{"id":127871,"date":"2018-03-07T06:30:05","date_gmt":"2018-03-06T22:30:05","guid":{"rendered":"\/\/m.iemloyee.com\/?p=127871"},"modified":"2018-03-06T21:16:22","modified_gmt":"2018-03-06T13:16:22","slug":"%e5%b9%b2%e8%b4%a7%ef%bc%9a%e9%ab%98%e5%88%86%e5%ad%90%e9%a2%86%e5%9f%9f%e5%b8%b8%e7%94%a8%e7%9a%84%e5%88%86%e6%9e%90%e6%89%8b%e6%ae%b5%e6%a2%b3%e7%90%86","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=127871","title":{"rendered":"\u5e72\u8d27\uff1a\u9ad8\u5206\u5b50\u9886\u57df\u5e38\u7528\u7684\u5206\u6790\u624b\u6bb5\u68b3\u7406"},"content":{"rendered":"

\"\"<\/a><\/p>\n

\u9ad8\u5206\u5b50\u6750\u6599\u7684\u94fe\u7ed3\u6784\uff0c\u51dd\u805a\u6001\u7ed3\u6784\uff0c\u529b\u5b66\u72b6\u6001\uff0c\u70ed\u8f6c\u53d8\u6e29\u5ea6\u4ee5\u53ca\u5728\u5916\u754c\u6761\u4ef6\u4e0b\u7684\u53cd\u5e94\u548c\u53d8\u5316\u8fc7\u7a0b\u7b49\u7b49\u5747\u5bf9\u9ad8\u5206\u5b50\u6750\u6599\u672c\u8eab\u7684\u4f7f\u7528\u6709\u7740\u91cd\u8981\u5f71\u54cd\uff0c\u800c\u8fd9\u4e9b\u5f71\u54cd\u56e0\u7d20\u90fd\u53d6\u51b3\u4e8e\u9ad8\u5206\u5b50\u6750\u6599\u7684\u7ed3\u6784\u4e0e\u6027\u80fd\u4e4b\u95f4\u5173\u7cfb\u3002\u6211\u4eec\u5728\u63a2\u7a76\u8fd9\u79cd\u5173\u7cfb\u65f6\u5019\u5e38\u5e38\u5e94\u7528\u5230\u8bb8\u591a\u4eea\u5668\u5206\u6790\u65b9\u6cd5\u548c\u624b\u6bb5\u3002<\/p>\n

\u4eca\u5929\u6211\u5e26\u5927\u5bb6\u68b3\u7406\u4e00\u4e0b\u9ad8\u5206\u5b50\u9886\u57df\u5e38\u7528\u7684\u8868\u5f81\u65b9\u6cd5\uff1a<\/p>\n

1. \u793a\u5dee\u626b\u63cf\u91cf\u70ed\u5206\u6790\uff08DSC\uff09<\/b><\/strong><\/p>\n

\u5f53\u7269\u8d28\u7684\u7269\u7406\u72b6\u6001\u53d1\u751f\u53d8\u5316\u65f6\uff0c\u5982\u7ed3\u6676\u3001\u7194\u878d\u3001\u76f8\u8f6c\u53d8\uff0c\u6216\u8005\u53d1\u751f\u5316\u5b66\u53cd\u5e94\uff0c\u5f80\u5f80\u4f34\u968f\u7740\u70ed\u5b66\u6027\u80fd\u5982\u70ed\u7113\u3001\u6bd4\u70ed\u5bb9\u3001\u70ed\u5bfc\u7387\u7684\u53d8\u5316\u3002\u793a\u5dee\u626b\u63cf\u91cf\u70ed\u6cd5\u5c31\u662f\u901a\u8fc7\u6d4b\u5b9a\u5176\u70ed\u5b66\u6027\u80fd\u7684\u53d8\u5316\u6765\u8868\u5f81\u7269\u8d28\u7684\u7269\u7406\u6216\u5316\u5b66\u53d8\u5316\u8fc7\u7a0b\u3002DSC\u5728\u805a\u5408\u7269\u7814\u7a76\u4e2d\u7684\u5e94\u7528\u6709\u4ee5\u4e0b\u51e0\u70b9\uff1a<\/p>\n

