{"id":204646,"date":"2020-07-06T12:00:16","date_gmt":"2020-07-06T04:00:16","guid":{"rendered":"\/\/m.iemloyee.com\/?p=204646"},"modified":"2020-07-06T09:58:15","modified_gmt":"2020-07-06T01:58:15","slug":"%e3%80%90%e5%b7%b2%e6%a0%a1%e7%a8%bf%e3%80%91%e6%94%af%e6%98%a5%e4%b9%89%e5%9b%a2%e9%98%9fsmall%ef%bc%9a%e9%80%9a%e8%bf%87%e5%9c%a8%e6%b0%a2%e6%b0%a7%e5%8c%96%e7%89%a9%e6%ad%a3%e6%9e%81%e4%b8%ad","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=204646","title":{"rendered":"\u652f\u6625\u4e49\u56e2\u961fSmall\uff1a\u901a\u8fc7\u5728\u6c22\u6c27\u5316\u7269\u6b63\u6781\u4e2d\u63ba\u6742F\u63d0\u9ad8\u6c34\u7cfb\u67d4\u6027Zn\u7535\u6c60\u7684\u5faa\u73af\u7a33\u5b9a\u6027"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n

\u00a0\u53ef\u5145\u7535\u6c34\u7cfb\u950c\u7535\u6c60\uff08RAZBs\uff09\u5df2\u7ecf\u53d6\u5f97\u4e86\u5de8\u5927\u7684\u8fdb\u6b65\uff0c\u4f46\u5176\u8f83\u5dee\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u4ecd\u7136\u4f1a\u963b\u788d\u5176\u5e7f\u6cdb\u5e94\u7528\u3002\u4e00\u65b9\u9762\uff0cRAZBs\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u4e0d\u7406\u60f3\u662f\u7531\u950c\u8d1f\u6781\u9020\u6210\u7684\uff0c\u950c\u8d1f\u6781\u901a\u5e38\u9762\u4e34\u7740\u5f62\u53d8\u3001\u949d\u5316\u548c\u679d\u6676\u7684\u5f62\u6210\u7b49\u95ee\u9898\uff0c\u5e78\u8fd0\u7684\u662f\uff0c\u8fd9\u4e9b\u95ee\u9898\u53ef\u4ee5\u901a\u8fc7\u5404\u79cd\u7b56\u7565\u6765\u89c4\u907f\uff0c\u5305\u62ec\u7ed3\u6784\u8bbe\u8ba1\u3001\u4fdd\u62a4\u5c42\u6d82\u8986\u548c\u7535\u89e3\u8d28\u8c03\u63a7\u7b49\u3002\u53e6\u4e00\u65b9\u9762\uff0c\u6b63\u6781\u6750\u6599\u7a33\u5b9a\u6027\u5dee\uff0c\u4f1a\u5bfc\u81f4RAZBs\u5bff\u547d\u77ed\u3002\u7531\u4e8e\u6b63\u6781\u6750\u6599\u7684\u591a\u6837\u6027\u548c\u4e0d\u540c\u7684\u50a8\u80fd\u673a\u5236\uff0c\u5bfc\u81f4\u6b63\u6781\u6750\u6599\u5faa\u73af\u7a33\u5b9a\u6027\u5dee\u7684\u539f\u56e0\u6bd4\u8f83\u590d\u6742\u3002\u6b63\u6781\u5728\u957f\u671f\u5145\u653e\u7535\u5faa\u73af\u8fc7\u7a0b\u4e2d\u901a\u5e38\u4f1a\u51fa\u73b0\u4e0d\u53ef\u9006\u76f8\u53d8\u3001\u7ed3\u6784\u574d\u584c\u3001\u4f53\u79ef\u81a8\u80c0\u6216\u6d3b\u6027\u91d1\u5c5e\u79bb\u5b50\u6eb6\u89e3\u7b49\u95ee\u9898\u3002\u4e3a\u4e86\u6539\u5584\u8fd9\u4e9b\u7531\u6b63\u6781\u5f15\u53d1\u7684\u95ee\u9898\uff0c\u79d1\u5b66\u5bb6\u4eec\u63d0\u51fa\u4e86\u8bb8\u591a\u6539\u5584\u