{"id":169081,"date":"2019-03-14T06:19:32","date_gmt":"2019-03-13T22:19:32","guid":{"rendered":"\/\/m.iemloyee.com\/?p=169081"},"modified":"2019-03-14T22:26:58","modified_gmt":"2019-03-14T14:26:58","slug":"%e5%8d%8e%e4%b8%ad%e7%a7%91%e6%8a%80%e5%a4%a7%e5%ad%a6%e7%8e%8b%e6%98%a5%e6%a0%8b%e8%af%be%e9%a2%98%e7%bb%84%e4%b8%8e%e4%b8%ad%e7%a7%91%e5%a4%a7%e7%86%8a%e5%ae%87%e6%9d%b0%e8%af%be%e9%a2%98%e7%bb%84","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=169081","title":{"rendered":"\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u738b\u6625\u680b\u8bfe\u9898\u7ec4\u4e0e\u4e2d\u79d1\u5927\u718a\u5b87\u6770\u8bfe\u9898\u7ec4\u5408\u4f5cAdv. Energy Mater.\u7efc\u8ff0: \u7528\u4e8e\u6790\u6c27\u53cd\u5e94\u76842D\u5c42\u72b6\u53cc\u6c22\u6c27\u5316\u7269\uff1a\u4ece\u57fa\u7840\u8bbe\u8ba1\u5230\u5e94\u7528"},"content":{"rendered":"

\u3010\u80cc\u666f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u968f\u7740\u7164\u70ad\u3001\u77f3\u6cb9\u3001\u5929\u7136\u6c14\u7b49\u4e0d\u53ef\u518d\u751f\u80fd\u6e90\u7684\u9010\u6e10\u67af\u7aed\uff0c\u53ef\u518d\u751f\u80fd\u6e90\u7684\u5f00\u53d1\u53d8\u5f97\u7d27\u8feb\u8d77\u6765\uff0c\u56e0\u6b64\u6025\u9700\u5f00\u53d1\u66f4\u52a0\u9ad8\u6548\u7684\u80fd\u91cf\u5b58\u50a8\u548c\u8f6c\u6362\u7cfb\u7edf\u3002\u7535\u5316\u5b66\u6c34\u6c27\u5316\u4f5c\u4e3a\u6c34\u5206\u89e3\u8fc7\u7a0b\u4e2d\u7684\u91cd\u8981\u90e8\u5206\u5f15\u8d77\u4e86\u4eba\u4eec\u7684\u5e7f\u6cdb\u5173\u6ce8\uff0c\u5728\u80fd\u91cf\u5b58\u50a8\u548c\u8f6c\u6362\u65b9\u9762\u6709\u7740\u5e7f\u9614\u7684\u5e94\u7528\u524d\u666f\u3002\u4e0e\u53c2\u4e0e\u6c34\u5206\u89e3\u7684\u9634\u6781\u90e8\u5206\u7684\u6790\u6c22\u53cd\u5e94\uff08HER\uff09\u76f8\u6bd4\uff0c\u9633\u6781\u7684\u6790\u6c27\u53cd\u5e94\uff08OER\uff09\u7531\u4e8e\u5176\u56db\u7535\u5b50\uff084e\uff09\u8f6c\u79fb\u8fc7\u7a0b\u4e2d\u7684\u60f0\u6027\u4f7f\u5176\u5177\u6709\u8fdf\u6ede\u7684\u53cd\u5e94\u52a8\u529b\u5b66\u8fc7\u7a0b\uff0c\u8fd9\u4e0d\u4ec5\u963b\u788d\u4e86\u6c34\u5206\u89e3\u7684\u9ad8\u6548\u5229\u7528\uff0c\u800c\u4e14\u4e5f\u662f\u51cf\u5c11\u4e8c\u6c27\u5316\u78b3\u6392\u653e\uff0c\u53d1\u5c55\u71c3\u6599\u7535\u6c60\u53ca\u53ef\u5145\u7535\u91d1\u5c5e\u7a7a\u6c14\u7535\u6c60\u7684\u4e3b\u8981\u969c\u788d\u4e4b\u4e00\u3002\u4e3a\u63d0\u9ad8\u7535\u89e3\u6c34\u8fc7\u7a0b\u4e2d\u7684OER\u6d3b\u6027\uff0c\u4e00\u4e9b\u5df2\u7ecf\u88ab\u5546\u4e1a\u5316\u7684\u50ac\u5316\u5242\u5982RuO2<\/sub>\u548cIrO2<\/sub>\uff0c\u5177\u6709\u4f18\u5f02\u7684\u50ac\u5316\u6d3b\u6027\uff0c\u4f46\u8fd9\u4e9b\u8d35\u91d1\u5c5e\u50ac\u5316\u5242\u5728\u9ad8\u9633\u6781\u7535\u4f4d\u4e0b\u7684\u78b1\u6027\u7535\u89e3\u6db2\u4e2d\u53ef\u80fd\u88ab\u6c27\u5316\u6210RuO4<\/sub>\u548cIrO3<\/sub>\uff0c\u4f7f\u5176\u9010\u6e10\u6eb6\u89e3\u5728\u7535\u89e3\u6db2\u4e2d\u3002\u6b64\u5916\uff0c\u8fd9\u4e9b\u8d35\u91d1\u5c5e\u542b\u91cf\u7a00\u7f3a\u6027\u4ef7\u683c\u6602\u8d35\uff0c\u9650\u5236\u4e86\u5b83\u4eec\u7684\u5927\u89c4\u6a21\u751f\u4ea7\u4f7f\u7528\u3002
