{"id":178680,"date":"2019-06-26T06:30:52","date_gmt":"2019-06-25T22:30:52","guid":{"rendered":"\/\/m.iemloyee.com\/?p=178680"},"modified":"2019-06-25T12:16:41","modified_gmt":"2019-06-25T04:16:41","slug":"%e3%80%90%e5%b7%b2%e6%a0%a1%e7%a8%bf%e3%80%91ees%ef%bc%9a%e6%96%b0%e5%9e%8b%e9%98%b3%e7%a6%bb%e5%ad%90%e6%97%a0%e5%ba%8fzncu-si-p%e5%8c%96%e5%90%88%e7%89%a9%e5%ae%b6%e6%97%8f%ef%bc%9a%e4%b8%8b","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=178680","title":{"rendered":"EES\uff1a\u65b0\u578b\u9633\u79bb\u5b50\u65e0\u5e8fZn(Cu)-Si-P\u5316\u5408\u7269\u5bb6\u65cf\uff1a\u4e0b\u4e00\u4ee3\u9502\u79bb\u5b50\u7535\u6c60\u7528\u9ad8\u6027\u80fd\u8d1f\u6781\u6750\u6599"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u9502\u79bb\u5b50\u7535\u6c60\u9010\u6e10\u6210\u4e3a\u7535\u52a8\u8f66\u548c\u667a\u80fd\u7535\u7f51\u7b49\u8bb8\u591a\u65b0\u5174\u6280\u672f\u4e2d\u6781\u5177\u524d\u666f\u7684\u7535\u6e90\u3002\u4e3a\u6ee1\u8db3\u5148\u8fdb\u7535\u6e90\u65e5\u76ca\u589e\u957f\u7684\u9700\u6c42\uff0c\u5f00\u53d1\u517c\u5177\u4f4e\u6210\u672c\u3001\u9ad8\u6027\u80fd\u7684\u9502\u79bb\u5b50\u7535\u6c60\u7528\u8d1f\u6781\u6750\u6599\u52bf\u5728\u5fc5\u884c\u3002\u9502\u79bb\u5b50\u7535\u6c60\u7528\u8d1f\u6781\u6750\u6599\u8981\u540c\u65f6\u5177\u6709\u5927\u5bb9\u91cf\u3001\u9ad8\u9996\u6548\u3001\u5b89\u5168\u7684\u5de5\u4f5c\u7535\u4f4d\u3001\u957f\u5faa\u73af\u5bff\u547d\u4ee5\u53ca\u9ad8\u500d\u7387\u7b49\u7efc\u5408\u6027\u80fd\u3002\u7845\u56e0\u5bb9\u91cf\u5927\u3001\u7535\u4f4d\u4f4e\u3001\u50a8\u91cf\u4e30\u5bcc\u548c\u5de5\u827a\u6210\u719f\u800c\u5177\u6709\u53d6\u4ee3\u5546\u7528\u77f3\u58a8\u7684\u524d\u666f\uff0c\u5907\u53d7\u5173\u6ce8\u3002\u7136\u800c\uff0c\u7845\u7684\u5546\u4e1a\u5316\u5e94\u7528\u53d7\u5230\u5176\u8f83\u5dee\u7684\u9502\u79bb\u5b50\u3001\u7535\u5b50\u8f93\u8fd0\u7684\u9650\u5236\u3002\u6b64\u5916\uff0c\u7845\u7684\u673a\u68b0\u6027\u80fd\u5dee\uff0c\u5728\u5d4c\u5165\u5927\u91cf\u9502\u79bb\u5b50\u7684\u8fc7\u7a0b\u4e2d\uff0c\u6613\u673a\u68b0\u7c89\u7cb9\uff0c\u56e0\u800c\u6076\u5316\u4e86\u5fae\u7c73\u7845\u8d1f\u6781\u6750\u6599\u7684\u5faa\u73af\u6027\u80fd\u3002\u901a\u8fc7\u7eb3\u7c73\u6280\u672f\u5df2\u5f00\u53d1\u51fa\u4e00\u4e9b\u53ef\u9760\u7684\u7535\u6781\u7ed3\u6784\uff0c\u83b7\u5f97\u4e86\u4f18\u5f02\u7efc\u5408\u6027\u80fd\uff0c\u7136\u800c\u590d\u6742\u7684\u5408\u6210\u65b9\u6cd5\u4ee5\u53ca\u4f4e\u4ea7\u7387\u589e\u52a0\u4e86\u7845\u8d1f\u6781\u7684\u5e94\u7528\u6210\u672c\u3002\u78f7\u56e0\u5177\u6709\u5927\u5bb9\u91cf\uff082596 mA hg-1<\/sup>\uff09\u3001\u9ad8\u50a8\u9502\u6d3b\u6027\u800c\u53d7\u5230\u5e7f\u6cdb\u5173\u6ce8\uff0c\u7136\u800c\u5dee\u7684\u7535\u5b50\u8f93\u8fd0\u963b\u788d\u4e86\u5176\u53d1\u5c55\u3002\u73b0\u6709\u7684\u7b56\u7565\u662f\u5c06\u5176\u4e0e\u78b3\u6750\u6599\u8fdb\u884c\u590d\u5408\u6765\u89e3\u51b3\u7535\u5b50\u4f20\u5230\u5dee\u548c\u4f53\u79ef\u81a8\u80c0\u7684\u95ee\u9898\u3002\u4f46\u662f\uff0c\u6784\u7b51P\/C\u590d\u5408\u6750\u6599\u6240\u91c7\u7528\u7684\u6db2\u76f8\u5408\u6210\u6d89\u53ca\u5230\u6709\u6bd2\u7684\u539f\u6599\u6216\u6eb6\u5242\uff0c\u6c14\u76f8\u5408\u6210\u5f80\u5f80\u4ea7\u751f\u6613\u71c3\u7684\u767d\u78f7\u3002\u5