{"id":192319,"date":"2019-12-26T06:57:01","date_gmt":"2019-12-25T22:57:01","guid":{"rendered":"\/\/m.iemloyee.com\/?p=192319"},"modified":"2019-12-25T21:58:45","modified_gmt":"2019-12-25T13:58:45","slug":"angew-chem-int-ed-%e7%b4%ab%e7%a3%b7%e6%99%b6%e4%bd%93%e5%8f%8a%e7%b4%ab%e7%a3%b7%e7%83%af%e7%9a%84%e5%90%88%e6%88%90%e4%b8%8e%e8%a1%a8%e5%be%81","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=192319","title":{"rendered":"Angew. Chem. Int. Ed. : \u7d2b\u78f7\u6676\u4f53\u53ca\u7d2b\u78f7\u70ef\u7684\u5408\u6210\u4e0e\u8868\u5f81"},"content":{"rendered":"
\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n \u9ed1\u78f7\u70ef\u4f5c\u4e3a\u4e00\u79cd\u534a\u5bfc\u4f53\u4e8c\u7ef4\u6750\u6599\u5907\u53d7\u5173\u6ce8\u3002\u7d2b\u78f7\u662f\u53e6\u4e00\u79cd\u5c42\u72b6\u78f7\u540c\u7d20\u5f02\u5f62\u4f53\uff0c\u5b83\u5177\u6709\u72ec\u7279\u7684\u7535\u5b50\u548c\u5149\u7535\u7279\u6027\u3002\u8ba1\u7b97\u7814\u7a76\u8868\u660e\u7d2b\u78f7\u53ef\u80fd\u662f\u78f7\u5143\u7d20\u57fa\u6001\u7684\u4e00\u79cd\u3002\u7136\u800c\uff0c\u81ea1865\u5e74Hittorf\u4ece\u7194\u878d\u94c5\u4e2d\u53d1\u73b0\u7d2b\u78f7\u5e76\u4e8e1969\u5e74\u7531Thurn\u548cKrebs\u8fdb\u884c\u7ed3\u6784\u8868\u5f81\u4ee5\u6765\uff0c\u5173\u4e8e\u7d2b\u78f7\u7684\u5b9e\u9a8c\u6570\u636e\u975e\u5e38\u6709\u9650\u3002\u53ea\u6709\u7d2b\u78f7\u7684\u9ad8\u5206\u8fa8\u7387\u900f\u5c04\u7535\u955c\uff08HRTEM\uff09\u56fe\u50cf\u88ab\u7528\u4f5c\u53d1\u73b0\u7ea4\u7ef4\u7ea2\u78f7\u7684\u6bd4\u8f83\u3002\u7136\u800c\uff0c\u7d2b\u78f7\u7684\u6676\u4f53\u6570\u636e\u5e76\u6ca1\u6709\u62a5\u9053\u3002\u8fd1\u5e74\u6765\uff0c\u6709\u62a5\u9053\u7528\u7b49\u79bb\u5b50\u4f53\u8f85\u52a9\u5408\u6210\u65b9\u6cd5\u5728InP\u886c\u5e95\u4e0a\u5236\u5907\u4e86\u539f\u5b50\u5c42\u72b6\u7d2b\u78f7\uff0c\u4f46\u5bf9\u5176\u7ed3\u6784\u7684\u8868\u5f81\u4ec5\u57fa\u4e8eHRTEM\u3001\u9009\u533a\u884d\u5c04\uff08SAED\uff09\u548c\u62c9\u66fc\u6563\u5c04\u3002\u76ee\u524d\u8fd8\u6ca1\u6709\u4ee4\u4eba\u4fe1\u670d\u7684\u5b9e\u9a8c\u6570\u636e\u6765\u8868\u5f81\u7d2b\u78f7\u3002\u7d2b\u78f7\u662f\u4e00\u79cd\u7a33\u5b9a\u7684\u540c\u7d20\u5f02\u5f62\u4f53\u8fd8\u662f\u7ea2\u78f7\u5230\u9ed1\u78f7\u7684\u4e9a\u7a33\u4e2d\u95f4\u4ea7\u7269\uff0c\u81f3\u4eca\u4ecd\u7136\u662f\u4e2a\u8ff7\u3002\u6b64\u5916\uff0c\u7d2b\u78f7\u70ef\u4e5f\u662f\u4e00\u79cd\u5f88\u6709\u524d\u9014\u7684