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2.1 X-<\/strong>\u5149<\/strong><\/p>\n

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\u56fe\u516b<\/strong>X<\/strong>\u5c04\u7ebf\u65ad\u5c42\u6444\u5f71\u663e\u5fae\u955c<\/strong><\/p>\n

\"\"<\/p>\n

\u8fd9\u662f\u4e00\u9879\u529f\u80fd\u5f3a\u5927\u4e14\u65e0\u635f\u7684\u6280\u672f\uff0c\u53ef\u4ee5\u5bf9\u5404\u79cd\u6837\u54c1\u8fdb\u884c\u5feb\u901f\u9ad8\u5206\u8fa8\u7387\u7684\u5b9a\u91cf\u4f53\u79ef\u7814\u7a76\u3002 \u4f7f\u7528\u7a7f\u900f\u6027\u7684X\u5c04\u7ebf\uff0c\u53ef\u4ee5\u901a\u8fc7\u6570\u5b66\u7a0b\u5e8f\u65ad\u5c42\u6444\u5f71\u91cd\u5efa\u751f\u6210\u6837\u54c1\u4e0d\u540c\u90e8\u5206\u76843D\u56fe\u50cf\u3002\u8be5\u6280\u672f\u63d0\u4f9b\u4e86\u6837\u54c1\u7684\u8be6\u7ec6\u5f62\u6001\u4fe1\u606f\uff0c\u5bf9\u4e8e\u76f4\u63a5\u76d1\u6d4b\u964d\u89e3\u8fc7\u7a0b\u4e2dNIBAM\u7684\u5f62\u6001\uff0c\u7ed3\u6784\u548c\u5316\u5b66\u53d8\u5316\u53ef\u80fd\u975e\u5e38\u6709\u7528\u3002<\/p>\n

\u56fe\u4e5d<\/strong>X<\/strong>\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\uff08<\/strong>XPS<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

XPS\u662f\u4e00\u79cd\u8868\u9762\u654f\u611f\u7684\u5b9a\u91cf\u5149\u8c31\u6280\u672f\uff0c\u53ef\u6d4b\u91cf\u6837\u54c1\u4e2d\u5143\u7d20\u7684\u5143\u7d20\u7ec4\u6210\uff0c\u5316\u5b66\u548c\u7535\u5b50\u72b6\u6001\u3002 XPS\u53ef\u4ee5\u68c0\u6d4b\u539f\u5b50\u5e8f\u6570\u5927\u4e8e\u6216\u7b49\u4e8e3\uff08Li\uff09\u7684\u6240\u6709\u5316\u5b66\u5143\u7d20\u3002 XPS\u4e0d\u4ec5\u663e\u793a\u5143\u7d20\u7ec4\u6210\uff0c\u8fd8\u663e\u793a\u5b83\u4eec\u5982\u4f55\u952e\u5408\u3002 \u5728XPS\u4e2d\uff0c\u7528X\u5c04\u7ebf\u675f\u7167\u5c04\u6837\u54c1\uff0c\u540c\u65f6\u6d4b\u91cf\u52a8\u80fd\u548c\u9038\u51fa\u7684\u7535\u5b50\u6570\uff08\u8868\u9762\u5206\u6790\u6df1\u5ea6\u7ea610 nm\uff09\u3002<\/p>\n

\u56fe\u5341<\/strong>X<\/strong>\u5c04\u7ebf\u8367\u5149\uff08<\/strong>XRF<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

\u8be5\u6280\u672f\u57fa\u4e8e\u4ece\u5148\u524d\u88ab\u9ad8\u80fdX\u5c04\u7ebf\u6fc0\u53d1\u7684\u6837\u54c1\u4e2d\u68c0\u6d4b\u6b21\u7ea7X\u5c04\u7ebf\uff08\u5373\u53d1\u5c04\u7684\u6216\u53d1\u8367\u5149\u7684\uff09\u3002 \u5bf9\u4e8e\u611f\u5174\u8da3\u7684\u5143\u7d20\uff0c\u53ef\u4ee5\u5c06X\u5c04\u7ebf\u80fd\u91cf\u8bbe\u7f6e\u5728\u5438\u6536\u8fb9\u7f18\u7684\u6b63\u4e0a\u65b9\u3002 \u5982\u679c\u5c06\u5165\u5c04\u7684X\u5c04\u7ebf\u80fd\u91cf\u8bbe\u7f6e\u4e3a\u6837\u54c1\u4e2d\u51e0\u79cd\u5143\u7d20\u7684\u5438\u6536\u8fb9\u4e4b\u4e0a\uff0c\u5219\u5b83\u4eec\u5c06\u5168\u90e8\u4ee5\u4e0d\u540c\u7684\u80fd\u91cf\u53d1\u51fa\u8367\u5149\u3002 \u56e0\u6b64\uff0cX\u5c04\u7ebf\u8367\u5149\u6210\u50cf\u53ef\u6bd4X\u5c04\u7ebf\u5438\u6536\u66f4\u6709\u5229\u4e8e\u6536\u96c6\u5143\u7d20\u5206\u5e03\uff0c\u5c24\u5176\u662f\u5728\u7a00\u6837\u54c1\u4e2d\u3002<\/p>\n

