{"id":200380,"date":"2020-04-28T06:47:43","date_gmt":"2020-04-27T22:47:43","guid":{"rendered":"\/\/m.iemloyee.com\/?p=200380"},"modified":"2020-04-27T20:48:18","modified_gmt":"2020-04-27T12:48:18","slug":"%e5%a4%8d%e6%97%a6%e5%a4%a7%e5%ad%a6%e9%9d%92%e5%b2%9b%e5%a4%a7%e5%ad%a6aenm-%e5%85%b7%e6%9c%89%e9%9b%b6%e5%ba%94%e5%8f%98%e5%92%8c%e4%bc%98%e5%bc%82%e5%82%a8%e9%94%82%e6%80%a7","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=200380","title":{"rendered":"\u590d\u65e6\u5927\u5b66&\u9752\u5c9b\u5927\u5b66AEnM: \u5177\u6709\u201c\u96f6\u5e94\u53d8\u201d\u548c\u4f18\u5f02\u50a8\u9502\u6027\u80fd\u7684Li3.08Cr0.02Si0.09V0.9O4\u8d1f\u6781\u6750\u6599"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u5982\u4eca\uff0c\u9502\u79bb\u5b50\u7535\u6c60(LIBs)\u5728\u4fbf\u643a\u5f0f\u7535\u5b50\u8bbe\u5907\uff08\u4f8b\u5982\u624b\u673a\u548c\u7b14\u8bb0\u672c\u7535\u8111\uff09\u4e2d\u53d6\u5f97\u4e86\u5de8\u5927\u7684\u6210\u529f\u3002\u4f46\u662f\uff0c\u5176\u5728\u7535\u52a8\u6c7d\u8f66\u4e0a\u7684\u5e94\u7528\u4ecd\u53d7\u9650\u4e8e\u7535\u6c60\u5bff\u547d\u77ed\uff0c\u5b89\u5168\u6027\u4ee5\u53ca\u80fd\u91cf\u5bc6\u5ea6\u7b49\u95ee\u9898\u7684\u5236\u7ea6\u3002\u7279\u522b\u5730\uff0c\u5faa\u73af\u5bff\u547d\u5728\u5b9e\u9645\u5e94\u7528\u4e2d\u81f3\u5173\u91cd\u8981\u3002LIBs\u7684\u5bb9\u91cf\u8870\u51cf\u4e3b\u8981\u6e90\u4e8e\u4ee5\u4e0b\u539f\u56e0\uff1a\u7535\u6781\u6750\u6599\u901a\u5e38\u627f\u53d7\u4e00\u5b9a\u7684\u673a\u68b0\u5e94\u529b\uff0c\u56e0\u4e3aLi+<\/sup>\u5728\u8131\u5d4c\u8fc7\u7a0b\u4f1a\u5f15\u8d77\u76f8\u53d8\u6216\u8005\u6676\u683c\u53c2\u6570\u53d8\u5316\u3002\u4e24\u76f8\u53cd\u5e94\u4e2d\u4e3b\u5bfc\u76f8\u548c\u5171\u5b58\u76f8\u4e4b\u95f4\u7684\u6676\u683c\u53c2\u6570\u4e0d\u5339\u914d\u6216\u8005\u56fa\u6eb6\u53cd\u5e94\u4e2d\u8f83\u5927\u7684\u6676\u80de\u4f53\u79ef\u53d8\u5316\u4f1a\u5bfc\u81f4\u76f8\u754c\u9762\u65ad\u88c2\uff0c\u4ece\u800c\u5bfc\u81f4\u5bb9\u91cf\u8870\u51cf\u3002\u5728\u201c\u96f6\u5e94\u53d8\u201d\u7535\u6781\u6750\u6599\u4e2d\uff0c\u8fd9\u4e9b\u95ee\u9898\u53ef\u4ee5\u5b8c\u5168\u907f\u514d\uff0c\u5728\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d\u5176\u6676\u80de\u4f53\u79ef\u7684\u53d8\u5316\u53ef\u4ee5\u5ffd\u7565\u4e0d\u8ba1(<1\uff05)\u3002\u4f17\u6240\u5468\u77e5\uff0c\u5c16\u6676\u77f3Li4<\/sub>Ti5<\/sub>O12<\/sub>\u662f\u4e00\u79cd\u5178\u578b\u7684\u201c\u96f6\u5e94\u53d8\u201d\u8d1f\u6781\u6750\u6599\uff0c\u53ef\u4ee5\u7a33\u5b9a\u5faa\u73af\u6570\u5343\u6b21\u3002\u5176\u51fa\u8272\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u6e90\u4e8e\u5faa\u73af\u65f6\u5fae\u5c0f\u7684\u4f53\u79ef\u53d8\u5316(\u22480.2\uff05)\u3002\u8fd8\u6709\u4e00\u4e9b\u5176\u4ed6\u201c\u96f6\u5e94\u53d8\u201d\u8d1f\u6781\u6750\u6599\uff0c\u4f8b\u5982LiCrTiO4<\/sub>\u548cLiY(MoO4<\/sub>)2<\/sub>\u4e5f\u5177\u6709\u4f18\u5f02\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002\u7136\u800c\uff0c\u5927\u591a\u6570\u7528\u4e8e\u9502\u79bb\u5b50\u7684\u201c\u96f6\u5e94\u53d8\u201d\u8d1f\u6781\u6750\u6599\u901a\u5e38\u5177\u6709\u8f83\u4f4e\u7684\u53ef\u9006\u5bb9\u91cf\u548c\u8fc7\u9ad8\u7684\u5de5\u4f5c\u7535\u52bf\uff0c\u8fd9\u4f1a\u6781\u5927\u964d\u4f4e\u4e86\u5168\u7535\u6c60\u7684\u80fd\u91cf\u5bc6\u5ea6\u3002<\/p>\n

