{"id":164565,"date":"2019-01-14T12:00:25","date_gmt":"2019-01-14T04:00:25","guid":{"rendered":"\/\/m.iemloyee.com\/?p=164565"},"modified":"2019-01-13T17:02:47","modified_gmt":"2019-01-13T09:02:47","slug":"%e5%8c%97%e7%90%86%e5%b7%a5%e6%9d%8e%e7%85%9c%e7%92%9fadv-funct-mater-%e9%92%a8%e6%8e%ba%e6%9d%82%e8%af%b1%e5%af%bc%e5%a4%9a%e5%ad%94%e4%b8%89%e5%85%83%e9%93%82%e5%9f%ba%e5%90%88%e9%87%91","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=164565","title":{"rendered":"\u5317\u7406\u5de5\u674e\u715c\u749fAdv. Funct. Mater. : \u94a8\u63ba\u6742\u8bf1\u5bfc\u591a\u5b54\u4e09\u5143\u94c2\u57fa\u5408\u91d1\u7535\u50ac\u5316\u5242\u7684\u8868\u9762\u91cd\u6784"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\n \u63d0\u9ad8ORR\u50ac\u5316\u5242\u7684\u6d3b\u6027\u548c\u7a33\u5b9a\u6027\u662f\u5f00\u53d1\u7528\u4e8e\u8d28\u5b50\u4ea4\u6362\u819c\u71c3\u6599\u7535\u6c60(PEMFCs)\u7684\u9ad8\u6027\u80fd\u819c\u7535\u6781\u7ec4\u4ef6(MEA)\u6240\u9762\u4e34\u7684\u4e3b\u8981\u6311\u6218\u3002\u957f\u671f\u4ee5\u6765\uff0c\u94a8\u57fa\u6750\u6599\u4e00\u76f4\u88ab\u8ba4\u4e3a\u662fPEMFC\u4e2d\u7684\u6f5c\u5728\u7535\u6781\u6750\u6599\u3002\u94a8\u57fa\u6750\u6599\u4f5c\u4e3a\u826f\u597d\u7684ORR\u7535\u6781\u6750\u6599\u5177\u6709\u5982\u4e0b\u4e24\u4e2a\u7279\u5f81\uff1a1) \u5f53\u4e0e\u6c27\u3001\u78b3\u6216\u91d1\u5c5e\u539f\u5b50\u5f62\u6210\u5316\u5b66\u952e\u65f6\uff0c\u94a8\u5728\u9178\u6027\u73af\u5883\u4e2d\u7684\u5316\u5b66\u7a33\u5b9a\u6027\u597d\uff1b2) \u5373\u4f7f\u6eb6\u89e3\u5e76\u6269\u6563\u5230\u9633\u6781\u4fa7\uff0c\u5bf9\u9633\u6781\u4e2d\u6bd2\u7684\u8010\u53d7\u6027\u4e5f\u5f88\u9ad8\u3002\u636e\u62a5\u9053\uff0c\u57fa\u4e8ePtW\u7684\u53cc\u91d1\u5c5e\u5408\u91d1\u867d\u7136\u6d3b\u6027\u5c1a\u5dee\u5f3a\u4eba\u610f\uff0c\u4f46\u8868\u73b0\u51fa\u5bf9\u6eb6\u89e3\u548c\u6d3b\u6027\u4e0b\u964d\u7684\u9ad8\u7a33\u5b9a\u6027\u3002\u7136\u800c\u5229\u7528\u6e7f\u5316\u5b66\u5408\u6210\u6cd5\uff0c\u51e0\u4e4e\u4e0d\u53ef\u80fd\u5c06W\u539f\u5b50\u7ed3\u5408\u5230\u7eb3\u7c73\u6676\u4f53\u4e2d\uff0c\u56e0\u4e3a\u5373\u4f7f\u7528\u5f3a\u8fd8\u539f\u5242\u4e5f\u5bb9\u6613\u5c06W(0)\u539f\u5b50\u6c27\u5316\u3002\u901a\u5e38\u9700\u8981\u9ad8\u6e29\u7145\u70e7\u6765\u514b\u670d\u5408\u91d1\u5f62\u6210\u7684\u80fd\u5792\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\n \u8fd1\u65e5\uff0c\u5317\u4eac\u7406\u5de5\u5927\u5b66\u674e\u715c\u749f\u6559\u6388(\u901a\u8baf\u4f5c\u8005)\u7b49<\/strong>\u4ee5PtCux<\/sub>Ni\u4e09\u5143\u5408\u91d1\u7eb3\u7c73\u6676(NC)\u4f5c\u4e3a\u6a21\u578b\u50ac\u5316\u5242\uff0c\u5229\u7528\u8868\u9762\u94a8(W)\u63ba\u6742\u7b56\u7565\u7ed3\u5408\u8868\u9762\u6c27\u5316\u9178\u5904\u7406\u53ef\u6709\u6548\u63d0\u9ad8NCs\u5728\u6c27\u8fd8\u539f\u53cd\u5e94\u4e2d\u7684\u7535\u50ac\u5316\u6d3b\u6027\uff0c\u5e76\u5728Adv. Funct. Mater.<\/strong>\u4e0a\u53d1\u8868\u4e86\u9898\u4e3a\u201cTungsten-Doping-Induced Surface Reconstruction of Porous Ternary Pt-Based Alloy Electrocatalyst for Oxygen Reduction<\/strong>\u201d\u7684\u7814\u7a76\u8bba\u6587\u3002\u4e0e\u672a\u63ba\u6742\u7684\u50ac\u5316\u5242\u76f8\u6bd4\uff0cW\u63ba\u6742\u7684PtCux<\/sub>Ni\u5408\u91d1\u50ac\u5316\u5242\u5728\u7535\u5316\u5b66\u8868\u9762\u79ef\u548c\u8d28\u91cf\u6d3b\u6027\u65b9\u9762\u8868\u73b0\u51fa\u660e\u663e\u7684\u589e\u5f3a\uff0c\u4e14\u6bd4\u6d3b\u6027\u7565\u6709\u589e\u5f3a\u3002\u57fa\u4e8e\u5b9e\u9a8c\u8bc1\u636e\uff0c\u4f5c\u8005\u63d0\u51faW\u63ba\u6742\u6d89\u53ca\u9996\u5148\u4eceNC\u53bb\u9664\u8868\u9762Pt\u539f\u5b50\u7136\u540e\u5c06\u5176\u8fd8\u539f\u81f3\u8868\u9762\u7684\u8868\u9762\u91cd\u6784\u3002\u8868\u9762Ni\u539f\u5b50\u7684\u5b58\u5728\u5bf9\u4e8e\u4fc3\u8fdb\u50ac\u5316\u6d3b\u6027\u53ef\u80fd\u662f\u81f3\u5173\u91cd\u8981\u7684\uff0c\u53ef\u80fd\u662f\u901a\u8fc7\u5176\u4e0e\u6d3b\u6027\u4f4d\u70b9\u7684\u7535\u5b50\u76f8\u4e92\u4f5c\u7528\u3002W\u63ba\u6742\u7684PtCux<\/sub>Ni\u50ac\u5316\u5242\u7684\u957f\u6548\u6027\u4e5f\u53ef\u80fd\u7531\u4e8e\u8868\u9762W\u539f\u5b50\u7684\u9489\u624e\u6548\u5e94\u800c\u589e\u5f3a\u3002\u56e0\u6b64\uff0cW\u539f\u5b50\u63ba\u6742PtCux<\/sub>Ni\u4e09\u5143\u5408\u91d1\u53ef\u6709\u6548\u5730\u8c03\u8282\u5176\u6d3b\u6027\u548c\u8010\u4e45\u6027\u3002<\/p>\n

