{"id":134191,"date":"2018-04-12T14:00:35","date_gmt":"2018-04-12T06:00:35","guid":{"rendered":"\/\/m.iemloyee.com\/?p=134191"},"modified":"2018-04-11T21:18:08","modified_gmt":"2018-04-11T13:18:08","slug":"adv-mater-%e5%af%8c%e5%90%ab%e6%b0%a7%e7%a9%ba%e4%bd%8d%e7%9a%84%e6%96%b0%e5%9e%8bbivo4%e5%8f%8c%e5%85%89%e9%98%b3%e6%9e%81%e7%94%a8%e4%ba%8e%e9%ab%98%e6%95%88%e5%a4%aa%e9%98%b3%e8%83%bd%e5%85%89","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=134191","title":{"rendered":"Adv. Mater. : \u5bcc\u542b\u6c27\u7a7a\u4f4d\u7684\u65b0\u578bBiVO4\u53cc\u5149\u9633\u6781\u7528\u4e8e\u9ad8\u6548\u592a\u9633\u80fd\u5149\u89e3\u6c34"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u9492\u9178\u94cb\uff08BiVO4<\/sub>\uff09\u88ab\u8ba4\u4e3a\u662f\u5149\u7535\u5206\u89e3\u6c34\u5236\u6c22\u6700\u6709\u524d\u666f\u7684\u5149\u9633\u6781\u6750\u6599\u4e4b\u4e00\u3002BiVO4<\/sub>\u7684\u5e26\u9699\u4e3a2.4 eV\uff0c\u5728AM 1.5 G\u7684\u7167\u5ea6\u4e0b\uff08100 mW\/cm2<\/sup>\uff09\uff0c\u53ef\u8fbe\u5230\u7684\u7406\u8bba\u5149\u7535\u6d41\u5bc6\u5ea6\u4e3a7.5 mA\/cm2<\/sup>\uff0c\u5bf9\u5e94\u7684\u592a\u9633\u80fd\u5230\u6c22\u6c14\uff08STH\uff09\u7684\u6548\u7387\u4e3a9.2%\u3002\u867d\u7136BiVO4<\/sub>\u7684\u5e26\u9699\u6bd4\u5149\u7535\u5206\u89e3\u6c34\u7684\u7406\u60f3\u5e26\u96992.0 eV\u7565\u5927\uff0c\u4f46\u5b83\u7684\u5bfc\u5e26\u8fb9\u7f18\u4f4d\u7f6e\u975e\u5e38\u9760\u8fd1H2<\/sub>\u6790\u51fa\u7535\u4f4d\uff0c\u56e0\u6b64\u4e0e\u8bb8\u591a\u5176\u5b83\u5149\u9633\u6781\u6750\u6599\u76f8\u6bd4\uff0c\u5728\u4f4e\u7535\u52bf\u533a\u57df\uff0cBiVO4<\/sub>\u5177\u6709\u66f4\u4f4e\u7684\u8d77\u59cb\u7535\u52bf\u548c\u66f4\u9ad8\u7684\u5149\u7535\u6d41\u5bc6\u5ea6\u3002<\/p>\n

