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\/><\/p>\n<p>2.3\u00a0\u71c3\u70e7\u5206\u6790\u6cd5<\/p>\n<p>\u71c3\u70e7\u5206\u6790\u5c31\u662f\u5c06\u6837\u54c1\u5728\u8fc7\u91cf\u6c27\u6c14\u4e2d\u8fdb\u884c\u71c3\u70e7\uff0c\u6837\u54c1\u7ecf\u9ad8\u6e29\u6c27\u5316\u71c3\u70e7\u751f\u6210\u6c2e\u6c14\u3001\u6c2e\u7684\u6c27\u5316\u7269\u3001\u4e8c\u6c27\u5316\u78b3\u3001\u4e8c\u6c27\u5316\u786b\u548c\u6c34\u7b49\uff0c\u5e76\u5728\u8f7d\u6c14\u7684\u63a8\u52a8\u4e0b\uff0c\u8fdb\u5165\u5206\u79bb\u68c0\u6d4b\u5355\u5143\u3002\u8be5\u6cd5\u901a\u5e38\u7528\u4e8e\u6d4b\u91cf\u6709\u673a\u5316\u5408\u7269\u4e2d\u7684C\u3001H\u3001O\u3001N\u548cS<sup>[4]<\/sup>\u3002\u73b0\u4ee3\u6709\u673a\u5143\u7d20\u5206\u6790\u4eea\uff08Elemental\u00a0analysis\uff0c\u7b80\u79f0EA\uff09\u5c31\u662f\u636e\u6b64\u5236\u9020\u7684\uff0c\u4e0e\u4f20\u7edf\u7684\u5316\u5b66\u5143\u7d20\u5206\u6790\u65b9\u6cd5\u76f8\u6bd4\uff0c\u5143\u7d20\u5206\u6790\u4eea\u81ea\u52a8\u5316\u7a0b\u5ea6\u9ad8\uff0c\u64cd\u4f5c\u7b80\u4fbf\u8fc5\u901f\uff0c\u6d4b\u91cfC\u3001H\u3001N\u3001S\u65f6\u7684\u7cbe\u786e\u5ea6\u5747\u5c0f\u4e8e0.2%\uff0c\u5df2\u9010\u6e10\u6210\u4e3a\u5143\u7d20\u5206\u6790\u7684\u4e3b\u8981\u65b9\u6cd5\u4e4b\u4e00\u3002\u9700\u8981\u6ce8\u610f\u7684\u662f\uff0c\u7531\u4e8e\u5438\u9644\u6c34\u7684\u5b58\u5728\uff0c\u6837\u54c1\u4e2dH\u548cO\u7684\u542b\u91cf\u901a\u5e38\u96be\u4ee5\u6d4b\u51c6\u3002\u6b64\u5916\uff0c\u7531\u4e8e\u662f\u91c7\u7528\u71c3\u70e7\u7684\u65b9\u5f0f\u8fdb\u884c\u6837\u54c1\u5904\u7406\uff0c\u56e0\u6b64\uff0c\u6613\u7206\u70b8\u7684\u6837\u54c1\u6d4b\u8bd5\u65f6\u4e5f\u9700\u8981\u7279\u522b\u6ce8\u610f\u3002<\/p>\n<p>\u56fe4\u00a0\u6709\u673a\u5143\u7d20\u5206\u6790\u7684\u539f\u7406<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"wp-image-161578 size-full aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72473-7.png\" alt=\"\" width=\"600\" height=\"305\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72473-7.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72473-7-300x153.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>LiFePO<sub>4<\/sub>\u662f\u4e00\u79cd\u5177\u6709\u8f83\u5927\u53d1\u5c55\u6f5c\u529b\u7684\u9502\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u6750\u6599\uff0c\u4f46\u662f\u5176\u8f83\u4f4e\u7684\u7535\u5b50\u7535\u5bfc\u7387\u963b\u788d\u4e86\u5176\u6027\u80fd\u7684\u53d1\u6325\u3002\u4e3a\u4e86\u63d0\u9ad8\u9502\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u6750\u6599LiFePO<sub>4<\/sub>\u7684\u7535\u5b50\u7535\u5bfc\u7387\uff0c\u4eba\u4eec\u5e38\u5e38\u5728\u5176\u8868\u9762\u5305\u8986\u78b3\u3002\u7136\u800c\u4e0d\u540c\u7684\u78b3\u542b\u91cf\u5bf9\u5176\u7535\u6c60\u6750\u6599\u7684\u6027\u80fd\u6709\u7740\u8f83\u5927\u7684\u5f71\u54cd<sup>[<\/sup><sup>9<\/sup><sup>]<\/sup>\uff0c\u56e0\u6b64\u6d4b\u91cf\u6240\u5408\u6210\u6750\u6599\u7684\u78b3\u542b\u91cf\u5c31\u663e\u5f97\u5f88\u91cd\u8981\u3002Jing Du\u7b49<sup>[<\/sup><sup>10<\/sup><sup>]<\/sup>\u5c31\u5229\u7528CHS\u5143\u7d20\u5206\u6790\u4eea\u5bf9\u5176\u5236\u5907\u7684\u591a\u5b54\u7684\u78b3\u5305\u8986\u7684LiFePO<sub>4<\/sub>\u4e2d\u7684\u78b3\u542b\u91cf\u8fdb\u884c\u4e86\u6d4b\u5b9a\uff0c\u7ed3\u679c\u663e\u793aC\u542b\u91cf\u4e3a6.5 wt%\u3002\u6b64\u5916\uff0c\u5143\u7d20\u5206\u6790\u4e5f\u5e38\u5e38\u7528\u4e8eLi-S\u7535\u6c60\u4e2d\u542b\u786b\u6750\u6599\u4e2d\u786b\u542b\u91cf\u7684\u6d4b\u5b9a\u3002<\/p>\n<p><strong>3\u00a0\u539f\u5b50\u5149\u8c31\u6cd5<\/strong><\/p>\n<p>\u539f\u5b50\u5149\u8c31\u662f\u539f\u5b50\u5438\u6536\u6216\u53d1\u51fa\uff08\u53d1\u5149\u548c\u8367\u5149\uff09\u5149\u5b50\u7684\u5f3a\u5ea6\u5173\u4e8e\u5149\u5b50\u80fd\u91cf\uff08\u901a\u5e38\u4ee5\u6ce2\u957f\u8868\u793a\uff09\u7684\u56fe\u8c31\uff0c\u5176\u53ef\u4ee5\u63d0\u4f9b\u5173\u4e8e\u6837\u54c1\u5316\u5b66\u7ec4\u6210\u7684\u76f8\u5173\u4fe1\u606f<sup>[1<\/sup><sup>1<\/sup><sup>]<\/sup>\u3002\u539f\u5b50\u5149\u8c31\u5206\u4e3a\u4e09\u5927\u7c7b\uff1a\u539f\u5b50\u5438\u6536\u5149\u8c31\u3001\u539f\u5b50\u53d1\u5c04\u5149\u8c31\u548c\u539f\u5b50\u8367\u5149\u5149\u8c31<sup>[1<\/sup><sup>2<\/sup><sup>]<\/sup>\u3002\u7531\u4e8e\u539f\u5b50\u5438\u6536\u5149\u8c31\u548c\u539f\u5b50\u53d1\u5c04\u5149\u8c31\u5e94\u7528\u6700\u4e3a\u5e7f\u6cdb\uff0c\u6545\u4e3b\u8981\u4ecb\u7ecd\u6b64\u4e24\u79cd\u3002<\/p>\n<p>3.1 \u539f\u5b50\u53d1\u5c04\u5149\u8c31\uff08OES\/AES\uff09<\/p>\n<p>\u539f\u5b50\u53d1\u5c04\u5149\u8c31\u662f\u4e00\u79cd\u5f88\u53e4\u8001\u7684\u6280\u672f\uff0c\u901a\u5e38\u7528\u4e8e\u5143\u7d20\u5206\u6790<sup>[1<\/sup><sup>3<\/sup><sup>, 1<\/sup><sup>4<\/sup><sup>]<\/sup>\u3002\u6bcf\u79cd\u5143\u7d20\u7684\u539f\u5b50\u53ca\u79bb\u5b50\u6fc0\u53d1\u540e\uff0c\u90fd\u4f1a\u8f90\u5c04\u51fa\u4e00\u7ec4\u8868\u5f81\u8be5\u5143\u7d20\u7684\u7279\u5f81\u5149\u8c31\u7ebf\u3002\u5176\u4e2d\u6709\u4e00\u6761\u6216\u6570\u6761\u8f90\u5c04\u7684\u5f3a\u5ea6\u6700\u5f3a\uff0c\u6700\u5bb9\u6613\u88ab\u68c0\u6d4b\u51fa\u6765\uff0c\u6240\u4ee5\u4e5f\u5e38\u5e38\u79f0\u4e3a\u6700\u7075\u654f\u7ebf\u3002\u6839\u636e\u5143\u7d20\u7075\u654f\u7ebf\u7684\u51fa\u73b0\u4e0e\u5426\u5c31\u53ef\u4ee5\u786e\u5b9a\u6837\u54c1\u4e2d\u662f\u5426\u5b58\u5728\u8fd9\u4e9b\u5143\u7d20\uff0c\u8fd9\u5c31\u662fOES\u5b9a\u6027\u5206\u6790\u7684\u57fa\u672c\u539f\u7406\u3002\u5728\u4e00\u5b9a\u6761\u4ef6\u4e0b\uff0c\u5143\u7d20\u7684\u7279\u5f81\u8c31\u7ebf\u7684\u5f3a\u5ea6\u968f\u7740\u5143\u7d20\u5728\u6837\u54c1\u4e2d\u7684\u542b\u91cf\u6216\u6d53\u5ea6\u7684\u589e\u5927\u800c\u589e\u5f3a\uff0c\u5229\u7528\u8fd9\u4e00\u6027\u8d28\u53ef\u4ee5\u6d4b\u5b9a\u5143\u7d20\u7684\u542b\u91cf\uff0c\u8fd9\u5c31\u662fOES\u5b9a\u91cf\u5206\u6790\u7684\u4f9d\u636e\u3002<\/p>\n<p>\u539f\u5b50\u53d1\u5c04\u5149\u8c31\u4eea\u5668\u4e3b\u8981\u7531\u5149\u6e90\u3001\u6837\u54c1\u5ba4\u3001\u5149\u5b66\u8272\u6563\u7cfb\u7edf\u548c\u68c0\u6d4b\u5668\u7b49\u7ec4\u6210<sup>[1<\/sup><sup>5<\/sup><sup>]<\/sup>\uff0c\u73b0\u5728\u6700\u5e38\u7528\u7684\u662fICP-OES\uff08\u7535\u611f\u8026\u5408\u7b49\u79bb\u5b50\u4f53\u539f\u5b50\u53d1\u5c04\u5149\u8c31\uff09\u3002ICP-OES\u662f\u4f7f\u7528\u7535\u611f\u8026\u5408\u7b49\u79bb\u5b50\u4f53\u505a\u4e3a\u5149\u6e90\u3002\u4f7f\u7528\u7535\u611f\u8026\u5408\u7b49\u79bb\u5b50\u4f53\u4f5c\u4e3a\u5149\u6e90\u662f\u56e0\u4e3a\u5176\u6709\u4e00\u4e9b\u72ec\u7279\u7684\u6027\u8d28<sup>[1<\/sup><sup>6<\/sup><sup>-1<\/sup><sup>8<\/sup><sup>]<\/sup>\uff0c\u5b83\u80fd\u4ea7\u751f\u66f4\u9ad8\u7684\u6e29\u5ea6\u5e76\u51cf\u5c11\u53ef\u80fd\u4f1a\u53d1\u751f\u7684\u5316\u5b66\u53cd\u5e94\u4e14\u5176\u7a33\u5b9a\u6027\u597d\uff0c\u8fd9\u4f1a\u4f7fOES\u7ebf\u6027\u5206\u6790\u8303\u56f4\u5e7f\uff0c\u7075\u654f\u5ea6\u9ad8\uff0c\u5316\u5b66\u5e72\u6270\u4f4e\uff0c\u66f4\u52a0\u9002\u7528\u4e8e\u5149\u8c31\u5b9a\u6027\u5206\u6790\u548c\u5b9a\u91cf\u5206\u6790\u3002OES\u5e7f\u6cdb\u5e94\u7528\u7684\u4e3b\u8981\u539f\u56e0\u5c31\u662f\u5176\u901a\u7528\u6027\u5f3a\u548c\u5177\u6709\u591a\u5143\u7d20\u5206\u6790\u80fd\u529b\u3002<\/p>\n<p>OES\u6709\u7740\u5f88\u9ad8\u7684\u7cbe\u786e\u5ea6\uff0c\u76f8\u5bf9\u6807\u51c6\u504f\u5dee\uff08%RSD\uff09\u53ea\u67091%\u6216\u66f4\u4f4e\u3002ICP-OES\u51e0\u4e4e\u53ef\u4ee5\u68c0\u6d4b\u5143\u7d20\u5468\u671f\u8868\u4e2d\u7684\u6240\u6709\u5143\u7d20\uff0c\u68c0\u6d4b\u9650\u4f4e\u81f30.1~50 