\n \u56e0\u6b64\u7814\u7a76\u8005\u4eec\u4e3a\u5f00\u53d1\u66ff\u4ee3\u7684\u50ac\u5316\u5242\u505a\u51fa\u4e86\u8bb8\u591a\u5b9e\u8d28\u6027\u7684\u52aa\u529b\uff0c\u5176\u4e2d\u4e00\u79cd\u7b56\u7565\u662f\u5229\u7528\u9ad8\u6548\u3001\u7a33\u5b9a\u3001\u5730\u8868\u542b\u91cf\u4e30\u5bcc\u548c\u4f4e\u6bd2\u6027\u7684\u975e\u8d35\u91d1\u5c5e\u7535\u50ac\u5316\u5242\u6765\u63d0\u9ad8OER\u6d3b\u6027\u3002\u5728\u8fd9\u4e9b\u4f17\u591a\u7684\u975e\u8d35\u91d1\u5c5e\u7535\u50ac\u5316\u5242\u4e2d\uff0c\u4e8c\u7ef4\u5c42\u72b6\u53cc\u6c22\u6c27\u5316\u7269\uff08LDHs\uff09\u4f5c\u4e3a\u6700\u5148\u8fdb\u7684OER\u7535\u50ac\u5316\u5242\u4e4b\u4e00\uff0c\u5176\u7ed3\u6784\u548c\u7ec4\u6210\u7075\u6d3b\u53ef\u8c03\uff0c\u5236\u5907\u65b9\u6cd5\u7b80\u5355\u53ef\u9760\uff0c\u6709\u671b\u6210\u4e3a\u9ad8\u6027\u80fd\u5927\u89c4\u6a21\u5de5\u4e1a\u5316\u5e94\u7528\u7684OER\u7535\u50ac\u5316\u5242\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u6700\u8fd1\uff0cAdv. Energy Mater.<\/strong>\u5728\u7ebf\u520a\u767b\u4e86\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u738b\u6625\u680b\u526f\u6559\u6388<\/strong>\u548c\u4e2d\u56fd\u79d1\u6280\u5927\u5b66\u718a\u5b87\u6770\u6559\u6388<\/strong>\u7b49\u4eba\u603b\u7ed3\u7684\u7528\u4e8e\u6c27\u6c14\u91ca\u653e\u53cd\u5e94\u76842D\u5c42\u72b6\u53cc\u6c22\u6c27\u5316\u7269\u7684\u7efc\u8ff0\u3002\u9898\u76ee\u662f\u201c2D Layered Double Hydroxides for Oxygen Evolution Reaction: From Fundamental Design to Application<\/strong>\u201d\u3002\u5728\u8fd9\u7bc7\u7efc\u8ff0\u4e2d\uff0c\u4f5c\u8005\u603b\u7ed3\u4e86\u57fa\u4e8e\u5c42\u72b6\u53cc\u6c22\u6c27\u5316\u7269\uff08LDH\uff09\u7684OER\u7535\u50ac\u5316\u5242\u7684\u5408\u7406\u8bbe\u8ba1\u7684\u6700\u65b0\u8fdb\u5c55\u3002\u8fdb\u4e00\u6b65\u603b\u7ed3\u4e86\u5236\u5907\u65b9\u6cd5\u7684\u5404\u79cd\u7b56\u7565\uff0c\u4ee5\u53caLDH\u7684\u7ed3\u6784\u548c\u7ec4\u6210\u8c03\u63a7\u89c4\u5f8b\uff0c\u5e76\u8ba8\u8bba\u4e86\u5f71\u54cdOER\u50ac\u5316\u6027\u80fd\u7684\u56e0\u7d20\u3002\u6700\u540e\uff0c\u4f5c\u8005\u6307\u51fa\u4e86\u63d0\u9ad8LDH\u7535\u50ac\u5316\u5242\u50ac\u5316\u6d3b\u6027\u6240\u9762\u4e34\u7684\u56f0\u96be\u548c\u6311\u6218\uff0c\u5e76\u5bf9LDH\u7535\u50ac\u5316\u5242\u7684\u53d1\u5c55\u524d\u666f\u8fdb\u884c\u4e86\u5c55\u671b\u3002\u6587\u7ae0\u7b2c\u4e00\u4f5c\u8005\u4e3a\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u535a\u58eb\u7814\u7a76\u751f\u5415\u7433<\/strong>\uff0c\u901a\u8baf\u4f5c\u8005\u4e3a\u738b\u6625\u680b\u526f\u6559\u6388<\/strong>\u548c\u718a\u5b87\u6770\u6559\u6388<\/strong>\u3002<\/p>\n

