347\u6c27\u5316\u7a33\u5b9a\u6027\u7684\u6709\u6548\u9014\u5f84\u3002\u7136\u800c\uff0c\u7531\u4e8e\u9634\u79bb\u5b50\u4e0e\u6eb6\u5242\u5206\u5b50\u7684\u4f5c\u7528\u8f83\u5f31\uff0c\u76ee\u524d\u6587\u732e\u5bf9\u4e8e\u9634\u79bb\u5b50\u7684\u6eb6\u5242\u5316\u7ed3\u6784\u53ca\u8c03\u63a7\u7814\u7a76\u8f83\u5c11\u3002\u6b64\u5916\uff0c\u4e0e\u9502\u76d0\u76f8\u6bd4\uff0c\u76f8\u5e94\u7684\u950c\u76d0\u6eb6\u89e3\u66f4\u52a0\u56f0\u96be\uff0c\u8fd9\u8fdb\u4e00\u6b65\u9650\u5236\u4e86\u5bf9\u950c\u76d0\u7535\u89e3\u8d28\u4f53\u7cfb\u4e2d\u9634\u79bb\u5b50\u6eb6\u5242\u5316\u7ed3\u6784\u7684\u7814\u7a76\u548c\u8ba4\u8bc6\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u4e2d\u56fd\u79d1\u5b66\u9662\u9752\u5c9b\u751f\u7269\u80fd\u6e90\u4e0e\u8fc7\u7a0b\u7814\u7a76\u6240<\/strong>\u7684\u5d14\u5149\u78ca\u7814\u7a76\u5458\u3001\u8d75\u4e95\u6587\u526f\u7814\u7a76\u5458\uff08\u901a\u8baf\u4f5c\u8005\uff09\u56e2\u961f<\/strong>\u57fa\u4e8e\u524d\u671f\u5bf9\u950c\u57fa\u7194\u76d0\u7535\u89e3\u8d28\u4f53\u7cfb\u7684\u7814\u7a76\u8ba4\u8bc6\uff08Nat. Commun. 2019, 10, 5374\uff1bNano Energy 2019, 57, 625\uff1bJoule 2020, 4, 1\uff09\uff0c\u5145\u5206\u5229\u7528\u4e8c\u4ef7\u950c\u79bb\u5b50\u6613\u4e0e\u9634\u79bb\u5b50\u5f62\u6210\u7f14\u5408\u79bb\u5b50\u5bf9\u8fd9\u4e00\u7279\u70b9\uff0c\u5728Zn(TFSI)2<\/sub>\/EMC\u7535\u89e3\u8d28\u4e2d\u901a\u8fc7\u5f15\u5165\u5177\u6709\u5f3a\u4f9b\u7535\u5b50\u80fd\u529b\u7684\u78f7\u9178\u4e09\u7532\u916f\uff08TMP\uff09\u6eb6\u5242\u5c06\u9634\u79bb\u5b50\u4ee5\u7f14\u5408\u79bb\u5b50\u5bf9\u7684\u5f62\u5f0f\u201c\u675f\u7f1a\u201d\u5728TMP\u7684\u6eb6\u5242\u5316\u533a\u57df\u4e2d\uff0c\u5b9e\u73b0\u4e86EMC\u6eb6\u5242\u5206\u5b50\u4e0e\u9634\u79bb\u5b50\u7684\u5206\u79bb\uff0c\u964d\u4f4e\u4e86\u6c27\u5316\u7a33\u5b9a\u6027\u8f83\u5dee\u7684EMC-TFSI\u2212<\/sup>\u7684\u6d53\u5ea6\u3002\u7535\u5316\u5b66\u6d4b\u8bd5\u7ed3\u679c\u8868\u660e\uff0c\u8fd9\u79cd\u9634\u79bb\u5b50\u6eb6\u5242\u5316\u7ed3\u6784\u8c03\u63a7\u7b56\u7565\u53ef\u5c06Zn(TFSI)2<\/sub>\/EMC\u7535\u89e3\u8d28\u7684\u7535\u5316\u5b66\u7a97\u53e3\u63d0\u9ad80.45 V\uff0c\u5e76\u4f7f\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u80fd\u57282.80 V\u7684\u9ad8\u622a\u6b62\u7535\u538b\u4e0b\u5145\u653e\u7535\u5faa\u73af1000\u6b21\uff08\u5bb9\u91cf\u4fdd\u6301\u7387\u8fbe\u523092\uff05\uff09\u3002\u6b64\u5916\uff0c\u52a0\u5165TMP\u540e\u7684Zn(TFSI)2<\/sub>\/EMC\u7535\u89e3\u8d28\u4ecd\u7136\u4fdd\u6301\u8f83\u9ad8\u7684\u79bb\u5b50\u7535\u5bfc\u7387\uff0c\u5e76\u5177\u5907\u963b\u71c3\u6027\u80fd\uff0c\u8fd9\u4e5f\u4fdd\u8bc1\u4e86\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u5177\u6709\u826f\u597d\u7684\u500d\u7387\u6027\u80fd\u548c\u5b89\u5168\u6027\u80fd\u3002\u76f8\u5173\u6210\u679c\u4ee5\u201c<\/strong>Anion solvation reconfiguration enables high-voltage carbonate electrolytes for stable Zn\/graphite cells<\/strong>\u201d\u53d1\u8868\u5728Angewandte Chemie International Edition<\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong> 1 <\/strong>\u91cd\u6784<\/strong>TFSI\u2212<\/sup><\/strong>\u9634\u79bb\u5b50\u7684\u6eb6\u5242\u5316\u7ed3\u6784\u6765\u63d0\u5347<\/strong>Zn(TFSI)2<\/sub>\/EMC<\/strong>\u7535\u89e3\u8d28\u7684\u6c27\u5316\u7a33\u5b9a\u6027\u5e76\u5e94\u7528\u4e8e\u9ad8\u7535\u538b\u950c<\/strong>\/<\/strong>\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u7684\u793a\u610f\u56fe<\/strong><\/p>\n

