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\u56fe6 \u57fa\u4e8e\u540c\u6b65\u8f90\u5c04\u88c5\u7f6e\u7684X\u5c04\u7ebf\u663e\u5fae\u6210\u50cf\u65b9\u6cd5\u793a\u610f\u56fe<\/strong><\/p>\n

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5\u3001\u8054\u5408\u6280\u672f<\/strong><\/p>\n

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Emanuel Schwaighofer\u7b49\u4eba\u5229\u7528\u5fb7\u56fd\u6c49\u5821\u7684\u540c\u6b65\u8f90\u5c04\u88c5\u7f6eDESY\uff0c\u5e76\u7ed3\u5408\u4e86\u5c0f\u89d2\u5ea6X\u5c04\u7ebf\u6563\u5c04\uff08SAXS\uff09\u3001\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c\uff08TEM\uff09\u548c\u9ad8\u80fdX\u5c04\u7ebf\u884d\u5c04\uff08HEXRD\uff09\u7b49\u65b9\u6cd5\u7814\u7a76\u4e86TiAl\u57fa\u5408\u91d1\u7684\u6c89\u6dc0\u52a8\u529b\u5b66\u3001\u5c3a\u5bf8\u6f14\u53d8\u548c\u70ed\u7a33\u5b9a\u6027\uff0c\u56fe8\u4e3a\u90e8\u5206\u68c0\u6d4b\u56fe\u50cf\u3002\u9274\u4e8eC\u5408\u91d1\u5316\u53ef\u4ee5\u901a\u8fc7\u56fa\u6eb6\u5f3a\u5316\u548c\u78b3\u5316\u7269\u8fdb\u4e00\u6b65\u63d0\u9ad8\u9ad8\u6e29\u6027\u80fd\uff0c\u4ed6\u4eec\u9009\u7528\u539f\u4f4dX\u5c04\u7ebf\u6563\u5c04\u68c0\u6d4b\u4e86\u5408\u91d1\u7ecf\u8fc7\u7b49\u6e29\u9000\u706b\u540e\u52a0\u70ed\u81f31200\u2103\u7684\u6c89\u6dc0\u6790\u51fa\u884c\u4e3a\u548c\u70ed\u7a33\u5b9a\u6027\uff0cXEXRD\u7814\u7a76\u4e86\u6790\u51fa\u76f8\u5728\u7eb3\u7c73\u5c3a\u5ea6\u7684\u5206\u5c42\u7ed3\u6784\uff0cTEM\u89e3\u91ca\u4e86\u03b3-lath\u7684\u539a\u5ea6\u4e0ep\u578b\u78b3\u5316\u7269\u7279\u5f81\u5c3a\u5bf8\u4e4b\u95f4\u7684\u5173\u7cfb[7]\u3002<\/p>\n

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X\u5c04\u7ebf\u5438\u6536\u7cbe\u7ec6\u7ed3\u6784\uff08X-ray absorption fine structure\uff0cXAFS\uff09\u662f\u4e00\u79cd\u540c\u6b65\u8f90\u5c04\u7279\u6709\u7684\u7ed3\u6784\u5206\u6790\u65b9\u6cd5\uff0c\u5176\u4fe1\u53f7\u662f\u7531\u5438\u6536\u539f\u5b50\u5468\u56f4\u7684\u8fd1\u7a0b\u7ed3\u6784\u51b3\u5b9a\uff0c\u80fd\u63d0\u4f9b\u5c0f\u8303\u56f4\u7684\u539f\u5b50\u7c07\u7ed3\u6784\u7684\u4fe1\u606f\uff0c\u5305\u62ec\u7535\u5b50\u7ed3\u6784\u4e0e\u51e0\u4f55\u7ed3\u6784\uff0c\u6837\u54c1\u53ef\u4ee5\u662f\u6676\u4f53\u6216\u975e\u6676\u4f53\uff0c\u4e5f\u53ef\u4ee5\u662f\u56fa\u3001\u6db2\u3001\u6c14\u76f8\uff0c\u8fd8\u80fd\u7528\u4e8e\u5355\u4e00\u7269\u76f8\u6216\u6df7\u5408\u7269\u3002<\/p>\n