\u3010\u56fe\u6587\u89e3\u8bfb\u3011<\/strong><\/p>\n

1\u3001\u5f15\u8a00<\/strong><\/p>\n

\u56fe\u4e00\u3001\u4e0d\u540cM2+<\/sup>\/M3+<\/sup>\u6469\u5c14\u6bd4\u7684\u78b3\u9178\u76d0\u5939\u5c42LDHs\u7684\u7406\u60f3\u7ed3\u6784<\/strong>
\n \"\"<\/a>\"\"\"\"
\n \u8868\u73b0\u4e3a\u91d1\u5c5e\u6c22\u6c27\u5316\u7269\u516b\u9762\u4f53\u6cbf\u6676\u4f53c\u8f74\u5806\u79ef\uff0c\u4ee5\u53ca\u6c34\u548c\u9634\u79bb\u5b50\u5728\u5939\u5c42\u533a\u57df\u5448\u73b0\u3002<\/p>\n

\u56fe\u4e8c\u3001\u5f71\u54cdLDHs\u7684\u50ac\u5316OER\u6027\u80fd\u56e0\u7d20<\/strong>
\n \"\"
\n 2\u3001\u7535\u89e3OER\u7684\u57fa\u672c\u539f\u7406<\/strong><\/p>\n

2.1\u3001\u8d85\u7535\u52bf<\/strong><\/p>\n

2.2\u3001\u4ea4\u6362\u7535\u6d41\u5bc6\u5ea6<\/strong><\/p>\n

2.3\u3001Tafel\u659c\u7387<\/strong><\/p>\n

2.4\u3001OER\u673a\u5236<\/strong><\/p>\n

3\u3001\u5236\u5907\u65b9\u6cd5<\/strong><\/p>\n

3.1\u3001\u6eb6\u5242\u70ed\u6cd5<\/strong><\/p>\n

3.2\u3001\u5fae\u6ce2\u8f90\u5c04\u6cd5<\/strong><\/p>\n

3.3\u3001\u7535\u6c89\u79ef\u6cd5<\/strong><\/p>\n

3.4\u3001\u8150\u8680\u5de5\u7a0b\u6cd5<\/strong><\/p>\n

3.5\u3001\u6eb6\u5242\u84b8\u53d1\u6cd5<\/strong><\/p>\n

3.6\u3001\u65cb\u6d82\u6cd5<\/strong><\/p>\n

3.7\u3001\u79bb\u5b50\u4ea4\u6362\u6cd5<\/strong><\/p>\n

4\u3001LDH\u7eb3\u7c73\u7247\u7684\u63d2\u5c42\u7ed3\u6784\u548c\u5265\u79bb<\/strong><\/p>\n

4.1\u3001\u63d2\u5c42\u7ed3\u6784<\/strong><\/p>\n

4.1.1\u3001\u539f\u4f4d\u63d2\u5c42<\/strong><\/p>\n

\u56fe\u4e09\u3001HPO3<\/sub>2\u2212<\/sup> \u63d2\u5c42\u7684NiFe LDH<\/strong>
\n \"\"
\n \uff08a\uff09HPO3<\/sub>2\u2212<\/sup> \u63d2\u5c42\u7684NiFe LDH\u7ed3\u6784\u6a21\u578b\uff1b<\/p>\n

\uff08b\uff09NiFe LDH\u4e0a\u7684OER\u8fc7\u7a0b\uff1b<\/p>\n

\uff08c\uff09Ni\u548c\uff08d\uff09Fe\u4f4d\u70b9\u7684\u7ed3\u5408\u80fd\u548cBader\u7535\u8377\u4f5c\u4e3a\u5b9e\u9a8c\u6d4b\u91cf\u7684\u5404\u79cd\u6240\u5236\u5907\u7684NiFe LDH\u7684\u8d77\u59cb\u7535\u4f4d\u7684\u51fd\u6570\uff08\u25cf\uff1a\u7ed3\u5408\u80fd;\u25b2\uff1aBader\u7535\u8377\uff09\u3002\u3002<\/p>\n

4.1.2\u3001\u79bb\u5b50\u4ea4\u6362<\/strong><\/p>\n

\u56fe\u56db\u3001\u79bb\u5b50\u4ea4\u6362\u5236\u5907\u5939\u5c42NiFe LDH\u7eb3\u7c73\u7247<\/strong>
\n \"\"
\n \uff08a\uff09\u5236\u5907\u7684\uff08\u84dd\u8272\uff09\u548c\u5728\u73af\u5883\u7a7a\u6c14\u4e0b1.0 M KOH\u6c34\u6eb6\u6db2\u4e2d\u60ac\u6d6e\u540e\uff08\u7ea2\u8272\uff09\u7684\uff0c\u5177\u6709\u4e0d\u540c\u5939\u5c42\u9634\u79bb\u5b50\u7684NiFe LDH\u7eb3\u7c73\u7247\u7684\u57fa\u5e95\u95f4\u8ddd\uff1b<\/p>\n

\uff08b\uff09\u5728\u51e0\u4e4e\u4e0d\u542b\u78b3\u9178\u76d0\u7684\u7535\u89e3\u8d28\u7684\u6c34\u6eb6\u6db2\uff081.0 M KOH\uff09\u4e2d\u5177\u6709\u4e0d\u540c\u5939\u5c42\u9634\u79bb\u5b50\u7684NiFe LDH\u6750\u6599\u7684\u6052\u7535\u6d41\u7535\u89e3\uff1a\u771f\u7a7a\u72b6\u6001\uff08\u84dd\u8272\uff09\u548c\u73af\u5883\u7a7a\u6c14\uff08\u7ea2\u8272\uff09\u3002\u7070\u8272\u663e\u793a\u88f8\u77f3\u58a8\u76d8\u7684\u8ba1\u65f6\u7535\u4f4d\u6570\u636e\u3002\u6240\u6709\u6570\u636e\u4ee51 mA cm-2<\/sup>\u7684\u6052\u5b9a\u7535\u6d41\u5bc6\u5ea6\u6536\u96c6\uff1b<\/p>\n

\uff08c\uff09\u4e0d\u540c\u5939\u5c42\u9634\u79bb\u5b50\u7684NiFe LDH\u8f6c\u5316\u4e3a\u78b3\u9178\u76d0\u5939\u5c42LDH\u7684\u5236\u5907\u8fc7\u7a0b\u53ca\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08d\uff09\u5404\u79cdNiFe LDH\u6837\u54c1\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

\uff08e\uff09\u4e0d\u540cNiFe LDH\u6837\u54c1\u5728ECSA\u5f52\u4e00\u5316\uff08\u865a\u7ebf\uff09\u4e4b\u524d\u548c\u4e4b\u540e\u7684\u5faa\u73af\u4f0f\u5b89\uff08CV\uff09\u66f2\u7ebf\uff1b<\/p>\n

\uff08f\uff09\u901a\u8fc7CV\u66f2\u7ebf\u7528\u4e8e\u53cc\u5c42\u7535\u5bb9\u4f30\u8ba1\u7684ECSA\u5206\u6790\u3002<\/p>\n

