{"id":131809,"date":"2018-03-31T14:00:54","date_gmt":"2018-03-31T06:00:54","guid":{"rendered":"\/\/m.iemloyee.com\/?p=131809"},"modified":"2018-03-31T19:46:01","modified_gmt":"2018-03-31T11:46:01","slug":"energy-environ-sci-%e8%a1%8d%e5%b0%84%e3%80%81%e7%94%b5%e5%8c%96%e5%ad%a6%e4%b8%8e%e7%90%86%e8%ae%ba%e8%ae%a1%e7%ae%97%e5%85%b1%e5%90%8c%e7%a0%94%e7%a9%b6%e9%92%a0%e7%a6%bb%e5%ad%90%e7%94%b5","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=131809","title":{"rendered":"Energy Environ. Sci.: \u884d\u5c04\u3001\u7535\u5316\u5b66\u4e0e\u7406\u8bba\u8ba1\u7b97\u5171\u540c\u7814\u7a76\u94a0\u79bb\u5b50\u7535\u6c60\u6b63\u6781\u6750\u6599\u7684\u9ad8\u7535\u538b\u7ed3\u6784\u6f14\u53d8\u548c\u589e\u5f3a\u7684\u79bb\u5b50\u6269\u6563"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u91c7\u7528P2\u578b\u548cO3\u578b\u7ed3\u6784\u3001\u901a\u5f0f\u4e3aNax<\/sub>TMO2<\/sub>\uff08TM =\u8fc7\u6e21\u91d1\u5c5e\uff09\u7684\u5c42\u72b6\u6c27\u5316\u7269\u7684\u94a0\u79bb\u5b50\u7535\u6c60\u5728\u5f53\u524d\u7535\u6c60\u5e94\u7528\u9886\u57df\u5177\u6709\u6781\u5927\u7684\u53d1\u5c55\u6f5c\u529b\u3002\u5c24\u5176\u662fP2-Na2\/3<\/sub>Ni1\/3<\/sub>Mn2\/3<\/sub>O2<\/sub>\uff0c\u7531\u4e8e\u5176\u9ad8\u7406\u8bba\u5bb9\u91cf\uff08\u7ea6170 mAh g-1<\/sup>\uff09\u548c\u9ad8\u5e73\u5747\u7535\u538b\uff08\u7ea63.5 V\uff09\u800c\u663e\u793a\u51fa\u5e7f\u9614\u7684\u524d\u666f\uff0c\u7136\u800c\uff0c\u76ee\u524d\u8f83\u5dee\u7684\u5faa\u73af\u5bff\u547d\u662f\u9650\u5236\u5176\u53d1\u5c55\u7684\u91cd\u8981\u56e0\u7d20\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u8fd1\u65e5\uff0c\u82f1\u56fd\u725b\u6d25\u5927\u5b66<\/strong>Peter G. Bruce<\/strong>\u6559\u6388<\/strong>\u7b49<\/strong>\u7814\u7a76\u4eba\u5458\u62a5\u9053\u4e86\u8fc4\u4eca\u4e3a\u6b62\u5728P2-Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\u5316\u5408\u7269\u4e2dMg\u53d6\u4ee3\u7684\u6700\u9ad8\u6c34\u5e73\u3002\u5728\u8fd9\u9879\u7814\u7a76\u4e2d\uff0c\u7814\u7a76\u4eba\u5458\u901a\u8fc7\u5e38\u89c4\u56fa\u6001\u65b9\u6cd5\u5236\u5907\u4e86\u4e00\u7cfb\u5217P2\u578bNa2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\uff080 <x <0.20\uff09\u6750\u6599\uff0c\u5e76\u4e14\u4f7f\u7528X\u5c04\u7ebf\u548c\u4e2d\u5b50\u884d\u5c04\u6280\u672f\u8fdb\u884c\u4e86\u7ed3\u6784\u8868\u5f81\u3002\u5faa\u73af\u6570\u636e\u5728\u5ba4\u6e29\u4e0b\u4e0eNa\u8fdb\u884c\u534a\u7535\u6c60\u5b9e\u9a8c\uff0c\u540c\u65f6\u7b2c\u4e00\u6027\u539f\u7406\u8ba1\u7b97\u8fdb\u884c\u6a21\u62df\u7814\u7a76\u4ee5\u68c0\u67e5Mg\u53d6\u4ee3\u7269\u7684\u7ed3\u6784\u548cNa\u79bb\u5b50\u7684\u6269\u6563\u6027\u8d28\uff0c\u4ee5\u8865\u5145\u5b9e\u9a8c\u89c2\u70b9\u3002\u8be5\u7814\u7a76\u53d1\u8868\u4e8eEnergy & Environmental Science<\/strong>\uff0c\u9898\u4e3a\u201cHigh voltage structural evolution and enhanced Na-ion diffusion in P2-Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub> (0 <x>< 0.20) cathodes from diffraction, electrochemical and ab-initio studies<\/strong>\u201d<\/strong>\u3002<\/p>\n