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PM\u578b\u539f\u5b50\u5438\u6536\u5206\u5149\u5149\u5ea6\u8ba1\u3002\u9996\u5148\u4f5c\u8005\u5236\u5b9a\u4e86\u5f85\u6d4b\u5143\u7d20\u7684\u6821\u51c6\u66f2\u7ebf\uff0c\u7136\u540e\u5bf9\u901a\u8fc7\u9178\u6d88\u89e3\u5904\u7406\u7684\u852c\u83dc\u6837\u54c1\u8fdb\u884c\u4e86\u6d4b\u5b9a\uff0c\u901a\u8fc7\u6821\u51c6\u66f2\u7ebf\u8ba1\u7b97\u4e86\u76f8\u5e94\u5143\u7d20\u7684\u542b\u91cf\u3002\u6b64\u5916\u4f5c\u8005\u8fd8\u6d4b\u8bd5\u4e86\u6837\u54c1\u7684\u52a0\u6807\u56de\u6536\u7387\u3002\u8bd5\u9a8c\u8868\u660e\u52a0\u6807\u56de\u6536\u7387\u572894.0%~106%\u4e4b\u95f4\uff0c\u8fd9\u4e5f\u8bf4\u660e\u65b9\u6cd5\u51c6\u786e\u53ef\u884c\u3002<\/p>\n<p>3.3 X\u5c04\u7ebf\u8367\u5149\u5149\u8c31\uff08XRF\uff09<\/p>\n<p>X\u5c04\u7ebf\u8367\u5149\u5149\u8c31\u5206\u6790(X Ray Fluorescence,\u00a0XRF)\u7684\u539f\u7406\u662f\u91c7\u7528X\u5c04\u7ebf\u7ba1\u4ea7\u751f\u7684\u5165\u5c04X\u5c04\u7ebf\uff08\u53c8\u53eb\u4e00\u6b21X\u5c04\u7ebf\u6216\u539f\u7ea7X\u5c04\u7ebf\uff09\u6fc0\u53d1\u88ab\u6d4b\u6837\u54c1\uff0c\u968f\u540e\u53d7\u6fc0\u53d1\u6837\u54c1\u4e2d\u7684\u5143\u7d20\u5c31\u4f1a\u53d1\u5c04\u51fa\u4e8c\u6b21X\u5c04\u7ebf\uff08\u53c8\u79f0X\u5c04\u7ebf\u8367\u5149\uff09\uff0c\u5e76\u4e14\u4e0d\u540c\u7684\u5143\u7d20\u6240\u653e\u5c04\u51fa\u7684\u4e8c\u6b21X\u5c04\u7ebf\u5177\u6709\u7279\u5b9a\u7684\u80fd\u91cf\u7279\u6027\u6216\u6ce2\u957f\u7279\u6027\u3002\u63a2\u6d4b\u7cfb\u7edf\u6d4b\u91cf\u8fd9\u4e9b\u653e\u5c04\u51fa\u6765\u7684\u4e8c\u6b21X\u5c04\u7ebf\u7684\u80fd\u91cf\u53ca\u6570\u91cf\uff0c\u5c31\u53ef\u5c06\u5176\u8f6c\u6362\u6210\u5404\u79cd\u5143\u7d20\u7684\u79cd\u7c7b\u53ca\u542b\u91cf\uff08\u5982\u56fe6\uff09\u3002\u5229\u7528X\u5c04\u7ebf\u8367\u5149\u539f\u7406\uff0c\u7406\u8bba\u4e0a\u53ef\u4ee5\u6d4b\u91cf\u5143\u7d20\u5468\u671f\u8868\u4e2dBe\u4ee5\u540e\u7684\u6bcf\u4e00\u79cd\u5143\u7d20\u3002\u5728\u5b9e\u9645\u5e94\u7528\u4e2d\uff0c\u6709\u6548\u7684\u5143\u7d20\u6d4b\u91cf\u8303\u56f4\u4e3a9\u53f7\u5143\u7d20 \uff08F\uff09\u523092\u53f7\u5143\u7d20\uff08U\uff09\u3002<\/p>\n<p>XRF\u5206\u6790\u7684\u7279\u70b9\u662f\u9002\u5408\u4e8e\u5404\u7c7b\u56fa\u4f53\u6837\u54c1\u4e2d\u4e3b\u3001\u6b21\u3001\u75d5\u91cf\u591a\u5143\u7d20\u540c\u65f6\u68c0\u6d4b\uff0c\u68c0\u51fa\u9650\u7ea6\u5728\u03bcg\/g\u91cf\u7ea7\u8303\u56f4\u5185\uff0c\u5236\u6837\u65b9\u6cd5\u7b80\u5355\uff0c\u73b0\u5df2\u5e7f\u6cdb\u5e94\u7528\u4e8e\u5730\u8d28\u3001\u6750\u6599\u3001\u73af\u5883\u3001\u51b6\u91d1\u6837\u54c1\u7684\u5e38\u89c4\u5206\u6790\u3002XRF\u662f\u4e00\u79cd\u65e0\u635f\u68c0\u6d4b\u6280\u672f\uff0c\u53ef\u76f4\u63a5\u5e94\u7528\u4e8e\u73b0\u573a\u3001\u539f\u4f4d\u53ca\u6d3b\u4f53\u5206\u6790\u3002XRF\u7684\u7f3a\u70b9\u662f\u68c0\u51fa\u9650\u4e0d\u591f\u4f4e\uff0c\u4e0d\u9002\u7528\u4e8e\u5206\u6790\u8f7b\u5143\u7d20\uff0c\u51c6\u786e\u5b9a\u91cf\u5206\u6790\u4f9d\u8d56\u6807\u6837\u3002XRF\u7684\u53e6\u4e00\u4e2a\u7f3a\u70b9\u662f\u9700\u8981\u7684\u6837\u54c1\u8f83\u591a\uff0c\u7c89\u672b\u4e00\u822c\u9700\u89812g\u4ee5\u4e0a\u3002<\/p>\n<p>\u5d14\u6885\u751f\u7b49<sup>[<\/sup><sup>23]<\/sup>\u5c31\u91c7\u7528\u624b\u6301 XRF \u6280\u672f\u5bf9\u6c7d\u8f66\u5c3e\u6c14\u50ac\u5316\u5242\u3001\u6c7d\u8f66\u5c3e\u6c14\u50ac\u5316\u5242\u7c89\u4f53\u3001\u91d1\u5c5e\u6574\u4f53\u5f0f\u6469\u6258\u8f66\u5c3e\u6c14\u50ac\u5316\u5242\u7b49\u6837\u54c1\u8fdb\u884c\u8d35\u91d1\u5c5e\u542b\u91cf\u6d4b\u8bd5\u3002\u4e0e\u5e38\u89c4 ICP-OES \u65b9\u6cd5\u76f8\u6bd4\uff0c\u624b\u6301 XRF \u6280\u672f\u662f\u4e00\u79cd\u5feb\u901f\u3001\u65b9\u4fbf\u3001\u5ec9\u4ef7\u7684\u8d35\u91d1\u5c5e\u542b\u91cf\u6d4b\u8bd5\u65b9\u6cd5\uff0c\u5bf9\u4e8e\u6c7d\u8f66\u5c3e\u6c14\u50ac\u5316\u5242\u7c89\u4f53\uff0c\u624b\u6301 XRF \u68c0\u6d4b\u4e0e ICP-OES \u8ba4\u8bc1\u503c\u5bf9\u4e8e Pd \u542b\u91cf\u76f8\u5bf9\u6807\u51c6\u504f\u5dee\u5c0f\u4e8e5%\u3002<\/p>\n<p>\u56fe6 XRF\u7684\u57fa\u672c\u539f\u7406<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"wp-image-161580 size-full aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72475-7.png\" alt=\"\" width=\"454\" height=\"257\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72475-7.png 454w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72475-7-300x170.png 300w\" sizes=\"(max-width: 454px) 100vw, 454px\" \/><\/p>\n<p><strong>4\u00a0X\u5c04\u7ebf\u80fd\u91cf\u8272\u6563\u8c31\u6cd5\uff08EDX\uff09<\/strong><\/p>\n<p>EDX\u5e38\u4e0e\u7535\u5b50\u663e\u5fae\u955c\u914d\u5408\u4f7f\u7528\uff0c\u5b83\u662f\u6d4b\u91cf\u7535\u5b50\u4e0e\u8bd5\u6837\u76f8\u4e92\u4f5c\u7528\u6240\u4ea7\u751f\u7684\u7279\u5f81X\u5c04\u7ebf\u7684\u6ce2\u957f\u4e0e\u5f3a\u5ea6\uff0c\u4ece\u800c\u5bf9\u5fae\u5c0f\u533a\u57df\u6240\u542b\u5143\u7d20\u8fdb\u884c\u5b9a\u6027\u6216\u5b9a\u91cf\u5206\u6790<sup>[2<\/sup><sup>4<\/sup><sup>]<\/sup>\u3002\u6bcf\u4e00\u79cd\u5143\u7d20\u90fd\u6709\u4e00\u4e2a\u7279\u5b9a\u6ce2\u957f\u7684\u7279\u5f81X\u5c04\u7ebf\u4e0e\u4e4b\u76f8\u5bf9\u5e94\uff0c\u5b83\u4e0d\u968f\u5165\u5c04\u7535\u5b50\u7684\u80fd\u91cf\u800c\u53d8\u5316\uff0c\u6d4b\u91cf\u7535\u5b50\u6fc0\u53d1\u8bd5\u6837\u6240\u4ea7\u751f\u7684\u7279\u5f81X\u5c04\u7ebf\u6ce2\u957f\u7684\u79cd\u7c7b\uff0c\u5373\u53ef\u786e\u5b9a\u8bd5\u6837\u4e2d\u6240\u5b58\u5728\u5143\u7d20\u7684\u79cd\u7c7b\u3002\u5143\u7d20\u7684\u542b\u91cf\u4e0e\u8be5\u5143\u7d20\u4ea7\u751f\u7684\u7279\u5f81X\u5c04\u7ebf\u5f3a\u5ea6\u6210\u6b63\u6bd4\uff0c\u636e\u6b64\