\u9274\u4e8e\u8fd9\u4e9b\u4f18\u52bf\uff0cBiVO4<\/sub>\u5149\u9633\u6781\u5e38\u88ab\u7528\u5728\u5149\u89e3\u6c34-\u5149\u4f0f\u4e32\u8054\u7cfb\u7edf\u4e0a\u8fdb\u884c\u592a\u9633\u80fd\u9a71\u52a8\u7684\u65e0\u504f\u538b\u6c34\u5206\u89e3\u3002\u4e3a\u4e86\u5728\u5149\u89e3\u6c34-\u5149\u4f0f\u4e32\u8054\u7cfb\u7edf\u4e2d\u5b9e\u73b0\u9ad8\u7684STH\u6548\u7387\uff0c\u8981\u6c42\u524d\u9762\u7684BiVO4<\/sub>\u5149\u9633\u6781\u5728\u5b9e\u73b0\u9ad8\u7684\u5149\u7535\u6d41\u5bc6\u5ea6\u7684\u540c\u65f6\uff0c\u5177\u6709\u597d\u7684\u900f\u5149\u6027\uff0c\u4ee5\u5b9e\u73b0\u5149\u900f\u8fc7BiVO4<\/sub>\u8584\u819c\u540e\u6fc0\u53d1\u5176\u540e\u7684\u592a\u9633\u80fd\u7535\u6c60\u3002BiVO4<\/sub>\u5149\u9633\u6781\u7684\u5b9e\u9645\u5149\u7535\u6d41\u5bc6\u5ea6\uff08J<\/em>p<\/sub>\uff09\u4e3b\u8981\u53d6\u51b3\u4e8e\u5149\u5438\u6536\u6548\u7387\uff08\u03b7<\/em>abs<\/sub>\uff09\u3001\u7535\u8377\u5206\u79bb\u6548\u7387\uff08\u03b7<\/em>sep<\/sub>\uff09\uff0c\u4ee5\u53ca\u7535\u8377\u8f93\u8fd0\u901f\u7387\uff08\u03b7<\/em>trans<\/sub>\uff09\uff0c\u5373\uff1aJ<\/em>p<\/sub>=J<\/em>max<\/sub> \u00d7 \u03b7<\/em>abs<\/sub> \u00d7 \u03b7<\/em>sep <\/sub>\u00d7 \u03b7<\/em>trans<\/sub>\u3002\u6700\u8fd1\u6709\u7814\u7a76\u663e\u793a\uff0c\u5f53BiVO4<\/sub>\u4e0e\u9002\u5b9c\u7684\u6790\u6c27\u50ac\u5316\u5242\u590d\u5408\u65f6\uff0c\u5728\u6790\u6c27\u53cd\u5e94\u8fc7\u7a0b\u4e2d\u5176\u7535\u8377\u8f93\u8fd0\u6548\u7387\uff08\u03b7<\/em>trans<\/sub>\uff09\u53ef\u63a5\u8fd1\u6700\u5927\u503c\u3002<\/p>\n