2.2 <\/strong>\u7535\u5b50\u663e\u5fae\u955c<\/strong><\/p>\n

\u7535\u5b50\u663e\u5fae\u955c\u4f7f\u7528\u52a0\u901f\u7535\u5b50\u675f\u4f5c\u4e3a\u7167\u660e\u6e90\uff0c\u63d0\u4f9b\u975e\u5e38\u77ed\u7684\u6ce2\u957f\u5e76\u83b7\u5f97\u9ad8\u5206\u8fa8\u7387\u56fe\u50cf\u3002 \u7535\u5b50\u663e\u5fae\u955c\u6280\u672f\u591a\u79cd\u591a\u6837\uff0c\u4f8b\u5982\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c\uff08TEM\uff09\uff0c\u626b\u63cf\u7535\u5b50\u663e\u5fae\u955c\uff08SEM\uff09\u548c\u7535\u5b50\u5168\u606f\uff08EH\uff09\uff0c\u5b83\u53ef\u4ee5\u63d0\u4f9b\u4f4e\u81f3\u539f\u5b50\u7ea7\u7684\u7eb3\u7c73\u7ea7\u7a7a\u95f4\u5206\u8fa8\u7387\u548c\u6beb\u79d2\u7ea7\u65f6\u95f4\u5206\u8fa8\u7387\u7684\u7ec4\u5408\uff0c\u8fd9\u662f\u4efb\u4f55\u5176\u4ed6\u6280\u672f\u90fd\u65e0\u6cd5\u5b9e\u73b0\u7684\u3002<\/p>\n

\u56fe\u5341\u4e00\u7535\u5b50\u5168\u606f\u56fe\uff08<\/strong>EH<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

EH\u662f\u4e00\u79cd\u57fa\u4e8e\u7535\u5b50\u663e\u5fae\u955c\u7684\u5e72\u6d89\u6280\u672f\uff0c\u5176\u4e2d\u6837\u54c1\u66b4\u9732\u4e8e\u7535\u5b50\u675f\uff0c\u5176\u76f8\u5c06\u901a\u8fc7\u6837\u54c1\u4e0a\u7684\u9759\u7535\u52bf\u548c\u78c1\u573a\u8fdb\u884c\u8c03\u5236\u3002 \u4f7f\u6765\u81ea\u6837\u672c\u7684\u4fe1\u53f7\u548c\u53c2\u8003\u4fe1\u53f7\u76f8\u4e92\u5e72\u6270\uff0c\u8fd9\u5bfc\u81f4\u5168\u606f\u56fe\uff0c\u5373\u5e72\u6d89\u6761\u7eb9\u56fe\u6848\u3002<\/p>\n

2.3<\/strong>\u626b\u63cf\u63a2\u9488\u663e\u5fae\u955c<\/strong><\/p>\n

\u626b\u63cf\u63a2\u9488\u663e\u5fae\u955c\uff08SPM\uff09\u662f\u663e\u5fae\u955c\u7684\u4e00\u4e2a\u5206\u652f\uff0c\u901a\u8fc7\u4f7f\u7528\u7269\u7406\u63a2\u9488\u626b\u63cf\u6837\u54c1\u7684\u8868\u9762\u6765\u521b\u5efa\u6837\u54c1\u7684\u56fe\u50cf\u3002 SPM\u53ef\u4ee5\u7eb3\u7c73\u7ea7\u5206\u8fa8\u7387\u76d1\u89c6\u754c\u9762\u5f62\u8c8c\/\u5f62\u6001\u548c\u7535\u5316\u5b66\u6027\u8d28\u3002 \u6709\u591a\u79cd\u6a21\u5f0f\u53ef\u4ee5\u6539\u53d8\u4f7f\u7528\u8fd9\u4e9b\u76f8\u4e92\u4f5c\u7528\u83b7\u5f97\u56fe\u50cf\u7684\u65b9\u5f0f\uff0c\u4f8b\u5982\u539f\u5b50\u529b\u663e\u5fae\u955c\uff08AFM\uff09\uff0c\u626b\u63cf\u7535\u5316\u5b66\u663e\u5fae\u955c\uff08SECM\uff09\uff0c\u626b\u63cf\u79bb\u5b50\u7535\u5bfc\u663e\u5fae\u955c\uff08SICM\uff09\uff0c\u7535\u5316\u5b66\u5e94\u53d8\u663e\u5fae\u955c\uff08ESM\uff09\u7b49\u3002<\/p>\n

\u56fe\u5341\u4e8c\u626b\u63cf\u7535\u5316\u5b66\u663e\u5fae\u955c\uff08<\/strong>SECM<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