4.2\u3001LDH\u7eb3\u7c73\u7247\u7684\u5265\u79bb<\/strong><\/p>\n

4.2.1\u3001\u6db2\u4f53\u5265\u79bb<\/strong><\/p>\n

\u56fe\u4e94\u3001NiFe LDH\u7684\u6db2\u4f53\u5265\u79bb<\/strong>
\n \"\"
\n \uff08a\uff09LDH\u7247\u72b6\u5265\u79bb\u8fc7\u7a0b\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b\uff09NiFe LDH-CO3<\/sub>2-<\/sup>\u7684TEM\u56fe\uff08\u6807\u5c3a\uff0c1 \u03bcm\uff09\uff1b<\/p>\n

\uff08c~d\uff09\u5927\u5757NiFe\u3001NiCo\u3001CoCo LDH\u53ca\u5176\u7247\u72b6\u5265\u843d\u7269\u7684\u6781\u5316\u66f2\u7ebf\u548c\u5bf9\u5e94\u8fc7\u7535\u4f4d\uff1b<\/p>\n

\uff08e\uff09NiFe LDH-NS @DG\u590d\u5408\u6750\u6599\u7684\u5236\u5907\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08f\uff09\u5757\u72b6NiFe LDH\u548c\u5265\u79bb\u7684NiFe LDH NS\u7684XRD\u56fe\uff1b<\/p>\n

\uff08g~h\uff09\u5265\u79bb\u7684NiFe LDH-NS\u548cDG\u7684AFM\u56fe\uff1b<\/p>\n

\uff08i~j\uff09\u4e0d\u540c\u653e\u5927\u500d\u6570\u7684NiFe LDH-NS @DG\u7684TEM\u56fe\uff0c\u4ee5\u53ca\u76f8\u5e94\u7684\u9009\u5b9a\u533a\u57df\u7535\u5b50\u884d\u5c04\uff08SAED\uff09\u56fe\u3002<\/p>\n

4.2.2\u3001\u7b49\u79bb\u5b50\u4f53\u8f85\u52a9\u5265\u79bb<\/strong><\/p>\n

\u56fe\u516d\u3001\u7b49\u79bb\u5b50\u4f53\u523b\u8680CoFe LDHs<\/strong>
\n \"\"
\n \uff08a\uff09\u4eceAFM\u6d4b\u8bd5\u4e2d\u5f97\u51fa\u7684\u5927\u5757CoFe LDHs\u548c\u8d85\u8584CoFe LDHs-Ar\u7eb3\u7c73\u7247\u7684\u9ad8\u5ea6\u66f2\u7ebf\uff1b<\/p>\n

\uff08b\uff09\u5757\u72b6CoFe LDH\u548c\u8d85\u8584CoFe LDHs-Ar\u7684XRD\u56fe\uff1b<\/p>\n

\uff08c~d\uff09CoFe LDHs\u548c\u8d85\u8584CoFe LDH-Ar\u4e2dCo\u548cFe\u7684FT-EXAFS\u5149\u8c31\u3002<\/p>\n

5\u3001Ni\u6216Co\u57faLDH OER\u50ac\u5316\u5242<\/strong><\/p>\n

\u56fe\u4e03\u3001Ni\u57faLDH OER\u50ac\u5316\u5242<\/strong>
\n \"\"
\n \uff08a~b\uff09\u03b1-Ni(OH)2<\/sub>\uff08\u7070\u8272\uff0cNi2+<\/sup>\uff1b\u7ea2\u8272\uff0cO2-<\/sup>\uff1b\u7c89\u7ea2\u8272\uff0cH+<\/sup>\uff09\u548c\u03b2-Ni(OH)2<\/sub>\uff08\u7070\u8272\uff0cNi2+<\/sup>\uff1b\u7ea2\u8272\uff0cO2<\/sub>\uff1b\u7c89\u7ea2\u8272\uff0cH+<\/sup>\uff09\u7684\u6676\u4f53\u7ed3\u6784\u56fe\uff1b<\/p>\n

\uff08c\uff09\u6c22\u6c27\u5316\u954d\u5728\u5145\/\u653e\u7535\u8fc7\u7a0b\u4e2d\u7684\u7535\u5316\u5b66\u8fc7\u7a0b\u3002<\/p>\n

5.1\u3001\u53cc\u91d1\u5c5eLDH<\/strong><\/p>\n

\u56fe\u516b\u3001NiFe LDH\u7a7a\u5fc3\u5fae\u7403\uff08NiFe LDH HMS\uff09<\/strong>
\n \"\"
\n \uff08a\uff09NiFe LDH HMS\u7684\u5408\u6210\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b~c\uff09NiFe LDH HMS\u7684SEM\u548cTEM\u56fe\uff1b<\/p>\n

\uff08d\uff09NiFe LDH HMS\u548cNiFe LDH NP\u7684N2<\/sub>\u5438\u9644\u7b49\u6e29\u7ebf\u548c\u5b54\u5f84\u5206\u5e03\uff1b<\/p>\n

\uff08e\uff09NiFe LDH HMS\u548cNiFe LDH NP\u7684\u63a5\u89e6\u89d2\u6d4b\u8bd5\uff1b<\/p>\n

\uff08f\uff09NiFe\u4e2d\u7a7a\u7eb3\u7c73\u68f1\u67f1\u7684\u5f62\u6210\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08g~h\uff09\u68f1\u67f1\u72b6Ni\u524d\u4f53\u7684SEM\u548cTEM\u56fe\uff1b<\/p>\n

\uff08i~l\uff09\u4e0d\u540c\u653e\u5927\u500d\u6570\u7684NiFe\u7a7a\u5fc3\u7eb3\u7c73\u68f1\u67f1\u7684SEM\u548cTEM\u56fe\u3002<\/p>\n

\u56fe\u4e5d\u3001CoMn LDH\u8d85\u8584\u7eb3\u7c73\u7247<\/strong>
\n \"\"
\n \uff08a\uff09CoMn LDH\u7684\u539f\u5b50\u6a21\u578b\uff1b<\/p>\n