\"\"<\/p>\n

\u56fe<\/strong> 2 <\/strong>\u57fa\u4e8e<\/strong>Zn(TFSI)2<\/sub><\/strong>\u76d0\u7684\u4e0d\u540c\u7535\u89e3\u8d28\u5bf9\u950c<\/strong>\/<\/strong>\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd\u7684\u5f71\u54cd<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u57fa\u4e8e\u4e0d\u540c\u7535\u89e3\u8d28\u7684\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u7684\u6052\u7535\u6d41\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

\uff08b\u2212c\uff09\u57fa\u4e8e\u4e0d\u540c\u7535\u89e3\u8d28\u7684\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u5145\u7535\u52302.65 V\u540e\u7684\u81ea\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

\uff08d\uff09\u57fa\u4e8e\u4e0d\u540c\u7535\u89e3\u8d28\u7684\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u7684\u653e\u7535\u6bd4\u5bb9\u91cf\u4fdd\u6301\u66f2\u7ebf\uff1b<\/p>\n

\uff08e\uff09\u91c7\u7528Zn(TFSI)2<\/sub>\/EMC-TMP\u7535\u89e3\u8d28\u7684\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u5728\u4e0d\u540c\u5145\u7535\u622a\u6b62\u7535\u538b\u4e0a\u9650\u6761\u4ef6\u4e0b\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

\uff08f\uff09\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u57281 C\u500d\u7387\u5145\u653e\u7535\u6d4b\u8bd5\u8fc7\u7a0b\u4e2d\u7684\u539f\u4f4dXRD\u8c31\u56fe\u3002<\/p>\n

\u56fe<\/strong> 3 <\/strong>\u63a2\u7a76\u91c7\u7528<\/strong>Zn(TFSI)2<\/sub>\/EMC-TMP<\/strong>\u7535\u89e3\u8d28\u7684\u950c<\/strong>\/<\/strong>\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u5177\u6709\u4f18\u5f02\u5faa\u73af\u6027\u80fd\u7684\u539f\u56e0<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u91c7\u7528Zn(TFSI)2<\/sub>\/EMC-TMP\u7535\u89e3\u8d28\u7684\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u57281.20\u22122.80 V\u7535\u538b\u8303\u56f4\u5185\u7684\u957f\u5faa\u73af\u66f2\u7ebf\uff1b<\/p>\n