a.<\/strong>\u73bb\u7483\u5316\u8f6c\u53d8\u8fc7\u7a0b\u7684\u7814\u7a76\uff1a\u975e\u6676\u6001\u805a\u5408\u7269\u7684\u73bb\u7483\u5316\u8f6c\u53d8\u662f\u4e0e\u94fe\u6bb5\u5fae\u5e03\u6717\u8fd0\u52a8\u89e3\u51bb\u6709\u5173\u7684\u4e00\u79cd\u677e\u5f1b\u73b0\u8c61\u3002\u7531\u4e8e\u88ab\u73bb\u7483\u5316\u8f6c\u53d8\u524d\u540e\u805a\u5408\u7269\u7684\u6bd4\u70ed\u5bb9\u53d1\u751f\u53d8\u5316\uff0c\u56e0\u6b64\u5728DSC\u70ed\u8c31\u56fe\u4e0a\u8868\u73b0\u4e3a\u57fa\u7ebf\u5411\u5438\u70ed\u65b9\u5411\u7684\u504f\u79fb\uff1b<\/p>\n

b.<\/strong>\u7ed3\u6676\u8fc7\u7a0b\u5bf9\u7194\u878d\u8fc7\u7a0b\u7684\u5f71\u54cd\uff1a\u5728\u7ed3\u6676\u8fc7\u7a0b\u4e2d\u7ed3\u6676\u6e29\u5ea6\u548c\u538b\u529b\u6761\u4ef6\u5bf9\u6676\u578b\u3001\u5fae\u6676\u5927\u5c0f\u7b49\u7684\u5f71\u54cd\u5f88\u5927\uff0c\u82e5\u5bf9\u7ed3\u6676\u805a\u5408\u7269\u8fdb\u884c\u8fde\u7eed\u7684\u91cd\u590d\u7684\u4e0d\u540c\u70ed\u5904\u7406\u540e\uff0c\u5f62\u6210\u4e86\u7ed3\u6676\u5927\u5c0f\u4e0d\u8fde\u7eed\u7684\u5206\u5e03\uff0c\u56e0\u800c\u7194\u878d\u65f6\u5c31\u51fa\u73b0\u82e5\u5e72\u4e0d\u8fde\u7eed\u7684\u7194\u878d\u5cf0\uff1b<\/p>\n

c.<\/strong>\u7ed3\u6676\u52a8\u529b\u5b66\u7814\u7a76\uff1a\u4e00\u822c\u60c5\u51b5\u4e0b\u805a\u5408\u7269\u7b49\u6e29\u7ed3\u6676\u7684\u8f6c\u5316\u7387\u7b26\u5408Avrami\u7ed3\u6676\u52a8\u529b\u5b66\u516c\u5f0f\uff1a<\/p>\n

1-\u03b1=exp\uff08-kt\uff09n<\/sup><\/p>\n

\u5f0f\u4e2d\uff0c\u03b1\u4e3a\u7ed3\u6676\u8f6c\u5316\u7387\uff1bk\u662f\u7ed3\u6676\u901f\u7387\u5e38\u6570\uff1bn\u662f\u4e0e\u7ed3\u6676\u6210\u6838\u548c\u751f\u957f\u8fc7\u7a0b\u6709\u5173\u7684\u6574\u6570\uff1b<\/p>\n

d.<\/strong>\u591a\u76f8\u4f53\u7cfb\u76f8\u5bb9\u6027\u7684\u7814\u7a76\uff1a\u6839\u636eDSC\u70ed\u8c31\u56fe\u4e0a\u9762\u7684Tg\u548cTm\u7684\u53d8\u5316\u6765\u786e\u5b9a\u975e\u6676\u6001\u805a\u5408\u7269\u548c\u7ed3\u6676\u805a\u5408\u7269\u7684\u591a\u76f8\u4f53\u7cfb\u76f8\u5bb9\u6027\uff1b<\/p>\n

