{"id":146269,"date":"2018-07-18T06:30:59","date_gmt":"2018-07-17T22:30:59","guid":{"rendered":"\/\/m.iemloyee.com\/?p=146269"},"modified":"2018-07-17T10:10:48","modified_gmt":"2018-07-17T02:10:48","slug":"nature-mater-%ef%bc%9a%e8%a1%a8%e9%9d%a2%e8%80%97%e5%b0%bd%e5%b1%82%e5%af%b9%e6%8e%ba%e6%9d%82%e5%8d%8a%e5%af%bc%e4%bd%93%e7%ba%b3%e7%b1%b3%e6%99%b6%e4%bd%93%e7%ad%89%e7%a6%bb%e5%ad%90%e4%bd%93","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=146269","title":{"rendered":"Nature Mater.\uff1a\u8868\u9762\u8017\u5c3d\u5c42\u5bf9\u63ba\u6742\u534a\u5bfc\u4f53\u7eb3\u7c73\u6676\u4f53\u7b49\u79bb\u5b50\u4f53\u7279\u6027\u7684\u5f71\u54cd"},"content":{"rendered":"

\u3010\u524d\u8a00\u3011<\/strong><\/p>\n

\u7b80\u5e76\u63ba\u6742\u534a\u5bfc\u4f53\u7eb3\u7c73\u6676(NCs)\u663e\u793a\u72ec\u7279\u7684\u5c40\u57df\u8868\u9762\u7b49\u79bb\u5b50\u4f53\u5171\u632f(LSPR)\u7279\u6027\uff0c\u5176\u4e2d\u4e0e\u91d1\u5c5e\u4e0d\u540c\u7684\u662f\u8f7d\u6d41\u5b50\u6d53\u5ea6\u53ef\u5728\u51e0\u4e2a\u6570\u91cf\u7ea7(1018\u20131021 cm\u2212<\/sup>3<\/sup>)\u4e0a\u8c03\u8c10\u3002\u8f7d\u6d41\u5b50\u6d53\u5ea6\u7684\u8fd9\u79cd\u7075\u6d3b\u6027\u5141\u8bb8LSPR\u9891\u7387(\u03c9LSPR<\/sub>)\u4ece\u53ef\u89c1\u5149\u5230\u4e2d\u7ea2\u5916(IR)\u5149\u8c31\u5e7f\u6cdb\u53d8\u5316\u3002\u03c9LSPR<\/sub>\u7684\u53ef\u8c03\u8c10\u6027\u6e90\u81ea\u4e0e\u7535\u8377\u7f3a\u9677\u76f8\u5173\u7684\u8fc7\u91cf\u7535\u8377\uff0c\u4f8b\u5982\u6c27\u7a7a\u4f4d\u548c\u4e09\u4ef7\u63ba\u6742\u5242\u3001\u6c27\u5316\u8fd8\u539f\u548c\u5149\u5316\u5b66\u5145\u7535\uff0c\u6216\u8005NC\u819c\u4e2d\u7684\u7535\u5316\u5b66\u8c03\u5236\u3002\u91d1\u5c5e\u6c27\u5316\u7269NCs\u7684LSPR\u5df2\u88ab\u5e7f\u6cdb\u5e94\u7528\u4e8e\u667a\u80fd\u7a97\u3001\u5149\u7535\u5b50\u5b66\u3001\u4f20\u611f\u548c\u50ac\u5316\u7b49\u9886\u57df\u3002<\/p>\n