7b56\u7565\uff0c\u5982\u5229\u7528\u7a33\u5b9a\u5242\u63d2\u5c42\u3001\u78b3\u5c42\u6d82\u8986\u3001\u7eb3\u7c73\u7ed3\u6784\u8bbe\u8ba1\u7b49\uff0c\u4ee5\u63d0\u9ad8\u6b63\u6781\u6750\u6599\u7684\u7a33\u5b9a\u6027\u3002\u867d\u7136\u4e0a\u8ff0\u7b56\u7565\u5df2\u7ecf\u5b9e\u73b0\u4e86\u5faa\u73af\u7a33\u5b9a\u6027\u7684\u589e\u5f3a\uff0c\u4f46\u901a\u5e38\u5176\u590d\u6742\u7684\u5408\u6210\u8fc7\u7a0b\u53ef\u80fd\u4f1a\u963b\u788d\u5927\u89c4\u6a21\u751f\u4ea7\u3002\u6b64\u5916\uff0c\u5355\u4e00\u7684\u7b56\u7565\u53ef\u80fd\u65e0\u6cd5\u5168\u9762\u987e\u53ca\u5230\u6b63\u6781\u6750\u6599\u7684\u6240\u6709\u95ee\u9898\uff0c\u53ea\u80fd\u5bf9\u5faa\u73af\u7a33\u5b9a\u6027\u4ea7\u751f\u6709\u9650\u7684\u6539\u5584\u3002\u5143\u7d20\u63ba\u6742\uff08\u5982\u6c2e\u3001\u786b\u3001\u787c\u3001\u78f7\u3001\u6c1f\u7b49\uff09\u88ab\u5e7f\u6cdb\u5e94\u7528\u4e8e\u7535\u6781\u6750\u6599\u6539\u6027\uff0c\u5bf9\u6750\u6599\u7684\u7406\u5316\u6027\u8d28\u3001\u7535\u5316\u5b66\u6027\u8d28\u6709\u660e\u663e\u7684\u5f71\u54cd\uff0c\u4f46\u6b64\u7c7b\u65b9\u6cd5\u5728\u950c\u7535\u6c60\u9886\u57df\u5c1a\u672a\u62a5\u9053\u3002F\u5177\u6709\u6781\u9ad8\u7684\u7535\u8d1f\u6027\uff0c\u88ab\u8ba4\u4e3a\u662f\u4e00\u79cd\u5f88\u6709\u524d\u9014\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u4f9b\u4f53\u63ba\u6742\u5242\u3002\u503c\u5f97\u6ce8\u610f\u7684\u662f\uff0cF\u548cO\u79bb\u5b50\u7684\u76f8\u4f3c\u7684\u79bb\u5b50\u534a\u5f84\u4f7fF\u80fd\u591f\u90e8\u5206\u53d6\u4ee3\u91d1\u5c5e\u6c27\u5316\u7269\u4e2d\u7684\u6676\u683c\u6c27\u4f4d\u70b9\u3002\u56e0\u6b64\uff0cF\u63ba\u6742\u7531\u4e8e\u6539\u53d8\u4e86\u91d1\u5c5e\u6c27\u5316\u7269\/\u6c22\u6c27\u5316\u7269\u7684\u7535\u5b50\u7ed3\u6784\u6216\u76f8\u7ed3\u6784\uff0c\u53ef\u80fd\u4f1a\u5bf9\u7535\u6781\u6750\u6599\u7684\u7535\u5316\u5b66\u53cd\u5e94\u52a8\u529b\u5b66\u3001\u5faa\u73af\u7a33\u5b9a\u6027\u7b49\u6709\u91cd\u8981\u5f71\u54cd\u3002\u91d1\u5c5e-F\u952e\u7684\u5f62\u6210\u5c06\u4ea7\u751f\u66f4\u7a33\u5b9a\u7684\u91d1\u5c5e\u6c27\u5316\u7269\/\u6c22\u6c27\u5316\u7269\u76f8\u7ed3\u6784\uff0c\u9632\u6b62\u91d1\u5c5e\u79bb\u5b50\u7684\u6eb6\u89e3\uff0c\u5e76\u80fd\u591f\u63d0\u4f9b\u66f4\u9ad8\u7684\u6676\u683c\u80fd\u548c\u66f4\u5c0f\u7684\u6781\u5316\u3002\u6b64\u5916\uff0cF\u539f\u5b50\u7684\u52a0\u5165\u80fd\u591f\u5e73\u8861\u7535\u89e3\u6db2\uff08\u5c24\u5176