e.<\/strong>\u591a\u76f8\u4f53\u7cfb\u7684\u5b9a\u91cf\u7814\u7a76\uff1a\u5bf9\u4e8e\u4e0d\u76f8\u5bb9\u7684\u975e\u6676\u6001\u591a\u76f8\u4f53\u7cfb\uff0c\u6709\u4e24\u4e2a\u73bb\u7483\u5316\u8f6c\u53d8\u3002\u5229\u7528DSC\u5b9a\u91cf\u6d4b\u5b9a\u4e0d\u76f8\u5bb9\u591a\u76f8\u4f53\u7cfb\u7ec4\u5206\u542b\u91cf\u7684\u57fa\u7840\u662f\u6d4b\u5b9a\u5404\u7ec4\u5206\u5728\u73bb\u7483\u5316\u8f6c\u53d8\u7684\u6bd4\u70ed\u5bb9\u53d8\u5316\u25b3Cp<\/sub>\uff1b\u76f8\u5bb9\u6027\u975e\u6676\u6001\u5171\u6df7\u7269\u7684Tg\u4e0e\u4e24\u7ec4\u5206\u7684\u76f8\u5bf9\u542b\u91cf\u5bc6\u5207\u6709\u5173\uff0c\u53ef\u7528Fox\u65b9\u7a0b\u8ba1\u7b97\uff1b<\/p>\n

f.<\/strong>\u53e6\u5916\uff0c\u5728\u7814\u7a76\u56fa\u5316\u53cd\u5e94\u8fc7\u7a0b\u65f6\u5e38\u5e38\u5e94\u7528DSC\u6d4b\u5b9a\u5176\u56fa\u5316\u53cd\u5e94\u70ed\uff0c\u5229\u7528\u52a8\u6001\u6cd5\u6216\u7b49\u6e29\u56fa\u5316\u6cd5\u7814\u7a76\u56fa\u5316\u8fc7\u7a0b\u7b49\u3002<\/p>\n

2. \u70ed\u91cd\u5206\u6790<\/b><\/strong>\uff08TGA\uff09<\/b><\/strong><\/p>\n

\u70ed\u91cd\u5206\u6790\u662f\u5728\u7a0b\u5e8f\u5347\u6e29\u7684\u73af\u5883\u4e2d\uff0c\u6d4b\u91cf\u8bd5\u6837\u7684\u91cd\u91cf\u5bf9\u6e29\u5ea6\u6216\u65f6\u95f4\u7684\u4f9d\u8d56\u5173\u7cfb\u7684\u4e00\u79cd\u5206\u6790\u65b9\u6cd5\u3002\u5728\u70ed\u8c31\u56fe\u4e0a\uff0c\u6a2a\u5750\u6807\u4e3a\u6e29\u5ea6T\u6216\u65f6\u95f4t\uff0c\u7eb5\u5750\u6807\u4e3a\u6837\u54c1\u4fdd\u7559\u91cd\u91cf\u7684\u5206\u6570\uff0c\u6240\u5f97\u5230\u7684\u91cd\u91cf-\u6e29\u5ea6\uff08\u65f6\u95f4\uff09\u66f2\u7ebf\u6210\u9636\u68af\u72b6\u3002\u6709\u7684\u805a\u5408\u7269\u53d7\u70ed\u65f6\u4e0d\u53ea\u4e00\u6b21\u5931\u91cd\uff0c\u6bcf\u6b21\u5931\u91cd\u7684\u767e\u5206\u6570\u53ef\u7531\u8be5\u5931\u91cd\u5e73\u53f0\u6240\u5bf9\u5e94\u7684\u7eb5\u5750\u6807\u6570\u503c\u76f4\u63a5\u5f97\u5230\uff0c\u5931\u91cd\u66f2\u7ebf\u5f00\u59cb\u4e0b\u6ed1\u7684\u8f6c\u6298\u5904\u5373\u5f00\u59cb\u5931\u91cd\u7684\u6e29\u5ea6\u4e3a\u8d77\u59cb\u5206\u89e3\u6e29\u5ea6\uff0c\u66f2\u7ebf\u4e0b\u964d\u7ec8\u6b62\u8f6c\u4e3a\u5e73\u53f0\u5904\u7684\u6e29\u5ea6\u4e3a\u5206\u89e3\u7ec8\u6b62\u6e29\u5ea6\u3002<\/p>\n