\u7136\u800c\uff0c\u5728\u5149\u89e3\u6c34-\u5149\u4f0f\u4e32\u8054\u7cfb\u7edf\u4e2d\uff0c\u4f7f\u900f\u660e\u7684BiVO4<\/sub>\u5149\u9633\u6781\u5b9e\u73b0\u9ad8\u7684\u5149\u5438\u6536\u6548\u7387\u548c\u7535\u8377\u5206\u79bb\u6548\u7387\uff08\u03b7<\/em>abs<\/sub> \u00d7 \u03b7<\/em>sep<\/sub>\uff09\u4f9d\u65e7\u6781\u5177\u6311\u6218\u6027\u3002\u8fd9\u662f\u56e0\u4e3a\u5149\u5438\u6536\u6548\u7387\uff08\u03b7<\/em>abs<\/sub>\uff09\u548c\u7535\u8377\u5206\u79bb\u6548\u7387\uff08\u03b7<\/em>sep<\/sub>\uff09\u662f\u8026\u5408\u5f71\u54cd\u7684\uff0c\u5373\uff1a\u8f83\u8584\u7684BiVO4<\/sub>\u819c\u901a\u5e38\u6709\u8f83\u9ad8\u7684\u5149\u5438\u6536\u6548\u7387\u548c\u8f83\u4f4e\u7684\u7535\u8377\u5206\u79bb\u6548\u7387\uff0c\u53cd\u4e4b\u4ea6\u7136\u3002\u56e0\u6b64\uff0c\u5982\u4f55\u8fdb\u4e00\u6b65\u63d0\u9ad8BiVO4<\/sub>\u5149\u9633\u6781\u8584\u819c\u7684\u900f\u5149\u6027\uff0c\u540c\u65f6\u4fdd\u6301\u9ad8\u7684\u5149\u7535\u6d41\u5bc6\u5ea6\uff0c\u5728\u5149\u89e3\u6c34-\u5149\u4f0f\u4e32\u8054\u7cfb\u7edf\u4e2d\u5b9e\u73b0\u9ad8\u7684STH\u6548\u7387\uff0c\u4ecd\u7136\u662f\u5177\u6709\u6311\u6218\u6027\u7684\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u8fd1\u65e5\uff0c\u6fb3\u5927\u5229\u4e9a\u6606\u58eb\u5170\u5927\u5b66\u7684\u738b\u8fde\u6d32\u6559\u6388\u548c\u4e2d\u79d1\u9662\u91d1\u5c5e\u7814\u7a76\u6240\u7684\u5218\u5c97\u7814\u7a76\u5458\uff08\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff09<\/strong>\u62a5\u9053\u4e86\u4e00\u79cd\u901a\u8fc7\u7535\u5316\u5b66\u6c89\u79ef\u53ca\u7145\u70e7\u8fc7\u7a0b\u5236\u5907\u5bcc\u542b\u6c27\u7a7a\u4f4d\u7684\u9ad8\u900f\u660eBiVO4<\/sub>\u5149\u9633\u6781\u7684\u65b0\u65b9\u6cd5\u3002\u8be5BiVO4<\/sub>\u53cc\u5149\u7535\u9633\u6781\u75312\u7247\u76f8\u540c\u7684\u900f\u660eBiVO4<\/sub>\u8584\u819c\u6784\u6210\uff0c\u5177\u6709\u6781\u9ad8\u7684\u5149\u7535\u6d41\u5bc6\u5ea6\uff0c\u57281.23 V\uff08vs. RHE\uff09\u4e0b\u8fbe6.22 mA\/cm2<\/sup>\uff08\u7167\u5ea6AM 1.5 G\uff09\uff0c\u5bf9\u5e94\u4e8e\u9ad8\u8fbe83%\u7684\u5149\u5438\u6536\u6548\u7387\u4e0e\u7535\u8377\u5206\u79bb\u6548\u7387\u4e4b\u79ef\uff08\u03b7<\/em>abs<\/sub> \u00d7 \u03b7<\/em>sep<\/sub>\uff09\u3002 \u901a\u8fc7\u6c89\u79ef\u6790\u6c27\u50ac\u5316\u5242FeOOH\/NiOOH\uff0cBiVO4<\/sub>\u53cc\u5149\u9633\u6781\u7684\u5149\u7535\u6d41\u5bc6\u5ea6\u53ef\u8fbe5.87 mA\/cm2<\/sup>\uff081.23 V vs. RHE\uff09\uff0c\u5149\u7535\u5206\u89e3\u6c34\u7684ABPE\u6548\u7387\u53ef\u8fbe2.2%\uff080.7 V vs. RHE\uff0c\u7167\u5ea6AM 1.5 G\uff09\u3002\u8be5\u5de5\u4f5c\u4e2d\u62a5\u9053\u7684\u5149\u7535\u50ac\u5316\u6548\u7387\u662f\u76ee\u524d\u4e0d\u4f7f\u7528\u654f\u5316\u5242\u53ca\u8d35\u91d1\u5c5e\u7684BiVO4<\/sub>\u5149\u9633\u6781\u4e2d\u6700\u9ad8\u7684\u3002\u8be5BiVO4<\/sub>\u53cc\u5149\u9633\u6781\u5728\u4e0e\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\u7ec4\u5408\u540e\uff0c\u5728\u65e0\u504f\u538b\u5149\u7535\u5206\u89e3\u6c34\u5b9e\u9a8c\u4e2d\u5b9e\u73b0\u4e866.5%\u7684STH\u6548\u7387\u3002\u8be5\u7814\u7a76\u901a\u8fc7\u5f15\u5165\u6c27\u7a7a\u4f4d\u63d0\u9ad8\u7535\u8377\u5206\u79bb\u6548\u7387\uff08\u03b7<\/em>sep<\/sub>\uff09\uff0c\u901a\u8fc7\u53cc\u5149\u9633\u6781\u63d0\u9ad8\u5149\u5438\u6536\u6548\u7387\uff08\u03b7<\/em>abs<\/sub>\uff09\u7684\u7b56\u7565\uff0c\u4e3a\u8bbe\u8ba1\u7528\u4e8e\u65e0\u504f\u538b\u5149\u7535\u5206\u89e3\u6c34\u7684\u9ad8\u6548\u5149\u7535\u6781\u63d0\u4f9b\u4e86\u65b0\u8def\u5f84\u3002\u76f8\u5173\u7814\u7a76\u6210\u679c\u4ee5\u201c<\/strong>New BiVO4<\/sub> Dual Photoanodes with Enriched Oxygen Vacancies for Efficient Solar-Driven Water Splitting<\/strong>\u201d<\/strong>\u4e3a\u9898\u53d1\u8868\u5728Advanced Materials<\/strong>\u4e0a\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe\u4e00<\/strong> \u901a\u8fc7\u7535\u5316\u5b66\u6c89\u79ef\u53ca\u7145\u70e7\u8fc7\u7a0b\u5236\u5907\u7684<\/strong>BiVO4<\/sub><\/strong>\u5149\u9633\u6781\u7684\u7167\u7247\u53ca\u5176<\/strong>SEM<\/strong>\u56fe\u50cf<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09BiVO4<\/sub>\u5149\u9633\u6781\u7684\u7167\u7247<\/p>\n