c3d\u7ba1\u6784\u5efa\u591a\u76f8\u590d\u5408\u6750\u6599\u4ee5\u534f\u540c\u4f5c\u7528\u80fd\u83b7\u5f97\u4f18\u5f02\u7efc\u5408\u6027\u80fd\uff0c\u4f46\u662f\u591a\u5143\u5316\u5408\u7269\u5f80\u5f80\u56e0\u4e3a\u5176\u672c\u8eab\u7279\u6b8a\u7684\u7406\u5316\u6027\u8d28\u53ca\u7535\u5316\u5b66\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u4ea7\u751f\u4e00\u7cfb\u5217\u4e2d\u95f4\u5316\u5408\u7269\u800c\u5177\u6709\u66f4\u4f18\u5f02\u7684\u7efc\u5408\u6027\u80fd\u3002\u4f46\u662f\u7531\u4e8e\u70ed\u7a33\u5b9a\u6027\u5dee\uff0c\u591a\u5143\u5316\u5408\u7269\u7684\u5408\u6210\u5f80\u5f80\u662f\u6bd4\u8f83\u56f0\u96be\u7684\u3002\u56e0\u6b64\u8bbe\u8ba1\u3001\u5408\u6210\u51fa\u9ad8\u6027\u80fd\u9502\u79bb\u5b50\u7535\u6c60\u8d1f\u6781\u7528\u591a\u5143\u5316\u5408\u7269\u9700\u8981\u5bf9\u591a\u5143\u5316\u5408\u7269\u7684\u7ed3\u6784-\u6027\u80fd\u5173\u7cfb\u6709\u6df1\u5165\u7406\u89e3\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u5e7f\u4e1c\u5de5\u4e1a\u5927\u5b66<\/strong>\u7684\u674e\u6587\u6b66\u526f\u6559\u6388\uff08\u7b2c\u4e00\u4f5c\u8005\uff09<\/strong>\u4e0e\u7f8e\u56fd\u4f50\u6cbb\u4e9a\u7406\u5de5\u5b66\u9662\u7684\u5218\u7f8e\u6797\u6559\u6388\uff08\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u3001\u5357\u65b9\u79d1\u6280\u5927\u5b66\u7684\u674e\u6b23\u851a\u535a\u58eb\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u5728Energy & Environmental Science<\/strong>\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201c<\/strong>A new family of cation-disordered Zn(Cu)-Si-P compounds as high-performance anodes for next-generation Li-ion batteries<\/strong>\u201d<\/strong>\u7684\u6587\u7ae0\u3002\u4f5c\u8005\u8bbe\u8ba1\u3001\u5408\u6210\u548c\u7cfb\u7edf\u8868\u5f81\u4e86\u7403\u78e8\u5236\u5907\u7684\u65b0\u578b\u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\u3002\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\u548c\u5b9e\u9a8c\u7ed3\u679c\u5171\u540c\u8868\u660e\uff0c\u4e0e\u9633\u79bb\u5b50\u6709\u5e8f\u7684ZnSiP2<\/sub>\uff08\u56db\u65b9\u76f8\uff09\u76f8\u6bd4\uff0c\u9633\u79bb\u5b50\u65e0\u5e8f\u7684ZnSiP2<\/sub>\uff08\u7acb\u65b9\u76f8\uff09\u5177\u6709\u66f4\u5feb\u7684\u9502\u79bb\u5b50\u3001\u7535\u5b50\u8f93\u8fd0\u548c\u66f4\u5f3a\u7684\u6297\u4f53\u79ef\u81a8\u80c0\u80fd\u529b\u3002\u8fdb\u4e00\u6b65\u4e0e\u77f3\u58a8\u590d\u5408\u6240\u5f62\u6210\u7684ZnSiP2<\/sub>\/C\u7eb3\u7c73\u590d\u5408\u6750\u6599\u8868\u73b0\u51fa\u6bd4\u5176\u5b83\u591a\u76f8\u590d\u5408\u6750\u6599\u66f4\u4f18\u5faa\u73af\u7a33\u5b9a\u6027\u548c\u500d\u7387\u6027\u80fd\u3002\u901a\u8fc7\u6539\u53d8\u9633\u79bb\u5b50\u6bd4\u4f8b\u4ee5\u53ca\u7528Cu\u4ee3Zn\uff0c\u53ef\u8fdb\u4e00\u6b65\u5408\u6210\u9633\u79bb\u5b50\u65e0\u5e8fZn(Cu)-Si-P\u5bb6\u65cf\u5316\u5408\u7269\uff0c\u4e30\u5bcc\u4e86\u65e0\u673a\u6750\u6599\u6570\u636e\u5e93\uff0c\u8be5\u5bb6\u65cf\u5316\u5408\u7269\u5747\u8868\u73b0\u51fa\u5927\u5bb9\u91cf\u3001\u9ad8\u9996\u6548\u3001\u5de5\u4f5c\u7535\u4f4d\u5b89\u5168\u7684\u50a8\u9502\u7279\u6027\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1.<\/strong> \u9633\u79bb\u5b50\u65e0\u5e8f\u3001\u6709\u5e8fZnSiP2<\/sub>\u7684\u5408\u6210\u4e0e\u8868\u5f81\u3002<\/p>\n