\u00a0<\/strong>\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/strong><\/p>\n

\u56fe<\/strong>1. Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub><\/strong>\uff08<\/strong>x = 0<\/strong>\uff09\u7684<\/strong>X<\/strong>\u5c04\u7ebf\u548c\u4e2d\u5b50\u884d\u5c04\u6570\u636e<\/strong><\/p>\n

\"\"<\/strong><\/p>\n

a\uff09Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\uff08\u5176\u4e2dx = 0\uff09\u7684X\u5c04\u7ebf\u548c\u4e2d\u5b50\u6570\u636e\u6bd4\u8f83\uff1b<\/p>\n

b\uff09\u663e\u793aNa2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\u4e2d\u5b50\u884d\u5c04\u6570\u636e\u7684\u5806\u79ef\u56fe\uff0c\u5176\u4e2d0 <x <0.20\uff1b c\uff09\u56fe1b\u4e2d\u9ec4\u8272\u9ad8\u4eae\u533a\u57df\u7684\u7f29\u653e\u3002<\/p>\n

\u56fe<\/strong>2. Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub><\/strong>\u7684\u5145\u7535\u548c\u653e\u7535\u66f2\u7ebf<\/strong><\/p>\n

\"\"<\/p>\n

a\uff09 Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\u7684\u7b2c\u4e00\u6b21\u5145\u7535\u548c\u653e\u7535\u66f2\u7ebf\uff0c\u5176\u4e2d0 <x <0.20\uff0c\u7535\u538b\u8303\u56f4\u572810mA g-1<\/sup>\u76842-4.5 V\u5185;<\/p>\n

b\uff09\u56fe1\u6240\u793a\u6837\u54c1\u7684\u653e\u7535\u5faa\u73af\u6570\u636e\uff08\u6700\u591a50\u6b21\u5faa\u73af\uff09;<\/p>\n

c\uff09\u56fe2a\u6240\u793a\u6570\u636e\u7684\u5fae\u5206\u5bb9\u91cf\u66f2\u7ebf\u3002<\/p>\n

\u56fe<\/strong>3.<\/strong> \u539f\u4f4d\u540c\u6b65\u52a0\u901f\u5668<\/strong>XRD<\/strong>\u6570\u636e<\/strong><\/p>\n

\"\"<\/p>\n

\u539f\u4f4d\u540c\u6b65\u52a0\u901f\u5668XRD\u6570\u636e\uff0c\u5176\u4e2d\u9009\u5b9a\u76842\u03b8\u533a\u57df\u7a81\u51fa\u663e\u793a\u4e86Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\u7684(002)\u548c(100)\u53cd\u5c04\u7684\u6f14\u53d8\uff0c\u5176\u4e2da\uff09x = 0 \u548cb\uff09x = 0.2\u3002\u8272\u6807\u4ee3\u8868\u53cd\u5c04\u5f3a\u5ea6\uff0c\u540c\u65f6\u4e5f\u5305\u62ec\u7535\u4f4d\u5206\u5e03\u3002<\/p>\n