\u6c34\u7cfb\u7535\u89e3\u6db2\uff09\u4e2d\u591a\u4f59\u7684\u8d28\u5b50\uff0c\u4ece\u800c\u7a33\u5b9a\u7535\u6781\u7684\u7ed3\u6784\u3002\u76ee\u524d\uff0cF\u63ba\u6742\u7b56\u7565\u5728Zn\u7535\u6c60\u4e2d\u7684\u5e94\u7528\u5c1a\u7f3a\u4e4f\u7814\u7a76\uff0cF\u63ba\u6742\u5bf9\u950c\u57fa\u7535\u6c60\u6b63\u6781\u6750\u6599\u7a33\u5b9a\u6027\u7684\u6539\u5584\u7f3a\u4e4f\u7cfb\u7edf\u7814\u7a76\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\u652f\u6625\u4e49\u6559\u6388<\/b><\/strong>\u3001\u677e\u5c71\u6e56\u6750\u6599\u5b9e\u9a8c\u5ba4\u674e\u6d2a\u98de\u526f\u7814\u7a76\u5458\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/b><\/strong>\u7b49\u4eba\u63d0\u51fa\u4e86\u4e00\u79cd\u7b80\u4fbf\u7684F\u63ba\u6742\u7b56\u7565\uff0c\u63d0\u9ad8\u954d\u94b4\u78b3\u9178\u76d0\u6c22\u6c27\u5316\u7269\uff08NiCo-CH\uff09\u6b63\u6781\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u5f97\u76ca\u4e8e\u6781\u9ad8\u7684\u7535\u8d1f\u6027\uff0cF\u7684\u63ba\u5165\uff08NiCo-CH-F\uff09\u663e\u8457\u63d0\u9ad8\u4e86NiCo-CH\u7684\u76f8\u548c\u5f62\u8c8c\u7a33\u5b9a\u6027\u4ee5\u53ca\u7535\u5bfc\u7387\u3002\u540c\u65f6\u8fd8\u5f15\u5165\u4e86\u6709\u5229\u4e8e\u6b63\u6781\u6750\u6599\u7a33\u5b9a\u7684\u5f02\u8d28\u754c\u9762\u548c\u975e\u6676\u5fae\u7574\u3002\u53d7\u76ca\u4e8e\u8fd9\u4e9b\u7279\u6027\uff0cNiCo-CH-F\u5177\u6709\u9ad8\u5bb9\u91cf\uff08245 mA hg-1<\/sup>\uff09\u3001\u4f18\u5f02\u7684\u500d\u7387\u80fd\u529b\uff08\u57288 A g-1<\/sup>\u4e0b\u4fdd\u630164\uff05\uff09\u548c\u4f18\u5f02\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff08\u572810000\u6b21\u5faa\u73af\u540e\u4fdd\u630190%\uff09\u3002\u6b64\u5916\uff0c\u51c6\u56fa\u6001\u7535\u6c60\u8fd8\u8868\u73b0\u51fa\u51fa\u8272\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff087200\u6b21\u5faa\u73af\u540e\u4fdd\u630190\uff05\uff09\u548c\u7406\u60f3\u7684\u67d4\u6027\u3002\u8fd9\u9879\u5de5\u4f5c\u4e3a\u63d0\u9ad8\u6c34\u7cfb\u950c\u7535\u6c60\u6b63\u6781\u6750\u6599\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u63d0\u4f9b\u4e86\u4e00\u79cd\u65b0\u7b56\u7565\u3002\u8be5\u6210\u679c\u4ee5\u9898\u4e3a\u201cBoosting the Cycling Stability of Aqueous Flexible Zn Batteries via F Doping in Nickel-Cobalt Carbonate Hydroxide Cathode\u201d<\/b><\/strong>\u53d1\u8868\u5728\u4e86Small<\/b><\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n