\uff08b\uff09CoMn LDH\u7684TEM\u56fe\uff1b<\/p>\n

\uff08c\uff09\u4e0d\u540c\u6837\u54c1\u57281 M KOH\u4e2d\u7684\u6781\u5316\u66f2\u7ebf\uff1b<\/p>\n

\uff08d\uff09\u8fc7\u7535\u4f4d\u548c\u7535\u6d41\u5bc6\u5ea6\uff1b<\/p>\n

\uff08e\uff09\u70ad\u5316\u7535\u6d41\u5bc6\u5ea6\u5dee\u4e0e\u626b\u63cf\u901f\u7387\u7684\u5173\u7cfb\uff1b<\/p>\n

\uff08f\uff09\u572810 mA cm\u22122<\/sup>\u8fde\u7eed\u9633\u6781\u6761\u4ef6\u4f5c\u7528\u4e0b\u7684\u6781\u5316\u66f2\u7ebf\uff1b<\/p>\n

\uff08g~h\uff09TEM\u56fe\u548cSAED\u56fe\uff1b<\/p>\n

\uff08i\uff09\u7eb3\u7c73\u7247\u7684AFM\u56fe\u50cf\u548c\u76f8\u5e94\u7684\u9ad8\u5ea6\u5256\u9762\uff1b<\/p>\n

\uff08j\uff09Ni0.75<\/sub>Fe0.25<\/sub> LDH\u548cNi0.75<\/sub>V0.25<\/sub> LDH\u7684Tafel\u56fe\uff1b<\/p>\n

\uff08k\uff09\u4e2d\u95f4\u4ea7\u7269\u5438\u9644\u7684\u81ea\u7531\u80fd\u5206\u5e03\u56fe: H2<\/sub>O\uff0c*OH\uff0c*O\u548c*OOH\u3002<\/p>\n

\u56fe\u5341\u3001NiFe LDH\u50ac\u5316OER\u8fc7\u7a0b\u7814\u7a76<\/strong>
\n \"\"
\n \uff08a\uff09\u5728NiFe LDH \/\u7f9f\u57fa\u6c27\u5316\u7269\u4e0d\u540c\u7535\u4f4d\u4e0b\u4f7f\u7528M\u00f6ssbauer\u8c31\u7684Operando\u5b9e\u9a8c\u7684CV\u6d4b\u8bd5\uff1b<\/p>\n

\uff08b\uff09NiFe LDH\u548c\u542b\u6c34Fe\u6c27\u5316\u7269\u4e2d\u7684\u7535\u5b50\u6548\u5e94\u56fe\uff1b<\/p>\n

\uff08c\uff09\u4e0d\u540c\u6761\u4ef6\u4e0b\u5355\u5c42Ni(OH)2<\/sub>\u7684AFM\u56fe\u50cf\u548c\u7ed3\u6784\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08d\uff09\u626b\u63cf\u901f\u7387\u4e3a50 mV s\u22121<\/sup>\u7684\u5355\u5c42Ni(OH)2<\/sub>\u548c\u57280.1 M KOH\u4e2d\u4e0d\u540c\u94c1\u63ba\u5165\u91cf\u7684Ni(OH)2<\/sub>\u7684CV\u66f2\u7ebf\uff1b<\/p>\n

\uff08e\uff09\u5728\u5faa\u73af\u8fc7\u7a0b\u4e2d\u540e\u7eed\u52a0\u5165\u4e0d\u540c\u91cf\u94c1\u7684\u4f53\u79ef\u53d8\u5316\uff1b<\/p>\n

\uff08f\uff09\u57280.1 M KOH\u548c\u4e0d\u540c\u76f8\u5bf9RHE\u7535\u4f4d\u7684OER\u8fc7\u7a0b\u4e2dNiFe LDH\u7684\u539f\u4f4d\u62c9\u66fc\u5149\u8c31\uff1b<\/p>\n

\uff08g\uff09NiFe LDH\u7684OER\u673a\u5236\u3002<\/p>\n

5.2\u3001\u4e09\u91d1\u5c5eLDH<\/strong><\/p>\n

\u56fe\u5341\u4e00\u3001NiFeV LDH\u7eb3\u7c73\u7247\u9635\u5217<\/strong>
\n \"\"
\n \uff08a\uff09NiFeV LDH\u7ed3\u6784\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b~c\uff09NiFeV LDH\u7eb3\u7c73\u7247\u9635\u5217\u7684SEM\u548cTEM\u56fe\uff1b<\/p>\n

\uff08d\uff09NiFe LDHs\u548cNiFeV LDHs\u76844e\u2212<\/sup> OER\u673a\u5236\uff1b<\/p>\n

\uff08e\uff09\u5728NiFe LDHs\u548cNiFeV LDHs\u4e0aOER\u56db\u4e2a\u6b65\u9aa4\u7684\u5409\u5e03\u65af\u81ea\u7531\u80fd\u56fe\uff1b<\/p>\n

\uff08f\uff09NiFe LDHs\u548cNiFeV LDHs\u7684\u603b\u6001\u5bc6\u5ea6\uff08TDOS\uff09\uff1b<\/p>\n

\uff08g\uff09MoFe:Ni(OH)2<\/sub>\/ NiOOH\u7eb3\u7c73\u7247\u5728\u6ce1\u6cabNi\u4e0a\u7684\u5236\u5907\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08h\uff09\u4ee5\u706b\u5c71\u56fe\u7684\u5f62\u5f0f\u5448\u73b0NiOOH, Fe:NiOOH\u548cMoFe:NiOOH\u7684OER\u6d3b\u6027\uff1b<\/p>\n

\uff08i\uff09NiOOH, Fe:NiOOH\u548cMoFe:NiOOH\u7684\u63ba\u6742\u5f62\u6210\u80fd\u53ca\u5176\u6a21\u578b\u7ed3\u6784\u3002<\/p>\n