\u56fe<\/strong>4. Na2\/3<\/sub>Ni1\/3<\/sub>Mn2\/3<\/sub>O2<\/sub><\/strong>\u7535\u6781\uff08<\/strong>x=0<\/strong>\uff09\u5728\u5145\u653e\u7535\u8fc7\u7a0b\u4e2d<\/strong>a<\/strong>\u548c<\/strong>c<\/strong>\u6676\u683c\u53c2\u6570\u7684\u53d8\u5316\u4ee5\u53ca\u7535\u5316\u5b66\u5206\u5e03<\/strong><\/p>\n

\"\"<\/p>\n

Na2\/3<\/sub>Ni1\/3<\/sub>Mn2\/3<\/sub>O2<\/sub>\u7535\u6781\uff08x=0\uff09\u5728\u5145\u653e\u7535\u8fc7\u7a0b\u4e2da\u548cc\u6676\u683c\u53c2\u6570\u7684\u53d8\u5316\u4ee5\u53ca\u7535\u5316\u5b66\u5206\u5e03\u3002P2\u6709\u5e8f\u76f8\u7684\u6676\u683c\u53c2\u6570\u4ee5\u9ed1\u8272\uff081\/3 Na\uff09\uff0c\u84dd\u8272\uff081\/2 Na\uff09\u548c\u7ea2\u8272\uff082\/3 Na\uff09\u793a\u51fa\uff0c\u5e76\u4e14\u6765\u81eaO2\u76f8\u7684002\u53cd\u5c04\u76842\u03b8\u4f4d\u7f6e\u4ee5\u7eff\u8272\u793a\u51fa\u3002\u4e24\u4e2a\u9ec4\u8272\u9634\u5f71\u533a\u57df\u8868\u793aP2\u94a0\u6709\u5e8f\u7ed3\u6784\u4e4b\u95f4\u7684\u76f8\u53d8\uff0c\u6a59\u8272\u9634\u5f71\u533a\u57df\u8868\u793aP2\u81f3O2\u76f8\u53d8\u3002<\/p>\n

\u56fe<\/strong>5. <\/strong>\u4e0d\u540c\u7535\u538b\u4e0b\u6676\u683c\u5e38\u6570\u4e0e\u53c2\u8003\u6587\u732e\u503c\u7684\u6bd4\u8f83<\/strong><\/p>\n

\"\"<\/p>\n

\u672c\u7814\u7a76\u57284.0 V\uff0c3.6 V\uff0c3.0 V\u548c2.3 V\u7684\u6676\u683c\u5e38\u6570\uff08\u586b\u5145\u6570\u636e\uff09\u4e0ex = 1\/3,1\/2\u548c2\/3\u5728\u53c2\u8003\u6587\u732e\u4e2d\u7684\u6709\u5e8f\u7ed3\u6784\uff08\u5206\u522b\u4e3a4.0 V\uff0c3.5 V\u548c\u5145\u7535\u524d\uff09\u7684\u6676\u683c\u53c2\u6570\u6bd4\u8f83\u3002<\/p>\n

\u56fe<\/strong>6. <\/strong>\u5145\u7535\u524d\u540e\u7684<\/strong>XRD<\/strong>\u56fe\u8c31<\/strong><\/p>\n

\"\"<\/p>\n

\u5728\u5145\u7535\u72b6\u6001\uff08\u9ed1\u8272\uff09\u548c\u5145\u7535\uff08\u7ea2\u8272\uff09\u4e4b\u524d\uff0cNa2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\u7684XRD\u56fe\uff0c\u5176\u4e2d0 <x <0.20\u3002<\/p>\n

\u00a0<\/strong>\u56fe<\/strong>7 \u00a04.2V<\/strong>\u65f6<\/strong>Mg2+<\/sup><\/strong>\u79bb\u5b50\u5468\u56f4\u4e24\u79cd\u53ef\u80fd\u7684\u5c40\u90e8\u7ed3\u6784<\/strong><\/p>\n