u53ef\u4ee5\u6d4b\u5b9a\u5143\u7d20\u7684\u542b\u91cf\u3002<\/p>\n<p>EDX\u53ef\u5206\u6790\u8868\u97621~5\u03bcm\u7684\u5143\u7d20\u6210\u5206\uff0c\u63a2\u6d4b\u7075\u654f\u5ea6\u5927\u7ea6\u4e3a0.1%\uff08\u539f\u5b50\u6469\u5c14\u5206\u6570\uff0c\u4e0e\u5143\u7d20\u79cd\u7c7b\u6709\u5173\uff09<sup>[2<\/sup><sup>5<\/sup><sup>]<\/sup>\u3002EDX\u53ef\u63a2\u6d4b\u5143\u7d20\u8303\u56f4\u5927\uff08<sub>4<\/sub>Be~<sub>92<\/sub>U\uff09\uff0c\u5bf9\u91cd\u5143\u7d20\u7684\u5206\u6790\u7279\u522b\u6709\u6548\u3002\u5b83\u53ef\u4ee5\u540c\u65f6\u6d4b\u91cf\u6240\u6709\u7684\u5143\u7d20\uff0c\u5206\u6790\u6548\u7387\u9ad8<sup>[2<\/sup><sup>6<\/sup><sup>]<\/sup>\u3002\u80fd\u8c31\u6240\u9700\u63a2\u9488\u7535\u6d41\u5c0f\uff0c\u5bf9\u5f85\u5206\u6790\u8bd5\u6837\u635f\u4f24\u5c0f\uff0c\u9002\u4e8e\u751f\u7269\u8bd5\u6837\u3001\u5feb\u79bb\u5b50\u5bfc\u4f53\u8bd5\u6837\u7b49\u3002<\/p>\n<p>EDX\u6709\u4e09\u79cd\u57fa\u672c\u5de5\u4f5c\u65b9\u5f0f\u3002\u4e00\u662f\u5b9a\u70b9\u5206\u6790\uff0c\u5bf9\u6837\u54c1\u8868\u9762\u9009\u5b9a\u5fae\u533a\u8fdb\u884c\u626b\u63cf\u5206\u6790\uff1b\u4e8c\u662f\u7ebf\u626b\u63cf\u5206\u6790\uff0c\u53ef\u4ee5\u5bf9\u6837\u54c1\u8868\u9762\u9009\u5b9a\u7684\u76f4\u7ebf\u8fdb\u884c\u5143\u7d20\u5b9a\u6027\u5b9a\u91cf\u5206\u6790\uff1b\u4e09\u662f\u9762\u626b\u63cf\u5206\u6790\uff0c\u53ef\u4ee5\u83b7\u5f97\u67d0\u79cd\u5143\u7d20\u8d28\u91cf\u5206\u5e03\u7684\u626b\u63cf\u56fe\u50cf\u3002\u7531\u4e8eEDX\u901a\u5e38\u662fSEM\u6216\u8005TEM\u7684\u9644\u4ef6\uff0c\u56e0\u6b64\uff0c\u91c7\u7528EDX\u8fdb\u884c\u5143\u7d20\u5206\u6790\u7684\u4e00\u5927\u4f18\u52bf\u5c31\u662f\u53ef\u89c6\u5316\u64cd\u4f5c\uff0c\u975e\u5e38\u76f4\u89c2\u3002<\/p>\n<p>\u4f46\u662f\u80fd\u8c31\u4eea\u5206\u8fa8\u7387\u8f83\u5dee\uff0c\u5cf0\u80cc\u6bd4\u4f4e\uff0c\u8c31\u5cf0\u91cd\u53e0\u4e25\u91cd<sup>[2<\/sup><sup>7<\/sup><sup>]<\/sup>\u3002\u6b64\u5916\uff0c\u80fd\u8c31\u4eea\u5de5\u4f5c\u6761\u4ef6\u8981\u6c42\u4e25\u683c\uff0c\u9700\u8981\u6db2\u6c2e\u51b7\u5374<sup>[1<\/sup><sup>2<\/sup><sup>]<\/sup>\u3002\u7531\u4e8e\u7535\u5b50\u8fdb\u5165\u7684\u6df1\u5ea6\u7684\u9650\u5236\uff0cEDX\u53ea\u80fd\u7528\u6765\u5206\u6790\u5c40\u90e8\u8868\u5c42\u7684\u5143\u7d20\u79cd\u7c7b\u548c\u542b\u91cf\uff0c\u4e0d\u9002\u7528\u4e8e\u5b9a\u91cf\u5206\u6790\uff0c\u7cbe\u5ea6\u6709\u65f6\u8f83\u5927\u3002<\/p>\n<p>Jang-Zern Tsai\u7b49<sup>[2<\/sup><sup>8<\/sup><sup>]<\/sup>\u5c31\u4f7f\u7528EDX\u8868\u5f81\u4e86COOH-P-SPCE\uff08\u5bcc\u7fa7\u57fa\u591a\u5b54\u4e1d\u7f51\u78b3\u7535\u6781\uff09\u8868\u9762\u4fee\u9970\u524d\u7684\u5143\u7d20\u5206\u5e03\u548c\u5143\u7d20\u542b\u91cf\u3002\u7ed3\u679c\u5982\u56fe7\u6240\u793a\uff0c\u5206\u6790\u8868\u660eCOOH-P-SPCE\u8868\u9762C\u548cCa\u7684\u542b\u91cf\u5206\u522b\u4e3a90.38wt%\u548c9.62 wt%\uff0c\u7ed3\u5408SEM\u56fe\u50cf\u4e5f\u53ef\u4ee5\u53d1\u73b0\u5143\u7d20\u5728\u8868\u9762\u5206\u5e03\u4e5f\u6bd4\u8f83\u5747\u5300\u3002<\/p>\n<p>\u56fe7 COOH-P-SPCE\u7684SEM\u56fe\u50cf\u548cEDS\u56fe\u8c31<sup>[26]<\/sup><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"wp-image-161581 size-full aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72476-6.png\" alt=\"\" width=\"600\" height=\"350\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72476-6.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72476-6-300x175.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p><strong>5\u00a0\u7535\u5b50\u80fd\u8c31\u5206\u6790\u6cd5<\/strong><\/p>\n<p>\u7535\u5b50\u80fd\u8c31\u5206\u6790\u6cd5\u662f\u91c7\u7528\u5355\u8272\u5149\u6e90\u6216\u7535\u5b50\u675f\u53bb\u7167\u5c04\u6837\u54c1\uff0c\u4f7f\u6837\u54c1\u4e2d\u7535\u5b50\u53d7\u5230\u6fc0\u53d1\u800c\u53d1\u5c04\u51fa\u6765\uff0c\u7136\u540e\u6d4b\u91cf\u8fd9\u4e9b\u7535\u5b50\u7684\u4ea7\u989d\uff08\u5f3a\u5ea6\uff09\u4e0e\u80fd\u91cf\u7684\u5206\u5e03\uff0c\u4ece\u800c\u83b7\u5f97\u6750\u6599\u4fe1\u606f\u3002\u7535\u5b50\u80fd\u8c31\u7684\u91c7\u6837\u6df1\u5ea6\u4ec5\u4e3a\u51e0\u7eb3\u7c73\uff0c\u6240\u4ee5\u5176\u4ec5\u662f\u8868\u9762\u6210\u5206\u7684\u53cd\u5e94<sup>[2<\/sup><sup>9<\/sup><sup>]<\/sup>\u3002\u672c\u6587\u4e3b\u8981\u4ecb\u7ecd\u5e94\u7528\u8f83\u4e3a\u5e7f\u6cdb\u7684\u4fc4\u6b47\u7535\u5b50\u80fd\u8c31\u6cd5\u548cX\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\u6cd5\u3002<\/p>\n<p>5.1\u00a0\u4fc4\u6b47\u7535\u5b50\u80fd\u8c31\u6cd5\uff08AES\uff09<\/p>\n<p>\u5f53\u539f\u5b50\u5438\u6536X\u5c04\u7ebf\u6216\u8005\u88ab\u7535\u5b50\u8f70\u51fb\u65f6\uff0c\u5982\u679c\u5728\u5176\u5185\u90e8\u4ea7\u751f\u4e86\u7a7a\u7a74\uff0c\u539f\u5b50\u5c31\u6709\u53ef\u80fd\u53d1\u5c04\u4fc4\u6b47\u7535\u5b50\uff08\u5982\u56fe8\u6240\u793a\uff09\uff0c\u901a\u8fc7\u68c0\u6d4b\u4fc4\u6b47\u7535\u5b50\u7684\u80fd\u91cf\u548c\u5f3a\u5ea6\u5c31\u53ef\u4ee5\u83b7\u5f97\u6837\u54c1\u8868\u9762\u5316\u5b66\u6210\u5206\u548c\u7ed3\u6784\u7684\u76f8\u5173\u4fe1\u606f<sup>[<\/sup><sup>30<\/sup><sup>]<\/sup>\u3002<\/p>\n<p>\u56fe8 \u4fc4\u6b47\u7535\u5b50\u53d1\u5c04\u793a\u610f\u56fe<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-161582 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72477-6.png\" alt=\"\" width=\"208\" height=\"135\" \/><\/p>\n<p>\u4fc4\u6b47\u7535\u5b50\u80fd\u8c31\u53ef\u4ee5\u7528\u6765\u5bf9\u5143\u7d20\u8fdb\u884c\u5b9a\u6027\u5206\u6790\uff0c\u4e3b\u8981\u662f\u5229\u7528\u4fc4\u6b47\u7535\u5b50\u7684\u7279\u5f81\u80fd\u91cf\u503c\u6765\u786e\u5b9a\u56fa\u4f53\u8868\u9762\u7684\u5143\u7d20\u7ec4\u6210<sup>[<\/sup><sup>31<\/sup><sup>]<\/sup>\uff0c\u65b9\u6cd5\u662f\u5c06\u6d4b\u5f97\u7684\u8c31\u56fe\u4e0e\u6807\u51c6\u8c31\u56fe\u8fdb\u884c\u5bf9\u6bd4\u3002\u4fc4\u6b47\u7535\u5b50\u80fd\u8c31\u53ef\u4ee5\u7528\u4ee5\u5b9a\u91cf\u5206\u6790\uff0c\u4f46\u56e0\u4e3a\u5f71\u54cd\u4fc4\u6b47\u4fe1\u53f7\u5f3a\u5f31\u7684\u56e0\u7d20\u5f88\u591a\uff0c\u5bfc\u81f4\u5176\u5b9a\u91cf\u5206\u6790\u6bd4\u8f83\u590d\u6742\uff0c\u56e0\u6b64\u4fc4\u6b47\u80fd\u8c31\u5206\u6790\u7cbe\u5ea6\u8f83\u4f4e\uff0c\u57fa\u672c\u4e0a\u662f\u534a\u5b9a\u91cf\u7684\u6c34\u5e73\uff0c\u4e00\u822c\u60c5\u51b5\u4e0b\u76f8\u5bf9\u7cbe\u5ea6\u4ec5\u4e3a30%\u3002<\/p>\n<p>AES\u7684\u4f18\u70b9\u662f\u5728\u8ddd\u8868\u97620.5~2nm\u8303\u56f4\u5185\u7075\u654f\u5ea6\u9ad8\u3001\u5206\u6790\u901f\u5ea6\u5feb\uff0c\u80fd\u63a2\u6d4b\u5468\u671f\u8868\u4e0aH\u548cHe\u4ee5\u5916\u7684\u6240\u6709\u5143\u7d20<sup>[1]<\/sup>\u3002\u7531\u4