\uff08b\uff09BVO-0.5h\uff0cBVO-1h\uff0cBVO-1.5h\uff0c\u4ee5\u53caBVO-2h\u7684XRD\u8c31\u56fe<\/p>\n

\uff08c\uff09~\uff08f\uff09BVO-0.5h\uff0cBVO-1h\uff0cBVO-1.5h\uff0c\u4ee5\u53caBVO-2h\u7684SEM\u56fe\u50cf<\/p>\n

\u56fe\u4e8c<\/strong> \u5149\u7535\u50ac\u5316\u6027\u80fd\u8868\u5f81\u53ca\u6c27\u7a7a\u4f4d\u7684<\/strong>XPS<\/strong>\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09BVO-1.5h\uff0c2-BVO-1.5h\u53caBVO-S\u7684J-V\u66f2\u7ebf<\/p>\n

\uff08b\uff09BVO-1.5h\uff0c2-BVO-1.5h\u53caBVO-S\u57281.23 V\uff08vs. RHE\uff09\u4e0b\u7684IPCE\u66f2\u7ebf<\/p>\n

\uff08c\uff09BVO-1.5h\uff0c2-BVO-1.5h\u4ee5\u53caBVO-S\u7684\u7d2b\u5916-\u53ef\u89c1\u5438\u6536\u66f2\u7ebf<\/p>\n

\uff08d\uff09BVO-1.5h\u548cBVO-S\u7684XPS O 1s\u56fe\u8c31\u5bf9\u6bd4<\/p>\n

\u56fe\u4e09<\/strong> \u4fee\u9970<\/strong>FeOOH\/NiOOH<\/strong>\u6790\u6c27\u50ac\u5316\u5242\u540e<\/strong>BiVO4<\/sub><\/strong>\u5149\u9633\u6781\u7684\u5149\u7535\u50ac\u5316\u6027\u80fd\u8868\u5f81<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09BVO-1.5h\uff0cBVO-1.5h\/FeOOH\/NiOOH\u53ca2-BVO-1.5h\/FeOOH\/NiOOH\u7684J-V\u66f2\u7ebf<\/p>\n

\uff08b\uff09BVO-1.5h\uff0cBVO-1.5h\/FeOOH\/NiOOH\u53ca2-BVO-1.5h\/FeOOH\/NiOOH\u7684ABPE\u66f2\u7ebf<\/p>\n

\uff08c\uff092-BVO-1.5h\/FeOOH\/NiOOH\u7684\u57281.23V \uff08vs. RHE\uff09\u53caAM 1.5 G\u7167\u5ea6\u4e0b\u7684\u7a33\u5b9a\u6027\u6d4b\u8bd5<\/p>\n