\u00a0<\/strong>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u590d\u65e6\u5927\u5b66\u8f66\u4ec1\u8d85\u6559\u6388<\/strong>\u3001\u9752\u5c9b\u5927\u5b66\u6797\u6625\u5bcc\u6559\u6388\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005<\/strong>\uff09\u901a\u8fc7\u5bf9Li3<\/sub>VO4<\/sub>\u6750\u6599\u8fdb\u884cCr3+<\/sup>\u2013Si4+<\/sup>\u5171\u63ba\u6742\u6539\u6027\uff0c\u5e76\u63a2\u7a76\u4e86\u5bfc\u7535\u03b3\u76f8Li3.08<\/sub>Cr0.02<\/sub>Si0.09<\/sub>V0.9<\/sub>O4<\/sub>\u65b0\u578b\u8d1f\u6781\u6750\u6599(\u03b3-LCSVO)\u7684\u50a8\u9502\u6027\u80fd\u3002\u5e26\u67093d\u6e38\u79bb\u7535\u5b50\u7684Cr3+<\/sup>\u53ef\u4ee5\u6709\u6548\u63d0\u9ad8\u7535\u5b50\u7535\u5bfc\u7387\u548c\u500d\u7387\u6027\u80fd\u3002\u5206\u522b\u901a\u8fc7\u9759\u7535\u7eba\u4e1d\u548c\u56fa\u76f8\u53cd\u5e94\u5236\u5907\u7684\u4e24\u79cd\u5f62\u6001\u5404\u5f02\u7684\u03b3-LCSVO\u6750\u6599\uff0c\u5373\u03b3-LCSVO\u7eb3\u7c73\u7ebf(\u03b3-LCSVO-NW)\u548c\u5fae\u7c73\u7ea7\u9897\u7c92(\u03b3-LCSVO-MP)\uff0c\u5747\u8868\u73b0\u51fa\u4f18\u5f02\u7684\u7535\u5316\u5b66\u6027\u80fd\u3002\u5229\u7528\u539f\u4f4d\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c\u5b9e\u65f6\u89c2\u6d4b\u4e86\u6750\u6599\u5728\u9502\u79bb\u5b50\u5d4c\u5165\/\u8131\u5d4c\u8fc7\u7a0b\u4e2d\u76f8\u7ed3\u6784\u53ca\u5f62\u8c8c\u7684\u6f14\u53d8\uff0c\u91c7\u7528\u51e0\u4f55\u76f8\u4f4d\u5206\u6790\u5bf9\u4e8e\u9502\u79bb\u5b50\u5d4c\u5165\/\u8131\u5d4c\u8fc7\u7a0b\u4e2d\u5e94\u529b\u5206\u5e03\u7684\u53d8\u5316\u8fdb\u884c\u4e86\u51c6\u786e\u7684\u6d4b\u91cf\u3002\u7ed3\u5408\u539f\u4f4dX\u5c04\u7ebf\u884d\u5c04\uff0c\u5bc6\u5ea6\u6cdb\u51fd\u7406\u8bba\u8ba1\u7b97\u548c\u7403\u5dee\u7535\u955c\u63ed\u793a\u4e86\u03b3-LCSVO\u7684\u50a8\u9502\u673a\u7406\u53ca\u5176\u201c\u96f6\u5e94\u53d8\u201d\u7279\u6027\u3002Li+<\/sup>\u4f9d\u6b21\u5d4c\u5165\u03b3-LCSVO\u76844c(1)\u548c8d\u4f4d\uff0c\u5176\u6700\u5927\u4f53\u79ef\u53d8\u5316\u548c\u5e73\u5747\u5e94\u53d8\u5206\u522b\u4ec5\u4e3a0.18\uff05\u548c0.07\uff05\uff0c\u8fd9\u8bc1\u5b9e\u03b3-LCSVO\u7684\u201c\u96f6\u5e94\u53d8\u201d\u7279\u6027\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u201cConductive Li3.08<\/sub>Cr0.02<\/sub>Si0.09<\/sub>V0.9<\/sub>O4<\/sub> Anode Material: Novel \u201cZero-Strain\u201d Characteristic and Superior Electrochemical Li+<\/sup> Storage<\/strong>\u201d\u4e3a\u9898\u53d1\u8868\u5728Advanced Energy Materials<\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00<\/strong> \u03b3<\/strong>-LCSVO<\/strong>\u7684\u7ed3\u6784\u548c\u5f62\u8c8c\u8868\u5f81\u3002\"\"<\/strong><\/p>\n