SECM\u63d0\u4f9b\u6709\u5173\u6c27\u5316\u8fd8\u539f\u6d3b\u6027\u7684\u7a7a\u95f4\u89e3\u6790\u4fe1\u606f\uff0c\u56e0\u6b64\u5df2\u7528\u4e8e\u7535\u50ac\u5316\uff0c\u8150\u8680\uff0c\u7535\u8377\u8f6c\u79fb\u52a8\u529b\u5b66\u548c\u673a\u7406\u7684\u9610\u660e\u3002\u6700\u8fd1\uff0cSECM\u5df2\u6210\u529f\u5e94\u7528\u4e8e\u7535\u6c60\u9886\u57df\uff0c\u8bc1\u660e\u5b83\u662f\u4e00\u79cd\u72ec\u7279\u800c\u5f3a\u5927\u7684\u5206\u6790\u5de5\u5177\uff0c\u53ef\u7528\u4e8e\u7814\u7a76\u7535\u6c60\u7535\u6781\u5904\u53d1\u751f\u7684\u51e0\u79cd\u8fc7\u7a0b\u3002<\/p>\n

\u56fe\u5341\u4e09\u626b\u63cf\u79bb\u5b50\u7535\u5bfc\u663e\u5fae\u955c\uff08<\/strong>SICM<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

SICM\u662f\u7528\u4e8e\u6c34\u7535\u89e3\u8d28\u4e2d\u7eb3\u7c73\u7ea7\u8868\u5f81\u7684\u975e\u63a5\u89e6\u6280\u672f\uff0c\u53ef\u4e3a\u7eb3\u7c73\u7ea7\u7535\u6c60\u7535\u6781\u7684\u5f62\u8c8c\u6210\u50cf\u548c\u7535\u5316\u5b66\u6027\u80fd\u63d0\u4f9b\u660e\u663e\u4f18\u52bf\u3002\u8be5\u6280\u672f\u7684\u63a2\u9488\u7531\u76f4\u5f84\u4e3a50-100 nm\u7684\u586b\u5145\u6709\u7535\u89e3\u8d28\u7684\u7eb3\u7c73\u6bdb\u7ec6\u7ba1\u5236\u6210\u3002 SICM\u7684\u5206\u8fa8\u7387\u53d6\u51b3\u4e8e\u9488\u5c16\u7684\u51e0\u4f55\u5f62\u72b6\u548c\u9488\u5c16\u7684\u8ddd\u79bb\u3002 \u901a\u5e38\uff0cSICM\u7684\u5782\u76f4\u5206\u8fa8\u7387\u4e3a10 nm\uff0c\u6a2a\u5411\u5206\u8fa8\u7387\u7ea6\u4e3a50 nm\u3002<\/p>\n

2.4 <\/strong>\u5149\u5b66\u6280\u672f<\/strong><\/p>\n

\u5149\u5b66\u6280\u672f\u5bf9\u4e8eNIBAM\u7684\u5f62\u6001\u5206\u6790\u7279\u522b\u6709\u7528\u3002 \u5b83\u4eec\u662f\u975e\u4fb5\u5165\u6027\uff0c\u975e\u7834\u574f\u6027\u548c\u975e\u771f\u7a7a\u7684\u5206\u6790\uff0c\u5bf9\u539f\u4f4d\u7535\u6c60\u7684\u8bbe\u8ba1\u7684\u9650\u5236\u8f83\u5c11\u3002\u6839\u636e\u5149\u6e90\u7684\u957f\u5ea6\u548c\u7c7b\u522b\uff0c\u5b83\u4eec\u53ef\u4ee5\u5206\u4e3a\u4ee5\u4e0b\u51e0\u7c7b\uff1a\u62c9\u66fc\u5149\u8c31\uff0c\u5085\u7acb\u53f6\u53d8\u6362\u7ea2\u5916\u5149\u8c31\uff08FTIR\uff09\uff0c\u5149\u5b66\u663e\u5fae\u955c\uff0c\u591a\u5149\u675f\u5149\u5b66\u5e94\u529b\u4f20\u611f\u5668\uff0c\u4ef7\u5dee\u5438\u6536\u5149\u8c31\u548c\u975e\u7ebf\u6027\u76f8\u5e72\u632f\u52a8\u5149\u8c31\u3002<\/p>\n

