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nm\u3002\u7279\u522b\u662f\uff0c\u5b83\u53ef\u4ee5\u4ece3D-GE\u7eb3\u7c73\u7247\u7684\u9ad8\u500d\u653e\u5927\u56fe\u50cf\u7f20\u7ed5\u5728\u8fb9\u7f18\u7ed3\u6784\u4e0a\uff0c\u5176\u539a\u5ea6\u5c0f\u4e8e10 nm\u3002\u6b64\u5916\uff0c\u4e0e3D-GE\u76f8\u6bd4\uff0c3D-AGE\u62e5\u6709\u66f4\u591a\u7684\u5c55\u5f00\u7eb3\u7c73\u7247\uff0c\u8fd9\u53ef\u80fd\u5f52\u56e0\u4e8e\u4e24\u8005\u7684\u7ed3\u5408\u5316\u5b66\u6d3b\u5316\u548c\u4e8c\u6b21\u52a0\u70ed\u8fc7\u7a0b\u7684\u4f5c\u7528\u3002<strong>\u603b\u4f53\u800c\u8a00\uff0c3D\u6d3b\u6027\u77f3\u58a8\u70ef\u4ea7\u54c1\u5df2\u7ecf\u83b7\u5f97\u6210\u529f\u901a\u8fc7\u50ac\u5316\u751f\u957f\u548c\u4e24\u6b65\u5316\u5b66\u6d3b\u5316\u5236\u5907\u8def\u7ebf\u3002<\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-192865\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/2-40.jpg\" alt=\"\" width=\"1098\" height=\"1283\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/2-40.jpg 1098w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/2-40-257x300.jpg 257w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/2-40-768x897.jpg 768w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/2-40-876x1024.jpg 876w\" sizes=\"(max-width: 1098px) 100vw, 1098px\" \/><\/p>\n<p style=\"text-align: center;\">\u626b\u63cf\u7535\u955c\u5206\u6790<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-192866\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/3-40.jpg\" alt=\"\" width=\"1016\" height=\"1016\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/3-40.jpg 1016w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/3-40-150x150.jpg 150w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/3-40-300x300.jpg 300w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/3-40-768x768.jpg 768w\" sizes=\"(max-width: 1016px) 100vw, 1016px\" \/><\/p>\n<p style=\"text-align: center;\">\u4e0d\u540c\u653e\u5927\u500d\u6570\u4e0b\u7684\u4e09\u7ef4\u6837\u54c1TEM\u56fe\u50cf<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-192867\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/4-40.jpg\" alt=\"\" width=\"1016\" height=\"367\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/4-40.jpg 1016w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/4-40-300x108.jpg 300w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/4-40-768x277.jpg 768w\" sizes=\"(max-width: 1016px) 100vw, 1016px\" \/><\/p>\n<p style=\"text-align: center;\">N<sub>2<\/sub> adsorption-desorption\u5206\u6790<\/p>\n<p>\u00a0 