{"id":135443,"date":"2018-04-23T06:30:35","date_gmt":"2018-04-22T22:30:35","guid":{"rendered":"\/\/m.iemloyee.com\/?p=135443"},"modified":"2018-04-19T22:53:41","modified_gmt":"2018-04-19T14:53:41","slug":"jacs%ef%bc%9a0-v%e5%88%9d%e5%a7%8b%e8%bf%87%e7%94%b5%e5%8a%bf%ef%bc%81ni-co-a-a-p-se-o%e5%a4%9a%e5%ad%94%e7%ba%b3%e7%b1%b3%e7%89%87%e9%ab%98%e6%95%88%e6%9e%90%e6%b0%a2","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=135443","title":{"rendered":"JACS\uff1a0 V\u521d\u59cb\u8fc7\u7535\u52bf\uff01Ni-Co-A (A = P, Se, O)\u591a\u5b54\u7eb3\u7c73\u7247\u9ad8\u6548\u6790\u6c22"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

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\u3010\u6210\u679c\u7b80\u4ecb<\/strong>\u3011<\/p>\n

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\u3010\u56fe\u6587\u89e3\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00<\/strong> Ni-Co-A<\/strong>\u5236\u5907\u8fc7\u7a0b<\/strong>\u00a0<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

NCO\u3001NCS\u4e0eNCP\u591a\u5b54\u7eb3\u7c73\u7247\u7684\u5236\u5907\u8fc7\u7a0b\u53ca\u76f8\u5e94\u7684STEM\u56fe\u50cf\uff08\u6bd4\u4f8b\u5c3a\u957f\u5ea6\u4e3a200 nm\uff09<\/p>\n

\u56fe\u4e8c<\/strong> Ni-Co-A<\/strong>\u7684\u7ed3\u6784\u4e0e\u8868\u9762\u5206\u6790<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a<\/strong>) Ni-Co-A\u6837\u54c1\u7684XRD\u56fe\u8c31\uff1b<\/p>\n

(b<\/strong>) NCP\u7684HRTEM\u4e0eSA-ED\u56fe\u8c31\uff08\u6bd4\u4f8b\u5c3a10 nm\uff09\uff1b<\/p>\n

(c<\/strong>) NCP\u5143\u7d20\u5206\u5e03\u56fe\uff08\u6bd4\u4f8b\u5c3a200 nm\uff09\uff1b<\/p>\n

(d<\/strong>) NCP\u7684Ni 2p3\/2<\/sub>\u56fe\u8c31\uff1b<\/p>\n

(e<\/strong>) Co 2p3\/2<\/sub>\u56fe\u8c31\uff1b<\/p>\n

(f<\/strong>) P 2p1\/2<\/sub>\u56fe\u8c31\u3002<\/p>\n

\u56fe\u4e09<\/strong> Ni-Co-A <\/strong>\u7684\u6027\u80fd\u5bf9\u6bd4\u4e0e\u6790\u6c22\u673a\u7406\u5206\u6790<\/strong>\u00a0<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a<\/strong>) Ni-Co-A\u6837\u54c1\u4e0e\u6ce1\u6cab\u954d\u7684LSV\u6781\u5316\u66f2\u7ebf\uff08\u7535\u89e3\u6db2\u4e3a1 M KOH\uff09\uff1b<\/p>\n

(b<\/strong>) Ni-Co-A\u6837\u54c1\u53d8\u6e29\u7535\u963b\u7387\u6d4b\u8bd5\u66f2\u7ebf\uff1b<\/p>\n

(c<\/strong>) \u6c22\u539f\u5b50\u5438\u9644\u6750\u6599\u8868\u9762\u7684\u539f\u5b50\u7ed3\u6784\u793a\u610f\u56fe\uff1b<\/p>\n

(d<\/strong>) NCO (111)\uff0c NCS (010)\uff0c \u4e0e NCP (001) \u6676\u9762\u7684\u6c22\u5438\u9644\u793a\u610f\u56fe\uff1b<\/p>\n

\uff08\u7c89\u8272\u4e0e\u7eff\u8272\u5c0f\u7403\u5206\u522b\u4ee3\u8868Co2+<\/sup>\u4e0eNi2+<\/sup>\uff1b\u68d5\u8272\uff0c\u7ea2\u8272\u4e0e\u84dd\u8272\u5c0f\u7403\u5206\u522b\u4ee3\u8868O\uff0cSe\u4e0eP\uff09<\/p>\n