\u56fe\u5341\u56db\u62c9\u66fc\u5149\u8c31<\/strong><\/p>\n

\"\"<\/p>\n

\u62c9\u66fc\u5149\u8c31\u6cd5\u662f\u4e00\u79cd\u5f3a\u5927\u7684\u8868\u5f81\u6280\u672f\uff0c\u901a\u5e38\u7528\u4e8e\u7814\u7a76\u7535\u6781\u5faa\u73af\u8fc7\u7a0b\u4e2d\u7ed3\u6784\u6570\u636e\u4e0e\u7535\u5316\u5b66\u6570\u636e\u4e4b\u95f4\u7684\u5173\u7cfb\u3002 \u8be5\u4fe1\u606f\u662f\u901a\u8fc7\u5206\u5b50\u7684\u632f\u52a8\uff0c\u65cb\u8f6c\u548c\u4f4e\u9891\u6a21\u5f0f\u83b7\u5f97\u7684\uff0c\u8fd9\u4e9b\u6a21\u5f0f\u53d6\u51b3\u4e8e\u5176\u6676\u4f53\u5bf9\u79f0\u6027\uff0c\u952e\u6216\u7ed3\u6784\uff08\u65e0\u5e8f\uff09\u548c\u5e94\u53d8\u3002 \u4e3a\u6b64\uff0c\u5728\u6d4b\u91cf\u80fd\u91cf\u8f6c\u79fb\u7684\u540c\u65f6\uff0c\u5355\u8272\u5149\u6e90\u5fc5\u987b\u4e0e\u5206\u5b50\u632f\u52a8\uff0c\u58f0\u5b50\u6216\u5176\u4ed6\u6fc0\u53d1\u76f8\u4e92\u4f5c\u7528\u3002<\/p>\n

\u56fe\u5341\u4e94\u591a\u5149\u675f\u5149\u5b66\u5e94\u529b\u4f20\u611f\u5668\uff08<\/strong>MOSS<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

\u5728MOSS\u4e2d\uff0c\u6fc0\u5149\u675f\u4ece\u57fa\u6750\u8868\u9762\u53cd\u5c04\u51fa\u6765\uff1b \u5f53\u57fa\u677f\u7531\u4e8e\u819c\u5e94\u529b\u800c\u83b7\u5f97\u66f2\u7387\u65f6\uff0c\u53cd\u5c04\u5149\u675f\u5728\u5149\u7535\u63a2\u6d4b\u5668\u4e0a\u7684\u4f4d\u7f6e\u6539\u53d8\u3002 \u901a\u8fc7\u6d4b\u91cf\u5149\u675f\u4f4d\u7f6e\u7684\u5e73\u79fb\uff0c\u53ef\u4ee5\u8ba1\u7b97\u51fa\u57fa\u677f\u66f2\u7387\uff0c\u53ef\u4ee5\u6839\u636eStoney\u65b9\u7a0b\u5c06\u5176\u8f6c\u6362\u4e3a\u5e94\u529b\u539a\u5ea6\u503c\u3002\u8be5\u6280\u672f\u63d0\u4f9b\u4e86\u7535\u538b\uff0c\u7535\u6d41\u548c\u5e94\u529b\u4e4b\u95f4\u7684\u76f4\u63a5\u5173\u8054\uff0c\u5e76\u4e14\u80fd\u591f\u6d4b\u91cf\u53ef\u9006\u6027\uff08\u901a\u8fc7\u5408\u91d1\u5316\u8131\u5408\u91d1\u6216\u63d2\u5c42\u8131\u5d4c\u8fc7\u7a0b\u751f\u6210\uff09\u4ee5\u53ca\u5728\u7535\u5316\u5b66\u8fc7\u7a0b\u4e2d\u4ea7\u751f\u7684\u4e0d\u53ef\u9006\u5e94\u529b\uff08\u7531\u4e0d\u53ef\u9006SEI\uff0c\u65e0\u673a\u6b8b\u7559\u7269\u548c\u6b7b\u9502\u5f62\u6210\uff09\u4ea7\u751f\u3002<\/p>\n

2.5 <\/strong>\u4e2d\u5b50\u6280\u672f<\/strong><\/p>\n

\u8fd9\u4e9b\u6280\u672f\u662f\u975e\u4fb5\u5165\u6027\u7684\uff0c\u56e0\u4e3a\u5b83\u4eec\u5177\u6709\u9ad8\u6837\u54c1\u7a7f\u900f\u6027\uff0c\u5bf9\u4f4e\u539f\u5b50\u5e8f\u6570\u5143\u7d20\u654f\u611f\u548c\u4f4e\u4e2d\u5b50\u80fd\u7684\u4f18\u70b9\u3002 \u6b64\u5916\uff0c\u4e2d\u5b50\u662f\u96f6\u7535\u8377\u7c92\u5b50\uff0c\u5b83\u4e0e\u539f\u5b50\u6838\u76f8\u4e92\u4f5c\u7528\uff0c\u800cX\u5c04\u7ebf\u548c\u03b3\u5c04\u7ebf\u5219\u4e0e\u539f\u5b50\u7535\u5b50\u76f8\u4e92\u4f5c\u7528\uff0c\u8fd9\u4f7f\u5f97\u4e2d\u5b50\u6280\u672f\u7279\u522b\u9002\u7528\u4e8e\u540c\u4f4d\u7d20\uff0c\u5c24\u5176\u662f\u8f83\u8f7b\u7684\u540c\u4f4d\u7d20\u3002\u56e0\u6b64\uff0c\u4e00\u4e9b\u4e2d\u5b50\u6280\u672f\u5bf9\u4e8eNIBAM\u7814\u7a76\u662f\u5fc5\u4e0d\u53ef\u5c11\u7684\uff0c\u4f8b\u5982\u5c0f\u89d2\u4e2d\u5b50\u6563\u5c04\uff0c\u4e2d\u5b50\u884d\u5c04\uff0c\u4e2d\u5b50\u53cd\u5c04\u8ba1\uff0c\u4e2d\u5b50\u5c04\u7ebf\u7167\u76f8\/\u65ad\u5c42\u6210\u50cf\uff0c\u4e2d\u5b50\u6df1\u5ea6\u8f6e\u5ed3\u5206\u6790\u3002<\/p>\n