5.3\u3001LDHs\u7684\u4e09\u7ef4\u5c42\u7ea7\u590d\u5408\u7eb3\u7c73\u7ed3\u6784<\/strong><\/p>\n

5.3.1\u3001LDH \/\u78b3\u57fa\u6750\u6599\u7684\u4e09\u7ef4\u5c42\u7ea7\u7eb3\u7c73\u7ed3\u6784<\/strong><\/p>\n

5.3.2\u3001LDH \/\u91d1\u5c5e\u57fa\u6750\u6599\u7684\u4e09\u7ef4\u5c42\u7ea7\u7eb3\u7c73\u7ed3\u6784<\/strong><\/p>\n

\u56fe\u5341\u4e8c\u3001\u4e09\u7ef4LDH \/\u91d1\u5c5e\u57fa\u7eb3\u7c73\u7247<\/strong>
\n \"\"
\n \uff08a\uff09\u4e09\u7ef4\u94dc\u7eb3\u7c73\u7ebf@NiFe LDH\u5728\u6ce1\u6cabCu\u4e0a\u7684\u5236\u5907\u5de5\u827a\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b~e\uff09\u4e09\u7ef4\u94dc\u7eb3\u7c73\u7ebf@NiFe LDH\u7684SEM\uff0cTEM\u56fe\u53ca\u5176\u6781\u5316\u66f2\u7ebf\uff1b<\/p>\n

\uff08f\uff09\u590d\u5408\u8868\u9762\u4e0a\u4e0d\u540c\u7535\u4f4d\u4e0b\u5355\u539f\u5b50Au\/NiFe LDH\u7684CO3<\/sub>2\u2212<\/sup>\u53ca\u5c42\u95f4\u6c34\u5206\u5b50\u7684\u5e73\u677f\u6a21\u578b\u3001OER\u8def\u5f84\u548cOER\u81ea\u7531\u80fd\u56fe\uff1b<\/p>\n

\uff08g\uff09TEM\u56fe\uff1b<\/p>\n

\uff08h\uff09HAADF-STEM\u56fe\uff1b<\/p>\n

\uff08i\uff09\u6781\u5316\u66f2\u7ebf\u53ca\u5176\u76f8\u5e94\u7684\u8fc7\u7535\u4f4d\u548cTafel\u659c\u7387\uff1b<\/p>\n

\uff08j\uff09\u542b\u6216\u4e0d\u542b\u91d1\u539f\u5b50\u7684NiFe LDH\u7684\u7535\u8377\u5bc6\u5ea6\u5206\u5e03\u56fe\u3002<\/p>\n

5.3.3\u3001LDH \/\u91d1\u5c5e\u590d\u5408\u7269\u7684\u4e09\u7ef4\u5c42\u7ea7\u7eb3\u7c73\u7ed3\u6784<\/strong><\/p>\n

\u56fe\u5341\u4e09\u3001NiFe LDH\u91d1\u5c5e\u590d\u5408\u7269<\/strong>
\n \"\"
\n \uff08a\uff09NiFe LDH@ NiFe\u78f7\u9178\u76d0\u6742\u5316\u7269\u7684\u5236\u5907\u5de5\u827a\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08b\uff09\u6742\u5316\u7269\u7684SEM\u56fe\uff1b<\/p>\n

\uff08c~d\uff09NiFe LDH\u548cNiFe LDH@NiFe\u78f7\u9178\u76d0\u6742\u5316\u7269\u7684\u63a5\u89e6\u89d2\u6d4b\u91cf\uff1b<\/p>\n

\uff08e~f\uff09\u5916\u52a0\u7535\u538b1.9 V\u4e0b\uff0c\u6c14\u6ce1\u5bf9NiFe LDH\u548cNiFe LDH@NiFe\u78f7\u9178\u76d0\u6742\u5316\u7269\u7684\u5f71\u54cd\uff1b<\/p>\n

\uff08g\uff09FeNi LDH\/Ti3<\/sub>C2<\/sub>\u2013Mxene\u7684\u5f62\u6210\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08h~i\uff09\u590d\u5408\u6750\u6599\u7684SEM\u56fe\u548cTEM\u56fe\uff1b<\/p>\n

\uff08j\uff09\u6781\u5316\u66f2\u7ebf\u53ca\u5176\u76f8\u5e94\u7684\u8fc7\u7535\u4f4d\uff1b<\/p>\n

\uff08k\uff09FeNi LDH\/Ti3<\/sub>C2<\/sub>\u2013Mxene\u6742\u5316\u6a21\u578b\u7ed3\u6784\u7684\u4fef\u89c6\u56fe\u548c\u4fa7\u89c6\u56fe\uff1b<\/p>\n

\uff08l\uff09FeNi LDH\u548cFeNi LDH\/Ti3<\/sub>C2<\/sub>\u2013Mxene\u7684Ni\u548cFe\u57283d\u8f68\u9053\u6001\u5bc6\u5ea6\uff08DOS\uff09\u548c\u9884\u6d4bDOS\uff08PDOS\uff09\uff0c\u865a\u7ebf\u8868\u793ad\u80fd\u5e26\u4e2d\u5fc3\u3002<\/p>\n

