{"id":186490,"date":"2019-10-05T06:30:41","date_gmt":"2019-10-04T22:30:41","guid":{"rendered":"\/\/m.iemloyee.com\/?p=186490"},"modified":"2019-10-04T17:25:05","modified_gmt":"2019-10-04T09:25:05","slug":"%e5%b7%b2%e6%a0%a1%e7%a8%bf%e4%bb%b6-%e8%83%a1%e8%89%af%e5%85%b5%e5%9b%a2%e9%98%9f-afm%e6%8a%a5%e9%81%93-%e9%80%9a%e8%bf%87%e5%bf%ab%e9%80%9f%e3%80%81%e9%ab%98%e6%b8%a93d%e5%be%ae%e6%b3%a2%e5%8a%a0","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=186490","title":{"rendered":"\u80e1\u826f\u5175\u56e2\u961f AFM\u62a5\u9053: \u901a\u8fc7\u5feb\u901f\u3001\u9ad8\u6e293D\u5fae\u6ce2\u52a0\u70ed\u5408\u6210\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u7c92\u5b50"},"content":{"rendered":"

\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u4f17\u6240\u5468\u77e5\uff0c\u78b3\u8d1f\u8f7d\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u88ab\u5e7f\u6cdb\u7528\u4e8e\u6c34\u5904\u7406\u3001\u5149\u4f0f\u7535\u6c60\u548c\u8d85\u7ea7\u7535\u5bb9\u5668\u7b49\u9886\u57df\u3002\u5176\u4e2d\uff0c\u78b3\u57fa\u5e95\u4e0d\u4ec5\u5145\u5f53\u5bfc\u7535\u4e3b\u4f53\uff0c\u800c\u4e14\u53ef\u4ee5\u9632\u6b62\u7eb3\u7c73\u9897\u7c92\u805a\u96c6\u4ee5\u4f18\u5316\u5176\u529f\u80fd\u3002\u901a\u5e38\u4f7f\u7528\u9ad8\u6e29\u5904\u7406\u6765\u5408\u6210\u88c5\u9970\u5728\u78b3\u4e0a\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u7c92\u5b50\u3002\u4f46\u5728\u4f20\u7edf\u7684\u52a0\u70ed\u6280\u672f\u4e2d\uff0c\u4ece\u57fa\u677f\u7684\u8868\u9762\u5230\u5185\u90e8\u5b58\u5728\u6e29\u5ea6\u68af\u5ea6\u3001\u4ee5\u53ca\u70ed\u91cf\u7684\u4f20\u5bfc\u3001\u8f90\u5c04\u548c\u5bf9\u6d41\u4f20\u9012\uff0c\u5bfc\u81f4\u5236\u5907\u7684\u7eb3\u7c73\u9897\u7c92\u4e0d\u5747\u5300\u4e14\u8017\u65f6\u957f\u3002\u5c3d\u7ba1\u6fc0\u5149\u52a0\u70ed\u5728\u5185\u7684\u975e\u4f20\u7edf\u52a0\u70ed\u6280\u672f\u4e3a\u7eb3\u7c73\u9897\u7c92\u7684\u5408\u6210\u63d0\u4f9b\u4e86\u5feb\u901f\u800c\u5c40\u90e8\u7684\u52a0\u70ed\uff0c\u4f46\u662f\u53ea\u80fd\u52a0\u70ed\u6837\u54c1\u8868\u9762\u7684\u8584\u5c42\u5e76\u4e14\u5f88\u96be\u63a7\u5236\u3002\u73b0\u4eca\uff0c\u5fae\u6ce2\u52a0\u70ed\u88ab\u5e7f\u6cdb\u7528\u4e8e\u529f\u80fd\u6750\u6599\u7684\u5408\u6210\u548c\u52a0\u5de5\u4e2d\uff0c\u5176\u6781\u5927\u7684\u51cf\u5c11\u4e86\u53cd\u5e94\u65f6\u95f4\u548c\u63d0\u9ad8\u4e86\u52a0\u70ed\u6548\u7387\u3002\u7136\u800c\uff0c\u5728\u9ad8\u8d28\u91cf\u7684\u77f3\u58a8\u70ef\u3001\u9676\u74f7\u7535\u89e3\u8d28\u7b49\u5927\u591a\u6570\u7814\u7a76\u4e2d\uff0c\u5176\u5408\u6210\u6e29\u5ea6\u88ab\u9650\u5236\u57281100 k\u4ee5\u4e0b\uff0c\u6781\u5927\u7684\u9650\u5236\u4e86\u5fae\u6ce2\u52a0\u70ed\u7684\u5e94\u7528\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u7f8e\u56fd\u9a6c\u91cc\u5170\u5927\u5b66\u7684\u80e1\u826f\u5175\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u56e2\u961f\u62a5\u9053\u4e86\u4e00\u79cd\u5229\u7528\u5fae\u6ce2\u4f5c\u4e3a\u52a8\u529b\u7684\u5feb\u901f\u3001\u539f\u7684\u4f4d3D\u52a0\u70ed\u65b9\u6cd5\uff0c\u4ee5\u57283D\u78b3\u5316\u6728\uff08C-\u6728\u6750\uff09\u4e3b\u4f53\u4e0a\u5236\u9020\u5206\u6563\u826f\u597d\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u3002C-\u6728\u6750\u7684\u9002\u5ea6\u7535\u5b50\u5bfc\u7535\u6027\u6709\u52a9\u4e8e\u5c40\u90e8\u7126\u8033\u52a0\u70ed\uff0c\u800c\u826f\u597d\u7684\u5bfc\u70ed\u6027\u53ef\u786e\u4fdd\u6574\u4e2a\u6750\u6599\u7684\u5feb\u901f3D\u52a0\u70ed\u3002C-\u6728\u6750\u7684\u6e29\u5ea6\u53ef\u57284 s\u5185\u4ece\u5ba4\u6e29\u5347\u9ad8\u52302200 K\uff0c\u7a33\u5b9a\u6e29\u5ea6\u4e3a1400 K\uff0c\u4e14\u57282 s\u5185\u53ef\u51b7\u5374\u56de\u5ba4\u6e29\u3002\u6b64\u5916\uff0c\u9884\u52a0\u8f7d\u7684\u524d\u4f53\u76d0\u7531\u4e8e\u9ad8\u6e29\u5728C-\u6728\u6750\u8868\u9762\u4e0a\u8fc5\u901f\u5206\u89e3\u5e76\u5728\u5feb\u901f\u6dec\u706d\u8fc7\u7a0b\u4e2d\u5f62\u6210\u8d85\u7ec6\u91d1\u5c5e\u6c27\u5316\u7269\uff08\u224811 nm\uff09\u7eb3\u7c73\u9897\u7c92\u3002\u8be5\u8fc7\u7a0b\u5728\u7a7a\u6c14\u4e2d\u8fdb\u884c\uff0c\u6709\u52a9\u4e8e\u9632\u6b62\u91d1\u5c5e\u6c27\u5316\u7269\u88abC\u8fd8\u539f\u3002\u603b\u4e4b\uff0c3D\u52a0\u70ed\u65b9\u6cd5\u4e3a\u5feb\u901f\u3001\u53ef\u6269\u5c55\u5730\u5408\u6210\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u63d0\u4f9b\u4e86\u4e00\u79cd\u65b0\u65b9\u6cd5\u3002\u8be5\u7814\u7a76\u6210\u679c\u4ee5\u9898\u4e3a\u201cSynthesis of Metal Oxide Nanoparticles by Rapid, High-Temperature 3D Microwave Heating\u201d<\/strong>\u53d1\u5e03\u5728\u56fd\u9645\u8457\u540d\u671f\u520aAdv. Funct. Mater.<\/strong>\u4e0a\uff08\u7b2c\u4e00\u4f5c\u8005\u4ef2\u803f\u3001\u5f90\u52ad\u61cb\u535a\u58eb\u3001\u9648\u671d\u5409\u535a\u58eb\uff09<\/strong>\u3002<\/p>\n