\uff08a\uff09\u03b3-LCSVO-NW\u7684XRD\u56fe\u8c31\u3002<\/p>\n

\uff08b\uff09\u03b3-LCSVO\u7684\u6676\u4f53\u7ed3\u6784\u793a\u610f\u56fe\u3002<\/p>\n

\uff08c\uff09\u03b3-LCSVO-MP\u7684FESEM\u56fe\u50cf\u3002<\/p>\n

\uff08d\uff0ce\uff09FESEM\u56fe\u50cf\uff0c<\/p>\n

\uff08f-j\uff09TEM\u56fe\u50cf\uff0cg\uff09HRTEM\u56fe\u50cf\uff0ch\uff09SAED\uff0ci\uff09N2<\/sub>\u5438\u9644-\u89e3\u5438\u7b49\u6e29\u7ebf\uff0cj\uff09\u03b3–LCSVO-NW\u7684EDX\u5143\u7d20\u6620\u5c04\u3002<\/p>\n

\u00a0<\/strong>\u56fe\u4e8c<\/strong>\u03b3<\/strong>-LCSVO<\/strong>\u7684\u7535\u5316\u5b66\u6027\u80fd\u8868\u5f81<\/strong>\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff0cb\uff09\u03b3-LCSVO-NW\u548c\u03b3-LCSVO-MP\u7684CV\u66f2\u7ebf\u3002<\/p>\n