\u56fe\u5341\u516d\u5c0f\u89d2\u4e2d\u5b50\u6563\u5c04\uff08<\/strong>SANS<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

SANS\u901a\u8fc7\u4f7f\u7528\u9ad8\u7a7f\u900f\u6df1\u5ea6\u6765\u63d0\u4f9b\u7eb3\u7c73\u7ed3\u6784\u7684\u53d8\u5316\uff08\u4f8b\u5982\u9897\u7c92\u7684\u5927\u5c0f\uff0c\u4f53\u79ef\u548c\u5f62\u72b6\uff09\u3002\u56e0\u6b64\uff0cSANS\u548c\u7535\u5316\u5b66\u6d4b\u8bd5\u76f8\u7ed3\u5408\u662f\u4e00\u79cd\u7528\u4e8e\u76d1\u6d4b\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0bNIBAM\u5f62\u6001\u53d8\u5316\u7684\u975e\u4fb5\u5165\u6027\u65b9\u6cd5\uff0c\u5305\u62ec\u4f53\u79ef\u81a8\u80c0\u548c\u88c2\u7f1d\u7684\u4ea7\u751f\u3002<\/p>\n

\u56fe\u5341\u4e03\u4e2d\u5b50\u5c04\u7ebf\u6210\u76f8<\/strong>\/<\/strong>\u65ad\u5c42\u626b\u63cf<\/strong><\/p>\n

\"\"<\/p>\n

\u4e2d\u5b50\u5c04\u7ebf\u6210\u76f8\u6280\u672f\u662f\u4e00\u79cd\u6709\u4ef7\u503c\u7684\u5de5\u5177\uff0c\u5df2\u88ab\u7528\u4e8e\u4f7f\u6c14\u4f53\u6d41\u52a8\u901a\u9053\u4e2d\u7684\u6db2\u4f53\u6210\u50cf\u5e76\u5728\u591a\u5b54\u6750\u6599\u4e2d\u8fdb\u884c\u79bb\u5b50\u4f20\u8f93\u3002 \u5728\u4e2d\u5b50\u5c04\u7ebf\u6210\u76f8\u4e2d\uff0c\u5c06\u68c0\u6d4b\u5668\u653e\u7f6e\u5728\u88ab\u7167\u660e\u7269\u4f53\u7684\u540e\u9762\uff0c\u4ee5\u6d4b\u91cf\u901a\u8fc7\u8be5\u7269\u4f53\u7684\u4e2d\u5b50\u4f20\u8f93\u7684\u53d8\u5316\uff0c\u56e0\u4e3a\u4e2d\u5b50\u4e0e\u7535\u6c60\u7684\u76f8\u4e92\u4f5c\u7528\u4f1a\u51cf\u5c11\u6240\u4f20\u8f93\u7684\u4e2d\u5b50\u7684\u6570\u91cf\u3002<\/p>\n