\"\"<\/p>\n

a) Zn-Si-2P\u7c89\u672b\u7403\u78e8\u8fc7\u7a0b\u7684\u76f8\u6f14\u53d8\u8fc7\u7a0b\u3002<\/p>\n

b) ZnSiP2<\/sub> XRD\u7684\u7cbe\u4fee\uff1b<\/p>\n

c) \u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\u7684\u6676\u4f53\u7ed3\u6784\u793a\u610f\u56fe\uff1b<\/p>\n

d) \u9633\u79bb\u5b50\u6709\u5e8f\u548c\u65e0\u5e8fZnSiP2<\/sub>\u7684XRD\uff1b<\/p>\n

e) \u9633\u79bb\u5b50\u6709\u5e8f\u548c\u65e0\u5e8fZnSiP2<\/sub>\u7684\u62c9\u66fc\u5149\u8c31\uff1b<\/p>\n

f) \u9633\u79bb\u5b50\u6709\u5e8fZnSiP2<\/sub>\u7684\u6676\u4f53\u7ed3\u6784\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe<\/strong>2. <\/strong>\u9633\u79bb\u5b50\u65e0\u5e8f\u548c\u6709\u5e8fZnSiP2<\/sub>\u6837\u54c1\u7684\u50a8\u9502\u6027\u80fd\u3002<\/p>\n