e8e\u91c7\u6837\u6df1\u5ea6\u4ec5\u4e3a\u57282nm\u4ee5\u5185\uff0c\u6240\u4ee5\u5176\u66f4\u9002\u5408\u4e8e\u8868\u9762\u5143\u7d20\u5b9a\u6027\u5206\u6790\uff0c\u914d\u5408\u79bb\u5b50\u675f\u5265\u79bb\u6280\u672f\uff0cAES\u8fd8\u6709\u5f88\u5f3a\u7684\u6df1\u5ea6\u5206\u6790\uff08\u6df1\u5ea6\u5206\u6790\u901f\u5ea6\u548c\u5206\u8fa8\u7387\u90fd\u6bd4XPS\u597d<sup>[2<\/sup><sup>9<\/sup><sup>]<\/sup>\uff09\u548c\u754c\u9762\u5206\u6790\u80fd\u529b\u3002AES\u62e5\u6709\u8005\u4e0eXPS\u76f8\u540c\u7684\u8868\u9762\u7075\u654f\u5ea6\u800c\u4e14\u76f8\u5bf9\u7b80\u5355\uff0c\u4f46\u51c6\u786e\u7a0b\u5ea6\u8f83XPS\u5dee<sup>[3<\/sup><sup>2<\/sup><sup>]<\/sup>\u3002\u6b64\u5916\uff0c\u901a\u8fc7\u663e\u5faeAES\u8fd8\u53ef\u4ee5\u83b7\u5f97\u4fc4\u6b47\u7535\u5b50\u80fd\u8c31\u5143\u7d20\u5206\u5e03\u56fe\uff08SAM\uff09\uff0c\u4f46\u7531\u4e8e\u8be5\u5206\u6790\u65b9\u6cd5\u8017\u65f6\u975e\u5e38\u957f\uff0c\u4e00\u822c\u5f88\u5c11\u4f7f\u7528\u3002<\/p>\n<p>AES\u4e5f\u6709\u4e00\u4e9b\u5c40\u9650\u6027\u3002\u9996\u5148\u5b83\u4e0d\u80fd\u7528\u4e8e\u5206\u6790H\u548cHe\u5143\u7d20\u3002\u5176\u6b21\u5b83\u7684\u5b9a\u91cf\u5206\u6790\u7684\u51c6\u786e\u5ea6\u4e0d\u9ad8\u3002\u53e6\u5916\u5176\u5bf9\u591a\u6570\u5143\u7d20\u7684\u63a2\u6d4b\u7075\u654f\u5ea6\u4e3a0.1%~1.0%\uff08\u539f\u5b50\u6469\u5c14\u5206\u6570\uff09\u3002\u6b64\u5916\u7535\u5b50\u675f\u8f70\u51fb\u635f\u4f24\u548c\u7535\u8377\u79ef\u7d2f\u95ee\u9898\u4e5f\u9650\u5236\u4e86\u5176\u5728\u6709\u673a\u6750\u6599\u3001\u751f\u7269\u6837\u54c1\u548c\u4e00\u4e9b\u9676\u74f7\u6750\u6599\u4e2d\u7684\u5e94\u7528\u3002\u4fc4\u6b47\u7535\u5b50\u80fd\u8c31\u5bf9\u6837\u54c1\u7684\u8981\u6c42\u9ad8\uff0c\u8868\u9762\u5fc5\u987b\u6e05\u6d01\u3002<\/p>\n<p>\u5c39\u71d5\u840d\u7b49<sup>[3<\/sup><sup>3<\/sup><sup>]<\/sup>\u4f7f\u7528AES\u914d\u5408\u6c29\u79bb\u5b50\u675f\u5265\u79bb\u6280\u672f\u7814\u7a76\u4e86\u6837\u54c1\u7684\u5143\u7d20\u5256\u9762\u5206\u5e03\u3002\u56fe9\u5c31\u662f\u662f\u7528\u4e8e\u5236\u4f5cCCD\u5668\u4ef6\u7684PtSi\/Si\u6837\u54c1\u7684AES\u6df1\u5ea6\u5206\u6790\u56fe\u3002\u7531\u56fe\u4e2d\u7684\u6df1\u5ea6\u5256\u9762\u5206\u5e03\u770b\uff0cSi\u4e0a\u7684PtSi\u5c42\u7ea64 nm\u539a\uff0c\u800c\u4e14\u754c\u9762\u5904\u6709\u8f83\u4e25\u91cd\u7684\u6c27\u5438\u9644\u3002<\/p>\n<p>\u56fe9 PtSi\/Si\u7684AES\u7ec4\u5206\u6df1\u5ea6\u5206\u5e03\u3002<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"wp-image-161583 size-full aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72478-5.png\" alt=\"\" width=\"600\" height=\"282\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72478-5.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72478-5-300x141.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/>5.2X\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\u6cd5\uff08XPS\uff09<\/p>\n<p>XPS\u662f\u7531\u745e\u5178Uppsala\u5927\u5b66\u7684Kaiser Siegbahn\u53ca\u5176\u540c\u4e8b\u57fa\u4e8e\u5149\u7535\u6548\u5e94\u7684\u539f\u7406\u7814\u5236\u53d1\u5c55\u7684\u7684\u4e00\u79cd\u8868\u9762\u5316\u5b66\u5206\u6790\u6280\u672f<sup>[3<\/sup><sup>4<\/sup><sup>-3<\/sup><sup>7<\/sup><sup>]<\/sup>\u3002XPS\u4f7f\u7528\u8f6fX\u5c04\u7ebf\u4f5c\u4e3a\u6fc0\u53d1\u5149\u6e90\uff0c\u6fc0\u53d1\u51fa\u7269\u8d28\u8868\u9762\u539f\u5b50\u7684\u5185\u5c42\u7535\u5b50\uff08\u5982\u56fe10\uff09\uff0c\u901a\u8fc7\u5bf9\u8fd9\u4e9b\u7535\u5b50\u8fdb\u884c\u80fd\u91cf\u5206\u6790\u800c\u83b7\u5f97\u6750\u6599\u4fe1\u606f\u3002<\/p>\n<p>\u56fe10 X\u5c04\u7ebf\u5149\u7535\u5b50\u53d1\u5c04\u793a\u610f\u56fe<\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-161584 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u72479-4.png\" alt=\"\" width=\"175\" height=\"122\" \/><\/p>\n<p>XPS\u5e7f\u6cdb\u4f7f\u7528\u7684\u539f\u56e0\u4e3b\u8981\u6709\u4ee5\u4e0b\u51e0\u70b9\u3002\uff081\uff09\u5b83\u53ef\u4ee5\u5bf9\u4ece<sub>3<\/sub>Li~<sub>92<\/sub>U\u7684\u4efb\u4f55\u5143\u7d20\u8fdb\u884c\u5b9a\u6027\u5b9a\u91cf\u5206\u6790\uff0c\u5206\u6790\u901f\u5ea6\u5feb\u3001\u53ef\u591a\u5143\u7d20\u540c\u65f6\u8fdb\u884c\u5206\u6790\uff0cXPS\u5b9a\u91cf\u5206\u6790\u4e0d\u9700\u8981\u53c2\u6bd4\u7269\u8d28\uff0c\u8bef\u5dee\u4e00\u822c\u57285%~10%\uff0c\uff1b\uff082\uff09\u7075\u654f\u5ea6\u4e3a0.1%\uff08\u91cd\u5143\u7d20\uff09~1.0%\uff08\u8f7b\u5143\u7d20\uff09\uff08\u539f\u5b50\u6469\u5c14\u5206\u6570\uff09\uff1b\uff083\uff09\u5bf9\u7269\u8d28\u8fdb\u884c\u8868\u9762\u8868\u5f81\uff08\u5c0f\u4e8e10nm\uff09\uff0c\u53ef\u4ee5\u8fdb\u884c\u5143\u7d20\u4ef7\u6001\u5206\u6790\u548c\u5316\u5b66\u7ed3\u6784\u5206\u6790<sup>[35]<\/sup>\uff0c\u7ed3\u5408\u6c29\u79bb\u5b50\u67aa\u4e5f\u53ef\u8fdb\u884c\u6df1\u5ea6\u5206\u6790\uff1b\uff084\uff09\u6d4b\u8bd5\u6bd4\u8f83\u5bb9\u6613\uff08\u53ea\u9700\u5236\u5907\u5f88\u5c11\u7684\u6837\u54c1\uff09<sup>[23]<\/sup>\u3002<\/p>\n<p>\u4f7f\u7528X \u5c04\u7ebf\u6fc0\u53d1\u6750\u6599\uff0c\u7edd\u5927\u90e8\u5206\u5143\u7d20\u9664\u6709\u5149\u7535\u5b50\u53d1\u5c04\u5916\uff0c\u8fd8\u53ef\u53d1\u5c04\u51fa\u4fc4\u6b47\u7535\u5b50\uff0c\u56e0\u6b64XPS \u8c31\u4e2d\u8fd8\u5e38\u4f34\u968f\u7740\u4fc4\u6b47\u7535\u5b50\u8c31\u7ebf<sup>[3<\/sup><sup>8<\/sup><sup>-3<\/sup><sup>9<\/sup><sup>]<\/sup>\u3002\u4fc4\u6b47\u7535\u5b50\u5cf0\u7684\u51fa\u73b0\u589e\u52a0\u4e86\u8c31\u56fe\u7684\u590d\u6742\u7a0b\u5ea6\uff0c\u4f46\u4e5f\u7ed9\u5206\u6790\u5e26\u6765\u4e86\u6709\u4ef7\u503c\u7684\u4fe1\u606f\uff0c\u662fXPS\u8c31\u4e2d\u5149\u7535\u5b50\u4fe1\u606f\u7684\u8865\u5145\u3002\u4f5c\u5143\u7d20\u5b9a\u6027\u5206\u6790\u65f6\uff0c\u4fc4\u6b47\u7535\u5b50\u8c31\u7ebf\u5f80\u5f80\u6bd4\u5149\u7535\u5b50\u8c31\u6709\u66f4\u9ad8\u7684\u7075\u654f\u5ea6\u3002\u5728\u5316\u5b66\u6001\u7684\u9274\u522b\u65f6\uff0c\u4e0e\u5149\u7535\u5b50\u5cf0\u4f4d\u79fb\u76f8\u6bd4\uff0c\u67d0\u4e9b\u5143\u7d20\u7684\u4fc4\u6b47\u8c31\u7ebf\u5177\u6709\u66f4\u52a0\u660e\u663e\u7684\u4f4d\u79fb\uff08\u89c1\u56fe11\uff09\u3002<\/p>\n<p>\u56fe11 \u4e00\u4e9b\u5143\u7d20\u7684\u4fc4\u6b47\u8c31\u7ebf\u4f4d\u79fb\u548c\u5149\u7535\u5b50\u8c31\u7ebf\u4f4d\u79fb\u5bf9\u6bd4<sup>[3<\/sup><sup>6<\/sup><sup>]<\/sup><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"wp-image-161585 size-full aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u724710-4.png\" alt=\"\" width=\"600\" height=\"342\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u724710-4.