\u56fe\u56db<\/strong> NCP<\/strong>\u7535\u5316\u5b66\u6027\u80fd\u4e0e\u7a33\u5b9a\u6027\u5206\u6790<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a<\/strong>) \u6ce1\u6cab\u954d\uff0c\u65e0\u5b54NCP\uff0c\u591a\u5b54NCP\u4e0ePt\/C \u7684LSV\u6781\u5316\u66f2\u7ebf\uff1b<\/p>\n

(b<\/strong>)\u6ce1\u6cab\u954d\uff0c NCP\uff0c\u591a\u5b54NCP\u4e0ePt\/C \u7684\u5854\u83f2\u5c14\u659c\u7387\u56fe\uff1b<\/p>\n

(c<\/strong>)\u6ce1\u6cab\u954d\uff0c\u591a\u5b54 Ni2<\/sub>P\uff0c\u591a\u5b54CoP\u4e0e\u591a\u5b54NCP\u7684LSV\u6781\u5316\u66f2\u7ebf\uff1b<\/p>\n

(d<\/strong>) \u591a\u5b54NCP\u7eb3\u7c73\u7247\u5728\u4e0d\u540c\u7535\u89e3\u6db2\u4e2d\u7684LSV\u6781\u5316\u66f2\u7ebf\uff080.5 M H2SO4\uff0c 1.0 M PBS\uff0c\u4e0e1.0 M KOH\uff09\uff1b<\/p>\n

(e-f<\/strong>) \u591a\u5b54NCP\u7eb3\u7c73\u7247\u7684\u7a33\u5b9a\u6027\u6d4b\u8bd5\u3002<\/p>\n

\u56fe\u4e94<\/strong> \u591a\u5b54<\/strong>NCP<\/strong>\u7eb3\u7c73\u7247\u7684<\/strong>OER<\/strong>\u6027\u80fd\u4e0e\u5168\u89e3\u6c34\u6027\u80fd\u6d4b\u8bd5<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

(a<\/strong>) \u591a\u5b54NCP\u4e0eNCO\u7eb3\u7c73\u7247\u7684\u6790\u6c27\u6027\u80fd\u5bf9\u6bd4\uff1b<\/p>\n

(b<\/strong>) \u591a\u5b54NCP\u7eb3\u7c73\u7247\u7684\u5168\u89e3\u6c34\u6781\u5316\u66f2\u7ebf\uff08\u4e24\u7535\u6781\u4f53\u7cfb\uff09\uff1b<\/p>\n

(c<\/strong>) \u591a\u5b54NCP\u7eb3\u7c73\u7247\u5168\u89e3\u6c34\u7684\u7a33\u5b9a\u6027\u6d4b\u8bd5\uff081.0 M KOH\uff09\u3002<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

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1. \u901a\u8fc7XPS\u8868\u5f81\u6d4b\u8bd5\uff0c\u53ef\u8bc1\u660e\uff0c\u5728\u78b1\u6027HER\u8fc7\u7a0b\u4e2d\uff0cNiCoA\u4e2d\u7684\u91d1\u5c5e\u9633\u79bb\u5b50\u4f5c\u4e3a\u6c34\u5206\u5b50\uff08\u6c22\u6c27\u6839\uff09\u7ed3\u5408\u4e2d\u5fc3\uff1bA\uff08O\uff0cSe\uff0cP\uff09\u9634\u79bb\u5b50\u53ef\u4f5c\u4e3a\u8d28\u5b50\u7ed3\u5408\u4e2d\u5fc3\u3002\u901a\u8fc7Ni\u03b4+<\/sup>\uff0c Co\u03b4+<\/sup>\uff0cand X\u03b4\u2212<\/sup> (P\u03b4\u2212<\/sup>\uff0c Se\u03b4\u2212<\/sup>) \u7684XPS\u8c31\u548c\u53d8\u6e29\u7535\u5bfc\u7387\u6d4b\u8bd5\uff0c\u53ef\u8bc1\u5b9e\uff0cP\/Se\u9634\u79bb\u5b50\u66ff\u4ee3\u6c27\u539f\u5b50\u53ef\u6709\u6548\u589e\u5f3a\u6240\u8c13\u7535\u5b50\u79bb\u57df\u6548\u5e94\uff0c\u4ece\u800c\u964d\u4f4e\u6790\u6c22\u8fc7\u7a0b\u4e2d\u7684\u7535\u5b50\u4f20\u8f93\u7535\u963b\uff1b\u540c\u65f6\uff0c\u78f7\u5316\u7269\u4e2d\u76f8\u5bf9\u8f83\u5f31\u7684\u7535\u5b50\u79bb\u57df\u6548\u5e94\u53ef\u4ee5\u7ef4\u6301P\u03b4\u2212<\/sup>\u7684\u8d1f\u7535\u6027\uff0c\u964d\u4f4e\u8d28\u5b50\u7684\u7ed3\u5408\u52bf\u5792\u3002<\/p>\n