\u3010\u56fe\u6587\u7b80\u4ecb\u3011<\/strong>
\n \u56fe1 \u4e0d\u540cPt\/Cu\/Ni\u6bd4\u7684PtCux<\/sub>Ni-r NCs\u5f62\u8c8c<\/strong><\/p>\n

\"\"<\/p>\n

a,b) Pt\/Cu\/Ni\u6bd4\u4e3a1\/1\/1\u7684PtCuxNi-r NCs(111-PtCuNi-r) TEM\u56fe\u50cf\uff1b
\n c,d) Pt\/Cu\/Ni\u6bd4\u4e3a1\/2\/1\u7684PtCuxNi-r NCs (121-PtCuNi-r) TEM\u56fe\u50cf\uff1b
\n e,f) Pt\/Cu\/Ni\u6bd4\u4e3a1\/3\/1\u7684PtCuxNi-r NCs (131-PtCuNi-r) TEM\u56fe\u50cf\u3002<\/p>\n

\u56fe2 \u9178\u5904\u7406\u548cW\u63ba\u6742\u8fc7\u7a0b\u4e2d\u7684\u5f62\u8c8c\u6f14\u53d8<\/strong><\/p>\n

\"\"<\/p>\n

\u9178\u5904\u7406\u548cW\u63ba\u6742\u8fc7\u7a0b\u4e2d\u5f62\u8c8c\u6f14\u53d8\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe3 131-PtCuNi-t\u548c131-PtCuNi-W NCs\u7684\u5f62\u8c8c<\/strong><\/p>\n

\"\"<\/p>\n

a,f) 131-PtCuNi-t\u548c131-PtCuNi-W NCs\u7684\u9ad8\u5206\u8fa8\u7387TEM\u56fe\u50cf\uff1b
\n b,c) 131-PtCuNi-t\u548c131-PtCuNi-W NCs\u7684FFT\u56fe\u50cf\uff1b
\n d,g) 131-PtCuNi-t\u548c131-PtCuNi-W NCs \u7684HAADF-STEM\u56fe\u50cf\uff1b
\n e,h) 131-PtCuNi-t\u548c131-PtCuNi-W NCs\u7684Pt\u3001Cu\u3001Ni\u548cW\u5143\u7d20\u5206\u5e03\u56fe\u50cf\u3002<\/p>\n

\u56fe4 \u4e0d\u540cPt\/Cu\/Ni\u6bd4\u7684PtCuxNi NCs\u7684\u7ed3\u6784\u4e0e\u7ec4\u6210<\/strong><\/p>\n

\"\"<\/p>\n

a) \u5408\u6210\u7684111-\u3001121-\u548c131-PtCuNi NC\u7684XRD\u56fe\u8c31\uff1b
\n b) \u901a\u8fc7ICP\u6d4b\u5b9a\u7684\u4e0a\u8ff0\u50ac\u5316\u5242\u548cW\u63ba\u6742\u50ac\u5316\u5242\u7684\u7ec4\u6210\u3002<\/p>\n

\u56fe5 \u4e0d\u540c\u7ec4\u6210PtCuNi\/C\u9178\u5904\u7406\u524d\u540e\u7684\u7535\u5316\u5b66\u6d3b\u6027\u6bd4\u8f83<\/strong><\/p>\n

\"\"<\/p>\n

a,b) \u9178\u5904\u7406\u524d(\u6df1\u9ec4\u8272)\u540e(\u7ea2\u8272)\u7684111-PtCuNi\/C\u50ac\u5316\u5242\u7684CV\u548cLSV\u66f2\u7ebf\uff0cb\u56fe\u5185\u63d2\u4e3a\u76f8\u5e94LSV\u66f2\u7ebf\u7684Tafel\u56fe\uff1b
\n c,d) \u9178\u5904\u7406\u540e\u7684111-PtCuNi-t\/C(\u7ea2\u8272)\u3001121-PtCuNi-t\/C(\u84dd\u8272)\u548c131-PtCuNi-t\/C(\u6a44\u6984\u8272)\u50ac\u5316\u5242\u7684CV\u548cLSV\u3002<\/p>\n

\u56fe6 PtCuNi-W NCs\u7684\u7535\u5316\u5b66\u6d3b\u6027\u6bd4\u8f83<\/strong><\/p>\n

\"\"<\/p>\n

a,b) W\u63ba\u6742\u524d(\u7ea2\u8272)\u540e(\u7d2b\u8272)\u7684111-PtCuNi\/C\u50ac\u5316\u5242\u7684CV\u548cLSV\u66f2\u7ebf\uff1b
\n c,d) \u9178\u5904\u7406\u540e111-PtCuNi-W\/C(\u7d2b\u7f57\u5170)\u3001121-PtCuNi-W\/C(\u6d77\u519b\u84dd)\u548c131-PtCuNi-W\/C(\u6df1\u9752\u8272)\u50ac\u5316\u5242\u7684CV\u548cLSV\u66f2\u7ebf\u3002<\/p>\n

\u56fe7 W\u63ba\u6742\u8fc7\u7a0b\u4e2d\u7684\u8868\u9762\u91cd\u6784<\/strong><\/p>\n