\u70ed\u91cd\u5206\u6790\u5728\u9ad8\u5206\u5b50\u6750\u6599\u7814\u7a76\u8fc7\u7a0b\u4e2d\uff0c\u6d4b\u91cf\u4e0e\u7814\u7a76\u6750\u6599\u7684\u70ed\u7a33\u5b9a\u6027\u3001\u5206\u89e3\u8fc7\u7a0b\u3001\u5438\u9644\u4e0e\u89e3\u5438\u3001\u6c27\u5316\u4e0e\u8fd8\u539f\u3001\u6210\u5206\u7684\u5b9a\u91cf\u5206\u6790\u3001\u6dfb\u52a0\u5242\u4e0e\u586b\u5145\u5242\u5f71\u54cd\u3001\u6c34\u5206\u4e0e\u6325\u53d1\u7269\u3001\u53cd\u5e94\u52a8\u529b\u5b66\u7b49\u7279\u6027\u3002<\/p>\n

3. \u7ea2\u5916\u5149\u8c31\u5206\u6790<\/b><\/strong>\uff08FTIR\uff09<\/b><\/strong><\/p>\n

\u7ea2\u5916\u5149\u8c31\u5206\u6790\u662f\u5229\u7528\u7ea2\u5916\u5149\u8c31\u5bf9\u7269\u8d28\u5206\u5b50\u8fdb\u884c\u7684\u5206\u6790\u548c\u9274\u5b9a\u3002\u5c06\u4e00\u675f\u4e0d\u540c\u6ce2\u957f\u7684\u7ea2\u5916\u5c04\u7ebf\u7167\u5c04\u5230\u7269\u8d28\u5206\u5b50\u4e0a\uff0c\u67d0\u4e9b\u7279\u5b9a\u6ce2\u957f\u7684\u7ea2\u5916\u5c04\u7ebf\u88ab\u5438\u6536\uff0c\u5f62\u6210\u8fd9\u4e00\u5206\u5b50\u7684\u7ea2\u5916\u5438\u6536\u5149\u8c31\u3002<\/p>\n

\u7ea2\u5916\u5149\u8c31\u5206\u6790\u5728\u9ad8\u5206\u5b50\u6750\u6599\u7814\u7a76\u9886\u57df\u5e94\u7528\u5e7f\u6cdb\u3002\u4e00\u65b9\u9762\uff0c\u7aef\u57fa\u5206\u6790\u5bf9\u4e8e\u6d4b\u5b9a\u5206\u5b50\u94fe\u7684\u5e73\u5747\u805a\u5408\u5ea6\u548c\u652f\u5316\u5ea6\u90fd\u5f88\u91cd\u8981\uff0c\u4f8b\u5982\u805a\u4e59\u70ef\u4e2d\u7532\u57fa\u542b\u91cf\u53ef\u7528\u6765\u6d4b\u5b9a\u5176\u652f\u5316\u5ea6\u3002\u53e6\u4e00\u65b9\u9762\uff0c\u8bb8\u591a\u805a\u5408\u7269\u542b\u6709\u5c11\u91cf\u6dfb\u52a0\u5242\u5982\u589e\u5851\u5242\u3001\u6297\u6c27\u5316\u5242\u3001\u586b\u5145\u5242\u7b49\uff0c\u8fd9\u4e9b\u5c11\u91cf\u6dfb\u52a0\u5242\u5728\u9ad8\u5206\u5b50\u6750\u6599\u5206\u6790\u9274\u5b9a\u524d\uff0c\u5f80\u5f80\u9700\u8981\u8fdb\u884c\u5206\u79bb\u548c\u63d0\u7eaf\u3002\u5e94\u7528\u7ea2\u5916\u5dee\u793a\u5149\u8c31\u6280\u672f\uff0c\u5c31\u53ef\u5c06\u9ad8\u5206\u5b50\u6750\u6599\u4e2d\u5c11\u91cf\u6dfb\u52a0\u7269\u7684\u6df7\u5408\u8c31\u56fe\u51cf\u53bb\uff0c\u8fd9\u6837\u65e0\u987b\u5206\u79bb\u5c31\u53ef\u9274\u5b9a\u5c11\u91cf\u6dfb\u52a0\u5242\u7684\u5316\u5b66\u7ec4\u6210\u548c\u7ed3\u6784\u3002<\/p>\n

