{"id":146410,"date":"2018-07-18T06:36:28","date_gmt":"2018-07-17T22:36:28","guid":{"rendered":"\/\/m.iemloyee.com\/?p=146410"},"modified":"2018-07-17T22:38:05","modified_gmt":"2018-07-17T14:38:05","slug":"nature%e5%ad%90%e5%88%8a%ef%bc%9a%e5%8c%97%e5%b7%a5%e5%a4%a7%e9%9a%8b%e6%9b%bc%e9%be%84%e8%af%be%e9%a2%98%e7%bb%84%e5%9c%a8%e5%85%89%e5%82%ac%e5%8c%96%e4%ba%a7%e6%b0%a2%e6%9c%ba%e7%90%86%e7%a0%94","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=146410","title":{"rendered":"Nature\u5b50\u520a\uff1a\u5317\u5de5\u5927\u968b\u66fc\u9f84\u8bfe\u9898\u7ec4\u5728\u5149\u50ac\u5316\u4ea7\u6c22\u673a\u7406\u7814\u7a76\u65b9\u9762\u53d6\u5f97\u7a81\u7834\u8fdb\u5c55"},"content":{"rendered":"<p><strong><b>\u3010\u5f15\u8a00\u3011<\/b><\/strong><\/p>\n<p>\u5149\u50ac\u5316\u6c34\u88c2\u89e3\u4ea7\u6c22\uff0c\u662f\u4e00\u79cd\u6709\u6548\u7684\u6c22\u80fd\u751f\u4ea7\u6280\u672f\u624b\u6bb5\u30021972\u5e74\uff0c\u65e5\u672c\u5b66\u8005Fujishima\u9996\u6b21\u62a5\u9053\u4e86TiO<sub>2<\/sub>\u53ef\u4ee5\u5728\u5149\u7167\u6761\u4ef6\u4e0b\uff0c\u50ac\u5316\u6c34\u88c2\u89e3\u4ea7\u6c22\u3002\u8fd140\u5e74\u6765\uff0c\u968f\u7740\u5149\u50ac\u5316\u79d1\u5b66\u7684\u4e0d\u65ad\u53d1\u5c55\u4ee5\u53ca\u5149\u50ac\u5316\u673a\u7406\u7814\u7a76\u7684\u4e0d\u65ad\u6df1\u5165\uff0c\u5229\u7528\u5404\u79cd\u6280\u672f\u624b\u6bb5\uff0c\u6765\u76f4\u63a5\u89c2\u5bdf\u6c34\u4e0e\u50ac\u5316\u5242\u754c\u9762\u7684\u5316\u5b66\u53d8\u5316\u8fc7\u7a0b\uff0c\u6210\u4e3a\u5f53\u4eca\u754c\u9762\u5316\u5b66\u7814\u7a76\u9886\u57df\u7684\u96be\u70b9\u4e0e\u70ed\u70b9\u3002\u5c3d\u7ba1\u6700\u8fd1\u51e0\u5e74\u6709\u4e9b\u7814\u7a76\u7ec4\u63a2\u7d22\u8fc7\u6c34\u4e0e\u50ac\u5316\u5242\u754c\u9762\u7684\u76f8\u4e92\u4f5c\u7528\uff0c\u7136\u800c\u5927\u591a\u6570\u5b9e\u9a8c\u548c\u7406\u8bba\u7814\u7a76\u4ecd\u7136\u5c40\u9650\u4e8e\u5728\u5355\u5206\u5b50\u6c34\u5c42\u6216\u8005\u6c34\u84b8\u6c14\u73af\u5883\u6761\u4ef6\u4e0b\u7684\u53cd\u5e94\u8fc7\u7a0b\uff0c\u8fd9\u4e0e\u5b9e\u9645\u5149\u50ac\u5316\u88c2\u89e3\u6c34\u8fc7\u7a0b\u4e2d\u7684\u5149\u7167\u4ee5\u53ca\u6db2\u6001\u6c34\u73af\u5883\u76f8\u5dee\u751a\u8fdc\u3002\u53e6\u5916\u9700\u8981\u6307\u51fa\u7684\u662f\uff0c\u81ea\u7136\u754c\u4e2d\u5927\u591a\u6570\u5149\u50ac\u5316\u4ea7\u6c22\u8fc7\u7a0b\u90fd\u662f\u5728\u56fa\u6db2\u754c\u9762\u8fdb\u884c\u7684\u3002\u56e0\u6b64\uff0c\u5982\u4f55\u53d1\u5c55\u4e00\u79cd\u65b0\u7684\u5b9e\u9a8c\u6280\u672f\u624b\u6bb5\u548c\u8ba1\u7b97\u65b9\u6cd5\uff0c\u80fd\u591f\u5b9e\u73b0\u5728\u6db2\u4f53\u6c34\u4ee5\u53ca\u5149\u7167\u6761\u4ef6\u4e0b\uff0c\u5728\u7eb3\u7c73\u751a\u81f3\u539f\u5b50\u5c3a\u5ea6\u89c2\u5bdf\u5149\u50ac\u5316\u88c2\u89e3\u6c34\u8fc7\u7a0b\u4e2d\u50ac\u5316\u5242\u4e0e\u6c34\u754c\u9762\u7684\u5316\u5b66\u53d8\u5316\u8fc7\u7a0b\uff0c\u8fdb\u800c\u5f04\u6e05\u771f\u5b9e\u5149\u50ac\u5316\