2.\u901a\u8fc7DFT\u8ba1\u7b97\uff0c\u901a\u8fc7\u5bf9NiCoA\u4e2d\u9634\u79bb\u5b50\uff08\u9009\u62e9NCP\u7684(001)\u9762\uff0cNCS\u7684(010)\u9762\u4e0eNCO\u7684(111)\u9762\u4f5c\u4e3a\u8868\u9762\u6a21\u578b\uff09\u7684\u6c22\u5438\u9644\u80fd\u8fdb\u884c\u8ba1\u7b97\uff0c\u591a\u5b54NCP\u7eb3\u7c73\u7247\u7684\u6c22\u5438\u9644\u80fd\u6700\u5c0f\uff0c\u4fc3\u8fdb\u6c22\u7684\u89e3\u5438\u9644\u8fc7\u7a0b\uff0c\u8fdb\u800c\u63d0\u9ad8HER\u6027\u80fd\u3002<\/p>\n

3.\u5bf9\u4e8eHER\uff0c\u591a\u5b54NCP\u7eb3\u7c73\u7247\u5728\u4e0d\u540c\u7535\u89e3\u6db2\u4e2d\u5b9e\u73b0\u8f83\u4f4e\u7684\u8fc7\u7535\u4f4d\uff08|J|=10 mA\/cm2<\/sup>\uff09\uff1a58 mV\uff081 M KOH\uff09\uff0c80 mV\uff080.5 M H2<\/sub>SO4<\/sub>\uff09\u4e0e170 mV\uff081 M PBS\uff09\uff1b\u5bf9\u4e8eOER\uff0c\u591a\u5b54NCP\u7eb3\u7c73\u7247\u57281 M KOH\u7684\u6790\u6c27\u8fc7\u7535\u4f4d\uff08|J|=10 mA\/cm2<\/sup>\uff09\u4ec5\u4e3a280 mV\uff1b\u56e0\u6b64\u8fd9\u79cd\u50ac\u5316\u5242\u53ef\u5b9e\u73b0\u78b1\u6027\u6761\u4ef6\u4e0b\u7684\u5168\u89e3\u6c34\uff0c\u5176\u8fc7\u7535\u4f4d\u4ec5\u4e3a340 mV\uff0c\u5e76\u4e14\u5168\u89e3\u6c34\u7a33\u5b9a\u6027\u5927\u4e8e6 h\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>Dual Tuning of Ni\u2013Co\u2013A (A = P, Se, O) Nanosheets by Anion Substitution and Holey Engineering for Efficient Hydrogen Evolution<\/a> (J. Am. Chem. Soc., April 2, 2018, DOI: 10.1021\/jacs.8b01548)<\/p>\n

\u6587\u7ae0\u76f8\u5173\u4fe1\u606f\uff1a<\/strong><\/p>\n

\u5fb7\u514b\u8428\u65af\u5927\u5b66\u5965\u65af\u6c40\u5206\u6821\u7684\u4f59\u6842\u534e\u6559\u6388\u4e3a\u672c\u6587\u7684\u901a\u8baf\u4f5c\u8005\uff0c\u535a\u58eb\u751f\u65b9\u5fd7\u4f1f\u548c\u5f6d\u4e50\u4e50\u4e3a\u6587\u7ae0\u7684\u5171\u540c\u7b2c\u4e00\u4f5c\u8005\u3002<\/p>\n

\u56e2\u961f\u4ecb\u7ecd\u53ca\u5728\u8be5\u9886\u57df\u5de5\u4f5c\u6c47\u603b\uff1a<\/strong><\/p>\n