\"\"<\/p>\n

a)\u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\u7684\u524d\u4e09\u5468\u7684\u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf\uff1b<\/p>\n

b)\u9633\u79bb\u5b50\u65e0\u5e8f\u548c\u6709\u5e8fZnSiP2<\/sub>\u6837\u54c1\u9996\u5468\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

c)\u9633\u79bb\u5b50\u65e0\u5e8f\u548c\u6709\u5e8fZnSiP2<\/sub>\u6837\u54c1\u7684\u5faa\u73af\u7a33\u5b9a\u6027\u3002<\/p>\n

d)\u9633\u79bb\u5b50\u65e0\u5e8f\u548c\u6709\u5e8fZnSiP2<\/sub>\u7684\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\uff1a<\/p>\n

e)\u7535\u5b50\u7ed3\u6784\uff1b<\/p>\n

f)\u9502\u79bb\u5b50\u8f93\u8fd0\u80fd\u5792\uff1b<\/p>\n

g)\u6768\u6c0f\u6a21\u91cf\u3002<\/p>\n

\u56fe<\/strong>3. <\/strong>\u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\u50a8\u9502\u673a\u5236\u8868\u5f81\u3002<\/p>\n

\"\"<\/p>\n

a)\u79bb\u7ebfXRD\uff1b<\/p>\n

b)\u79bb\u7ebfXPS\uff08P 2p\uff09\u8bc1\u660e\u7ed3\u6784\u53ef\u9006\uff1b<\/p>\n

c)\u79bb\u7ebfXPS\uff08Si 2p\uff09\u8bc1\u660e\u7ed3\u6784\u53ef\u9006\uff1b<\/p>\n

d)\u79bb\u7ebfRaman\u8bc1\u660e\u7ed3\u6784\u53ef\u9006\uff1b<\/p>\n

e)\u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\u50a8\u9502\u673a\u5236\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe<\/strong>4.<\/strong> \u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\/\u77f3\u58a8\u590d\u5408\u6750\u6599\u8868\u5f81\u3001\u6027\u80fd\u53ca\u6bd4\u8f83\u3002<\/p>\n

\"\"<\/p>\n

(a-c) \u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\/\u77f3\u58a8\u590d\u5408\u6750\u6599\u7684TEM\u8868\u5f81\uff1b<\/p>\n

(d) \u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\/\u77f3\u58a8\u590d\u5408\u6750\u6599\u7684\u5faa\u73af\u548c\u500d\u7387\u6027\u80fd\uff1b<\/p>\n

(e-f) \u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\/\u77f3\u58a8\u590d\u5408\u6750\u6599\u4e0e\u76f8\u5173\u4e8c\u5143\u76f8\u548c\u5355\u7ec4\u5206\u76f8\u7684\u6027\u80fd(\u500d\u7387\u548c\u9996\u6548)\u6bd4\u8f83;<\/p>\n

(g-h) \u9633\u79bb\u5b50\u65e0\u5e8fZnSiP2<\/sub>\/\u77f3\u58a8\u590d\u5408\u6750\u6599\u4e0e\u5176\u5b83\u591a\u76f8\u8d1f\u6781\u6750\u6599\u7684\u5faa\u73af\u548c\u500d\u7387\u6027\u80fd\u6bd4\u8f83\u3002<\/p>\n

\u56fe<\/strong>5.<\/strong> \u9633\u79bb\u5b50\u65e0\u5e8f\u7684Zn(Cu)-Si-P\u5bb6\u65cf\u5316\u5408\u7269\u7684\u5408\u6210\u53ca\u50a8\u9502\u7279\u6027\u3002<\/p>\n

\"\"<\/p>\n

(a-b) Zn-Si-P\u5316\u5408\u7269(ZnSi2<\/sub>P3<\/sub>\u3001ZnSi3<\/sub>P4<\/sub>\u3001ZnSi4<\/sub>P5<\/sub>)\u7684XRD\uff1b<\/p>\n

(c-d) Cu-Si-P\u5316\u5408\u7269(CuSi2<\/sub>P3<\/sub>\u3001CuSi3<\/sub>P4<\/sub>\u3001CuSi4<\/sub>P5<\/sub>)\u7684XRD\uff1b<\/p>\n

(e) Zn(Cu)-Si-P\u5316\u5408\u7269\u7684\u9996\u5468\u5145\u653e\u7535\u66f2\u7ebf\uff1b<\/p>\n

(f) Zn(Cu)-Si-P\u5316\u5408\u7269\u3001P\/C\u4e0eSi\u7684\u9996\u5468\u653e\u7535\u66f2\u7ebf\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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\u3010\u56e2\u961f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1aA new family of cation-disordered Zn(Cu)\u2013Si\u2013P compounds as high-performance anodes for next-generation Li-ion batteries<\/a>\uff08EES\uff0c2019\uff0cDOI\uff1a10.1039\/C9EE00953A\uff09<\/p>\n

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