Tamao Ishida\u7b49\u4eba\u91c7\u7528\u539f\u4f4dXAFS\u7814\u7a76\u4e86Pd\u7684\u6d3b\u6027\u5c3a\u5bf8\u548c\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u5316\u5b66\u72b6\u6001\u548c\u7ed3\u6784\u7684\u53d8\u5316\u3002\u56fe10\u4e3aPd\/ZrO2\u548cPd\/Ceo2\u7684XANES\uff08X-ray absorption near edge spectra\uff09\u68c0\u6d4b\u7ed3\u679c\uff0c\u7814\u7a76\u8868\u660e\u5355\u4e2aPd\u539f\u5b50\u662f\u65e0\u6d3b\u6027\u7684\uff0cPd\u6613\u4e8e\u5728\u5177\u6709\u8f83\u4f4e\u5438\u9644\u548c\u8fc1\u79fb\u80fd\u91cf\u7684ZrO2<\/sub>\u8868\u9762\u6269\u6563\u5f62\u6210\u5c0f\u5c3a\u5bf8\u7684Pd\u56e2\u7c07\uff0c\u6709\u5229\u7528\u8131\u7fb0\u8fc7\u7a0b\u7684\u8fdb\u884c[9]\u3002<\/p>\n

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Iman Ja\u2019baz\u7b49\u4eba\u5728\u6fb3\u5927\u5229\u4e9a\u540c\u6b65\u52a0\u901f\u5668\u7684XFM\u5149\u675f\u7ebf\uff0c\u5bf9\u5408\u91d1\u6a2a\u622a\u9762\u4e0aFe\u3001Cr\u3001Mn\u3001Co\u7b49\u5143\u7d20\u7684\u7a7a\u95f4\u5206\u5e03\u60c5\u51b5\u8fdb\u884c\u4e86SXRF\u548cXANES\u68c0\u6d4b\uff0c\u90e8\u5206\u7ed3\u679c\u89c1\u56fe11 \uff0c\u5e76\u5206\u6790Cr\u542b\u91cf\u548c\u6c27\u5316\u3001\u6e17\u78b3\u7b49\u884c\u4e3a\u5bf912Cr1MoVG\u7ba1\u5b50\u8150\u8680\u6027\u80fd\u7684\u5f71\u54cd[10]\u3002<\/p>\n

\u56fe11 12Cr1MoVG\u6a2a\u622a\u9762\u7684XFM\u68c0\u6d4b\u7ed3\u679c<\/p>\n

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\u6d59\u6c5f\u5927\u5b66\u8521\u6625\u950b\u7b49\u4eba\u5229\u7528\u540c\u6b65\u8f90\u5c04\u5149\u7535\u5b50\u80fd\u8c31\u6280\u672f\u6d4b\u91cf\u4e86ZnO\/PbTe\u5f02\u8d28\u7ed3\u7ed3\u6784\u7684\u80fd\u5e26\u5e26\u9636\uff0c\u5982\u56fe12\u6240\u793a\uff0c\u7814\u7a76\u53d1\u73b0\u5728\u8be5\u5f02\u8d28\u7ed3\u754c\u9762\u7684\u80fd\u5e26\u6392\u5217\u4e2d\u5bfc\u5e26\u5e26\u9636\u8f83\u5c0f\uff0c\u4ef7\u5e26\u5e26\u9636\u8f83\u5927\uff0c\u8fd9\u79cd\u7ed3\u6784\u6709\u5229\u7528PbTe\u4e2d\u7684\u6fc0\u53d1\u7535\u5b50\u8f93\u8fd0\u5230ZnO\u5bfc\u7535\u5c42\u4e2d\uff0c\u5728\u65b0\u578b\u592a\u9633\u7535\u6c60\u3001\u7ea2\u5916\u63a2\u6d4b\u5668\u3001\u6fc0\u5149\u5668\u7b49\u5668\u4ef6\u4e2d\u5177\u6709\u6f5c\u5728\u7684\u5e94\u7528\u4ef7\u503c[11]\u3002<\/p>\n

\u56fe12 ZnO\/PbTe\u5f02\u8d28\u7ed3\u6837\u54c1\u7684SRPES<\/p>\n

\"\"\"\"<\/p>\n

\u516d\u3001\u8f6fX\u5c04\u7ebf\u663e\u5fae\u672f<\/strong><\/p>\n

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\u4e03\u3001\u540c\u6b65\u8f90\u5c04\u7ea2\u5916\u5149\u8c31<\/strong><\/p>\n