\u56fe\u5341\u516b\u4e2d\u5b50\u6df1\u5ea6\u5256\u6790<\/strong><\/p>\n

\"\"<\/p>\n

NDP\u662f\u4e00\u79cd\u57fa\u4e8e\u4f4e\u80fd\u4e2d\u5b50\u7684\u6280\u672f\uff0c\u53ef\u4ee5\u5728\u7535\u6c60\u5faa\u73af\u671f\u95f4\u8f7b\u677e\u68c0\u6d4b\u79bb\u5b50\u5bc6\u5ea6\u968f\u7535\u6781\u6df1\u5ea6\u53d8\u5316\u7684\u5b9e\u65f6\u4fe1\u606f\u3002 \u5b83\u901a\u8fc7\u4ea7\u751f\u5206\u522b\u4e3a2055 keV\u548c2727 keV\u7684\u660e\u786e\u5b9a\u4e49\u7684\u80fd\u91cf\u76844He\uff08\u5982\u03b1\uff09\u548c3H\uff08\u5982tri\u6838\u7c92\u5b50\uff09\u6765\u5f15\u53d1\u88ab\u5206\u6790\u8868\u9762\u6216\u754c\u9762\u4e2d\u7ec4\u6210\u5143\u7d20\u7684\u6838\u53cd\u5e94\u3002\u8fd9\u4e9b\u751f\u6210\u7684\u7c92\u5b50\u5728\u8986\u76d6\u5230\u68c0\u6d4b\u5668\u4e4b\u524d\u4f1a\u901a\u8fc7\u7535\u6781\u5c42\u635f\u5931\u80fd\u91cf\u3002 \u53ef\u4ee5\u901a\u8fc7\u68c0\u6d4b\u539f\u5b50\u7684\u80fd\u91cf\u635f\u5931\u6765\u63a2\u7d22\u539f\u5b50\u7684\u5206\u5e03\u3002 \u56e0\u6b64\uff0c\u901a\u8fc7\u4f7f\u7528\u540c\u4f4d\u7d20\u79bb\u5b50\u6807\u8bb0\u7684\u7535\u6781\u6750\u6599\u548c\u7535\u89e3\u8d28\uff0c\u53ef\u4ee5\u5e2e\u52a9\u5728NDP\u671f\u95f4\u83b7\u5f97\u66f4\u597d\u7684\u4fe1\u53f7\u5f3a\u5ea6\u3002<\/p>\n

2.6<\/strong>\u78c1\u6027\u6280\u672f<\/strong><\/p>\n

\u53ef\u4ee5\u4f7f\u7528\u78c1\u6027\u6280\u672f\u6765\u539f\u4f4d\u63a2\u6d4b\u7535\u6781\u4e2d\u7684\u5316\u5b66\u73af\u5883\u3002\u6700\u5e38\u7814\u7a76\u7684\u7535\u6c60\u7cfb\u7edf\u5305\u542b\u9502\uff087<\/sup>Li\uff09\u6216\u94a0\uff0823<\/sup>Na\uff09\u5316\u5b66\u7269\u8d28\uff0c\u5b83\u4eec\u672c\u8d28\u4e0a\u662f\u987a\u78c1\u6027\u7684\uff0c\u5e76\u4e14\u5bf9\u65bd\u52a0\u7684\u78c1\u573a\u6709\u53cd\u5e94\u3002 \u5982\u4eca\uff0c\u5e38\u7528\u7684\u78c1\u6027\u6280\u672f\u662f\u6838\u78c1\u5171\u632f\u5149\u8c31\uff0c\u78c1\u5171\u632f\u6210\u50cf\uff0c\u7a46\u65af\u5821\u5c14\u5149\u8c31\uff0c\u7535\u5b50\u987a\u78c1\u5171\u632f\u5149\u8c31\u548c\u7535\u78c1\u6d4b\u91cf\u3002<\/p>\n

\u56fe\u5341\u4e5d\u78c1\u5171\u632f\u6210\u50cf\uff08<\/strong>MRI<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

MRI\u662fNMR\u7684\u81ea\u7136\u5ef6\u4f38\uff0c\u5e76\u63d0\u4f9b\u6709\u5173\u6807\u8bb0\u7684NMR\u6d3b\u6027\u6838\u7684\u7a7a\u95f4\u4fe1\u606f\u3002 MRI\u4f7f\u7528\u7279\u5b9a\u7684\u5316\u5b66\u4f4d\u79fb\u70b9\u5728\u7535\u5316\u5b66\u53cd\u5e94\u7684\u65f6\u95f4\u5c3a\u5ea6\u4e0a\u751f\u6210\u7535\u6c60\u76843D\u77e9\u9635\u56fe\u50cf\uff0c\u8fd9\u63d0\u4f9b\u4e86\u8db3\u591f\u7684\u65f6\u95f4\u5206\u8fa8\u7387\u6765\u5206\u6790\u6b63\u5728\u8fdb\u884c\u7684\u7535\u5316\u5b66\u8fc7\u7a0b\u3002 \u56e0\u6b64\uff0c\u5b83\u53ef\u4ee5\u6d4b\u91cf\u5177\u6709NMR\u6d3b\u6027\u7684\u7279\u5b9a\u6d53\u5ea6\u7269\u8d28\u7684\u7a7a\u95f4\u5206\u5e03\u3002<\/p>\n

\u56fe\u4e8c\u5341\u7535\u5b50\u987a\u78c1\u5171\u632f\uff08<\/strong>EPR<\/strong>\uff09<\/strong>\/<\/strong>\u7535\u5b50\u81ea\u65cb\u5171\u632f\uff08<\/strong>ESR<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