u8fc7\u7a0b\u4e2d\u7684\u539f\u5b50\u548c\u7535\u5b50\u7ed3\u6784\uff0c\u5177\u6709\u975e\u5e38\u91cd\u8981\u7684\u79d1\u5b66\u7814\u7a76\u4ef7\u503c\u3002<\/p>\n<p><strong><b>\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/b><\/strong><\/p>\n<p>\u8fd1\u65e5\uff0c\u5317\u4eac\u5de5\u4e1a\u5927\u5b66\u56fa\u4f53\u5fae\u7ed3\u6784\u4e0e\u6027\u80fd\u7814\u7a76\u6240<strong><b>\u968b\u66fc\u9f84\u6559\u6388<\/b><\/strong>\uff08\u901a\u8baf\u4f5c\u8005\uff09\u548c<strong><b>\u5362\u5cb3\u535a\u58eb<\/b><\/strong>\uff08\u7b2c\u4e00\u4f5c\u8005\uff09\uff0c\u4e0e\u9999\u6e2f\u57ce\u5e02\u5927\u5b66\uff08\u539f\u53f0\u6e7e\u6e05\u534e\u5927\u5b66\uff09<strong><b>\u9648\u798f\u8363\u6559\u6388<\/b><\/strong>\uff08\u5171\u540c\u901a\u8baf\uff09\u548c\u5317\u4eac\u822a\u7a7a\u5927\u5b66\u7269\u7406\u5b66\u9662<strong><b>\u5218\u5229\u6c11\u6559\u6388<\/b><\/strong>(\u5171\u540c\u901a\u8baf)\u5408\u4f5c\uff0c\u5728<strong><b>Nature Communication<\/b><\/strong><strong><b>s<\/b><\/strong>\u4e0a\u53d1\u8868\u4e86\u4e00\u7bc7\u9898\u4e3a\u201c<strong><b>Self-hydrogenated shell promoting photocatalytic H<\/b><\/strong><strong><sub><b>2<\/b><\/sub><\/strong><strong><b>\u00a0evolution on anatase TiO<\/b><\/strong><strong><sub><b>2<\/b><\/sub><\/strong>\u201d\u7684\u6587\u7ae0\u3002\u8be5\u79d1\u7814\u56e2\u961f\u6210\u529f\u5c06\u5149\u7ea4\u5f15\u5165\u6db2\u4f53\u73af\u5883\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c\u4e2d\u6765\u539f\u4f4d\u89c2\u5bdf\u5149\u50ac\u5316\u6c34\u88c2\u89e3\u4ea7\u6c22\u53cd\u5e94\u8fc7\u7a0b\u3002\u4ed6\u4eec\u5728\u5176\u524d\u671f\u7814\u7a76\u7535\u5b50\u675f\u8f90\u7167\u5bf9\u6c34\u4ee5\u53ca\u6c27\u5316\u7269\u635f\u4f24\u4f5c\u7528\u673a\u7406\u7684\u57fa\u7840\u4e0a\uff0c\u901a\u8fc7\u7cbe\u786e\u5730\u8c03\u63a7\u7535\u5b50\u675f\u5242\u91cf\uff0c\u6210\u529f\u5730\u5f00\u5c55\u4e86\u53ef\u4ee5\u628a\u7535\u5b50\u8f90\u7167\u635f\u4f24\u548c\u5149\u50ac\u5316\u8fd9\u4e24\u4e2a\u7269\u7406\u73b0\u8c61\u5206\u5f00\u6765\u7684\u539f\u4f4d\u89c2\u5bdf\u5b9e\u9a8c\u3002\u9996\u6b21\u5728\u5b9e\u9a8c\u4e0a\u53d1\u73b0\uff1aTiO<sub>2<\/sub>\u5149\u50ac\u5316\u6c34\u88c2\u89e3\u8fc7\u7a0b\u4e2d\uff0c\u6c22\u539f\u5b50H\u4f1a\u4f18\u5148\u8fdb\u5165\u5230TiO<sub>2<\/sub>\u6676\u683c\u5185\u90e8\uff0c\u5bfc\u81f4Ti<sup>4+<\/sup>\u5411\u4f4e\u4ef7\u6001\u7684Ti<sup>3+<\/sup>\u8f6c\u53d8\uff0c\u8fdb\u800c\u5728TiO<sub>2<\/sub>\u8868\u9762\u5f62\u6210\u7eb3\u7c73\u5c3a\u5ea6\u7684\u6c22\u5316\u5c42\u3002\u7ed3\u5408\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\u8fdb\u4e00\u6b65\u53d1\u73b0\uff0c\u8be5\u5c42\u6c22\u5316\u5c42\u4f1a\u964d\u4f4e\u00a0H<sub>2<\/sub>\u5728\u4e9a\u8868\u9762\u7684\u5f62\u6210\u80fd\uff0c\u663e\u8457\u52a0\u901fH<sub>2<\/sub>\u7684\u5f62\u6210\uff1b\u53e6\u4e00\u65b9\u9762\uff0c\u6c22\u5316\u5c42\u8fd8\u53ef\u4ee5\u4fc3\u4f7fTiO<sub>2<\/sub>\u8868\u9762\u7684\u6c34\u5206\u5b50\u5904\u4e8e\u88c2\u89e3\u6001\uff0c\u8fdb\u800c\u63d0\u9ad8\u5149\u50ac\u5316\u4ea7\u6c22\u6548\u7387\u3002\u8be5\u7814\u7a76\u7ed3\u679c\u63ed\u793a\u51fa\uff1a\u5728\u771f\u5b9e\u5149\u50ac\u5316\u6761\u4ef6\u4e0b\uff0c\u662f\u7387\u5148\u5f62\u6210\u7684TiO<sub>2<\/sub>\u8868\u9762\u6c22\u5316\u5c42\u5bf9\u5149\u50ac\u5316\u8fc7\u7a0b\u8d77\u5230\u5173\u952e\u7684\u4f5c\u7528\uff1b\u800c\u5e76\u975e\u4f20\u7edf\u7406\u8bba\u6240\u8ba4\u4e3a\u7684\u7eafTiO<sub>2<\/sub>\u8868\u9762\u7684\u4f5c\u7528\u3002\u8be5\u7814\u7a76\u7ed3\u679c\u6253\u7834\u4e86\u4f20\u7edf\u8ba4\u77e5\u4e2dTiO<sub>2<\/sub>\u8868\u9762\u672c\u8eab\u51b3\u5b9aTiO<sub>2<\/sub>\u5149\u50ac\u5316\u6548\u7387\u7684\u673a\u7406\uff0c\u5e76\u4e3a\u7406\u89e3\u5b9e\u9645\u5149\u50ac\u5316\u8fc7\u7a0b\u4e2d\u6750\u6599\u8868\u9762\u6210\u5206\u548c\u7535\u5b50\u6001\u7ed3\u6784\uff08Ti<sup>3+<\/sup>\uff09\u53d8\u5316\u5bf9\u5149\u50ac\u5316\u7684\u4f5c\u7528\u673a\u7406\uff0c\u63d0\u4f9b\u4e86\u5168\u65b0\u7684\u8ba4\u8bc6\u548c\u7406\u8bba\u652f\u6301\u3002<\/p>\n<p><strong><b>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/b><\/strong><\/p>\n<p><strong>\u56fe1\uff1a\u5149\u50ac\u5316\u6c34\u88c2\u89e3\u4ea7\u6c22\u8fc7\u7a0b\u4e2dTiO<sub>2<\/sub>\u8868\u9762\u6c22\u5316\u5c42\u7684\u6f14\u53d8<\/strong><br \/>\n <img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-146413 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72471-11.png\" alt=\"\" width=\"600\" height=\"822\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72471-11.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72471-11-219x300.png 219w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/>\uff08a\uff09\u5149\u7167\u6761\u4ef6\u4e0b\uff0c\u6db2\u4f53\u73af\u5883\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c\u88c5\u7f6e\u793a\u610f\u56fe\u3002<\/p>\n<p>\uff08b\uff0cc\uff09\u6db2\u6001\u6c34\u73af\u5883\u4ee5\u53ca\u5149\u7167\u6761\u4ef6\u4e0b\uff0cTiO<sub>2<\/sub>\u8868\u9762\u6c22\u5316\u5c42\u7684\u51fa\u73b0\u4ee5\u53ca\u6c14\u6ce1\u7684\u4ea7\u751f\u3002<\/p>\n<p>\uff08d\uff09 TiO<sub>2<\/sub>\u8868\u9762\u6c22\u5316\u5c42\u7684\u539a\u5ea6\u968f\u7740\u5149\u7167\u65f6\u95f4\u7684\u6f14\u53d8\u3002<\/p>\n<p>\uff08e\uff0cf\uff09 EELS\u8868\u5f81\u6c14\u6ce1\u7684\u6210\u5206\u4ee5\u53caTiO<sub>2<\/sub>\u8868\u9762\u6c22\u5316\u5c42\u7684\u5316\u5b66\u4ef7\u6001\u53d8\u5316\u3002<\/p>\n<p><strong><b>\u56fe<\/b><\/strong><strong><b>2<\/b><\/strong><strong><b>\uff1a<\/b><\/strong><strong><b>H<\/b><\/strong><strong><b>\u539f\u5b50\u8fdb\u5165<\/b><\/strong><strong><b>TiO<\/b><\/strong><strong><sub><b>2<\/b><\/sub><\/strong><strong><b>\u8868\u9762\u7684\u52bf\u5792\u4ee5\u53ca\u6c22\u5316\u5c42\u5bf9\u4ea7\u6c22\u7684\u5f71\u54cd<\/b><\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-146414 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72472-11.png\" alt=\"\" width=\"600\" height=\"760\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72472-11.