\u3010\u56fe\u6587\u89e3\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00\u3001C-\u6728\u6750\u7684\u5236\u5907\u8fc7\u7a0b\u548c\u793a\u610f\u56fe<\/strong>
\n \"\"\uff08a\uff09\u5fae\u6ce2\u52a0\u70ed\u88c5\u7f6e\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b\uff09\u52a0\u70ed\u8fc7\u7a0b\u4ee5\u53ca\u4ece\u6750\u6599\u53d1\u51fa\u7684\u5149\u7684\u56fe\u50cf\uff1b<\/p>\n

\uff08c\uff09\u5728\u22481400 K\u4e0b\u8fdb\u884c4 s\u76843D\u70ed\u5904\u7406\uff0c\u5728C-\u6728\u6750\u57fa\u677f\u5185\u5236\u9020\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u7c92\u5b50\u7684\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08d\uff09\u5e73\u5747\u7eb3\u7c73\u9897\u7c92\u5c3a\u5bf8\u4e0e\u52a0\u70ed\u65f6\u95f4\u7684\u5173\u7cfb\uff1b<\/p>\n

\uff08e\uff09\u7535\u5b50\u4f20\u5bfc\u7387\u5bf9\u5fae\u6ce2\u8026\u5408\u7684\u5f71\u54cd\u4ee5\u53ca\u7531\u6b64\u4ea7\u751f\u7684C\u578b\u6728\u7684\u52a0\u70ed\u6548\u679c\u3002<\/p>\n