\"\"<\/p>\n

a,b) \u63ba\u674212\u300124\u548c48 h\u540e111-PtCuNi-W\/C\u7684LSV\u548cCV\u66f2\u7ebf\uff1b
\n c) \u4e0a\u8ff0\u50ac\u5316\u5242ECSA\u3001MA\u548cSA\u7684\u603b\u7ed3\u6bd4\u8f83\uff1b
\n d) \u4e0d\u540c(W\u524d\u9a71\u4f53)\u63ba\u6742\u91cf\u6216\u4fdd\u6e29(\u65e0W\u524d\u9a71\u4f53)\u65f6\u95f4(12\u548c24 h)\u68c0\u6d4b\u53cd\u5e94\u6eb6\u6db2\u4e0a\u6e05\u6db2\u4e2d\u7684Pt\u3001Cu\u3001Ni\u548cW\u7684\u542b\u91cf\uff1b
\n e) \u8868\u9762\u91cd\u6784\u7684\u793a\u610f\u56fe\u3002<\/p>\n

\u56fe8 PtCuNi-W NCs\u7684\u7a33\u5b9a\u6027\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/p>\n

a) 111-PtCuNi-W\/C\u7684\u521d\u59cb\u548c\u7b2c20000\u6b21\u5faa\u73afCV\u66f2\u7ebf\uff1b
\n b) 111-PtCuNi-t\/C\u3001111-PtCuNi-W\/C\u548cJM Pt\/C\u7684ECSAs\u53d8\u5316\uff1b
\n c) 111-PtCuNi-W\/C\u7684\u521d\u59cb\u548c20000\u6b21\u5faa\u73afCV\u66f2\u7ebf\u76f8\u5e94\u7684LSV\u66f2\u7ebf\uff1b
\n d) \u4e09\u79cd\u50ac\u5316\u5242\u7684SA\u548cMA\u7684\u53d8\u5316\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\n \u7efc\u4e0a\u6240\u8ff0\uff0c\u4f5c\u8005\u9996\u5148\u901a\u8fc7\u6c27\u5316\u9178\u5904\u7406\u5236\u5907\u4e86\u9ad8\u6027\u80fd\u591a\u5b54PtCuNi\u4e09\u5143\u5408\u91d1\u50ac\u5316\u5242\u3002\u8be5\u5904\u7406\u6709\u6548\u5730\u53bb\u9664\u6709\u673a\u8986\u76d6\u5206\u5b50\u5e76\u8680\u523bNi\u539f\u5b50\u4ee5\u5f62\u6210\u591a\u5b54\u5f62\u6001\uff0c\u56e0\u6b64\u6539\u5584\u4e86\u7535\u50ac\u5316ORR\u6d3b\u6027\u3002\u4e4b\u540e\u901a\u8fc7W\u539f\u5b50\u8868\u9762\u63ba\u6742\u53ef\u4ee5\u8fdb\u4e00\u6b65\u63d0\u9ad8\u50ac\u5316\u6d3b\u6027\u548c\u957f\u6548\u6027\u3002\u63ba\u6742\u8fc7\u7a0b\u6d89\u53ca\u8868\u9762\u91cd\u6784\uff0c\u5176\u4e2dPt\u539f\u5b50\u9996\u5148\u6eb6\u89e3\u7136\u540e\u5438\u9644\u4e8eNC\u8868\u9762\uff0c\u540c\u65f6\u8868\u9762Ni\u539f\u5b50\u6301\u7eed\u6eb6\u89e3\uff0c\u8be5\u8fc7\u7a0b\u4ea7\u751f\u4e86\u66f4\u591a\u7684\u50ac\u5316\u6d3b\u6027\u8868\u9762\u4f4d\u70b9\u5e76\u589e\u52a0ECSA\u3002\u9002\u91cf\u7684Ni\u539f\u5b50\u5bf9\u4e8e\u6d3b\u6027\u589e\u5f3a\u662f\u5fc5\u4e0d\u53ef\u5c11\u7684\uff0c\u8fd9\u53ef\u80fd\u6e90\u4e8eNi\u4e0e\u5305\u62ecPt\u3001W\u548cNi\u539f\u5b50\u7684\u6d3b\u6027\u8868\u9762\u4f4d\u70b9\u4e4b\u95f4\u7684\u534f\u540c\u76f8\u4e92\u4f5c\u7528\u3002\u56e0\u6b64\uff0cW\u63ba\u6742\u548c\u6c27\u5316\u5904\u7406\u53ef\u4f5c\u4e3a\u4e00\u79cd\u589e\u5f3a\u4e8c\u5143\u6216\u4e09\u5143Pt\u57fa\u5408\u91d1ORR\u50ac\u5316\u5242\u6d3b\u6027\u548c\u8010\u4e45\u6027\u7684\u6709\u6548 \u7b56\u7565\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a\u00a0Tungsten-Doping-Induced Surface Reconstruction of Porous Ternary Pt-Based Alloy Electrocatalyst for Oxygen Reduction<\/a> <\/strong>(Adv. Funct. Mater.<\/strong>, 2019, DOI: 10.1002\/adfm.201807070)<\/p>\n