6\u3001\u603b\u7ed3\u4e0e\u5c55\u671b<\/strong><\/p>\n

\u603b\u7684\u6765\u8bf4\uff0cLDH\u7531\u4e8e\u5176\u5236\u5907\u5de5\u827a\u7b80\u5355\u3001\u6210\u672c\u4f4e\u3001\u7075\u6d3b\u6027\u597d\u3001\u57fa\u4f53\u91d1\u5c5e\u79bb\u5b50\u53ef\u8c03\u3001\u5c42\u95f4\u9634\u79bb\u5b50\u53ef\u66ff\u4ee3\u7b49\u7279\u70b9\uff0c\u88ab\u8ba4\u4e3a\u662f\u76ee\u524d\u6700\u53d7\u6b22\u8fce\u7684\u9ad8\u6d3b\u6027\u7535\u50ac\u5316OER\u6750\u6599\u4e4b\u4e00\u3002\u5c3d\u7ba1\u6587\u4e2d\u603b\u7ed3\u7684\u5404\u79cd\u6280\u672f\u6781\u5927\u5730\u63d0\u9ad8\u4e86LDHs\u7684\u50ac\u5316\u6d3b\u6027\uff0c\u4f46\u5728\u5f3a\u7535\u6d41\u7535\u89e3\u4e2d\u5bf9OER\u7684\u50ac\u5316\u6027\u80fd\u4ecd\u8fdc\u672a\u80fd\u8fbe\u5230\u9884\u671f\uff0c\u4e14\u4e0d\u53ef\u9006\u526f\u53cd\u5e94\u4e5f\u4f1a\u5bfc\u81f4\u5176\u8010\u4e45\u6027\u5dee\uff0c\u8fd9\u4e9b\u7f3a\u9677\u4f7f\u5176\u4e0d\u80fd\u6ee1\u8db3\u5b9e\u9645\u5e94\u7528\u5de5\u4e1a\u5316\u7684\u8981\u6c42\u3002\u56e0\u6b64\uff0c\u4f5c\u8005\u6307\u51fa\u5bf9\u4e8eLDHs\u7684\u5c42\u538b\u7ed3\u6784\uff0c\u7406\u89e3\u5176\u4e3b\u4f53\u5c42\u4e2d\u91d1\u5c5e\u7ec4\u5206\u4e0e\u6d3b\u6027\u4f4d\u70b9\u4e4b\u95f4\u7684\u5173\u7cfb\uff0c\u4ee5\u53ca\u5c42\u95f4\u9634\u79bb\u5b50\u5bf9\u50ac\u5316\u6d3b\u6027\u7684\u5f71\u54cd\u662f\u81f3\u5173\u91cd\u8981\u548c\u6781\u5177\u6311\u6218\u6027\u7684\u3002\u5c3d\u7ba1\u901a\u8fc7\u64cd\u7eb5\u5c42\u538b\u7ed3\u6784\u8c03\u8282LDH\u7684\u7535\u5b50\u7ed3\u6784\u662f\u4e00\u4e2a\u5de8\u5927\u7684\u6311\u6218\uff0c\u4f46\u4f5c\u8005\u8ba4\u4e3a\u4ee5\u6b64\u6765\u5b9e\u73b0\u5bf9\u6d3b\u6027\u4f4d\u70b9\u7684\u7c7b\u578b\u548c\u6570\u91cf\u7684\u63a7\u5236\u4ee5\u53ca\u63d0\u9ad8\u76f8\u5e94\u7684\u50ac\u5316\u52a8\u529b\u5b66\u4ecd\u662f\u53ef\u884c\u7684\u3002\u6b64\u5916\uff0c\u7814\u7a76OER\u50ac\u5316\u8fc7\u7a0b\u4e2dLDHs\u4e2d\u7684\u7ec4\u5206\u53d8\u5316\u548c\u91d1\u5c5e\u79bb\u5b50\u5316\u5b66\u72b6\u6001\u8f6c\u53d8\uff0c\u6709\u52a9\u4e8e\u786e\u5b9a\u8fd9\u4e9b\u4f4d\u70b9\u7684\u771f\u6b63\u6d3b\u6027\u4f4d\u70b9\u6216\u8f6c\u53d8\u7684\u6d3b\u6027\u4f4d\u70b9\u3002\u867d\u7136\u4ee5\u6b64\u6765\u76d1\u6d4bLDH\u5411OER\u7684\u7535\u89e3\u8fc7\u7a0b\uff0c\u5bf9\u4e8e\u6307\u5bfc\u6574\u4e2aOER\u8fc7\u7a0b\u4e2d\u7684\u53cd\u5e94\u662f\u76ee\u524d\u5f88\u96be\u5b9e\u73b0\u7684\uff0c\u4f46\u4e3a\u4e86\u907f\u514d\u526f\u53cd\u5e94\u53d1\u751f\u548c\u83b7\u5f97\u66f4\u957f\u4e45\u7684\u8010\u4e45\u6027\u7535\u50ac\u5316\u5242\uff0c\u5b9e\u73b0\u5176\u5de5\u4e1a\u5316\u5b9e\u9645\u5e94\u7528\u662f\u975e\u5e38\u6709\u610f\u4e49\u7684\u3002<\/p>\n

\n \u6587\u732e\u94fe\u63a5\uff1a2D Layered Double Hydroxides for Oxygen Evolution Reaction: From Fundamental Design to Application<\/a>\uff08Adv. Energy Mater.<\/em> 2019,<\/strong> 1803358\uff09<\/p>\n