\u56fe\u4e8c\u30013D\u5feb\u901f\u52a0\u70ed\u65b9\u6cd5\u7684\u8868\u5f81<\/strong>
\n \"\"\uff08a-b\uff09\u5fae\u6ce2\u52a0\u70ed\u8fc7\u7a0b\u4e4b\u540e\u7684c-\u6728\u6750\/Co(NO3<\/sub>)2<\/sub>\u8d77\u59cb\u6750\u6599\u548c\u5fae\u6ce2\u540e\u7684\u6240\u5f97C-\u6728\u6750\/CoOx<\/sub>\u7684\u7167\u7247\u3002<\/p>\n

\uff08c-f\uff09C-\u6728\u6750\/Co(NO3<\/sub>)2<\/sub>\u548cC-\u6728\u6750\/CoOx<\/sub>\u6750\u6599\u7684SEM\u56fe\u4ee5\u53ca\u76f8\u5e94\u7684\u9ad8\u5206\u8fa8\u7387\u56fe\u50cf\uff1b<\/p>\n

\uff08g\uff09\u57281000 W\u5fae\u6ce2\u529f\u7387\u4e0b\u8fdb\u884c3D\u52a0\u70ed\u7684\u6700\u521d200 ms\u7684\u53d1\u5149\u5f3a\u5ea6\uff1b<\/p>\n

\uff08h\uff09\u6839\u636e\u9ed1\u4f53\u7406\u8bba\u4ece\u5149\u5f3a\u5ea6\u4f30\u8ba1\u7684\u6e29\u5ea6\u968f\u65f6\u95f4\u7684\u53d8\u5316\uff0c\u6e29\u5ea6\u6700\u9ad8\u8fbe\u52302200K\u5e76\u7a33\u5b9a\u57281400K\uff1b<\/p>\n

\uff08i\uff09\u6839\u636e\u9ad8\u6e29\u6d4b\u5b9a\u7684\u591a\u5e27\u56fe\u50cf\u8ba1\u7b97\u7684\u6700\u521d70 ms\u7167\u660e\u7684\u6e29\u5ea6\u66f2\u7ebf\u3002<\/p>\n

\u56fe\u4e09\u30013D\u52a0\u70ed6s\u5feb\u901f\u5236\u6210\u7684C-\u6728\u6750\/CoOx<\/sub>\u7684\u5fae\u89c2\u7ed3\u6784<\/strong>
\n \"\"\uff08a\uff09C-\u6728\u6750\/CoOx<\/sub>\u590d\u5408\u6750\u6599\u7684SEM\u56fe\u50cf\uff1b<\/p>\n

\uff08b-d\uff09\u4ece\uff08a\uff09\u4e2d\u4e09\u4e2a\u76f8\u5e94\u533a\u57df\u4e2d\u9009\u62e9\u7684\u6837\u54c1\u7684TEM\u56fe\u50cf\u4ee5\u793a\u7eb3\u7c73\u9897\u7c92\u5206\u5e03\u5747\u5300\uff1b<\/p>\n

\uff08e\uff09C-\u6728\u6750\/CoOx<\/sub>\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

\uff08f-g\uff09\u901a\u8fc7\u52a0\u70ed6 s\u5236\u5f97\u7684C-\u6728\u6750\/CoOx<\/sub>\u4e2d\u53d1\u73b0\u7684\u7eb3\u7c73\u7c92\u5b50\u7684\u7ec4\u5408\u548c\u5355\u4e2aCo\u548cO EDX\u56fe\u3002<\/p>\n

\u56fe\u56db\u30013D\u52a0\u70ed\u65b9\u6cd5\u7684\u673a\u7406<\/strong>
\n \"\"\uff08a-c\uff09\u4e0d\u540c\u7535\u5b50\u7535\u5bfc\u7387\u7684C-\u6728\u6750\u7684\u5fae\u6ce2\u8026\u5408\u884c\u4e3a\u548c\u52a0\u70ed\u6548\u679c\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08d\uff09\u4e0d\u540c\u6e29\u5ea6\u4e0b\u78b3\u5316\u7684C-\u6728\u6750\u7684\u7535\u5bfc\u7387\uff1b<\/p>\n

\uff08e\uff09\u4e0d\u540c\u6e29\u5ea6\u4e0b\u5236\u6210\u7684\u4e0d\u540c\u7535\u5b50\u7535\u5bfc\u7387\u7684C-\u6728\u6750\u7684\u5fae\u6ce2\u5438\u6536\u6027\u80fd\uff1b<\/p>\n