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\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6765\u81ea\u7f8e\u56fd\u5fb7\u5dde\u5927\u5b66\u5965\u65af\u6c40\u5206\u6821\u7684Delia J. Milliron\u6559\u6388<\/strong>\u5728Nature Materials<\/strong>\u4e0a\u53d1\u8868\u6587\u7ae0\uff0c\u9898\u4e3a\uff1aImpacts of surface depletion on the plasmonic properties of doped semiconductor nanocrystals<\/strong>\u3002\u901a\u8fc7\u52a8\u6001\u8f7d\u6d41\u5b50\u5bc6\u5ea6\u8c03\u8c10\u6765\u9610\u9521\u63ba\u6742In2<\/sub>O3<\/sub> (Sn:In2<\/sub>O3<\/sub>) NCs\u4e2dLSPR\u8c03\u5236\u3002\u7814\u7a76\u4eba\u5458\u5408\u6210\u4e86\u4e0d\u540c\u63ba\u6742\u6c34\u5e73\u548c\u5c3a\u5bf8\u7684\u5355\u5206\u6563Sn:In2<\/sub>O3 <\/sub>NCs\uff0c\u5e76\u7ec4\u88c5\u6210\u5747\u5300\u7684\u8584\u819c\u3002\u7136\u540e\u5c06NC\u819c\u5728\u539f\u4f4d\u7535\u5316\u5b66\u7535\u6c60\u4e2d\u5145\u7535\uff0c\u5e76\u76d1\u6d4bLSPR\u8c03\u5236\u5149\u8c31\u3002\u57fa\u4e8eLSPR\u7684\u5149\u8c31\u4f4d\u79fb\u548c\u5f3a\u5ea6\u8c03\u5236\uff0c\u7ed3\u5408\u5149\u5b66\u5efa\u6a21\uff0c\u7814\u7a76\u4eba\u5458\u53d1\u73b0\u7ecf\u5e38\u88ab\u5ffd\u7565\u7684\u534a\u5bfc\u4f53\u7279\u6027\uff0c\u7279\u522b\u662f\u7531\u4e8e\u63ba\u6742\u548c\u8868\u9762\u72b6\u6001\u5f15\u8d77\u7684\u80fd\u5e26\u7ed3\u6784\u6539\u53d8\uff0c\u5f3a\u70c8\u5f71\u54cdLSPR\u8c03\u5236\u3002\u901a\u8fc7\u8868\u9762\u7f3a\u9677\u6001\u7684\u8d39\u7c73\u80fd\u7ea7\u9489\u4ea7\u751f\u6539\u53d8LSPR\u6027\u8d28\u7684\u8868\u9762\u8017\u5c3d\u5c42\uff1b\u5b83\u51b3\u5b9a\u4e86LSPR\u9891\u7387\u8c03\u5236\u7684\u7a0b\u5ea6\uff0c\u964d\u4f4e\u4e86\u9884\u671f\u7684\u8fd1\u573a\u589e\u5f3a\uff0c\u5e76\u4e14\u5927\u5927\u964d\u4f4e\u4e86LSPR\u5bf9\u5468\u56f4\u73af\u5883\u7684\u7075\u654f\u5ea6\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe1. \u534a\u5bfc\u4f53NCs\u4e2d\u7684LSPR<\/strong><\/p>\n

\"\"<\/p>\n

a\u3001\u5e73\u9762\u5e26\u548c\u5f2f\u66f2\u5e26\u6761\u4ef6\u4e0bNC\u80fd\u5e26\u80fd\u91cf\u5b66\u7684\u793a\u610f\u56fe\uff0c\u5176\u4e2dES\u4ee3\u8868\u8868\u9762\u6001\u7535\u52bf\uff1b<\/p>\n

b\u3001\u76f4\u5f84\u5206\u522b\u4e3a8.19 ~ 0.90 nm (i)\u548c13.30 ~ 1.90 nm (ii)\u7684\u5355\u5206\u65633 %\u63ba\u6742Sn:In2<\/sub>O3 <\/sub>NCs\u7684\u900f\u5c04\u7535\u955c\u56fe\u50cf\uff1b<\/p>\n