\n \u3010\u7814\u7a76\u56e2\u961f\u4ecb\u7ecd\u3011<\/strong><\/p>\n

\u674e\u715c\u749f<\/strong>\uff0c\u5317\u4eac\u7406\u5de5\u5927\u5b66\u6750\u6599\u5b66\u9662\u7279\u522b\u7814\u7a76\u5458\uff0c\u535a\u58eb\u751f\u5bfc\u5e08\u3002
\n \u4e3b\u8981\u7814\u7a76\u65b9\u5411\u4e3a\u8d35\u91d1\u5c5e\u5408\u91d1\u53ca\u65e0\u673a\u7eb3\u7c73\u6676\u4f53\u7684\u53ef\u63a7\u5236\u5907\u53ca\u6750\u6599\u5728\u7535\u50ac\u5316\u3001\u5149\u7535\u8f6c\u6362\u8fc7\u7a0b\u4e2d\u7684\u754c\u9762\u73b0\u8c61\u4e0e\u673a\u5236\uff0c\u5728Nature Chemistry\u3001Angewandte\u3001Nano Lett\u7b49\u671f\u520a\u53d1\u8868\u8bba\u658750\u4f59\u7bc7\uff0c\u4ee5\u7b2c\u4e00\u4f5c\u8005\u5728JACS\u3001Advanced Materials\u7b49\u671f\u520a\u53d1\u8868\u8bba\u658710\u7bc7\uff0c\u4e3b\u6301\u56fd\u5bb6\u81ea\u7136\u79d1\u5b66\u57fa\u91d1\u3001\u6559\u80b2\u90e8\u535a\u58eb\u70b9\u57fa\u91d1\u7b49\u3002
\n \u4e2a\u4eba\u4e3b\u9875\uff1ahttp:\/\/teacher.bit.edu.cn\/yjli\/index.htm<\/a><\/strong>
\n \u9ec4\u6631<\/strong>\uff0c\u52a0\u5dde\u5927\u5b66\u6d1b\u6749\u77f6\u5206\u6821\u6750\u6599\u79d1\u5b66\u4e0e\u5de5\u7a0b\u7cfb\u6559\u6388\uff0c\u535a\u58eb\u751f\u5bfc\u5e08\u3002
\n \u8bfe\u9898\u7ec4\u4e3b\u9875\uff1ahttp:\/\/yhuang.seas.ucla.edu\/<\/a><\/strong><\/p>\n

\u3010\u56e2\u961f\u5176\u4ed6\u76f8\u5173\u6587\u7ae0\u3011<\/strong><\/p>\n

1. H. Wang, W. Luo, L. Zhu, Z. Zhao, B. E, W. Tu, X. Ke, M. Sui, C. Chen, Q. Chen, Y. Li,* and Y. Huang*. Synergistically Enhanced Oxygen Reduction Electrocatalysis by Subsurface Atoms in Ternary PdCuNi Alloy Catalysts<\/a><\/strong>. Adv. Funct. Mater.<\/strong>, 2018, 1707219<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7f16\u8f91\u90e8\u65b0\u80fd\u6e90\u5c0f\u7ec4abc940504\u3010\u8096\u6770\u3011\u7f16\u8bd1\u6574\u7406\uff0c\u53c2\u4e0e\u65b0\u80fd\u6e90\u8bdd\u9898\u8ba8\u8bba\u8bf7\u52a0\u5165\u201c\u6750\u6599\u4eba\u65b0\u80fd\u6e90\u6750\u6599\u4ea4\u6d41\u7fa4 422065953\u201d\u3002<\/p>\n

\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1acailiaokefu\uff0c\u6211\u4eec\u4f1a\u9080\u8bf7\u5404\u4f4d\u8001\u5e08\u52a0\u5165\u4e13\u5bb6\u7fa4\u3002<\/strong><\/p>\n

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