\uff08d\uff091.23V \uff08vs. RHE\uff09\u53caAM 1.5 G\u7167\u5ea6\u4e0b\uff0c\u4f7f\u75282-BVO-1.5h\/FeOOH\/NiOOH\u5149\u9633\u6781\u4f53\u7cfb\u7684H2<\/sub>\u53caO2<\/sub>\u6790\u51fa\u91cf\u968f\u65f6\u95f4\u7684\u53d8\u5316<\/p>\n

\u56fe\u56db<\/strong> BiVO4<\/sub><\/strong>\u53cc\u5149\u9633\u6781\u53ca\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\u4e32\u8054\u4f53\u7cfb\uff08<\/strong>PEC-PSC<\/strong>\uff09\u7684\u6784\u7b51\u53ca\u5176\u5149\u7535\u50ac\u5316\u6027\u80fd\u8bc4\u4ef7<\/strong><\/p>\n

\"\"<\/p>\n

\uff08a\uff09BiVO4<\/sub>\u53cc\u5149\u9633\u6781\u53ca\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\u4e32\u8054\u4f53\u7cfb\u793a\u610f\u56fe<\/p>\n

\uff08b\uff09AM 1.5 G\u7167\u5ea6\u4e0b\uff0c\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\uff08I\uff09\uff0c\u4f53\u7cfb\u4e2d\u4f4d\u4e8e2-BVO-FeOOH\/NiOOH\u4e4b\u540e\u7684\u9499\u949b\u77ff\u592a\u9633\u80fd\u7535\u6c60\uff08II\uff09\uff0c\u4ee5\u53ca2-BVO-FeOOH\/NiOOH\u7535\u6781\uff08III\uff09\u7684J-V\u66f2\u7ebf<\/p>\n

\uff08c\uff09\u975e\u8f85\u52a9\u6761\u4ef6\u4e0b\uff080 V vs. Pt\u5bf9\u7535\u6781\uff09\u4f53\u7cfb\u5206\u89e3\u6c34\u7684\u7a33\u5b9a\u6027<\/p>\n

\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u8be5\u7814\u7a76\u62a5\u9053\u4e86\u4e00\u79cd\u901a\u8fc7\u7535\u5316\u5b66\u6c89\u79ef\u548c\u70ed\u5904\u7406\u5236\u5907\u5bcc\u542b\u6c27\u7a7a\u4f4dBiVO4<\/sub>\u819c\u7684\u7b80\u6613\u65b9\u6cd5\u3002\u5728\u6c89\u79efFeOOH\/NiOOH\u6790\u6c27\u50ac\u5316\u5242\u540e\uff0c\u8be5\u5149\u9633\u6781\u57281.23 V vs. RHE\u4e0b\u663e\u793a\u4e86\u6781\u9ad8\u7684\u5149\u7535\u6d41\u5bc6\u5ea6\uff085.13 mA\/cm2<\/sup>\uff09\u3002\u5f53\u524d\u540e\u5e03\u7f6e2\u7247\u76f8\u540c\u7684\u8be5\u5149\u9633\u6781\u65f6\uff0c400-520 nm\u8303\u56f4\u5185\u7684\u5149\u5438\u6536\u589e\u5f3a\uff0c\u57281.23 V vs. RHE\u6761\u4ef6\u4e0b\u5149\u7535\u6d41\u5bc6\u5ea6\u63d0\u9ad8\u52305.87 mA\/cm2<\/sup>\uff0c\u76f8\u5f53\u4e8e6.5%\u7684STH\u6548\u7387\u3002\u8be5\u7814\u7a76\u5bf9\u4e8e\u53d1\u5c55\u7b80\u4fbf\u3001\u4f4e\u6210\u672c\u7684BiVO4<\/sub>\u819c\u4ee5\u5b9e\u73b0\u9ad8\u6548\u3001\u7a33\u5b9a\u7684\u65e0\u504f\u538b\u5149\u89e3\u6c34\u6307\u660e\u4e86\u65b9\u5411\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a<\/strong>New BiVO4<\/sub> Dual Photoanodes with Enriched Oxygen Vacancies for Efficient Solar-Driven Water Splitting<\/a>\uff08Adv. Mater. 2018, DOI: 10.1002\/adma.201800486\uff09<\/p>\n