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\u590d\u65e6\u5927\u5b66\u9648\u65b0\u8bfe\u9898\u7ec4\u5bf9\u5355\u6839\u4e1d\u7ea4\u7ef4\u8fdb\u884c\u4e86\u7ea2\u5916\u663e\u5fae\u8c31\u5b66\u7814\u7a76[12]\uff0c\u7ed3\u5408\u4e86\u540c\u6b65\u8f90\u5c04\u7ea2\u5916\u5149\u8c31\u6280\u672f\u548c\u540c\u6b65\u8f90\u5c04X\u5c04\u7ebf\u884d\u5c04\u6280\u672f\uff0c\u5bf9\u5185\u90e8\u4e1d\u86cb\u767d\u7684\u4e8c\u7ea7\u7ed3\u6784\u8fdb\u884c\u4e86\u5b9a\u91cf\u5206\u6790\uff0c\u5f97\u5230\u4e86\u5fae\u89c2\u7ed3\u6784\u4e0e\u7ea4\u7ef4\u5b8f\u89c2\u529b\u5b66\u6027\u80fd\u7684\u5173\u7cfb\uff0c\u5982\u56fe13\u6240\u793a\u3002<\/p>\n

\u56fe13 SR-FTIR\u4e1d\u7ea4\u7ef4\u7814\u7a76<\/p>\n

\"\" \u00a0\u00a0<\/p>\n

\u516b\u3001\u8f6fX\u5c04\u7ebf\u78c1\u6027\u5706\u4e8c\u8272<\/strong><\/p>\n

\u8f6fX\u5c04\u7ebf\u78c1\u6027\u5706\u4e8c\u8272\uff08SXMCD\uff0cSoft X-ray Magnetic Circular Dichroism\uff09\u662f\u4e00\u79cd\u65b0\u578b\u7684\u5b9e\u9a8c\u624b\u6bb5\uff0c\u5b83\u6240\u7814\u7a76\u7684\u662f\u7269\u8d28\u5bf9\u4e24\u79cd\u5706\u504f\u632f\u5149\u7684\u5438\u6536\u8c31\u4e4b\u5dee\uff0c\u5373\u5de6\u65cb\u548c\u53f3\u65cb\u5706\u504f\u632f\u5149\u5438\u6536\u8c31\u7684\u975e\u5bf9\u79f0\u6027\u3002<\/p>\n

O.Toulemonde\u7b49\u4eba\u5229\u7528SXMCD\u7814\u7a76\u4e86\u63ba\u6742\u4e9a\u9530\u9178\u76d0\u4e2dCo2+<\/sup>\u548cNi2+<\/sup>\u9633\u79bb\u5b50\u7684\u7535\u5b50\u7ed3\u6784\u548c\u78c1\u77e9[13]\uff0c\u5982\u56fe14\u6240\u793a\uff0c\u7ed3\u679c\u8868\u660eCo\u3001Ni\u78c1\u77e9\u4e0eMn\u78c1\u77e9\u5bf9\u79f0\uff0c\u800c\u4e0eCr\u78c1\u77e9\u76f8\u53cd\uff0c\u610f\u5473\u7740\u5b83\u4eec\u7684\u4f5c\u7528\u673a\u7406\u4e5f\u662f\u4e0d\u540c\u7684\u3002<\/p>\n

\u56fe14 Mn L2,3<\/sub>-edges\u7684SXMCD\u5206\u6790\u7ed3\u679c<\/p>\n

\"\"<\/p>\n

SXMCD\u7684\u7814\u7a76\u65b9\u5411\u4e3b\u8981\u6709\uff1a\u8fc7\u6e21\u91d1\u5c5e2p-3d\u8dc3\u8fc1\u7684L2,3<\/sub>\u5438\u6536\u8fb9\u548c\u7a00\u571f\u91d1\u5c5e3d-4f\u8dc3\u8fc1\u7684M3,4<\/sub>\u5438\u6536\u8fb9\u3001\u8fc7\u6e21\u91d1\u5c5e\u8584\u819c\u548c\u4e9a\u5355\u5c42\u819c\u7684\u78c1\u6027\u53ca\u5c42\u95f4\u7684\u78c1\u76f8\u4e92\u8026\u5408\u3001\u591a\u5c42\u819c\u548c\u78c1\u5408\u91d1\u6750\u6599\u4e2d\u7279\u5b9a\u5143\u7d20\u7684\u7279\u5f81\u78c1\u6ede\u56de\u7ebf\u53ca\u5176\u4ed6\u6027\u8d28\u3001\u590d\u6742\u6676\u4f53\u7ed3\u6784\u5316\u5408\u7269\u7684\u78c1\u6709\u5e8f\u7b49\u3002<\/p>\n