\u518d\u8005\uff0c\u5728\u9ad8\u5206\u5b50\u6750\u6599\u6784\u8c61\u53ca\u6709\u5e8f\u6001\u7684\u9274\u5b9a\u65f6\uff0c\u6d4b\u5b9a\u7194\u878d\u540e\u6dec\u706b\u53ca\u9000\u706b\u7684\u534a\u7ed3\u6676\u805a\u5408\u7269\u8bd5\u6837\u6216\u5728\u76f8\u540c\u6e29\u5ea6\u4e0b\u6d4b\u5b9a\u8bd5\u6837\u7684\u7ea2\u5916\u5149\u8c31\u7136\u540e\u8fdb\u884c\u5149\u8c31\u7684\u5dee\u51cf\uff0c\u5c31\u53ef\u4ee5\u5f97\u5230\u8be5\u805a\u5408\u7269\u4e0d\u540c\u6784\u8c61\u6216\u6709\u5e8f\u6001\u7684\u5149\u8c31\u3002\u540c\u65f6\uff0c\u5728\u8868\u5f81\u805a\u5408\u7269\u5206\u5b50\u95f4\u7684\u76f8\u4e92\u4f5c\u7528\u5982\u76f8\u5bb9\u6027\u00b7\u3001\u6c22\u952e\u7b49\uff0c\u9ad8\u5206\u5b50\u6750\u6599\u7684\u8868\u9762\u548c\u754c\u9762\u4ee5\u53ca\u9ad8\u5206\u5b50\u6750\u6599\u53d1\u751f\u7684\u53cd\u5e94\u7b49\u7b49\uff0c\u7ea2\u5916\u5149\u8c31\u5206\u6790\u4e5f\u662f\u4e00\u79cd\u65b9\u4fbf\u5feb\u6377\u7684\u624b\u6bb5\u3002<\/p>\n

4. \u51dd\u80f6\u6e17\u900f\u8272\u8c31\u5206\u6790<\/b><\/strong>\uff08GPC\uff09<\/b><\/strong><\/p>\n

\u51dd\u80f6\u6e17\u900f\u8272\u8c31\u4e3b\u8981\u5e94\u7528\u4e8e\u9ad8\u5206\u5b50\u6750\u6599\u548c\u86cb\u767d\u8d28\u7684\u5206\u79bb\uff0c\u53ef\u7528\u6765\u5206\u79bb\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u4ece\u51e0\u767e\u4e07\u5230100\u8fd9\u6837\u7684\u4e00\u4e2a\u5bbd\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u8303\u56f4\u7684\u5206\u5b50\u3002<\/p>\n

\u7531\u4e8e\u9ad8\u5206\u5b50\u6750\u6599\u7684\u7269\u7406\u6027\u8d28\u4e0e\u5176\u5e73\u5747\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u79ef\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u5206\u5e03\u5bc6\u5207\u76f8\u5173\uff0c\u6240\u4ee5\u51dd\u80f6\u6e17\u900f\u8272\u8c31\u6210\u4e86\u4e00\u4e2a\u5feb\u901f\u9274\u5b9a\u805a\u5408\u7269\u9ad8\u3001\u4f4e\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u6210\u5206\u7684\u552f\u4e00\u7684\u5206\u6790\u5de5\u5177\u3002\u51dd\u80f6\u6e17\u900f\u8272\u8c31\u80fd\u7528\u4f5c\u8868\u793a\u805a\u5408\u7269\u4e4b\u95f4\u5dee\u522b\u7684\u4e00\u79cd\u5b9a\u6027\u5de5\u5177\uff0c\u6216\u7528\u4f5c\u8ba1\u7b97\u805a\u5408\u7269\u7684\u5e73\u5747\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u548c\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u5206\u5e03\u7684\u4e00\u79cd\u5b9a\u91cf\u5de5\u5177\u3002\u5173\u4e8e\u51dd\u80f6\u8272\u8c31\u5728\u9ad8\u5206\u5b50\u6750\u6599\u7684\u751f\u4ea7\u53ca\u7814\u7a76\u5de5\u4f5c\u4e2d\u7684\u5e94\u7528\u53ef\u6982\u62ec\u4e3a\u4ee5\u4e0b\u56db\u70b9\uff1a<\/p>\n

a.<\/strong>\u7528\u4e8e\u9ad8\u805a\u7269\u751f\u4ea7\u8fc7\u7a0b\u4e2d\u4e2d\u805a\u5408\u5de5\u827a\u7684\u9009\u62e9\uff0c\u805a\u5408\u53cd\u5e94\u673a\u7406\u7684\u7814\u7a76\u4ee5\u53ca\u63a7\u5236\u548c\u76d1\u89c6\u805a\u5408\u8fc7\u7a0b\uff1b<\/p>\n