\u56fe<\/b><\/strong>1 <\/b><\/strong>NiCo-CH-F\u7684<\/b><\/strong>\u5f62\u8c8c\u8868\u5f81<\/b><\/strong>\"\"<\/p>\n

a\uff09NiCo-CH\u548cNiCo-CH-F\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

b\uff09NiCo-CH\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

c\uff0cd\uff09NiCo\u2013CH\u2013F\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

e\uff0cf\uff09NiCo\u2013CH\u2013F\u7684HRTEM\u56fe\u50cf\uff1b<\/p>\n

g\uff09NiCo\u2013CH\u2013F\u7684EDX\u5143\u7d20\u5206\u5e03\u56fe\u3002<\/p>\n

\u56fe<\/b><\/strong>2 <\/b><\/strong>NiCo\u2013CH\u2013F\u7684<\/b><\/strong>XPS\u5149\u8c31\u8868\u5f81<\/b><\/strong>\"\"<\/p>\n

a,b\uff09NiCo-CH\u548cNiCo-CH-F\u7684XPS\u6d4b\u91cf\u5149\u8c31\uff1b<\/p>\n

c-f\uff09NiCo\u2013CH\u2013F\u7684c\uff09Ni 2p\uff0cd\uff09Co 2p\uff0ce\uff09F 1s\u548cf\uff09O 1s\u7684\u9ad8\u5206\u8fa8\u7387XPS\u5149\u8c31\u3002<\/p>\n

\u56fe<\/b><\/strong>3 <\/b><\/strong>NiCo-CH-F<\/b><\/strong>\u7684\u7535\u5316\u5b66<\/b><\/strong>\u6027\u80fd<\/b><\/strong>\u8868\u5f81<\/b><\/strong>\"\"<\/p>\n

a\uff09NiCo-CH\u548cNiCo-CH-F\u57285 mV s-1<\/sup>\u65f6\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

b\uff09Ipa<\/sub>\u548c\u626b\u63cf\u901f\u7387\u7684\u5e73\u65b9\u6839\u4e4b\u95f4\u7684\u7ebf\u6027\u5173\u7cfb\uff1b<\/p>\n

c\uff09NiCo-CH\u548cNiCo-CH-F\u57281 A g-1<\/sup>\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

d\uff09\u6837\u54c1\u7684\u500d\u7387\u6027\u80fd\uff1b<\/p>\n

e\uff09\u4e0d\u540c\u7535\u6d41\u5bc6\u5ea6\u4e0bNiCo-CH-F\u7684\u5145\u7535\/\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

f\uff09\u6837\u54c1\u7684Nyquist\u56fe\uff1b<\/p>\n

g\uff09\u6837\u54c1\u7684\u5faa\u73af\u6027\u80fd\u3002<\/p>\n

\u56fe<\/b><\/strong>4<\/b><\/strong>\u00a0<\/b><\/strong>NiCo\u2013CH\u2013F\/\/Zn\u7684\u5145\/\u653e\u7535\u66f2\u7ebf<\/b><\/strong>\"\"<\/p>\n

a,b\uff09\u5728\u4e0d\u540c\u5145\/\u653e\u7535\u72b6\u6001\u4e0b\u7684a\uff09Ni 2p\u548cb\uff09Co 2p\u00a0XPS\u5149\u8c31\uff1b<\/p>\n

c\uff09NiCo\u2013CH\u2013F\/\/Zn\u7684\u5145\/\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

d,\u00a0e\uff09\u5145\u653e\u7535\u8fc7\u7a0b\u4e2dd\uff09Ni2+<\/sup>\u548cNi3+<\/sup>\u548ce\uff09Co2+<\/sup>\u3001\u00a0Co3+<\/sup>\u548cCo4+<\/sup>\u7684\u539f\u5b50\u542b\u91cf\u53d8\u5316\u3002<\/p>\n