\uff08c-e\uff09\u03b3-LCSVO-NW\u548c\u03b3-LCSVO-MP\u7684\u500d\u7387\u6027\u80fd\u53ca\u5bf9\u5e94\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

\uff08f\uff09\u03b3-LCSVO-NW\u548c\u03b3-LCSVO-MP\u7684\u957f\u5faa\u73af\u6027\u80fd\u3002<\/p>\n

\uff08g-h\uff09\u03b3-LCSVO-MP\u7684GITT\u6d4b\u8bd5\u7684\u5145\u653e\u7535\u66f2\u7ebf\u548cDLi<\/sub>\u7684\u53d8\u5316\u60c5\u51b5<\/p>\n

\u00a0<\/strong>\u56fe\u4e09<\/strong>\u03b3<\/strong>-LCSVO<\/strong>\u7684\u52a8\u529b\u5b66\u5206\u6790<\/strong>\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff0cc\uff0ce\uff09\u03b3-LCSVO-MP\u5728\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u7684CV\u66f2\u7ebf\u4ee5\u53ca\u76f8\u5e94\u7684\u8d5d\u7535\u5bb9\u8d21\u732e\u3002<\/p>\n

\uff08b\uff0cd\uff0cf\uff09\u03b3-LCSVO-NW\u5728\u4e0d\u540c\u626b\u63cf\u901f\u7387\u4e0b\u7684CV\u66f2\u7ebf\u4ee5\u53ca\u76f8\u5e94\u7684\u8d5d\u7535\u5bb9\u8d21\u732e\u3002<\/p>\n

\u00a0<\/strong>\u56fe\u56db<\/strong>LiFePO4<\/sub>\/<\/strong>\u03b3<\/strong>-LCSVO-NW<\/strong>\u5168\u7535\u6c60\u7684\u7535\u5316\u5b66\u6027\u80fd<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09LiFePO4<\/sub>\/\u03b3-LCSVO-NW\u5168\u7535\u6c60\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\uff08b\uff09LiFePO4<\/sub>\u548c\u03b3-LCSVO-NW\u5404\u81ea\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

\uff08c\uff0cd\uff09LiFePO4<\/sub>\/\u03b3-LCSVO-NW\u5168\u7535\u6c60\u7684\u500d\u7387\u6027\u80fd\u53ca\u76f8\u5e94\u7684\u5145\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

\uff08e\uff09LiFePO4<\/sub>\/\u03b3-LCSVO-NW\u5168\u7535\u6c60\u7684\u957f\u5faa\u73af\u6027\u80fd\u3002<\/p>\n

\uff08f\uff09\u4e0eLiFePO4<\/sub>\/Li4Ti5<\/sub>O12<\/sub>\u7684\u7535\u5316\u5b66\u6027\u80fd\u6bd4\u8f83\u3002<\/p>\n

\u00a0\u56fe\u4e94\u00a0\u96f6\u5e94\u53d8\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a-c\uff09\u539f\u59cb\u548c\u4e8c\u7ef4\u7684\u539f\u4f4dXRD\u56fe\u8c31\uff0c\u4ee5\u53cac\uff09\u03b3-LCSVO-MP\u7684\u5355\u4f4d\u6676\u80de\u4f53\u79ef\u53d8\u5316\u60c5\u51b5\u3002<\/p>\n

\uff08d\uff09\u03b3-LCSVO-MP\u4e0e\u5176\u4ed6\u8131\u5d4c\u578b\u7535\u6781\u6750\u6599\u6676\u80de\u4f53\u79ef\u53d8\u5316\u7684\u5bf9\u6bd4\u3002<\/p>\n