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u724710-4-300x171.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\u4f46\u662fX\u5c04\u7ebf\u5149\u7535\u5b50\u8c31\u4eea\u4ef7\u683c\u8f83\u8d35\uff0c\u5e38\u89c4XPS\u53ea\u80fd\u5bf9\u5341\u51e0\u5e73\u65b9\u6beb\u7c73\u7684\u5927\u9762\u79ef\u8fdb\u884c\u5206\u6790\uff0c\u63d0\u4f9b\u7684\u4ec5\u662f\u5927\u9762\u79ef\u5185\u5e73\u5747\u4fe1\u606f\uff0c\u4e14\u6240\u7528\u7684\u6fc0\u53d1\u6e90\u4e3a\u975e\u5355\u8272\u5316X\u5149\uff0c\u5f97\u5230\u7684XPS\u8c31\u80fd\u91cf\u5206\u8fa8\u4e0d\u591f<sup>[<\/sup><sup>40<\/sup><sup>]<\/sup>\u3002\u9700\u8981\u6ce8\u610f\u7684\u662fXPS\u4e5f\u53ea\u662f\u5bf9\u7269\u8d28\u8868\u5c42\u8fdb\u884c\u5206\u6790\uff082-10 nm\uff09\uff0c\u4e14\u539a\u5ea6\u4e0d\u5982EDX\uff0c\u4e5f\u65e0\u6cd5\u8fdb\u884c\u53ef\u89c6\u5316\u64cd\u4f5c\u3002<\/p>\n<p>Mojca Bo\u017ei\u010d\u7b49<sup>[<\/sup><sup>41<\/sup><sup>]<\/sup>\u5c31\u4f7f\u7528XPS\u6280\u672f\u5bf9\u5176\u5236\u5907\u7684\u5149\u50ac\u5316\u6750\u6599\u8fdb\u884c\u4e86\u8868\u5f81\u3002\u9996\u5148\u4ed6\u7814\u7a76\u4e86\u6837\u54c1\u7684\u8868\u9762\u6210\u5206\uff0c\u6839\u636eXPS\u5cf0\u5f3a\u7ed3\u5408\u4eea\u5668\u5236\u9020\u5546\u63d0\u4f9b\u7684\u76f8\u5bf9\u7075\u654f\u5ea6\u56e0\u5b50\u5bf9\u6837\u54c1\u8fdb\u884c\u4e86\u5b9a\u91cf\u5206\u6790\uff0c\u7ed3\u679c\u5982\u88681\u6240\u793a\u3002\u7531\u4e8eTi<sup>3+<\/sup>\u7684\u5bf9\u6750\u6599\u5149\u50ac\u5316\u6027\u80fd\u6709\u8f83\u5927\u5f71\u54cd\uff0c\u4f5c\u8005\u53c8\u901a\u8fc7XPS\u5bf9\u6750\u6599\u8fdb\u884c\u4e86\u4ef7\u6001\u5206\u6790\uff0c\u7814\u7a76\u4e86\u6750\u6599\u5728\u8868\u9762\u529f\u80fd\u5316\u4fee\u9970\u524d\u540eTi<sup>3+<\/sup>\u7684\u542b\u91cf\uff08\u89c1\u56fe12\uff09\u3002<\/p>\n<p style=\"text-align: left;\">\u88681 \u6837\u54c1\u7684\u8868\u9762\u6210\u5206<sup>[<\/sup><sup>39<\/sup><sup>]<\/sup><\/p>\n<table class=\" aligncenter\" style=\"height: 556px; width: 346px;\">\n<tbody>\n<tr style=\"height: 56px;\">\n<td style=\"width: 158px; height: 56px;\">\n<p>&nbsp;<\/p>\n<\/td>\n<td style=\"width: 174px; height: 56px;\" colspan=\"3\">\n<p style=\"text-align: center;\">Concentration (at.%)<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 56px;\">\n<td style=\"width: 158px; height: 56px;\">\n<p>Sample<\/p>\n<\/td>\n<td style=\"width: 51px; height: 56px;\">\n<p>C\u00a01s<\/p>\n<\/td>\n<td style=\"width: 53px; height: 56px;\">\n<p>O\u00a01s<\/p>\n<\/td>\n<td style=\"width: 58px; height: 56px;\">\n<p>Ti 2p<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 58px;\">\n<td style=\"width: 158px; height: 58px;\">\n<p>TiO<sub>2<\/sub><\/p>\n<\/td>\n<td style=\"width: 51px; height: 58px;\">\n<p>12.1<\/p>\n<\/td>\n<td style=\"width: 53px; height: 58px;\">\n<p>57.4<\/p>\n<\/td>\n<td style=\"width: 58px; height: 58px;\">\n<p>30.5<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 58px;\">\n<td style=\"width: 158px; height: 58px;\">\n<p>TiO<sub>2<\/sub>-A4HBSA<\/p>\n<\/td>\n<td style=\"width: 51px; height: 58px;\">\n<p>32.8<\/p>\n<\/td>\n<td style=\"width: 53px; height: 58px;\">\n<p>48.5<\/p>\n<\/td>\n<td style=\"width: 58px; height: 58px;\">\n<p>18.7<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 58px;\">\n<td style=\"width: 158px; height: 58px;\">\n<p>TiO<sub>2<\/sub>-MWCNT(10:1)<\/p>\n<\/td>\n<td style=\"width: 51px; height: 58px;\">\n<p>32.8<\/p>\n<\/td>\n<td style=\"width: 53px; height: 58px;\">\n<p>46.7<\/p>\n<\/td>\n<td style=\"width: 58px; height: 58px;\">\n<p>20.5<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 82px;\">\n<td style=\"width: 158px; height: 82px;\">\n<p>TiO<sub>2<\/sub>-MWCNT(10:1)-A4HBSA<\/p>\n<\/td>\n<td style=\"width: 51px; height: 82px;\">\n<p>37.1<\/p>\n<\/td>\n<td style=\"width: 53px; height: 82px;\">\n<p>45.5<\/p>\n<\/td>\n<td style=\"width: 58px; height: 82px;\">\n<p>17.4<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 58px;\">\n<td style=\"width: 158px; height: 58px;\">\n<p>TiO<sub>2<\/sub>-MWCNT(17:1)<\/p>\n<\/td>\n<td style=\"width: 51px; height: 58px;\">\n<p>33.6<\/p>\n<\/td>\n<td style=\"width: 53px; height: 58px;\">\n<p>40.7<\/p>\n<\/td>\n<td style=\"width: 58px; height: 58px;\">\n<p>25.7<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 82px;\">\n<td style=\"width: 158px; height: 82px;\">\n<p style=\"text-align: left;\">TiO<sub>2<\/sub>-MWCNT(17:1)-A4HBSA<\/p>\n<\/td>\n<td style=\"width: 51px; height: 82px;\">\n<p>36.8<\/p>\n<\/td>\n<td style=\"width: 53px; height: 82px;\">\n<p>45.4<\/p>\n<\/td>\n<td style=\"width: 58px; height: 82px;\">\n<p>17.8<\/p>\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p style=\"text-align: left;\">\u56fe12 TiO<sub>2<\/sub>-MWCNT (10:1)\u8868\u9762\u529f\u80fd\u5316\u4fee\u9970\u524d\u540eTi 2p\u7684\u9ad8\u5206\u8fa8\u7387XPS\u8c31\u56fe<sup>[41]<\/sup><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"wp-image-161586 size-full aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u724711-4.png\" alt=\"\" width=\"600\" height=\"368\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u724711-4.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/12\/\u56fe\u724711-4-300x184.png 300w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p style=\"text-align: left;\"><strong>6 \u5176\u4ed6\u65b9\u6cd5<\/strong><\/p>\n<p style=\"text-align: left;\">X\u5c04\u7ebf\u884d\u5c04\uff08XRD\uff09\u6cd5\uff1aXRD\u4e5f\u53ef\u4ee5\u8f85\u52a9\u7528\u6765\u8fdb\u884c\u7269\u76f8\u7684\u5b9a\u91cf\u5206\u6790\u3002\u5b83\u7684\u4f9d\u636e\u662f\uff0c\u7269\u76f8\u7684\u884d\u5c04\u7ebf\u5f3a\u5ea6\u968f\u7740\u542b\u91cf\u7684\u589e\u52a0\u800c\u63d0\u9ad8\u3002\u4f46\u662f\u5e76\u4e0d\u6210\u6b63\u6bd4\uff0c\u9700\u8981\u52a0\u4ee5\u4fee\u6b63\uff0c\u91c7\u7528Jade\u7a0b\u5e8f\u5c31\u53ef\u5bf9\u5bf9\u7269\u76f8\u8fdb\u884c\u5b9a\u91cf\u5206\u6790\u3002<\/p>\n<p style=\"text-align: left;\">\u8d28\u8c31\u6cd5\uff08MS\uff09\uff1a\u5b83\u662f\u5c06\u88ab\u6d4b\u7269\u8d28\u79bb\u5b50\u5316\uff0c\u6309\u79bb\u5b50\u7684\u8d28\u8377\u6bd4\u5206\u79bb\uff0c\u6d4b\u91cf\u5404\u79cd\u79bb\u5b50\u8c31\u5cf0\u7684\u5f3a\u5ea6\u800c\u5b9e\u73b0\u5206\u6790\u76ee\u7684\u7684\u4e00\u79cd\u5206\u6790\u65b9\u6cd5\u3002\u8d28\u91cf\u662f\u7269\u8d28\u7684\u56fa\u6709\u7279\u5f81\u4e4b\u4e00\uff0c\u4e0d\u540c\u7684\u7269\u8d28\u6709\u4e0d\u540c\u7684\u8d28\u91cf\u8c31\uff08\u8d28\u8c31\uff09\uff0c\u5229\u7528\u8fd9\u4e00\u6027\u8d28\uff0c\u53ef\u4ee5\u8fdb\u884c\u5b9a\u6027\u5206\u6790\uff08\u5305\u62ec\u5206\u5b50\u8d28\u91cf\u548c\u76f8\u5173\u7ed3\u6784\u4fe1\u606f\uff09\uff1b\u8c31\u5cf0\u5f3a\u5ea6\u4e5f\u4e0e\u5b83\u4ee3\u8868\u7684\u5316\u5408\u7269\u542b\u91cf\u6709\u5173\uff0c\u53ef\u4ee5\u7528\u4e8e\u5b9a\u91cf\u5206\u6790\u3002<\/p>\n<p