EPR\u6216ESR\u662f\u4e00\u79cd\u5206\u6790\u6280\u672f\uff0c\u53ef\u663e\u793a\u7531\u4e8e\u5b58\u5728\u672a\u914d\u5bf9\u7684\u7535\u5b50\u800c\u5bfc\u81f4\u7684\u6750\u6599\u7684\u987a\u78c1\u884c\u4e3a\u3002 ESR\u6bd4NMR\u66f4\u654f\u611f\uff0c\u56e0\u4e3a\u672a\u914d\u5bf9\u7684\u7535\u5b50\u81ea\u65cb\u6bd4\u6838\u81ea\u65cb\u66f4\u53d7\u6fc0\u53d1\u3002 \u5b83\u5df2\u7528\u4e8e\u4f30\u8ba1\u7535\u6781\u8868\u9762\u79ef\uff0c\u5e94\u5bf9\u5fae\u7ed3\u6784\u751f\u957f\u7684\u521d\u59cb\u5316\u4ee5\u53ca\u4f30\u8ba1\u987a\u78c1\u53cd\u5e94\u4e2d\u95f4\u4f53\u3002 \u5e94\u8be5\u6ce8\u610f\u7684\u662f\uff0c\u7528\u4e8e\u7535\u6c60\u7ed3\u6784\u7684\u6750\u6599\u5e94\u5bf9\u5fae\u6ce2\u8f90\u5c04\u900f\u660e\uff0c\u5e76\u4e14\u5bf9EPR\u65e0\u6548\u3002<\/p>\n

2.7 <\/strong>\u5176\u4ed6\u6280\u672f<\/strong><\/p>\n

\u56fe\u4e8c\u5341\u4e00\u58f0\u53d1\u5c04\uff08<\/strong>AE<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

AE\u65b9\u6cd5\u662f\u7528\u4e8e\u68c0\u6d4b\u7531\u7535\u6781\u6750\u6599\u65ad\u88c2\u4ea7\u751f\u7684\u5f39\u6027\u6ce2\u7684\u7075\u654f\u4e14\u65e0\u635f\u7684\u6280\u672f\u3002AE\u662f\u4e00\u79cd\u538b\u7535\u4f20\u611f\u5668\uff0c\u7528\u4e8e\u6307\u793a\u4ece\u6837\u54c1\u53d1\u51fa\u7684\u632f\u52a8\uff0c\u8be5\u632f\u52a8\u7ecf\u8fc7\u5404\u79cd\u5e94\u529b\u800c\u53d1\u751f\u673a\u68b0\u53d8\u5f62\u3002\u5b83\u53ef\u4ee5\u88ab\u8ba4\u4e3a\u662f\u7814\u7a76\u9502\u79bb\u5b50\u7535\u6c60\u8d1f\u6781\u4e2d\u673a\u68b0\u964d\u89e3\u7684\u6709\u4ef7\u503c\u7684\u5de5\u5177\uff0c\u8fd9\u4e9b\u7535\u6c60\u5728\u7535\u5316\u5b66\u5faa\u73af\u8fc7\u7a0b\u4e2d\u4f1a\u627f\u53d7\u4e25\u91cd\u7684\u5e94\u529b\u3002\u800c\u4e14\uff0c\u4e0e\u4e0a\u8ff0\u5927\u591a\u6570\u73b0\u573a\/\u64cd\u4f5c\u6570\u5206\u6790\u6280\u672f\u76f8\u6bd4\uff0c\u4f8b\u5982X\u5c04\u7ebf\uff0c\u7535\u5b50\uff0c\u4e2d\u5b50\uff0c\u5b83\u662f\u4f4e\u6210\u672c\u7684\u3002<\/p>\n

\u56fe\u4e8c\u5341\u4e8c\u98de\u884c\u65f6\u95f4\u4e8c\u6b21\u79bb\u5b50\u8d28\u8c31\uff08<\/strong>ToFSIMS<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

ToF-SIMS\u662f\u4e00\u79cd\u9ad8\u5ea6\u7075\u654f\u7684\u8868\u9762\u5206\u6790\u6280\u672f\uff0c\u5176\u4e2d\u4f7f\u7528\u8109\u51b2\u7684\u4e00\u6b21\u79bb\u5b50\u675f\u6765\u63d0\u53d6\u4e8c\u6b21\u79bb\u5b50\uff0c\u8be5\u4e8c\u6b21\u79bb\u5b50\u901a\u8fc7\u98de\u884c\u65f6\u95f4\u5149\u8c31\u6cd5\u8fdb\u884c\u5206\u6790\u3002 \u7528\u6e85\u5c04\u79bb\u5b50\u675f\u4ea4\u7ec7\uff0c\u53ef\u4ee5\u5bb9\u6613\u5730\u83b7\u5f97\u5177\u6709\u6781\u597d\u7684\u6df1\u5ea6\u5206\u8fa8\u7387\uff08\u5355\u5c42\uff09\u548c\u9ad8\u7075\u654f\u5ea6\uff08ppb\uff09\u7684\u7ec4\u6210\u6df1\u5ea6\u5206\u5e03\u56fe\u3002 SIMS\u80fd\u591f\u5206\u6790\u5143\u7d20\u5468\u671f\u8868\u4e2d\u7684\u6240\u6709\u5143\u7d20\uff08\u8f83\u8f7b\u6216\u8f83\u91cd\uff09\u3002 \u56e0\u6b64\uff0cSIMS\u53ef\u7528\u4e8e\u6700\u5927\u7a0b\u5ea6\u5730\u51cf\u5c11\u7e41\u7410\u7684\u57fa\u4e8e\u6838\u6280\u672f\u68c0\u6d4b\u8f83\u8f7b\u5143\u7d20\u7684\u7e41\u7410\u5e94\u7528\u3002 ToF-SIMS\u5df2\u5e94\u7528\u4e8e\u5faa\u73af\u7535\u6781\u6750\u6599\uff0c\u53ef\u63d0\u4f9b\u6709\u5173SEI\u5c42\u4ee5\u53ca\u5757\u72b6\u7535\u6781\u6750\u6599\u4e2d\u7269\u8d28\u7684\u6df1\u5ea6\u548c\u6a2a\u5411\u5206\u5e03\u7684\u4fe1\u606f\u3002<\/p>\n