\u53c2\u8003\u6587\u732e\uff1a<\/b><\/strong><\/p>\n

1.Xu, Y. Liu, et al. The complesity of thermoelectric materials: why we need powerful and brilliant aynchrotron radiation sources? Materials Today Physics 6 (2018) 68-82<\/p>\n

2.\u674e\u5b9c\u5c55\uff0c\u6a0a\u6f47\u6f47\uff0c\u540c\u6b65\u8f90\u5c04\u5149\u6e90\u7684\u79d1\u6280\u53d1\u5c55\u53ca\u79d1\u5b66\u5f71\u54cd\u7814\u7a76\uff0c\u4e16\u754c\u79d1\u6280\u7814\u7a76\u4e0e\u53d1\u5c55\uff0c2019,41\uff081\uff09\uff1a16-31<\/p>\n

3.\u674e\u859b\u5b87. \u540c\u6b65\u8f90\u5c04X\u5c04\u7ebf\u6563\u5c04\u7814\u7a76\u805a\u4e59\u70ef\u5fae\u5b54\u9694\u819c\u52a0\u5de5\u7269\u7406[D].\u4e2d\u56fd\u79d1\u5b66\u6280\u672f\u5927\u5b66,2017<\/p>\n

4.Jia N, Cong Z H, Sun X, et al. Acta Materialia [J], 2009, 57(13):3965-3977<\/p>\n

5.\u8881\u6e05\u4e60\uff0c\u9093\u5f6a\uff0c\u5173\u52c7\uff0c\u5f20\u51ef\uff0c\u5218\u5b9c\u664b\uff0c\u540c\u6b65\u8f90\u5c04\u7eb3\u7c73\u6210\u50cf\u6280\u672f\u7684\u53d1\u5c55\u4e0e\u5e94\u7528\uff0c\u7269\u7406\uff0c2019,48\uff084\uff09\uff1a205-219<\/p>\n

6.Iberl A, Schuster M, Gobel H, Meyer A, et al. J Phys D (Appl Phys), 1995, 28:A200<\/p>\n

7.Emanuel Schwaighofer, Peter Staron, et al. In situ small-angle X-ray scattering study of the perovskite-type\u00a0carbide precipitation behavior in a carbon-containing intermetallic\u00a0TiAl alloy using synchrotron radiation\u00a0[J], Acta Materialia 77 (2014) 360\u2013369<\/p>\n

8.\u5b97\u5e7f\u519b\uff0c\u522b\u6bd4\u96c4\uff0c\u8303\u7aef\uff0c\u57fa\u4e8e\u540c\u6b65\u8f90\u5c04X\u5c04\u7ebf\u7684SiCp\/Al\u590d\u5408\u6750\u6599\u53d8\u5f62\u635f\u4f24\u7814\u7a76[J]\uff0c\u590d\u5408\u6750\u6599\u5b66\u62a5\uff0c2019,36<\/p>\n

9.Tamao Ishida, Tetsuo Honma, et al. Pd-catalyzed decarbonylation of furfural: Elucidation of support effect\u00a0on Pd size and catalytic activity using in-situ XAFS\u00a0[J], Journal of Catalysis 374 (2019) 320\u2013327<\/p>\n

10.Iman Ja\u2019baz, Song Zhou, et al. Spatial distribution of Cr-bearing species\u00a0on the corroded tube surface characterized\u00a0by synchrotron X-ray fluorescence (SXRF) mapping\u00a0and micro-XANES: exposure of tubes in oxy-firing flue\u00a0gas\u00a0[J], J Mater Sci (2018) 53:11791\u201311812<\/p>\n

11.\u8521\u6625\u950b\uff0c\u5f20\u5175\u5761\uff0c\u5229\u7528\u540c\u6b65\u8f90\u5c04\u5149\u7535\u5b50\u80fd\u8c31\u6280\u672f\u6d4b\u91cfZnO\/PbTe\u5f02\u8d28\u7ed3\u7684\u80fd\u5e26\u5e26\u9636\uff0c\u7269\u7406\u5b66\u62a5\uff0c2014\uff0c16\uff0863\uff09167301<\/p>\n

12.Fang G, Tang Y, Qi Z, et al. J. Mater. Chem. B, 2017, 5(30)<\/p>\n

13.Toulemonde, F. Studer, B. Raveau, Magnetic interactions studies of Co and Ni-doped manganites\u00a0using soft XMCD\u00a0[J], Solid State Communications 118 (2001) 107-112<\/p>\n

 <\/p>\n

\u672c\u6587\u7531\u80e1\u51e1\u4f9b\u7a3f\u3002<\/p>\n

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