\"\"<\/p>\n

4.2V\u65f6Mg2+<\/sup>\u79bb\u5b50\u5468\u56f4\u7684\u4e24\u79cd\u53ef\u80fd\u7684\u5c40\u90e8\u7ed3\u6784\u3002\uff08a\uff09\u4f4e\u80fd\u91cf\u6784\u578b\uff0c\u5176\u4e2d\u4e24\u4e2aNa\u79bb\u5b50\u4f4d\u4e8eMO2<\/sub>\u7247\u7684\u540c\u4e00\u4fa7\uff0c\u800c\u7a7aNa\u5c42\u5141\u8bb8\u4eceP \u5806\u53e0\u5230O\u5806\u53e0\u3002\uff08b\uff09\u9ad8\u80fd\u91cf\u6784\u578b\uff0c\u5176\u4e2d\u4e24\u4e2aNa\u79bb\u5b50\u4f4d\u4e8eMO2<\/sub>\u7247\u6750\u7684\u6bcf\u4e00\u4fa7\u3002<\/p>\n

\u00a0<\/strong>\u56fe<\/strong>8 <\/strong>\u6a21\u62df\u7684\u5747\u65b9\u4f4d\u79fb<\/strong><\/p>\n

\"\"<\/p>\n

Na0.56<\/sub>Ni0.33<\/sub>Mn0.67<\/sub>O2<\/sub>\u548cNa0.56<\/sub>Mg0.11<\/sub>Ni0.22<\/sub>Mn0.67<\/sub>O2<\/sub>\u4e2d\u7684Na\u79bb\u5b50\u4ece\u6700\u521d\u7684\u5206\u5b50\u52a8\u529b\u5b66\uff08AIMD\uff09\u6a21\u62df\u4e2d\u7684\u5747\u65b9\u4f4d\u79fb\uff0c\u8868\u660e\u5728\u542bMg\u5316\u5408\u7269\u4e2dNa\u79bb\u5b50\u6269\u6563\u66f4\u5feb\u3002<\/p>\n

\u00a0<\/strong>\u56fe<\/strong>9 <\/strong>AIMD\u6a21\u62df\u8fc7\u7a0b\u7684z\u65b9\u5411\u4f4d\u79fb<\/strong><\/p>\n

\"\"<\/p>\n

\u572850 ps AIMD\u6a21\u62df\u8fc7\u7a0b\u4e2d\uff0cNa0.56<\/sub>Mg0.11<\/sub>Ni0.22<\/sub>Mn0.67<\/sub>O2<\/sub>\u4e2dMg\uff0cNi\u548cMn\u79bb\u5b50\u5728z\u65b9\u5411\u7684\u4f4d\u79fb\uff0c\u8868\u660eMg\u7684\u632f\u5e45\u8f83\u5927\u3002<\/p>\n

\u00a0<\/strong>\u3010\u5c0f\u7ed3\u3011<\/strong><\/p>\n

\u00a0<\/strong>\u8be5\u9879\u7814\u7a76\u8bc1\u660e\u4e86Mg\u53d6\u4ee3\u5bf9\u4e00\u7cfb\u5217P2-Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\u5316\u5408\u7269\u7ed3\u6784\u7684\u5f71\u54cd\u3002\u7efc\u5408XRD\u548c\u4e2d\u5b50\u5206\u6790\u8868\u660e\uff0c\u9541\u5728\u954d\u9530\u7684\u8702\u7a9d\u5c42\u4e2d\u66ff\u4ee3\u954d\uff0c\u5f62\u6210\u4e0e\u6bcd\u6750\u4e00\u6837\u7684AB\u578b\u7ed3\u6784\u3002\u56e0\u6b64\uff0c\u5728Mg\u53d6\u4ee3\u65f6c\u8f74\u4e0a\u6ca1\u6709\u7ed3\u6784\u91cd\u6392\u3002\u540c\u65f6\u8fd8\u8868\u660e\u7ed3\u6784\u4e2d\u7684\u9ad8\u542b\u91cfMg\uff08\u5373x = 0.2\uff09\u5bfc\u81f4\u4e86\u94a0\u5728\u539f\u59cb\u6750\u6599\u4e2d\u66f4\u65e0\u5e8f\u7684\u5206\u5e03\uff0c\u7535\u5316\u5b66\u7ed3\u679c\u901a\u8fc7\u663e\u793a\u56fa\u6eb6\u5256\u9762\u6765\u8bc1\u5b9e\u5176\u7ed3\u6784\u6570\u636e\u3002\u6b64\u7814\u7a76\u662f\u8fc4\u4eca\u4e3a\u6b62\u62a5\u9053\u7684P2-Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub>\u5316\u5408\u7269\u4e2dMg\u53d6\u4ee3\u7684\u6700\u9ad8\u6c34\u5e73\u3002\u539f\u4f4d\u540c\u6b65\u52a0\u901f\u5668XRD\u5b9e\u9a8c\u548c\u4ece\u5934\u7b97\u5206\u5b50\u52a8\u529b\u5b66\u7814\u7a76\u5171\u540c\u63ed\u793a\u4e86\u9541\u5728\u9ad8\u538bP2-Na2\/3<\/sub>Ni1\/3<\/sub>Mn2\/3<\/sub>O2<\/sub>\u9634\u6781\u4e2d\u7684\u4f5c\u7528\u3002\u5728\u6dfb\u52a0\u63ba\u6742\u5242\u5230\u4f53\u7cfb\u4e2d\u65f6\uff0c\u4e86\u89e3\u5728\u9634\u6781\u6750\u6599\u4e2d\u53d1\u751f\u7684\u7ed3\u6784\u548c\u7535\u5316\u5b66\u53d8\u5316\u5728\u8bbe\u8ba1\u5177\u6709\u589e\u5f3a\u7684\u7535\u5316\u5b66\u6027\u80fd\u7684\u65b0\u578b\u6750\u6599\u4e2d\u662f\u6781\u4e3a\u91cd\u8981\u7684\u3002<\/p>\n

\u6587\u732e\u94fe\u63a5\uff1a <\/strong>High voltage structural evolution and enhanced Na-ion diffusion in P2-Na2\/3<\/sub>Ni1\/3-x<\/sub>Mgx<\/sub>Mn2\/3<\/sub>O2<\/sub> (0 <x>< 0.20) cathodes from diffraction, electrochemical and ab-initio studies <\/a>(Energy & Environmental Science 2018, DOI: 10.1039\/C7EE02995K)<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u8ba1\u7b97\u6750\u6599\u7ec4Annay\u4f9b\u7a3f\uff0c\u6750\u6599\u725b\u6574\u7406\u7f16\u8f91\u3002<\/p>\n

\u6750\u6599\u725b\u7f51\u4e13\u6ce8\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u53ca\u884c\u4e1a\u8fdb\u5c55\uff0c\u8fd9\u91cc\u6c47\u96c6\u4e86\u5404\u5927\u9ad8\u6821\u7855\u535a\u751f\u3001\u4e00\u7ebf\u79d1\u7814\u4eba\u5458\u4ee5\u53ca\u884c\u4e1a\u4ece\u4e1a\u8005\uff0c\u5982\u679c\u60a8\u5bf9\u4e8e\u8ddf\u8e2a\u6750\u6599\u9886\u57df\u79d1\u6280\u8fdb\u5c55\uff0c\u89e3\u8bfb\u9ad8\u6c34\u5e73\u6587\u7ae0\u6216\u662f\u8bc4\u8ff0\u884c\u4e1a\u6709\u5174\u8da3\uff0c\u70b9\u6211\u52a0\u5165\u7f16\u8f91\u90e8\u5927\u5bb6\u5ead<\/a>\u3002<\/p>\n

\u6b22\u8fce\u5927\u5bb6\u5230\u6750\u6599\u4eba\u5ba3\u4f20\u79d1\u6280\u6210\u679c\u5e76\u5bf9\u6587\u732e\u8fdb\u884c\u6df1\u5165\u89e3\u8bfb\uff0c\u6295\u7a3f\u90ae\u7bb1tougao@cailiaoren.com<\/a>\u3002<\/p>\n

\u6295\u7a3f\u4ee5\u53ca\u5185\u5bb9\u5408\u4f5c\u53ef\u52a0\u7f16\u8f91\u5fae\u4fe1\uff1acailiaokefu<\/strong>\u3002<\/strong><\/p>\n

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