c\u3001Sn:In2<\/sub>O3<\/sub> NCs\u7684LSPR\u6d88\u5149\u5149\u8c31\uff1b<\/p>\n

\u56fe2. \u7535\u5316\u5b66LSPR\u8c03\u5236<\/strong><\/p>\n

\"\"<\/p>\n

a\u3001\u4f4e\u63ba\u6742\u548c\u9ad8\u63ba\u6742NCs\u7684\u80fd\u5e26\u80fd\u91cf\u5b66\uff1b<\/p>\n

b\u2013e\u3001\u539f\u4f4dFTIR SEC\u5149\u8c31\uff1b<\/p>\n

\u56fe3. NC\u5c3a\u5bf8\u548c\u63ba\u6742\u6d53\u5ea6\u5bf9\u7535\u5316\u5b66LSPR\u8c03\u5236\u7684\u5f71\u54cd<\/strong><\/p>\n

\"\"<\/p>\n

\u4e0d\u540c\u5c3a\u5bf8(a)\u548c\u63ba\u6742\u6d53\u5ea6(b)\u7684Sn:In2<\/sub>O3<\/sub> NCs\u5728\u4e0d\u540c\u7535\u4f4d\u4e0b\u7684LSPR\u5cf0\u503c\u9891\u7387\u4e0e\u57281.5v (\u0394\u03c9LSPR<\/sub>)\u4e0b\u7684LSPR\u5cf0\u503c\u9891\u7387\u7684\u5b9e\u9a8c\u89c2\u5bdf\uff1b<\/p>\n

\u56fe4. \u7535\u5316\u5b66LSPR\u8c03\u5236\u7684\u5149\u5b66\u6a21\u578b<\/strong><\/p>\n

\"\"<\/p>\n

a\u3001\u7528\u4e8e\u83b7\u5f97\u8868\u9762\u8017\u5c3d\u7684Sn:In2<\/sub>O3<\/sub> NC (i)\u7684\u6709\u6548\u4ecb\u7535\u51fd\u6570(\u03b5eff<\/sub>)\u7684\u793a\u610f\u6027\u8fed\u4ee3\u8fc7\u7a0b\uff0c\u4ee5\u53ca\u5c06\u5177\u6709\u6709\u6548\u4ecb\u7535\u51fd\u6570\u7684Sn:In2<\/sub>O3<\/sub> NC\u6d82\u8986\u5728\u6709Sn:In2<\/sub>O3<\/sub>\u8584\u819c\u6d82\u8986\u7684\u73bb\u7483\u886c\u5e95( ii\uff0c\u4e0d\u6309\u6bd4\u4f8b)\u4e0a\u7684\u6a21\u62df\u5939\u5c42\u5355\u5143\u7ed3\u6784\uff1b<\/p>\n

b\u3001c\u3001\u542b1 %\u63ba\u6742- 6 nm (b)\u548c10 %\u63ba\u6742- 14 nm (c) NCs\u7684Sn:In2<\/sub>O3<\/sub> NC\u8584\u819c\u7684\u8ba1\u7b97\u8f7d\u6d41\u5b50\u6d53\u5ea6(Ne<\/sub>)\u5206\u5e03(i)\u548c\u76f8\u5e94\u7684LSPR\u8c31(ii)\uff1b<\/p>\n

\u56fe5. \u6a21\u62df\u5c3a\u5bf8\u548c\u63ba\u6742\u5bf9\u5355\u4e2a\u7684NC\u7684\u0394\u03c9LSPR<\/sub>\u7684\u5f71\u54cd<\/strong><\/p>\n

\"\"<\/p>\n

\u5bf9\u4e8e\u4e0d\u540c\u5c3a\u5bf8(a)\u548c\u63ba\u6742\u6d53\u5ea6(b)\u7684Sn:In2<\/sub>O3<\/sub> NCs\u5728\u4e0d\u540c\u7535\u4f4d\u4e0b\u7684LSPR\u5cf0\u503c\u9891\u79fb(\u0394\u03c9LSPR<\/sub>)\uff1b<\/p>\n

\u56fe6. NC\u7b49\u79bb\u5b50\u4f53\u6fc0\u5143\u7075\u654f\u5ea6<\/strong><\/p>\n