\uff08e\uff0932.3\u00b0-32.6\u00b0\u8303\u56f4\u5185\u7684\u539f\u4f4dXRD\u56fe\u8c31\u4ee5\u53ca\uff08220\uff09\u6676\u9762\u7684\u793a\u610f\u56fe\u3002\u3002<\/p>\n

\uff08f\uff09\u572834.9\u00b0\u81f335.1\u00b0\u8303\u56f4\u5185\u7684\u539f\u4f4dXRD\u56fe\u8c31\u4ee5\u53ca\uff08002\uff09\u6676\u9762\u7684\u793a\u610f\u56fe\u3002\u3002<\/p>\n

\u00a0<\/strong>\u56fe\u516d<\/strong> \u5d4c\u9502\u8fc7\u7a0b\u4e2d<\/strong>\u03b3-LCSVO<\/strong>\u7684\u539f\u4f4d<\/strong>TEM<\/strong>\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09\u7528\u4e8e\u539f\u4f4dTEM\u5b9e\u9a8c\u7684\u5fae\u7c73\u7ea7\u56fa\u6001\u5168\u7535\u6c60\u7684SEM\u56fe\u50cf<\/p>\n

\uff08b\uff09\u56fa\u6001\u5168\u7535\u6c60\u4e2d\u03b3-LCSVO\u7684TEM\u56fe\u50cf\u3002<\/p>\n

\uff08c\uff09\u5d4c\u9502\u8fc7\u7a0b\u4e2d\u03b3-LCSVO\u4e2d\u7684\u5ef6\u65f6TEM\u56fe\u50cf\u3002<\/p>\n

\uff08d\uff09\u539f\u59cb\u7684\u03b3-LCSVO\u548ce\uff09\u9502\u5316\u7684\u03b3-LCSVO\u7684SAED\u5bf9\u6bd4\u3002<\/p>\n

\uff08f\uff09\u539f\u59cb\u548c\u9502\u5316\u7684\u03b3-LCSVO\u7684V L-edge\u8c31\u56fe and O K-\u8c31\u56fe\u3002<\/p>\n

\u00a0<\/strong>\u56fe\u4e03\u539f\u4f4d\u56fa\u6001\u5168\u7535\u6c60\u4e2d<\/strong>\u03b3-LCSVO<\/strong>\u7684<\/strong>HRTEM<\/strong>\u548c<\/strong>GPA<\/strong>\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\u00a0<\/strong>\u56fe\u516b<\/strong>\u03b3-LCSVO<\/strong>\u7684\u50a8\u9502\u673a\u5236\u3002<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff0cb\uff09\u03b3-LCSVO\u5d4c\u9502\u540e\u7684HAADF STEM\u56fe\u50cf\uff0cb\uff09\u6cbfABF-STEM\u65b9\u5411\u89c2\u5bdf\u3002<\/p>\n

\uff08c\uff09\u653e\u5927\u7684ABF-STEM\u5f69\u8272\u56fe\u50cf\u3002<\/p>\n

\uff08d\uff09\u5bf9\u5e94\u4e8eHAADF-STEM\u56fe\u50cf\u548cABF-STEM\u56fe\u50cf\u7684\u6676\u4f53\u7ed3\u6784\u6a21\u578b\u3002<\/p>\n

\u00a0<\/strong>\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u00a0<\/strong>\u6587\u732e\u94fe\u63a5\uff1a\u201c<\/strong>Conductive Li3.08<\/sub>Cr0.02<\/sub>Si0.09<\/sub>V0.9<\/sub>O4<\/sub> Anode Material: Novel \u201cZero-Strain\u201d Characteristic and Superior Electrochemical Li+<\/sup> Storage<\/strong><\/a>\u201d<\/strong>(DOI: 10.1002\/aenm.201904267)<\/strong><\/p>\n

\u672c\u6587\u7531\u5fae\u89c2\u4e16\u754c\u7f16\u8bd1\u4f9b\u7a3f\u3002<\/p>\n

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