b.<\/strong>\u5728\u9ad8\u805a\u7269\u6750\u6599\u7684\u52a0\u5de5\u53ca\u4f7f\u7528\u8fc7\u7a0b\u4e2d\u7528\u4e8e\u7814\u7a76\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u53ca\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u5206\u5e03\u4e0e\u52a0\u5de5\u4f7f\u7528\u6027\u80fd\u7684\u5173\u7cfb\uff0c\u52a9\u5242\u5728\u52a0\u5de5\u548c\u4f7f\u7528\u8fc7\u7a0b\u7684\u4f5c\u7528\u4ee5\u53ca\u8001\u5316\u673a\u7406\u7684\u7814\u7a76\uff1b<\/p>\n

c.<\/strong>\u7528\u4e8e\u5206\u79bb\u548c\u5206\u6790\u9ad8\u805a\u7269\u6750\u6599\u7684\u7ec4\u6210\u3001\u7ed3\u6784\u3001\u4ee5\u53ca\u9ad8\u805a\u7269\u5355\u5206\u6563\u8bd5\u6837\u7684\u5236\u5907\uff1b<\/p>\n

d.<\/strong>\u7528\u4e8e\u5c0f\u5206\u5b50\u7269\u8d28\u65b9\u9762\u7684\u5206\u6790\uff0c\u5982\u5728\u77f3\u6cb9\u53ca\u8868\u9762\u6d82\u5c42\u5de5\u4e1a\u65b9\u9762\u7684\u5e94\u7528\u7b49\u3002<\/p>\n

5. \u6838\u78c1\u5171\u632f\u5206\u6790<\/b><\/strong>\uff08NMR\uff09<\/b><\/strong><\/p>\n

\u6838\u78c1\u5171\u632f\u5206\u6790\u4f5c\u4e3a\u4e00\u79cd\u5de5\u5177\u5728\u9ad8\u805a\u7269\u7814\u7a76\u4e2d\u5e94\u7528\u751a\u5e7f\uff0c\u5982\u76f8\u5bf9\u5206\u5b50\u8d28\u91cf\u6d4b\u5b9a\u3001\u7ec4\u6210\u5206\u6790\u3001\u52a8\u529b\u5b66\u8fc7\u7a0b\u3001\u7ed3\u6676\u5ea6\u3001\u76f8\u53d8\u7b49\u3002\u4f46\u6700\u4e3a\u7a81\u51fa\u4e4b\u5904\uff0c\u662f\u5bf9\u9ad8\u5206\u5b50\u6750\u6599\u5206\u5b50\u94fe\u7684\u7acb\u4f53\u89c4\u6574\u6027\u3001\u94fe\u8282\u4e0d\u540c\u53d6\u5411\u7684\u8854\u63a5\uff08\u5982\u5934-\u5934\u3001\u5934-\u5c3e\u952e\u63a5\u7b49\uff09\uff0c\u94fe\u8282\u5e8f\u5217\u5206\u5e03\u53ca\u5fae\u7ed3\u6784\u7684\u786e\u5b9a\u3002\u800c\u6838\u78c1\u5171\u632f\u5206\u6790\u5728\u805a\u5408\u7269\u8868\u5f81\u65b9\u9762\u7684\u5e94\u7528\u4e3b\u8981\u5305\u62ec\uff1a<\/p>\n

a.<\/strong>\u7814\u7a76\u805a\u5408\u7269\u94fe\u7684\u6784\u578b\uff1b<\/p>\n

b.<\/strong>\u7814\u7a76\u805a\u5408\u7269\u94fe\u7684\u6784\u8c61\uff1b<\/p>\n

c.<\/strong>\u7814\u7a76\u805a\u5408\u7269\u548c\u5171\u805a\u7269\u4e2d\u7684\u5e8f\u5217\u5206\u5e03\u53ca\u7acb\u6784\u89c4\u6574\u6027\uff1b<\/p>\n

d.<\/strong>\u9274\u522b\u805a\u5408\u7269\u7684\u6df7\u5408\u7269\u3001\u5d4c\u6bb5\u5171\u805a\u7269\u3001\u4ea4\u66ff\u5171\u805a\u7269\u548c\u65e0\u89c4\u5171\u805a\u7269\uff1b<\/p>\n