\u4e8c\u7ef4\u6750\u6599\uff0c\u7531\u4e8e\u5176\u4f53\u7ed3\u6784\u7684\u4e0d\u786e\u5b9a\u6027\uff0c\u4eba\u4eec\u5bf9\u5176\u8fd8\u672a\u8fdb\u884c\u8fc7\u63a2\u7d22\u3002\u603b\u4e4b\uff0c\u5757\u72b6\u548c\u5c42\u72b6\u7d2b\u78f7\u7684\u7ed3\u6784\u548c\u6027\u8d28\u5c1a\u4e0d\u6e05\u695a\uff0c\u8fd9\u963b\u788d\u4e86\u7d2b\u78f7\u53ca\u7d2b\u78f7\u70ef\u7684\u8fdb\u4e00\u6b65\u5e94\u7528\u3002<\/p>\n \u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n \u8fd1\u65e5\uff0c\u897f\u5b89\u4ea4\u901a\u5927\u5b66\u5f20\u9526\u82f1\u8bfe\u9898\u7ec4\u6210\u529f\u5408\u6210\u4e86\u5b8f\u89c2\u5c3a\u5bf8\u7d2b\u78f7\u5355\u6676\u5e76\u5265\u79bb\u51fa\u7d2b\u78f7\u70ef\uff0c\u9996\u6b21\u7cbe\u786e\u63a5\u89e6\u7d2b\u78f7\u7684\u6676\u4f53\u7ed3\u6784\uff0c\u5e76\u8be6\u7ec6\u7684\u7814\u7a76\u4e86\u5176\u6027\u8d28\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u53d1\u8868\u5728\u56fd\u9645\u8457\u540d\u671f\u520aAngew. Chem. Int. Ed.\u4e0a\uff0c\u9898\u76ee\u4e3a\u201cStructure and Properties of Violet Phosphorus and Its Phosphorene Exfoliation\u201d<\/p>\n \u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/strong><\/p>\n \u56fe<\/strong>1<\/strong><\/p>\n \uff08a\uff09\u7d2b\u78f7\u7684\u4e0d\u5bf9\u79f0\u5355\u5143\uff1b<\/p>\n \uff08b\uff09\u7d2b\u78f7\u7684\u5c42\u72b6\u7ed3\u6784\uff1b<\/p>\n \uff08c\uff09\u7d2b\u78f7\u5355\u6676\u7684\u5149\u5b66\u56fe\u50cf\uff1b<\/p>\n \uff08d\uff091969\u5e74\u62a5\u9053\u548c\uff08e\uff09\u8be5\u5de5\u4f5c\u5408\u6210\u7684\u7d2b\u78f7\u5728\u5e03\u91cc\u6e0a\u533a\u7684\u58f0\u5b50\u8c31\u3002<\/p>\n \u56fe<\/strong>2<\/strong><\/p>\n \uff08a\uff09\u7d2b\u78f7\u6676\u4f53\u5757\u548c\uff08b\uff09\u673a\u68b0\u7834\u788e\u540e\u7d2b\u78f7\u7684SEM\u56fe\u50cf\uff1b<\/p>\n \uff08c\uff09\u7d2b\u78f7\u6676\u4f53\u7684EDS\u5149\u8c31\uff08\u63d2\u56fe\u4e3a\u653e\u5927\u8c31\u56fe\uff0c\u9ec4\u8272\u7bad\u5934\u663e\u793aI\u7684\u4f4d\u7f6e\uff0c\u84dd\u8272\u7bad\u5934\u8868\u793aSn\u7684\u4f4d\u7f6e\uff09\uff1b<\/p>\n \uff08d\uff09\u7d2b\u78f7\u5355\u6676\u7684\u62c9\u66fc\u5149\u8c31\uff08\u6fc0\u53d1\u6ce2\u957f\u4e3a633 nm\uff09\uff1b<\/p>\n \uff08e\uff09\u7814\u78e8\u540e\u7d2b\u78f7\u788e\u6676\u7684XRD\u56fe\u3002<\/p>\n \u56fe<\/strong>3<\/strong><\/p>\n \uff08a\uff09\u7d2b\u78f7\u548c\uff08b\uff09\u7d2b\u78f7\u70ef\u7684\u80fd\u5e26\u7ed3\u6784\uff1b<\/p>\n \uff08c\uff09\u7814\u78e8\u540e\u7d2b\u78f7\u788e\u6676\u7684\u6f2b\u53cd\u5c04\u5149\u8c31\uff1b<\/p>\n \uff08d\uff09\u7d2b\u78f7\u548c\u9ed1\u78f7\u7684TGA\u66f2\u7ebf\u3002<\/p>\n \u56fe<\/strong>4<\/strong><\/p>\n \uff08a\uff09\u7d2b\u78f7\u70ef\u7eb3\u7c73\u5e26\u7684SEM\u56fe\u548c\uff1b<\/p>\n \uff08b\uff09\u5265\u79bb\u7d2b\u78f7\u70ef\u7eb3\u7c73\u5e26\u7684TEM\u56fe\uff08\u63d2\u56fe\u4e3a\u5bf9\u5e94EELS\u80fd\u8c31\uff09\uff1b<\/p>\n \uff08c\uff09\u4e3b\u4f53\u78f7\u7eb3\u7c73\u5e26\u7684CS-\u77eb\u6b63HRTEM\u56fe\uff1b<\/p>\n \uff08d\uff09[001]\u6676\u5e26\u8f74\u65b9\u5411\u76f8\u5e94\u7684\u00a0SAED\u56fe\uff1b<\/p>\n \uff08e\uff09\u78f7\u70ef\u7eb3\u7c73\u5e26\u503e\u659c\u7aefCS-\u77eb\u6b63HRTEM\u56fe\u53ca\u5bf9\u5e94\u6a21\u578b\u56fe\u3002<\/p>\n \u56fe<\/strong>5<\/strong><\/p>\n \uff08a\uff09\u673a\u68b0\u5265\u79bb\u548c\uff08b\uff09\u6db2\u76f8\u5265\u79bb\u83b7\u5f97\u7684\u7d2b\u78f7\u70ef\u7eb3\u7c73\u5e26\u7684AFM\u56fe\uff1b<\/p>\n \uff08c\uff09\u5265\u79bb\u7684\u7d2b\u78f7\u70ef\u7eb3\u7c73\u5e26\u7684\u9ad8\u5ea6\u5206\u5e03\u3002<\/p>\n \u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n \u8be5\u7814\u7a76\u5408\u6210\u5236\u5907\u4e86\u5b8f\u89c2\u5c3a\u5bf8\u7684\u7d2b\u78f7\u5355\u6676\uff0c\u5e76\u5728\u5b9e\u9a8c\u4e0a\u786e\u5b9a\u4e86\u7d2b\u78f7\u7684\u6676\u4f53\u7ed3\u6784\u4e3a\u5355\u659cP2\/n\uff08a=9.210, b=9.128, c=21.893 \u00c5, \u03b2=97.776\u00b0\uff09\uff0c\u540c\u65f6\u901a\u8fc7\u58f0\u5b50\u8c31\u8ba1\u7b97\u53d1\u73b01969\u5e74\u63d0\u51fa\u7d2b\u78f7\u7ed3\u6784\u7684\u4e0d\u5408\u7406\u6027\uff0c\u800c\u8be5\u5de5\u4f5c\u6240\u83b7\u5f97\u7684\u6676\u683c\u7ed3\u6784\u5df2\u786e\u8ba4\u662f\u53ef\u9760\u4e14\u7a33\u5b9a\u7684\u3002\u6d4b\u8bd5\u4e86\u7d2b\u78f7\u7684\u5149\u5b66\u5e26\u9699\u7ea6\u4e3a1.7 eV\uff0c\u7565\u9ad8\u4e8e\u8ba1\u7b97\u7684\u80fd\u5e26\u3002\u7d2b\u78f7\u5728\u6c29\u6c14\u6c1b\u56f4\u4e2d\u7684\u70ed\u89e3\u6e29\u5ea6\u8fbe\u5230512\u2103\u4ee5\u4e0a\uff0c\u6bd4\u9ed1\u78f7\u9ad8\u51fa52\u2103\uff0c\u8fd9\u8868\u660e\u7d2b\u78f7\u662f\u6700\u7a33\u5b9a\u7684\u78f7\u540c\u7d20\u5f02\u5f62\u4f53\u3002\u6b64\u5916\uff0c\u901a\u8fc7\u673a\u68b0\u5265\u79bb\u548c\u6eb6\u6db2\u5265\u79bb\u4e24\u79cd\u65b9\u6cd5\u90fd\u53ef\u4ee5\u5f88\u5bb9\u6613\u83b7\u5f97\u7d2b\u78f7\u70ef\u3002<\/p>\n
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