style=\"text-align: left;\">\u5206\u5149\u5149\u5ea6\u8ba1\u6cd5\uff1a\u5206\u5149\u5149\u5ea6\u8ba1\u91c7\u7528\u4e00\u4e2a\u53ef\u4ee5\u4ea7\u751f\u591a\u4e2a\u6ce2\u957f\u7684\u5149\u6e90\uff0c\u901a\u8fc7\u7cfb\u5217\u5206\u5149\u88c5\u7f6e\uff0c\u4ece\u800c\u4ea7\u751f\u7279\u5b9a\u6ce2\u957f\u7684\u5149\u6e90\uff0c\u5149\u7ebf\u900f\u8fc7\u6d4b\u8bd5\u7684\u6837\u54c1\u540e\uff0c\u90e8\u5206\u5149\u7ebf\u88ab\u5438\u6536\uff0c\u8ba1\u7b97\u6837\u54c1\u7684\u5438\u5149\u503c\uff0c\u4ece\u800c\u8f6c\u5316\u6210\u6837\u54c1\u7684\u6d53\u5ea6\uff0c\u5438\u5149\u503c\u4e0e\u6837\u54c1\u7684\u6d53\u5ea6\u6210\u6b63\u6bd4\u3002\u5b83\u5305\u62ec\u53ef\u89c1\u5206\u5149\u5149\u5ea6\u8ba1\u548c\u7d2b\u5916\u5206\u5149\u5149\u5ea6\u8ba1\u3002<\/p>\n<p style=\"text-align: left;\">\u706b\u82b1\u76f4\u8bfb\u5149\u8c31\u4eea\uff1a\u706b\u82b1\u76f4\u8bfb\u5149\u8c31\u4eea\u7528\u7535\u5f27\uff08\u6216\u706b\u82b1\uff09\u7684\u9ad8\u6e29\u4f7f\u6837\u54c1\u4e2d\u5404\u5143\u7d20\u4ece\u56fa\u6001\u76f4\u63a5\u6c14\u5316\u5e76\u88ab\u6fc0\u53d1\u800c\u53d1\u5c04\u51fa\u5404\u5143\u7d20\u7684\u7279\u5f81\u6ce2\u957f\uff0c\u7528\u5149\u6805\u5206\u5149\u540e\uff0c\u6210\u4e3a\u6309\u6ce2\u957f\u6392\u5217\u7684\u201c\u5149\u8c31\u201d\uff0c\u8fd9\u4e9b\u5143\u7d20\u7684\u7279\u5f81\u5149\u8c31\u7ebf\u901a\u8fc7\u51fa\u5c04\u72ed\u7f1d\uff0c\u5c04\u5165\u5404\u81ea\u7684\u5149\u7535\u500d\u589e\u7ba1\uff0c\u5149\u4fe1\u53f7\u53d8\u6210\u7535\u4fe1\u53f7\uff0c\u7ecf\u4eea\u5668\u7684\u63a7\u5236\u6d4b\u91cf\u7cfb\u7edf\u5c06\u7535\u4fe1\u53f7\u79ef\u5206\u5e76\u8fdb\u884c\u6a21\/\u6570\u8f6c\u6362\uff0c\u7136\u540e\u7531\u8ba1\u7b97\u673a\u5904\u7406\uff0c\u5e76\u6253\u5370\u51fa\u5404\u5143\u7d20\u7684\u767e\u5206\u542b\u91cf\u3002<\/p>\n<p style=\"text-align: left;\"><strong>7 \u603b\u7ed3<\/strong><\/p>\n<p style=\"text-align: left;\">\u672c\u6587\u4e3b\u8981\u4ecb\u7ecd\u4e86\u6750\u6599\u6210\u5206\u542b\u91cf\u5206\u6790\u7684\u5e38\u7528\u65b9\u6cd5\uff0c\u8fd9\u4e9b\u65b9\u6cd5\u5404\u6709\u5176\u7279\u70b9\uff0c\u73b0\u901a\u8fc7\u88682\u5c06\u5b83\u4eec\u8fdb\u884c\u7b80\u5355\u7684\u6c47\u603b\u3001\u6bd4\u8f83\u3002\u5728\u4e86\u89e3\u4e86\u8bd5\u6837\u7684\u7279\u6027\u548c\u5206\u6790\u65b9\u6cd5\u7684\u7279\u70b9\u540e\uff0c\u53ef\u4ee5\u901a\u8fc7\u88682\u5bf9\u6750\u6599\u6210\u5206\u6d4b\u8bd5\u65b9\u6cd5\u8fdb\u884c\u7b80\u5355\u7684\u9009\u62e9\uff0c\u6216\u8005\u8fdb\u884c\u7ec4\u5408\u5df2\u8fbe\u5230\u5206\u6790\u76ee\u7684\u3002<\/p>\n<p style=\"text-align: left;\">\u88682 \u6750\u6599\u6210\u5206\u5206\u6790\u65b9\u6cd5\u7684\u6c47\u603b\u6bd4\u8f83<\/p>\n<table class=\" aligncenter\" style=\"height: 1228px;\" width=\"637\">\n<tbody>\n<tr style=\"height: 56px;\">\n<td style=\"width: 55px; height: 56px;\">\n<p>\u9879\u76ee<\/p>\n<\/td>\n<td style=\"width: 84px; height: 56px;\">\n<p>\u6837\u54c1<\/p>\n<\/td>\n<td style=\"width: 84px; height: 56px;\">\n<p>\u5206\u6790\u9879\u76ee<\/p>\n<\/td>\n<td style=\"width: 150px; height: 56px;\">\n<p>\u4e3b\u8981\u4f18\u70b9<\/p>\n<\/td>\n<td style=\"width: 104px; height: 56px;\">\n<p>\u4e3b\u8981\u7f3a\u70b9<\/p>\n<\/td>\n<td style=\"width: 122px; height: 56px;\">\n<p>\u5907\u6ce8<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 152px;\">\n<td style=\"width: 55px; height: 152px;\">\n<p>\u5316\u5b66\u6cd5<\/p>\n<\/td>\n<td style=\"width: 84px; height: 152px;\">\n<p>\u6ef4\u5b9a\u6cd5\u4e3a\u6db2\u4f53\uff1b\u91cd\u91cf\u6cd5\u548c\u71c3\u70e7\u5206\u6790\u6cd5\u53ef\u4ee5\u4e3a\u6db2\u4f53\u6216\u56fa\u4f53<\/p>\n<\/td>\n<td style=\"width: 84px; height: 152px;\">\n<p>\u6210\u5206\u5b9a\u6027\u5206\u6790\uff1b\u6210\u5206\u5b9a\u91cf\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 150px; height: 152px;\">\n<p>\u51c6\u786e\u5ea6\u9ad8\uff1b\u6210\u672c\u4f4e<\/p>\n<\/td>\n<td style=\"width: 104px; height: 152px;\">\n<p>\u7e41\u7410\u590d\u6742\uff1b\u8d39\u65f6\u8d39\u529b<\/p>\n<\/td>\n<td style=\"width: 122px; height: 152px;\">\n<p>\u53ef\u4f5c\u4e3a\u6821\u6b63\u4eea\u5668\u7684\u6807\u51c6\uff1b\u5176\u4ed6\u65b9\u6cd5\u4e0d\u51c6\u786e\u65f6\u4f7f\u7528<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 104px;\">\n<td style=\"width: 55px; height: 104px;\">\n<p>OES<\/p>\n<\/td>\n<td style=\"width: 84px; height: 104px;\">\n<p>\u6db2\u4f53\uff0c\u5206\u6790\u65f6\u4e3a\u6c14\u6001\u539f\u5b50<\/p>\n<\/td>\n<td style=\"width: 84px; height: 104px;\">\n<p>\u5143\u7d20\u5b9a\u6027\u5206\u6790\uff1b\u5143\u7d20\u5b9a\u91cf\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 150px; height: 104px;\">\n<p>\u7075\u654f\u5ea6\u9ad8\uff1b\u51c6\u786e\u5ea6\u9ad8\uff1b\u6837\u54c1\u7528\u91cf\u5c11\uff1b\u5206\u6790\u901f\u5ea6\u5feb<\/p>\n<\/td>\n<td style=\"width: 104px; height: 104px;\">\n<p>\u4e0d\u9002\u4e8e\u68c0\u6d4b\u78b1\u91d1\u5c5e\uff1b\u56fa\u4f53\u6837\u54c1\u5236\u6837\u7e41\u7410<\/p>\n<\/td>\n<td style=\"width: 122px; height: 104px;\">\n<p>\u662f\u5206\u6790\u65e0\u673a\u7269\u6700\u597d\u7684\u5b9a\u6027\u548c\u534a\u5b9a\u91cf\u5206\u6790\u65b9\u6cd5<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 128px;\">\n<td style=\"width: 55px; height: 128px;\">\n<p>AAS<\/p>\n<\/td>\n<td style=\"width: 84px; height: 128px;\">\n<p>\u6db2\u4f53\uff0c\u5206\u6790\u65f6\u4e3a\u539f\u5b50\u84b8\u6c7d<\/p>\n<\/td>\n<td style=\"width: 84px; height: 128px;\">\n<p>\u5143\u7d20\u5b9a\u91cf\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 150px; height: 128px;\">\n<p>\u7075\u654f\u5ea6\u9ad8\uff1b\u51c6\u786e\u5ea6\u8f83\u9ad8\uff1b\u8bbe\u5907\u7b80\u5355\uff0c\u64cd\u4f5c\u65b9\u4fbf\uff0c\u5206\u6790\u901f\u5ea6\u5feb<\/p>\n<\/td>\n<td style=\"width: 104px; height: 128px;\">\n<p>\u4e0d\u80fd\u505a\u5b9a\u6027\u5206\u6790\uff1b\u4e0d\u4fbf\u4e8e\u5355\u5143\u7d20\u6d4b\u5b9a<\/p>\n<\/td>\n<td style=\"width: 122px; height: 128px;\">\n<p>\u96be\u5bb9\u5143\u7d20\u7075\u654f\u5ea6\u4f4e\uff1b\u67d0\u4e9b\u5143\u7d20\u65e0\u6cd5\u6d4b\u5b9a\uff08P\u3001S\uff09\uff1b<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 176px;\">\n<td style=\"width: 55px; height: 176px;\">\n<p>XRF<\/p>\n<\/td>\n<td