\u3010\u901a\u8baf\u4f5c\u8005\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u738b\u6625\u680b\uff0c\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u526f\u6559\u6388\u3001\u535a\u58eb\u751f\u5bfc\u5e08\u3002<\/strong>2013 \u5e74\u6bd5\u4e1a\u4e8e\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\u7269\u7406\u4e0e\u6750\u6599\u79d1\u5b66\u7cfb\uff0c\u83b7\u5f97\u535a\u58eb\u5b66\u4f4d\uff1b 2013 \u5e74-2015 \u5e74\u5148\u540e\u5728\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\uff0c\u6bd4\u5229\u65f6\u8377\u8bed\u9c81\u6c76\u5927\u5b66\u62c5\u4efb\u9ad8\u7ea7\u52a9\u7406\u7814\u7a76\u5458\uff0c\u9ad8\u7ea7\u526f\u7814\u7a76\u5458\uff0c\u9c81\u6c76\u5927\u5b66 F+\u7814\u7a76\u5458\uff0c\u6bd4\u5229\u65f6FWO\u56fd\u5bb6\u535a\u58eb\u540e\u30022015 \u5e74\u52a0\u5165\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u5149\u5b66\u4e0e\u7535\u5b50\u4fe1\u606f\u5b66\u9662\uff0c\u4efb\u526f\u6559\u6388\u81f3\u4eca\u30022013\u5e74\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\u4f18\u79c0\u535a\u58eb\u8bba\u6587\u5956\u83b7\u5f97\u8005\uff0c2015\u5e74\u83b7\u8bc4\u6e56\u5317\u7701\u201c\u695a\u5929\u5b66\u8005\u201d\u8ba1\u5212\u695a\u5929\u5b66\u5b50\uff0c2019\u5e74\u5165\u9009\u6fb3\u95e8\u5927\u5b66\u6770\u51fa\u8bbf\u95ee\u5b66\u8005\uff08\u6fb3\u95e8\u5927\u5b66\u4eba\u624d\u8ba1\u5212\uff09\uff0c\u56fd\u5bb6\u91cd\u70b9\u7814\u53d1\u8ba1\u5212\uff08\u56fd\u9645\u5408\u4f5c\u91cd\u70b9\u4e13\u9879\uff09\u9879\u76ee\u8d1f\u8d23\u4eba\u3002\u4e3b\u8981\u7814\u7a76\u65b9\u5411\u662f\u975e\u8d35\u91d1\u5c5e\u7535\u50ac\u5316\u5242\u8bbe\u8ba1\u53ca\u5e94\u7528\u7814\u7a76\u3002\u5728Angew. Chem. Int. Ed.\u7b49\u56fd\u9645\u520a\u7269\u53d1\u8868SCI\u8bba\u6587100\u4f59\u7bc7\u3002
\n \u738b\u6625\u680b\u8bfe\u9898\u7ec4\u4e3b\u9875\uff1ahttps:\/\/apcdwang.wixsite.com\/hust-cdwang<\/a><\/p>\n

\u8fd1\u671f\u7535\u50ac\u5316\u65b9\u5411\u4ee3\u8868\u6027\u5de5\u4f5c\u6709\uff1a
\n 1. J.G. Li, H.C. Sun, L. Lv, Z.S. Li, X. Ao, C.H. Xu,Y. Li, C.D. Wang*<\/strong>, Metal-Organic Framework-Derived Hierarchical (Co, Ni)Se2@NiFe LDH Hollow Nanocages for Enhanced Oxygen Evolution, ACS Appl. Mater. Interf.<\/em><\/strong>\uff0c2019, 11, 8106-8114.
\n 2. J.-Y. Zhang, H.M. Wang, Y.F. Tian, Y. Yan, Q. Xue, T. He, H.F. Liu, C.D. Wang,*<\/strong> Y. Chen,* and B.Y. Xia*,Anodic Hydrazine Oxidation Assists Energy-Efficient Hydrogen Evolution over a Bifunctional Cobalt Perselenide Nanosheet Electrode, Angew. Chem. Int. Ed.<\/strong> <\/em>2018, 130, 7775-7779.
\n 3. L. Lv, D.C. Zha, Y.J. Ruan, Z.S. Li, X. Ao, J. Zheng, J.J. Jiang, H.M. Chen, W.H. Chiang, J. Chen*, C.D. Wang*<\/strong>, A Universal Method to Engineer Metal Oxide-Metal-Carbon Interface for Highly Efficient Oxygen Reduction, ACS Nano,<\/em><\/strong> 2018, 12(3), 3042-3051.
\n 4. L. Lv, Z.S. Li, K.H. Xue*, Y.J. Ruan, X. Ao, H.Z. Wan, X.S. Miao, B.S. Zhang, J.J. Jiang, C.D. Wang*<\/strong>, K. Ostrikove, Tailoring the electrocatalytic activity of bimetallic nickel-iron diselenide hollow nanochains for water oxidation, Nano Energy,<\/strong> <\/em>2018, 47, 275-284.
\n 5. Z.S. Li, L. Lv, J.S. Wang, X. Ao, Y.J. Ruan, D.C. Zha, G. Hong, Q.-H. Wu, Y.C. Lan, C.D. Wang*<\/strong>, J.J. Jiang, M.L. Liu*, Engineering phosphorus-doped LaFeO3-\u03b4 perovskite oxide as robust bifunctional oxygen electrocatalysts in alkaline solutions, Nano Energy,<\/em><\/strong> 2018, 47, 199-209.
\n 6. Z.X. Yang, J.-Y. Zhang, Z.Y. Liu, Z.S. Li, L. Lv, X. Ao, Y.F. Tian, Y. Zhang*, J.J. Jiang, C.D. Wang*<\/strong>, \u201cCuju\u201d-Structured Iron Diselenide-Derived Oxide: A Highly Efficient Electrocatalyst for Water Oxidation, ACS Appl. Mater. Interf.,<\/em><\/strong> 2017, 9, 40351-40359.
\n 7. J.-Y. Zhang, L. Lv, Y.F. Tian, Z.S. Li, X. Ao, Y.C. Lan, J.J. Jiang*, C.D. Wang*<\/strong>, Rational Design of Cobalt-Iron Selenides for Highly Efficient Electrochemical Water Oxidation, ACS Appl. Mater. Interf.,<\/em><\/strong> 2017, 9, 33833-33840.<\/p>\n

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\n \u718a\u5b87\u6770\u8bfe\u9898\u7ec4\u4e3b\u9875\uff1ahttp:\/\/staff.ustc.edu.cn\/~yjxiong\/chinese.html<\/a><\/p>\n

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\n Li, Y.; Chen, S.; Xi, D.; Bo, Y.; Long, R.; Wang, C.; Song, L. and Xiong, Y.*<\/strong>, Scalable Fabrication of Highly Active and Durable Membrane Electrodes toward Water Oxidation, Small<\/strong> <\/em>14, 1702109 (2018).<\/p>\n

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