\uff08f\uff09\u4e0d\u540c\u6e29\u5ea6\u4e0b\u78b3\u5316\u7684C-\u6728\u6750\u7684\u70ed\u5bfc\u7387\u3002<\/p>\n

\u56fe\u4e94\u30013D\u52a0\u70ed\u4f5c\u4e3a\u901a\u7528\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u5408\u6210\u65b9\u6cd5<\/strong>
\n \"\"\uff08a-d\uff09\u901a\u8fc73D\u52a0\u70ed\u5408\u6210\u7684C-\u6728\u6750\/NiO\u7684SEM\u3001TEM\u548c\u5143\u7d20\u5206\u6790\uff1b<\/p>\n

\uff08e-h\uff09\u901a\u8fc73D\u52a0\u70ed\u5408\u6210\u7684C-\u6728\u6750\/Fe3<\/sub>O4<\/sub>\u7684SEM\u3001TEM\u548c\u5143\u7d20\u5206\u6790\uff1b<\/p>\n

\uff08i-j\uff09C-\u6728\u6750\/NiO\u548cC-\u6728\u6750\/Fe3<\/sub>O4<\/sub>\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

\uff08k\uff09\u76f8\u5bf9\u4e8e\u62a5\u9053\u76843D\u52a0\u70ed\u65b9\u6cd5\u7684\u5e73\u57471400 K\u6e29\u5ea6\uff0c\u6240\u9009\u91d1\u5c5e\u785d\u9178\u76d0\u7684\u5206\u89e3\u6e29\u5ea6\u3002<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/p>\n

\u7efc\u4e0a\u6240\u8ff0\uff0c\u4f5c\u8005\u62a5\u9053\u4e86\u4e00\u79cd\u5feb\u901f\u5fae\u6ce23D\u52a0\u70ed\u7684\u65b9\u6cd5\u7528\u4e8e\u5728\u901a\u9053\u7ed3\u6784\u7684C-\u6728\u6750\u4e0a\u539f\u4f4d\u5408\u6210\u8d85\u7ec6\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u3002\u8be53D\u52a0\u70ed\u6280\u672f\u5177\u6709\u66f4\u7b80\u5355\u3001\u66f4\u5feb\u3001\u66f4\u9ad8\u6548\u7684\u4f18\u70b9\u3002C-\u6728\u6750\u7684\u6e29\u5ea6\u53ef\u57284 s\u5185\u8fbe\u52302200 K\uff0c\u5e76\u57281400 K\u4fdd\u6301\u7a33\u5b9a\uff0c\u6700\u5927\u77ac\u65f6\u5347\u6e29\u901f\u7387\u7ea6\u4e3a272 000 K s-1<\/sup>\u3002\u7531\u4e8e\u8fd9\u79cd\u6750\u6599\u5177\u6709\u5438\u6536\u5fae\u6ce2\u80fd\u91cf\u7684\u80fd\u529b\uff0cC-\u6728\u6750\u57fa\u677f\u5177\u6709\u9002\u5ea6\u5bfc\u7535\u6027\u3001\u826f\u597d\u7684\u5bfc\u70ed\u6027\u548c\u5b8c\u6574\u7684\u901a\u9053\u7ed3\u6784\u3002\u9664\u4e86CoOx<\/sub>\u4e4b\u5916\uff0c\u4f5c\u8005\u8fd8\u6210\u529f\u7684\u5408\u6210\u4e86Fe3<\/sub>O4<\/sub>\u548cNiO\u7b49\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u3002\u8fd9\u8868\u660e\u53ea\u8981\u524d\u4f53\u5206\u89e3\u6e29\u5ea6\u4f4e\u4e8e1400 K\uff0c\u8be5\u65b9\u6cd5\u5c31\u53ef\u4ee5\u6269\u5c55\u5230\u5e7f\u6cdb\u8303\u56f4\u7684\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u7684\u5408\u6210\u4e2d\u3002\u57fa\u4e8e\u5fae\u6ce2\u7684\u5feb\u901f\uff0c\u8be5\u52a0\u70ed\u65b9\u6cd5\u4ee3\u8868\u4e86\u8d85\u7ec6\u91d1\u5c5e\u6c27\u5316\u7269\u7eb3\u7c73\u9897\u7c92\u53ef\u6269\u5c55\u5408\u6210\u7684\u6709\u5e0c\u671b\u7684\u65b9\u5411\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1aSynthesis of Metal Oxide Nanoparticles by Rapid, High-Temperature 3D Microwave Heating<\/a><\/strong>\uff08Adv. Funct. Mater.<\/em>, 2019<\/strong>, DOI:10.1002\/adfm.201904282\uff09<\/p>\n

\u672c\u6587\u7531CQR\u7f16\u8bd1\u3002<\/p>\n

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