style=\"width: 84px; height: 176px;\">\n<p>\u56fa\u4f53\uff1b\u6db2\u4f53<\/p>\n<\/td>\n<td style=\"width: 84px; height: 176px;\">\n<p>\u5143\u7d20\u5b9a\u6027\u5206\u6790\uff1b\u5143\u7d20\u5b9a\u91cf\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 150px; height: 176px;\">\n<p>\u65b9\u4fbf\u5feb\u6377\uff0c\u53ef\u4e00\u6b21\u6d4b\u5b9a\u591a\u4e2a\u5143\u7d20\uff1b\u5236\u6837\u7b80\u5355<\/p>\n<\/td>\n<td style=\"width: 104px; height: 176px;\">\n<p>\u9700\u8981\u6837\u54c1\u8f83\u591a\uff1b\u68c0\u51fa\u9650\u4e0d\u591f\u4f4e\uff0c\u4e0d\u9002\u7528\u4e8e\u5206\u6790\u8f7b\u5143\u7d20\uff0c\u51c6\u786e\u5b9a\u91cf\u5206\u6790\u4f9d\u8d56\u6807\u6837<\/p>\n<\/td>\n<td style=\"width: 122px; height: 176px;\">\n<p>\u65b9\u4fbf\u7528\u4e8e\u539f\u4f4d\u548c\u73b0\u573a\u7684\u5206\u6790<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 128px;\">\n<td style=\"width: 55px; height: 128px;\">\n<p>EDX<\/p>\n<\/td>\n<td style=\"width: 84px; height: 128px;\">\n<p>\u56fa\u4f53<\/p>\n<\/td>\n<td style=\"width: 84px; height: 128px;\">\n<p>\u5143\u7d20\u5b9a\u6027\u5206\u6790\uff1b\u534a\u5b9a\u91cf\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 150px; height: 128px;\">\n<p>\u7075\u654f\u5ea6\u9ad8\uff080.1%\uff09\uff1b\u53ef\u540c\u65f6\u6d4b\u91cf\u6240\u6709\u5143\u7d20\uff0c\u5206\u6790\u6548\u7387\u9ad8\uff1b\u5bf9\u6837\u54c1\u635f\u4f24\u5c0f<\/p>\n<\/td>\n<td style=\"width: 104px; height: 128px;\">\n<p>\u5206\u8fa8\u7387\u8f83\u5dee\uff1b\u8c31\u5cf0\u91cd\u53e0\u4e25\u91cd\uff1b\u5b9a\u91cf\u5206\u6790\u51c6\u786e\u5ea6\u4e00\u822c<\/p>\n<\/td>\n<td style=\"width: 122px; height: 128px;\">\n<p>\u53ef\u4ee5\u4e0eSEM\u6216TEM\u7ed3\u5408\u4f7f\u7528\uff0c\u8fdb\u884c\u70b9\u3001\u7ebf\u3001\u9762\u626b\u63cf<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 152px;\">\n<td style=\"width: 55px; height: 152px;\">\n<p>AES<\/p>\n<\/td>\n<td style=\"width: 84px; height: 152px;\">\n<p>\u5bfc\u7535\u56fa\u4f53<\/p>\n<\/td>\n<td style=\"width: 84px; height: 152px;\">\n<p>\u6210\u5206\u5b9a\u6027\u5206\u6790\uff1b\u534a\u5b9a\u91cf\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 150px; height: 152px;\">\n<p>\u76f8\u5bf9\u7075\u654f\u5ea6\u9ad8\uff1b\u5206\u6790\u901f\u5ea6\u5feb\uff1b\u9002\u4e8e\u6df1\u5ea6\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 104px; height: 152px;\">\n<p>\u5b9a\u91cf\u5206\u6790\u51c6\u786e\u5ea6\u4e00\u822c\uff1b\u5bf9\u6837\u54c1\u8981\u6c42\u9ad8\uff0c\u8868\u9762\u5fc5\u987b\u6e05\u6d01<\/p>\n<\/td>\n<td style=\"width: 122px; height: 152px;\">\n<p>\u975e\u5e38\u9002\u7528\u4e8e\u5b9a\u6027\u5206\u6790\uff1b\u9002\u4e8e\u539f\u5b50\u5e8f\u6570\u8f83\u5c0f\uff08Z\uff1c33\uff09\u7684\u7684\u5143\u7d20\u5206\u6790<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 176px;\">\n<td style=\"width: 55px; height: 176px;\">\n<p>XPS<\/p>\n<\/td>\n<td style=\"width: 84px; height: 176px;\">\n<p>\u6c14\u4f53\u6216\u56fa\u4f53<\/p>\n<\/td>\n<td style=\"width: 84px; height: 176px;\">\n<p>\u5143\u7d20\u5b9a\u6027\u5206\u6790\uff1b\u5143\u7d20\u5b9a\u91cf\u5206\u6790<\/p>\n<\/td>\n<td style=\"width: 150px; height: 176px;\">\n<p>\u7edd\u5bf9\u7075\u654f\u5ea6\u9ad8\uff1b\u5206\u6790\u901f\u5ea6\u5feb\uff0c\u53ef\u591a\u5143\u7d20\u540c\u65f6\u8fdb\u884c\uff1b\u5b9a\u91cf\u5206\u6790\u4e0d\u9700\u53c2\u6bd4\u7269<\/p>\n<\/td>\n<td style=\"width: 104px; height: 176px;\">\n<p>\u76f8\u5bf9\u7075\u654f\u5ea6\u4e0d\u9ad8\uff08\uff1e0.1%\uff09<\/p>\n<\/td>\n<td style=\"width: 122px; height: 176px;\">\n<p>\u9002\u7528\u4e8e\u539f\u5b50\u5e8f\u6570\u8f83\u5927\u7684\u5143\u7d20\u5206\u6790\uff1b\u83b7\u5f97\u7684\u4fe1\u606f\u591a\uff1b\u53ef\u4ee5\u8fdb\u884c\u4ef7\u6001\u5206\u6790\u548c\u5316\u5b66\u73af\u5883\u7814\u7a76<\/p>\n<\/td>\n<\/tr>\n<tr style=\"height: 104px;\">\n<td style=\"width: 55px; height: 104px;\">\n<p>\u5176\u4ed6\u65b9\u6cd5<\/p>\n<\/td>\n<td style=\"width: 568px; height: 104px;\" colspan=\"5\">\n<p>\u5176\u4ed6\u65b9\u6cd5\u4e0d\u592a\u9002\u7528\u65f6\u4f7f\u7528\u3002XRD\u53ef\u7528\u4e8e\u533a\u5206\u7269\u76f8\uff0c\u800c\u4e0a\u8ff0\u4e00\u4e9b\u65b9\u6cd5\u53ea\u80fd\u7528\u6765\u533a\u5206\u5143\u7d20\uff1b\u5206\u5149\u5149\u5ea6\u8ba1\u6cd5\u5219\u6bd4\u8f83\u65b9\u4fbf\uff0c\u6210\u672c\u5f88\u4f4e\uff0c\u5bf9\u67d0\u4e9b\u5b9e\u9a8c\u7279\u522b\u4f7f\u7528\uff1b\u706b\u82b1\u76f4\u8bfb\u5149\u8c31\u4eea\u5219\u5e38\u5e38\u7528\u5728\u51b6\u91d1\u65b9\u9762\u3002<\/p>\n<\/td>\n<\/tr>\n<\/tbody>\n<\/table>\n<p><strong>\u53c2\u8003\u6587\u732e\uff1a<\/strong><\/p>\n<p>[1]\u6731\u6c38\u6cd5, \u5b97\u745e\u9686, \u59da\u6587\u6e05, \u7b49. \u6750\u6599\u5206\u6790\u5316\u5b66[M], \u5317\u4eac: \u5316\u5b66\u5de5\u4e1a\u51fa\u7248\u793e, 2009.<\/p>\n<p style=\"text-align: left;\">[2]\u5434\u521a. \u6750\u6599\u7ed3\u6784\u8868\u5f81\u53ca\u5e94\u7528[M], \u5317\u4eac: \u5316\u5b66\u5de5\u4e1a\u51fa\u7248\u793e, 2002.<\/p>\n<p style=\"text-align: left;\">[3]\u6234\u6625\u9e3f. \u4e1c\u7535\u6750\u6599\u5316\u5b66\u6210\u5206\u5206\u6790\u6280\u672f\u53d1\u5c55\u7efc\u8ff0[J], \u4e1c\u65b9\u673a\u7535, 2007(3): 77-79.<\/p>\n<p style=\"text-align: left;\">[4]Daniel C Harris. Quantitative Chemical Analysis[M], New York: W. H. Freeman and Company, 2010.<\/p>\n<p style=\"text-align: left;\">[5]Pei\u00a0J. Method for determining metallic iron in reduction product of titanium powder, involves weighing dried sample, placing in flask, adding ferric chloride, stirring followed by adding diphenylamine sulfonate indicator, cooling and determining: China, CN104678048-A[P], 2015.<\/p>\n<p style=\"text-align: left;\">[6]\u9648\u654f\u82b3, \u674e\u6c38\u6ce2. \u7528\u56db\u82ef\u787c\u94a0\u548c\u55b9\u94bc\u67e0\u916e\u91cd\u91cf\u6cd5\u6d4b\u5b9a\u78f7\u9178\u4e8c\u6c22\u94be\u5316\u80a5[J], \u571f\u58e4\u80a5\u6599, 1994(2), 45-46.<\/p>\n<p style=\"text-align: left;\">[7]Muhammad Nawaz Tahir , Bernd Oschmann , Daniel Buchholz, et al. Extraordinary Performance of Carbon-Coated Anatase TiO2 as Sodium-Ion Anode[J], Advanced energy materials, 2016, 6,1501489.<\/p>\n<p style=\"text-align: left;\">[8]Zou HT. Discussion on Quimociac reagent solution for determination of P<sub>2<\/sub>O<sub>5<\/sub>[J], Phosphate &amp; Compound Fertilizer, 2000, 14(4): 58-60.<\/p>\n<p style=\"text-align: left;\">[9]Hsieh\u00a0CT, Pai\u00a0CT, Chen\u00a0YF,\u00a0et al.