\uff08b\uff09\u901a\u8fc7CV\u6d4b\u8bd5\u83b7\u5f97\u7684\u4e0d\u540c\u7535\u89e3\u8d28\u4e2d\u950c\u6c89\u79ef\/\u6eb6\u89e3\u7684\u5e93\u4f26\u6548\u7387\u56fe\uff1b<\/p>\n

\uff08c\uff09\u901a\u8fc7LSV\u66f2\u7ebf\u6bd4\u8f83\u4e0d\u540c\u7535\u89e3\u6db2\u7684\u7535\u5316\u5b66\u7a97\u53e3\uff1b<\/p>\n

\uff08d\uff09\u91c7\u7528\u4e0d\u540c\u7535\u89e3\u8d28\u7ec4\u88c5\u7684\u950c\/\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u5728\u4e0d\u540c\u5145\u7535\u500d\u7387\u4e0b\u80fd\u591f\u8fbe\u5230\u7684\u5145\u7535\u622a\u6b62\u7535\u538b\u4e0a\u9650\u3002<\/p>\n

\u56fe<\/strong> 4 <\/strong>\u7535\u89e3\u8d28\u7684\u6eb6\u5242\u5316\u7ed3\u6784\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\u2212c\uff09\u4e0d\u540c\u7535\u89e3\u8d28\u4e2dTFSI\u2212<\/sup>\u3001EMC\u548cTMP\u5206\u522b\u5bf9\u5e94\u7684\u62c9\u66fc\u5149\u8c31\uff1b<\/p>\n

\uff08d\uff09\u91c7\u7528\u950c\u7b94\u4f5c\u4e3a\u5bf9\u7535\u6781\u548c\u53c2\u6bd4\u7535\u6781\uff0c\u4e0d\u540c\u7535\u89e3\u8d28\u4e2dTFSI\u2212<\/sup>\u5d4c\u5165\/\u8131\u51fa\u77f3\u58a8\u7535\u6781\u7684CV\u66f2\u7ebf\u3002<\/p>\n

\u56fe<\/strong> 5<\/strong> \u5206\u5b50\u52a8\u529b\u5b66\u6a21\u62df\u6eb6\u5242\u5316\u7ed3\u6784<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff091.5 M Zn(TFSI)2<\/sub>\/EMC\u548c\uff08b\uff091.5 M Zn(TFSI)2<\/sub>\/EMC-TMP\u7535\u89e3\u8d28\u6eb6\u6db2\u7684\u5206\u5b50\u52a8\u529b\u5b66\u6a21\u62df\u7ed3\u6784\u53ca\u76f8\u5e94\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08c\uff09\u4e0d\u540c\u7535\u89e3\u8d28\u4e2d\uff0cH(EMC)-F(TFSI\u2212<\/sup>)\u7684\u5f84\u5411\u5206\u5e03\u51fd\u6570\u56fe;<\/p>\n

\uff08d\uff091.5 M Zn(TFSI)2<\/sub>\/EMC-TMP\u7535\u89e3\u8d28\u4e2d\uff0cZn-O(TFSI\u2212<\/sup>)\u3001Zn-O(TMP)\u548cZn-O(EMC)\u7684\u5f84\u5411\u5206\u5e03\u51fd\u6570\u3002<\/p>\n

\u56fe<\/strong> 6 <\/strong>\u91c7\u7528<\/strong>Zn(TFSI)2<\/sub>\/EMC-TMP<\/strong>\u7535\u89e3\u8d28\u3001\u9ad8\u6d53\u76d0\u7535\u89e3\u8d28\u4ee5\u53ca\u79bb\u5b50\u6db2\u4f53\u7535\u89e3\u8d28\u7684\u950c<\/strong>\/<\/strong>\u77f3\u58a8\u53cc\u79bb\u5b50\u7535\u6c60\u7684\u500d\u7387\u6027\u80fd\u5bf9\u6bd4<\/strong><\/p>\n

\"\"<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5<\/strong>Anion solvation reconfiguration enables high-voltage carbonate electrolytes for stable Zn\/graphite cells<\/strong><\/a>\uff08Angewandte Chemie International Edition DOI: 10.1002\/anie.202010423\uff09\u3002<\/p>\n

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