\u4f59\u6842\u534e\u6559\u6388\u7814\u7a76\u56e2\u961f\u957f\u671f\u81f4\u529b\u4e8e\u65e0\u673a\u4e8c\u7ef4\u6750\u6599\uff0c\u5c24\u5176\u662f\u53ef\u7528\u4e8e\u7535\u5316\u5b66\u50a8\u80fd\u548c\u8f6c\u6362\u7684\u4e8c\u7ef4\u6750\u6599\u7684\u7ed3\u6784\u8bbe\u8ba1\u5408\u6210\u53ca\u6709\u673a\u5206\u5b50\/\u805a\u5408\u7269\u5bfc\u5411\u7684\u7ec4\u88c5\u751f\u957f\u3001\u7efc\u5408\u7535\u5316\u5b66\u3001\u7269\u7406\u5316\u5b66\u3001\u65e0\u673a\u5316\u5b66\u548c\u6750\u6599\u79d1\u5b66\u7b49\u5185\u5bb9\u3002\u4f59\u56e2\u961f\u5bf9\u6240\u5f97\u4e8c\u7ef4\u6750\u6599\u7684\u7535\u8377\u4f20\u8f93\u3001\u5b58\u50a8\u548c\u8f6c\u6362\u7b49\u57fa\u672c\u7535\u5316\u5b66\u7279\u6027\u8fdb\u884c\u4e86\u7cfb\u7edf\u7814\u7a76\uff0c\u5e76\u4e3a\u8bbe\u8ba1\u4e0b\u4e00\u4ee3\u9ad8\u6027\u80fd\u7684\u7535\u5316\u5b66\u50a8\u80fd\u548c\u8f6c\u6362\u6750\u6599\u63d0\u4f9b\u4e86\u91cd\u8981\u7406\u5ff5\u548c\u65b9\u6cd5,\u53d7\u5230\u4e86\u56fd\u5185\u5916\u5b66\u8005\u7684\u5e7f\u6cdb\u5173\u6ce8\uff0c\u5728\u56fd\u9645\u77e5\u540d\u671f\u520a\u4e0a\u53d1\u8868\u8fc7\u8bb8\u591a\u76f8\u5173\u5de5\u4f5c\uff0c\u5305\u62ec\uff1aScience, Nature Nanotech., Nature Commun., PNAS, Acc. Chem. Res., Chem. Soc. Rev., Nano Today, Angew. Chem. Int. Ed., Adv. Mater., Nano Lett., ACS Nano, Adv. Energy Mater.\u7b49\u3002<\/p>\n

\u8fd1\u671f\u76f8\u5173\u6587\u732e\u63a8\u8350\uff1a<\/strong><\/p>\n

“Holey Transition Metal Oxide Nanosheets for Efficient Energy Storage<\/strong><\/a>“,\u00a0Nature Commun.\u00a0<\/em>8, 15139 (2017).\u00a0<\/p>\n

“<\/em>Holey Two-Dimensional Nanomaterials for Electrochemical Energy Storage<\/strong><\/a>“,\u00a0Adv. Energy Mater. 7<\/strong><\/em>, 1702179 (2017).\u00a0\u00a0<\/p>\n

“Structural Engineering of 2D Materials for Energy Storage and Catalysis<\/strong><\/a>“,\u00a0Adv.\u00a0Mater.<\/em><\/strong>\u00a0 30, 1706347 (2018).\u00a0<\/p>\n

“2D Holey Nanoarchitectures Created by Confined Self-Assembly of Nanoparticles via Block Copolymers<\/strong><\/a>“,\u00a0ACS Nano,\u00a0<\/em><\/strong>12, 820 (2018).<\/p>\n

“Metallic Transition Metal Selenide Holey Nanosheets for Efficient Oxygen Evolution<\/strong><\/a>“,\u00a0ACS Nano<\/em><\/strong>, 11, 9550 (2017).<\/p>\n

Engineering Two-dimensional Nanofluidic Li-Ion Transport Channels<\/strong><\/a>,\u00a0Adv. Mater., <\/em><\/strong>29, 1703909 (2017).<\/p>\n

“2D Holey Co3<\/sub>O4<\/sub>Nanosheets for High-Rate Alkali-Ion Batteries: from Rational Synthesis to in situ Probing<\/strong><\/a>“,\u00a0Nano Lett.<\/em><\/strong>\u00a017, 3907\u00a0(2017).\u00a0<\/p>\n

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