\u00a0Preparation of lithium iron phosphate cathode materials with different carbon contents using glucose additive for Li-ion batteries[J], Journal of the Taiwan Institute of Chemical Engineers, 2014, 45: 1501-1508.<\/p>\n<p style=\"text-align: left;\">[10]Jing Du, Kong\u00a0LB, Liu\u00a0H,\u00a0et al.\u00a0Template-free synthesis of porous\u2013LiFePO<sub>4<\/sub>\/C nanocomposite for high\u00a0power lithium-ion batteries[J], Electrochimica Acta, 2014, 123: 1-6.<\/p>\n<p style=\"text-align: left;\">[11]Jose M Andrade Garda. Basic Chemometric Techniques in Atomic Spectroscopy[M], Cambridge: The Royal Society of Chemistry, 2013.<\/p>\n<p style=\"text-align: left;\">[12]\u5de6\u6f14\u58f0, \u9648\u6587\u54f2, \u6881\u4f1f. \u6750\u6599\u73b0\u4ee3\u5206\u6790\u65b9\u6cd5[M], \u5317\u4eac: \u5317\u4eac\u5de5\u4e1a\u5927\u5b66\u51fa\u7248\u793e, 2000.<\/p>\n<p style=\"text-align: left;\">[13]Schrenk\u00a0WG. Historical development of flame excitation sources for analytical spectroscopy[J], Applied Spectroscopy, 1986, 40(1): 19.<\/p>\n<p style=\"text-align: left;\">[14]Mavrodineanu R, Boiteux H. Flame Spectroscopy[M], New York: John Wiley, 1965.<\/p>\n<p style=\"text-align: left;\">[15]R Kellner, JM Mermet, M Otto, et al. Analytical Chemistry[M], New York: Wiley-VCH, 1998.<\/p>\n<p style=\"text-align: left;\">[16]Montaser A, Golightly DW(Eds.). Inductively Coupled Plasmas in Analytical Atomic Spectrometry[M], New York: VCH Publishers, 1987.<\/p>\n<p style=\"text-align: left;\">[17]Moore GL. Introduction to Inductively Coupled Plasmas in Analytical Atomic Spectrometry[M], Amsterdam: Elsevier, 1989.<\/p>\n<p style=\"text-align: left;\">[18]Thompson M, Walsh JN. Handbook of Inductively Coupled Plasmas Spectrometry[M], Glasgow: Blackie, 1989.<\/p>\n<p style=\"text-align: left;\">[19]\u90b9\u672c\u4e1c, \u6556\u767b\u9ad8\u5a03, \u5c1a\u6d2a\u5c71, \u7b49. \u53cc\u5411\u89c6ICP-OES \u6cd5\u540c\u65f6\u6d4b\u5b9a\u8910\u7164\u4e2d\u9517\u548c\u4e00\u4e9b\u4e3b\u8981\u6210\u7070\u5143\u7d20[J], \u5149\u8c31\u5b66\u4e0e\u5149\u8c31\u5206\u6790, 2005, 25(9): 1496-1499.<\/p>\n<p style=\"text-align: left;\">[20]\u674e\u4ed5\u8f89, \u8d75\u8273. \u539f\u5b50\u5438\u6536\u5149\u8c31\u5206\u6790\u6280\u672f\u4e0e\u5e94\u7528[J], \u5ffb\u5dde\u5e08\u8303\u5b66\u9662\u5b66\u62a5, 2008, 24(2): 25-27.<\/p>\n<p style=\"text-align: left;\">[21]\u674e\u96ef, \u675c\u79c0\u6708. \u539f\u5b50\u5438\u6536\u5149\u8c31\u6cd5\u53ca\u5176\u5e94\u7528[J], \u76d0\u6e56\u7814\u7a76, 2003, 1(4): 67-72.<\/p>\n<p style=\"text-align: left;\">[22]\u5d14\u6885\u751f, \u5f20\u6c38\u5947, \u949f\u5f3a\u7b49. \u6c7d\u8f66\u5c3e\u6c14\u50ac\u5316\u5242\u8d35\u91d1\u5c5e\u542b\u91cf\u624b\u6301 XRF \u68c0\u6d4b\u6280\u672f\u7814\u7a76[J], \u9ec4\u91d1, 2018(11).<\/p>\n<p style=\"text-align: left;\">[23]\u5f20\u8f89, \u5510\u6770. \u539f\u5b50\u5438\u6536\u5149\u8c31\u6cd5\u6d4b\u5b9a\u852c\u83dc\u4e2d\u7684\u94c1\u3001\u9530\u3001\u94dc\u3001\u94c5\u548c\u9549[J], \u5149\u8c31\u5b9e\u9a8c\u5ba4, 2011, 28(1): 72-74.<\/p>\n<p style=\"text-align: left;\">[24]\u5f20\u9510.\u00a0\u73b0\u4ee3\u6750\u6599\u5206\u6790\u65b9\u6cd5[M], \u5317\u4eac: \u5316\u5b66\u5de5\u4e1a\u51fa\u7248\u793e, 2007.<\/p>\n<p style=\"text-align: left;\">[25]Paul van der Heide. X-ray photoelectron spectroscopy: an introduction to principles and practices[M], Hoboken: John Wiley &amp; Sons, 2012.<\/p>\n<p style=\"text-align: left;\">[26]\u7fdf\u9752\u971e, \u9ec4\u6d77\u86df, \u5218\u4e1c. \u89e3\u6790SEM&amp;EDS\u5206\u6790\u539f\u7406\u53ca\u5e94\u7528[J], \u68c0\u6d4b\u4e0e\u6d4b\u8bd5, 2012, 5: 66-70.<\/p>\n<p style=\"text-align: left;\">[27]\u5468\u7389.\u00a0\u6750\u6599\u5206\u6790\u65b9\u6cd5[M], \u5317\u4eac: \u673a\u68b0\u5de5\u4e1a\u51fa\u7248\u793e, 2011.<\/p>\n<p style=\"text-align: left;\">[28]Tsai\u00a0JZ, Chen\u00a0CJ, Kalpana\u00a0Settu,\u00a0et al.\u00a0Screen-printed\u00a0carbon\u00a0electrode-based\u00a0electrochemical\u00a0immunosensor\u00a0for rapid\u00a0detection\u00a0of\u00a0microalbuminuria[J], Biosensors\u00a0and\u00a0Bioelectronics, 2016, 77: 1175\u20131182.<\/p>\n<p style=\"text-align: left;\">[29]\u675c\u5e0c\u6587, \u539f\u7eed\u6ce2. \u6750\u6599\u5206\u6790\u65b9\u6cd5[M], \u5929\u6d25: \u5929\u6d25\u5927\u5b66\u51fa\u7248\u793e, 2014.<\/p>\n<p style=\"text-align: left;\">[30]Watts J F, Wolstenholme J. 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Enhanced catalytic activity of the surface modified TiO<sub>2<\/sub>-MWCNT\u00a0nanocomposites under visible light[J],\u00a0Journal of Colloid and Interface Science, 2016, 465: 93-105.<\/p>\n<p>\u672c\u6587\u7531<strong>\u6750\u6599\u4eba\u79d1\u6280\u987e\u95ee\u738b\u535a\u96c5<\/strong>\u4f9b\u7a3f\uff0c\u7f16\u8f91\u90e8\u7f16\u8f91\u6574\u7406\u3002<\/p>\n<p><strong><b>\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1acailiaorenVIP<\/b><\/strong><\/p>\n<p>\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com\u3002<\/p>\n","protected":false},"excerpt":{"rendered":"<p>1\u00a0\u524d\u8a00 \u6750\u6599\u79d1\u5b66\u7684\u4e3b\u8981\u5185\u5bb9\u5c31\u662f\u7814\u7a76\u6750\u6599\u7684\u7ec4\u6210\u4e0e\u7ed3\u6784\u3001\u5f62\u8c8c\u4e0e\u7f3a\u9677\u7b49\u5bf9\u6750\u6599\u6027\u80fd\u7684\u5f71\u54cd\uff0c\u800c\u8fd9\u4e9b\u7814\u7a76\u4e0e\u6750\u6599\u5206\u6790\u65b9\u6cd5\u7d27\u5bc6\u76f8\u5173[1]\u3002\u6750\u6599\u5206\u6790\u53ef\u5206\u4e3a\u4e09\u5927\u65b9\u9762\uff1a\u6750\u6599\u7ed3\u6784\u7684\u6d4b&#8230;<\/p>\n","protected":false},"author":10213,"featured_media":0,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[533],"tags":[],"class_list":["post-161573","post","type-post","status-publish","format-standard","hentry","category-zongshu"],"_links":{"self":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/161573"}],"collection":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/users\/10213"}],"replies":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=161573"}],"version-history":[{"count":8,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/161573\/revisions"}],"predecessor-version":[{"id":161607,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/161573\/revisions\/161607"}],"wp:attachment":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=161573"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=161573"},{"taxonomy":"post_tag","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=161573"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}