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72472-11-237x300.png 237w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/>\uff08a\uff09H\u539f\u5b50\u8fdb\u5165TiO<sub>2<\/sub>\u6676\u683c\u7684\u539f\u5b50\u901a\u9053\u3002<\/p>\n<p>\uff08b\uff09H\u539f\u5b50\u8fdb\u5165TiO<sub>2<\/sub>\u6676\u683c\u4e0d\u540c\u901a\u9053\u7684\u8dc3\u8fc1\u52bf\u5792\u3002<\/p>\n<p>\uff08c\uff0cd\uff09\u5149\u50ac\u5316\u8fc7\u7a0b\u4e2dTiO<sub>2<\/sub>\u8868\u9762\u6c22\u5316\u5c42\u4ea7\u751f\u53ca\u5f71\u54cd\u793a\u610f\u56fe\u3002<\/p>\n<p>\uff08e\uff0cf\uff09\u5728\u4e0d\u540cH\/O\u6bd4\u4f8b\u7684\u6c22\u5316TiO<sub>2<\/sub>\u8868\u9762\u4e0aH<sub>2<\/sub>\u5f62\u6210\u4ee5\u53ca\u8131\u5438\u9644\u7684\u52bf\u5792\u3002<\/p>\n<p><strong><b>\u56fe<\/b><\/strong><strong><b>3<\/b><\/strong><strong><b>\uff1a\u5149\u50ac\u5316\u540e\uff0c\u6c22\u5316<\/b><\/strong><strong><b>TiO<\/b><\/strong><strong><sub><b>2<\/b><\/sub><\/strong><strong><b>\u8868\u9762\u8131\u6c22\u540e\u7ed3\u6784\u6f14\u53d8<\/b><\/strong><\/p>\n<p><strong><b>\u00a0<img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-146415 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72473-11.png\" alt=\"\" width=\"600\" height=\"882\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72473-11.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72473-11-204x300.png 204w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/b><\/strong><\/p>\n<p>(a-d) \u5149\u50ac\u5316\u4e0d\u540c\u65f6\u95f4\u540e\u6c22\u5316TiO<sub>2<\/sub>\u8868\u9762\u8131\u6c22\u6240\u5f15\u8d77\u7ed3\u6784\u6f14\u53d8\u7684\u4f4e\u500d\u548c\u9ad8\u500dTEM\u50cf\u53ca\u8868\u5c42\u4e0e\u5185\u90e8\u7684\u5085\u6c0f\u53d8\u6362\u56fe\u3002<\/p>\n<p>(e, f) HAADF\u4ee5\u53caEELS\u89c2\u5bdf\u8131\u6c22\u540eTiO<sub>2<\/sub>\u8868\u9762Ti\u4ef7\u6001\u6f14\u53d8\u3002<\/p>\n<p><strong><b>\u56fe<\/b><\/strong><strong><b>4<\/b><\/strong><strong><b>\uff1a\u8d1f\u8f7d\u50ac\u5316\u5242<\/b><\/strong><strong><b>Pt<\/b><\/strong><strong><b>\u5bf9\u5149\u50ac\u5316<\/b><\/strong><strong><b>TiO<\/b><\/strong><strong><sub><b>2<\/b><\/sub><\/strong><strong><b>\u8868\u9762\u7684\u5f71\u54cd<\/b><\/strong><\/p>\n<p><img loading=\"lazy\" decoding=\"async\" class=\"size-full wp-image-146416 aligncenter\" src=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72474-11.png\" alt=\"\" width=\"600\" height=\"898\" srcset=\"\/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72474-11.png 600w, \/\/m.iemloyee.com\/wp-content\/uploads\/2018\/07\/\u56fe\u72474-11-200x300.png 200w\" sizes=\"(max-width: 600px) 100vw, 600px\" \/><\/p>\n<p>\uff08a\uff09 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