\u56fe<\/b><\/strong>5 NiCo-CH-F<\/b><\/strong>\u5faa\u73af\u540e\u7684\u7535\u5316\u5b66\u6027\u80fd\u8868\u5f81<\/b><\/strong>\"\"<\/p>\n

a\uff09\u4e0d\u540c\u5faa\u73af\u540eNiCo-CH-F\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

b,c\uff09NiCo\u2013CH\u2013F\u57282500\u6b21\u5faa\u73af\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

d,e\uff09NiCo\u2013CH\u2013F\u572810000\u6b21\u5faa\u73af\u540e\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

f,g\uff09\u4e0d\u540c\u5faa\u73af\u540e\uff0cNiCo\u2013CH\u2013F\u7684f\uff09Nyquist\u56fe\u548cg\uff09CV\u66f2\u7ebf\uff1b<\/p>\n

h\uff09NiCo\u2013CH\u2013F\u5728\u4e0d\u540c\u5faa\u73af\u540e\u7684\u53cc\u7535\u5c42\u7535\u5bb9\u6d4b\u8bd5\u3002<\/p>\n

i\uff09NiCo\u2013CH\u548cNiCo\u2013CH\u2013F\u57285000\u6b21\u5faa\u73af\u540e\u7684\u53cc\u7535\u5c42\u7535\u5bb9\u5bf9\u6bd4\u3002<\/p>\n

\u56fe<\/b><\/strong>6<\/b><\/strong>\u00a0NiCo-CH-F\/\/Zn\u67d4\u6027\u7535\u6c60\u5728\u6c34\u51dd\u80f6\u7535\u89e3\u8d28\u4e0b\u7684\u7535\u5316\u5b66\u6027\u80fd<\/b><\/strong>\"\"<\/p>\n

a\uff09\u6c34\u7cfb\u7535\u89e3\u8d28\u548c\u6c34\u51dd\u80f6\u7535\u89e3\u8d28\u57285 mV s-1<\/sup>\u65f6\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

b-f\uff09NiCo-CH-F\/\/Zn\u67d4\u6027\u7535\u6c60\u5728\u6c34\u51dd\u80f6\u7535\u89e3\u8d28\u4e0b\u7684b\uff09\u500d\u7387\u6027\u80fd\uff0cc\uff09\u572850 mV s-1<\/sup>\u7684CV\u66f2\u7ebf\uff0cd\uff09Nyquist\u56fe\uff0ce\uff09\u5728\u4e0d\u540c\u53d8\u5f62\u4e0b\u7684\u5faa\u73af\u7a33\u5b9a\u6027\uff08\u63d2\u56fe\u4e3a\u76f8\u5e94\u7684\u5145\u653e\u7535\u66f2\u7ebf\uff09\uff0cf\uff09\u957f\u5faa\u73af\u7a33\u5b9a\u6027\u6d4b\u8bd5\uff1b<\/p>\n

g\uff09\u7ec4\u88c5\u7684\u7535\u6c60\u4e32\u8054\u8d77\u6765\uff0c\u4e3a\u4e00\u575715\u00d710 cm2<\/sup>\u7684\u7535\u81f4\u53d1\u5149\u9762\u677f\u4f9b\u7535\uff1b<\/p>\n

h\uff09\u5728\u5f2f\u66f2\u72b6\u6001\u4e0b\u7684\u7535\u5b50\u7eb8\uff1b<\/p>\n

i\uff09\u5728\u4e0d\u540c\u53d8\u5f62\u4e0b\u7531\u5355\u7535\u6c60\u4f9b\u7535\u7684\u6570\u5b57\u6e7f\u5ea6\u8ba1\u3002<\/p>\n

\u3010\u5c0f\u7ed3<\/b><\/strong>\u3011<\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1a<\/b><\/strong>Boosting the Cycling Stability of Aqueous Flexible Zn Batteries via F Doping in Nickel<\/u>-Cobalt Carbonate Hydroxide Cathode<\/u><\/a>\uff08Small\uff0c\u00a02020\uff0cDOI:10.1002\/smll.202001935\uff09<\/p>\n

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