\u56fe\u4e8c\u5341\u4e09\u7535\u5316\u5b66\u77f3\u82f1\u6676\u4f53\u5fae\u91cf\u5929\u5e73\uff08<\/strong>EQCM<\/strong>\uff09<\/strong><\/p>\n

\"\"<\/p>\n

EQCM\u662f\u4e00\u79cd\u7528\u4e8e\u975e\u5e38\u7cbe\u786e\u5730\u6d4b\u91cf\u6a21\u578b\u7535\u6781\u8d28\u91cf\u53d8\u5316\u7684\u6280\u672f\u3002 \u88ab\u7814\u7a76\u7684\u7535\u6781\u6c89\u79ef\u5728\u4e00\u4e2a\u632f\u8361\u77f3\u82f1\u4f20\u611f\u5668\u4e0a\uff0c\u5728\u4f17\u6240\u5468\u77e5\u7684\u5747\u5300\u4e14\u521a\u6027\u5c42\u7c98\u9644\u5230\u4f20\u611f\u5668\u8868\u9762\u7684\u7406\u60f3\u60c5\u51b5\u4e0b\uff0c\u6839\u636eSauerbrey\u65b9\u7a0b\uff0c\u5176\u8c10\u632f\u9891\u7387\u4e0e\u4f20\u611f\u5668\u8d28\u91cf\u7ebf\u6027\u76f8\u5173\u3002<\/p>\n

\u56fe\u4e8c\u5341\u56db\u7535\u5316\u5b66\u81a8\u80c0\u6cd5<\/strong><\/p>\n

\"\"<\/p>\n

\u539f\u4f4d\u7535\u5316\u5b66\u81a8\u80c0\u6cd5\uff08ECD\uff09\u662f\u7814\u7a76\u590d\u5408\u7535\u6781\u6709\u6548\u9ad8\u5ea6\u53d8\u5316\u7684\u6700\u5408\u9002\u6280\u672f\uff0c\u8be5\u6280\u672f\u6700\u65e9\u4e8e1970\u5e74\u4ee3\u540e\u671f\u5f15\u5165\u3002\u539f\u4f4dECD\u5728\u7535\u6c60\u5185\u96c6\u6210\u4e86\u4f4d\u79fb\u4f20\u611f\u5668\uff0c\u4ee5\u6d4b\u91cf\u7535\u6781\u7684\u5782\u76f4\u5b8f\u89c2\u4f4d\u79fb\uff0c\u4ee5\u83b7\u5f97\u4e0e\u4f53\u79ef\u81a8\u80c0\u6709\u5173\u7684\u4fe1\u606f\u3002\u5df2\u8bc1\u660e\u539f\u4f4dECD\u53ef\u63d0\u4f9b\u6709\u5173\u7535\u6781\u53d8\u5f62\uff0c\u5206\u5c42\u6750\u6599\u7684\u7535\u5d4c\u5165\u4ee5\u53ca\u4e0d\u53ef\u9006\u53cd\u5e94\uff08\u4f8b\u5982SEI\u5f62\u6210\uff09\u7684\u91cd\u8981\u4fe1\u606f\u3002XRD\u548cECD\u6280\u672f\u7684\u7ed3\u5408\u6700\u6709\u53ef\u80fd\u63ed\u793a\u5fae\u89c2\u6676\u4f53\u7ed3\u6784\u53d8\u5316\u5bf9\u6574\u4e2a\u590d\u5408\u7535\u6781\u7684\u5b8f\u89c2\u81a8\u80c0\/\u6536\u7f29\u884c\u4e3a\u7684\u8d21\u732e\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a<\/strong>\u201c<\/strong>Electroanalytical methods and their hyphenated techniques for novel ion battery anode research<\/strong><\/a>\u201d(Energ. Environ. Sci. DOI: 10.1039\/D0EE01184C)<\/strong><\/p>\n

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