XPS\u5206\u6790\u4ee5\u83b7\u5f97\u66f4\u591a\u5173\u4e8e\u8fdb\u4e00\u6b65\u6267\u884c3D-AGE\u7684\u5316\u5b66\u6210\u4efd\uff0cXPS\u5206\u6790\u5e76\u5f97\u51fa\u7ed3\u679c\u6240\u793a\u3002\u4e09\u7ef4\u5e74\u9f84\u7684XPS\u8c31(\u8c03\u67e5\u626b\u63cf)\u6837\u54c1\u5448\u73b0\u4e86c1s\u3001o1s\u3001s2p\u548cNi\u7684\u7279\u5f81\u5149\u8c312p\uff0c\u5176\u4e2dC\u3001O\u3001S\u3001Ni\u5143\u7d20\u7684\u539f\u5b50\u6bd4\u5206\u522b\u4e3a91.59%\u30017.76%\u30010.41%\u548c0.24%\u3002\u8fd9\u4e9bC\u3001O\u3001S\u5143\u7d20\u6765\u6e90\u4e8e\u786b\u8132\u6811\u8102\u70ed\u89e3\u8fc7\u7a0b\u4e2d\u7684\u78b3\u3001\u6c27\u548c\u542b\u786b\u6c14\u4f53\u3002Ni\u542b\u91cf\u4ec5\u4e3a0.24%\uff0c\u53ef\u4ee5\u786e\u5b9a\u4e3aNi\u5143\u7d20\u7ecf\u76d0\u9178\u6cbb\u7597\u540e\u5df2\u57fa\u672c\u6e05\u9664\u3002O\u7684\u542b\u91cf\u4e0a\u5347\u4e86\u52307.76%\uff0c\u8fd9\u8bf4\u660e3d\u5e74\u9f84\u7684\u6837\u672c\u91cf\u5f88\u5927oxygen-doped\u78b3\u6750\u6599\u3002\u5982\u6240\u793a-COOH\u5728290eV,C=O\u5728287eV,C-OH\u5728285eV,C-C\u5728284.5eV\uff0c\u8868\u660e\u77f3\u58a8\u70ef\u8868\u9762\u5f62\u6210\u4e86\u4e30\u5bcc\u7684\u542b\u6c27\u5b98\u80fd\u56e2\u3002\u4ece\u53ef\u4ee5\u770b\u51fa\uff0c\u5728531eV\u5904\u662fC=O\uff0c\u5728531eV\u5904\u662fC-OH533eV\u548c536eV\u7684-COOH\uff0c\u8fdb\u4e00\u6b65\u8bc1\u5b9e\u4e86\u4e09\u7ef4\u6837\u54c1\u4e2d\u542b\u6c27\u5b98\u80fd\u56e2\u7684\u5b58\u5728\u3002<strong>\u4ee5\u524d\u7684\u7814\u7a76\u8868\u660e\u8fd9\u4e9b\u542b\u6c27\u7269\u8d28\u5b98\u80fd\u56e2\u4e0d\u4ec5\u63d0\u9ad8\u4e86\u77f3\u58a8\u70ef\u7684\u4eb2\u6c34\u6027\uff0c\u4ece\u800c\u63d0\u9ad8\u4e86\u7535\u89e3\u8d28\u4e2d\u79bb\u5b50\u7684\u6d41\u52a8\u6027\uff0c\u8fd8\u63d0\u4f9b\u4e86\u6cd5\u62c9\u7b2c\u4f2a\u7535\u5bb9\uff0c\u589e\u52a0\u4e86\u77f3\u58a8\u70ef\u7684\u6bd4\u7535\u5bb9<\/strong>\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-192868\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/5-33.jpg\" alt=\"\" width=\"1016\" height=\"773\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/5-33.jpg 1016w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/5-33-300x228.jpg 300w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/5-33-768x584.jpg 768w\" sizes=\"(max-width: 1016px) 100vw, 1016px\" \/><\/p>\n<p style=\"text-align: center;\">XPS\u5206\u6790<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter size-full wp-image-192869\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/6-20.jpg\" alt=\"\" width=\"1016\" height=\"395\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/6-20.jpg 1016w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/6-20-300x117.jpg 300w, \/\/m.iemloyee.com\/wp-content\/uploads\/2019\/12\/6-20-768x299.jpg 768w\" sizes=\"(max-width: 1016px) 100vw, 1016px\" \/><\/p>\n<p style=\"text-align: center;\">\u5faa\u73af\u4f0f\u5b89\u6cd5(CV)\u548c\u5145\u653e\u7535(CDC)\u5206\u6790<\/p>\n<p><strong>\u7ed3\u8bba<\/strong><\/p>\n<p>\u6d3b\u5316\u76843-D\u77f3\u58a8\u70ef\u7c89\u672b\u6750\u6599\u5df2\u7ecf\u5f97\u5230\u4e86\u5e94\u7528\u901a\u8fc7\u91d1\u5c5e\u786b\u5316\u7269\u50ac\u5316\u751f\u957f\u548cKOH\u5316\u5b66\u5408\u6210\u7535\u5316\u5b66\u50a8\u80fd\u7684\u6d3b\u5316\u5728\u8d85\u7ea7\u7535\u5bb9\u5668\u3002\u7531\u4e8e\u5176\u4f18\u79c0\u76843D\u7f51\u7edc\u67b6\u6784\uff0c\u5927\u7684\u8868\u9762\u79ef(1687.8m<sup>2<\/sup>g<sup>-1)<\/sup>\u548c\u9ad8\u6c34\u5e73\u7684O\u6742\u539f\u5b50\u63ba\u6742(7.76%)\uff0c\u5f97\u52303-D\u6d3b\u5316\u77f3\u58a8\u70ef\u6837\u54c1\u8868\u73b0\u51fa\u9ad8\u7684\u6bd4\u7535\u5bb9(285.2Fg<sup>-1<\/sup>~1Ag<sup>-1<\/sup>),\u4f18\u5f02\u7684\u7535\u5316\u5b66\u7a33\u5b9a\u6027(\u968f\u77402000\u5e74\u540e\u768421%)\u3002\u6709\u4eba\u5efa\u8bae\u672c\u8bfe\u9898\u7684\u7814\u7a76\u4e3a\u4eca\u540e\u7684\u7814\u7a76\u63d0\u4f9b\u4e86\u4e00\u6761\u53ef\u884c\u7684\u9014\u5f84\u9ad8\u6027\u80fd\u6d3b\u5316\u4e09\u7ef4\u77f3\u58a8\u70ef\u7c89\u672b\u6750\u6599\u7535\u5316\u5b66\u50a8\u80fd\u7684\u6f5c\u5728\u5de5\u4e1a\u5e94\u7528\u3002<\/p>\n<p>\u8bba\u6587\u5730\u5740\uff1ahttps:\/\/doi.org\/10.1016\/j.electacta.2019.134878<\/p>\n<p>\u672c\u6587\u7531\u674e\u6cfd\u80dc\u8bfe\u9898\u7ec4\u4f9b\u7a3f\u3002<\/p>\n<p>\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1\uff1a<a href=\"mailto:tougao@cailiaoren.com\">tougao@cailiaoren.com<\/a><\/p>\n<p>\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1acailiaorenvip<\/p>\n","protected":false},"excerpt":{"rendered":"<p>\u6458\u8981 \u6d3b\u5316\u7684\u4e09\u7ef4\u77f3\u58a8\u70ef(3D-AGE)\u7c89\u672b\u5177\u6709\u8f83\u9ad8\u7684\u6bd4\u8868\u9762\u79ef\u91c7\u7528\u50ac\u5316\u751f\u957f\u548c\u5316\u5b66\u6d3b\u5316\u76f8\u7ed3\u5408\u7684\u65b9\u6cd5\u6210\u529f\u5730\u5236\u5907\u4e86\u8be5\u50ac\u5316\u5242\u5728\u8d85\u7ea7\u7535\u5bb9\u5668\u3002\u7528\u626b\u63cf\u6cd5\u5bf9\u5176\u5f62\u8c8c\u3001\u7ed3\u6784\u548c\u7ec4\u6210\u8fdb\u884c&#8230;<\/p>\n","protected":false},"author":2,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[215],"tags":[],"class_list":["post-192863","post","type-post","status-publish","format-standard","hentry","category-jiedu"],"_links":{"self":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/192863"}],"collection":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/users\/2"}],"replies":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=192863"}],"version-history":[{"count":3,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/192863\/revisions"}],"predecessor-version":[{"id":192947,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/192863\/revisions\/192947"}],"wp:attachment":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=192863"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=192863"},{"taxonomy":"post_tag","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=192863"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}