\u3010\u901a\u8baf\u4f5c\u8005\u7b80\u4ecb\u3011<\/strong><\/p>\n

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\u738b\u8fde\u6d32<\/strong>\uff0c\u73b0\u4e3a\u6fb3\u5927\u5229\u4e9a\u6606\u58eb\u5170\u5927\u5b66\u5316\u5de5\u5b66\u9662\u6559\u6388\uff0c\u7eb3\u7c73\u6750\u6599\u7814\u7a76\u4e2d\u5fc3\u4e3b\u4efb\uff0c\u6fb3\u5927\u5229\u4e9a\u751f\u7269\u5de5\u7a0b\u4e0e\u7eb3\u7c73\u79d1\u6280\u7814\u7a76\u6240\uff08AIBN\uff09\u517c\u804c\u8bfe\u9898\u7ec4\u957f\u3002\u4e3b\u8981\u4ece\u4e8b\u529f\u80fd\u7eb3\u7c73\u6750\u6599\u548c\u7eb3\u7c73\u5668\u4ef6\u7814\u53d1\u53ca\u5176\u5728\u6e05\u6d01\u80fd\u6e90\u8f6c\u6362\u9886\u57df\u7684\u5e94\u7528\u7814\u7a76, \u5305\u62ec\u7eb3\u7c73\u5149\u50ac\u5316\u6750\u6599\uff0c\u65b0\u4e00\u4ee3\u592a\u9633\u80fd\u7535\u6c60\uff0c\u53ca\u65b0\u578b\u5145\u7535\u7535\u6c60\u7b49\u3002\u5728\u8bf8\u591a\u56fd\u9645\u671f\u520a\u5305\u62ecChem Rev. Chem. Soc. Rev., Adv. Mater., J. Am.Chem. Soc, Angew. Chem. \u7b49\u53d1\u8868\u8bba\u6587220\u4f59\u7bc7\uff0c\u4e13\u8457\u7ae0\u82829\u90e8\uff0c\u7533\u8bf7\u4e13\u522912\u9879\u3002\u8fd1\u5e74\u4f5c\u4e3a\u4e3b\u8981\u8d1f\u8d23\u4eba\u5148\u540e\u627f\u62c5\u4e86\u6fb3\u5927\u5229\u4e9a\u57fa\u91d1\u59d4\u3001\u6fb3\u6d32\u79d1\u5b66\u9662\u3001\u6fb3\u6d32\u534f\u540c\u521b\u65b0\u4e2d\u5fc3\uff0c\u6606\u58eb\u5170\u5dde\u653f\u5e9c\u4ee5\u53ca\u5de5\u4e1a\u754c\u7b4930\u4f59\u9879\u7ade\u4e89\u6027\u7814\u7a76\u9879\u76ee\uff0c\u603b\u91d1\u989d\u8d851600\u4e07\u6fb3\u5143\u3002\u62c5\u4efb\u300a\u79d1\u5b66\u901a\u62a5\u300b\u82f1\u6587\u7248Science Bulletin\u53caJournal of Nanoparticles Research\u7b49\u56fd\u9645\u671f\u520a\u526f\u4e3b\u7f16\u3002\u83b7\u5f97\u6fb3\u6d32\u57fa\u91d1\u59d4\u5973\u738b\u4f0a\u4e3d\u838e\u767d\u5b66\u8005(2006)\u53ca\u672a\u6765\u5b66\u8005(2012)\u79f0\u53f7\uff0c\u6606\u58eb\u5170\u5927\u5b66\u7814\u7a76\u4f18\u79c0\u5956(2008)\uff0c\u6fb3\u6d32Scopus\u5bfb\u627e\u79d1\u6280\u65b0\u661f\u5956(2011)\uff0c\u76ee\u524d\u62c5\u4efb\u6fb3\u6d32\u57fa\u91d1\u59d4\u4e13\u5bb6\u7ec4\u5927\u8bc4\u59d4\uff0c\u5165\u9009\u82f1\u56fd\u7687\u5bb6\u5316\u5b66\u4f1a\u4f1a\u58eb\u3002<\/p>\n

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