\"\"<\/p>\n

a\u3001Sn:In2<\/sub>O3<\/sub> NCs\u7684\u5c0f\u5c3a\u5bf8\u548c\u5927\u5c3a\u5bf8\u7b49\u79bb\u5b50\u4f53\u7075\u654f\u5ea6;<\/p>\n

b\u3001\u4e0d\u540c\u5c3a\u5bf8\u548c\u63ba\u6742\u6d53\u5ea6\u7684Sn:In2<\/sub>O3<\/sub> NCs\u7684\u7b49\u79bb\u5b50\u4f53\u6fc0\u5143\u7075\u654f\u5ea6\uff1b<\/p>\n

c\u3001\u4e00\u79cd\u7403\u5f621 %\u63ba\u6742Sn:In2<\/sub>O3<\/sub> NCs\u7684\u8fd1\u573a\u589e\u5f3a\u56fe;<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/p>\n

LSPR\u8c03\u5236\u7684\u5f3a\u4f9d\u8d56\u6027\u3001\u5bf9\u5468\u56f4\u73af\u5883\u7684\u654f\u611f\u6027\u4ee5\u53ca\u8fd1\u573a\u589e\u5f3a\u5bf9NCs\u7684\u5c3a\u5bf8\u548c\u63ba\u6742\u6d53\u5ea6\u7684\u4f9d\u8d56\u2014\u2014\u6240\u6709\u8fd9\u4e9b\u90fd\u662f\u7531\u4e8e\u8868\u9762\u8017\u5c3d\u2014\u2014\u7a81\u51fa\u4e86\u5bf9\u4e8e\u7ed9\u5b9a\u5e94\u7528\u5408\u7406\u9009\u62e9NCs\u7684\u91cd\u8981\u6027\u3002\u5bf9\u4e8e\u9700\u8981\u6700\u5927LSPR\u9891\u7387\u548c\u5f3a\u5ea6\u8c03\u5236\u7684\u667a\u80fd\u7a97\u5e94\u7528\uff0c\u4f4e\u63ba\u6742\u548c\u5c0f\u5c3a\u5bf8NCs\u662f\u4f18\u9009\u7684\u3002\u76f8\u6bd4\u4e4b\u4e0b\uff0c\u5bf9\u4e8e\u5149\u5b50\u4e0a\u8f6c\u6362\u3001SEIRA\u548c\u4f20\u611f\u7b49\u5e94\u7528\uff0c\u5176\u4e2d\u529f\u6548\u53d6\u51b3\u4e8eLSPR\u4e0eNC\u9644\u8fd1\u7684\u5176\u4ed6\u5149\u5b66\u5143\u4ef6\u7684\u8026\u5408\uff0c\u9700\u8981\u6700\u5c0f\u5316\u8868\u9762\u635f\u8017\u3002\u6b64\u5916\uff0c\u5c06\u7075\u654f\u5ea6\u3001\u8fd1\u573a\u589e\u5f3a\u548cLSPR\u9891\u7387\u4f5c\u4e3a\u8868\u9762\u7535\u4f4d\u7684\u51fd\u6570\u8fdb\u884c\u8c03\u5236\u7684\u80fd\u529b\u5bf9\u4e8e\u8bf8\u5982\u7535\u5149\u8c03\u5236\u5668\u4ee5\u53ca\u53ef\u8c03\u8c10SEIRA\u548c\u611f\u6d4b\u886c\u5e95\u7684\u5e7f\u6cdb\u5e94\u7528\u5177\u6709\u5f88\u5927\u7684\u5e0c\u671b\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Impacts of surface depletion on the plasmonic properties of doped semiconductor nanocrystals<\/a>, (Nature Materials, 2018, DOI: 10.1038\/s41563-018-0130-5)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u7535\u5b50\u7535\u5de5\u5b66\u672f\u7ec4Z. Chen\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

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