e.<\/strong>\u7814\u7a76\u805a\u5408\u7269\u7684\u76f8\u5bb9\u6027\u548c\u805a\u5408\u7269\u7684\u5171\u6df7\u7269\uff1b<\/p>\n

f.<\/strong>\u7814\u7a76\u805a\u5408\u7269\u6eb6\u6db2\u4e2d\u7684\u5206\u5b50\u76f8\u4e92\u4f5c\u7528\uff1b<\/p>\n

g.<\/strong>\u7814\u7a76\u805a\u5408\u7269\u7684\u4ea4\u8054\u7b49\u7b49\u3002<\/p>\n

6. X\u5c04\u7ebf\u884d\u5c04\u5206\u6790<\/b><\/strong>\uff08XRD\uff09<\/b><\/strong><\/p>\n

\u5f53\u4e00\u675f\u5355\u8272X\u5c04\u7ebf\u5165\u5c04\u5230\u6676\u4f53\u65f6\uff0c\u7531\u4e8e\u6676\u4f53\u662f\u7531\u539f\u5b50\u6709\u89c4\u5219\u6392\u5217\u6210\u7684\u6676\u80de\u6240\u7ec4\u6210\u7684\uff0c\u800c\u8fd9\u4e9b\u6709\u89c4\u5219\u6392\u5217\u6210\u7684\u539f\u5b50\u95f4\u8ddd\u79bb\u4e0e\u5165\u5c04X\u5c04\u7ebf\u6ce2\u957f\u5177\u6709\u76f8\u540c\u6570\u91cf\u7ea7\uff0c\u6545\u7531\u4e0d\u540c\u539f\u5b50\u6563\u5c04\u7684X\u5c04\u7ebf\u76f8\u4e92\u5e72\u6d89\u53e0\u52a0\uff0c\u53ef\u5728\u67d0\u4e9b\u7279\u6b8a\u65b9\u5411\u4e0a\u4ea7\u751f\u5f3a\u7684X\u5c04\u7ebf\u884d\u5c04\u3002\u884d\u5c04\u65b9\u5411\u4e0e\u6676\u80de\u7684\u5f62\u72b6\u53ca\u5927\u5c0f\u6709\u5173\u3002\u884d\u5c04\u5f3a\u5ea6\u5219\u4e0e\u539f\u5b50\u5728\u6676\u80de\u4e2d\u7684\u6392\u5217\u65b9\u5f0f\u6709\u5173\u3002X\u5c04\u7ebf\u884d\u5c04\u5728\u9ad8\u5206\u5b50\u6750\u6599\u7814\u7a76\u4e2d\u626e\u6f14\u91cd\u8981\u89d2\u8272\uff0c\u4e3b\u8981\u5e94\u7528\u5982\u4e0b\uff1a<\/p>\n

a.<\/strong>\u7528X\u5c04\u7ebf\u884d\u5c04\u65b9\u6cd5\u6d4b\u5b9a\u805a\u5408\u7269\u7684\u7ed3\u6676\u5ea6\uff08X<\/i><\/em>0<\/sub>\uff09\uff1a<\/p>\n

X<\/i><\/em>0<\/sub>=\uff08W0<\/sub>\/W\uff09\u00d7100%<\/p>\n

\u800c \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 Wa<\/sub>\/W0<\/sub>=KIa<\/sub>\/I0<\/sub><\/p>\n

\u6545 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0 \u00a0X<\/i><\/em>0<\/sub>=[ I0<\/sub>\/( I0<\/sub>+ KIa<\/sub>)] \u00d7100%<\/p>\n

\u5f0f\u4e2dW\u4e3a\u9ad8\u805a\u7269\u6837\u54c1\u7684\u603b\u8d28\u91cf\uff1bW0<\/sub>\u4e3a\u9ad8\u805a\u7269\u6837\u54c1\u7ed3\u6676\u90e8\u5206\u91cd\u91cf\uff1bWa<\/sub>\u4e3a\u9ad8\u805a\u7269\u6837\u54c1\u975e\u6676\u90e8\u5206\u91cd\u91cf\uff1bI0<\/sub>\u4e3a\u9ad8\u805a\u7269\u6837\u54c1\u7ed3\u6676\u90e8\u5206\u884d\u5c04\u79ef\u5206\u5f3a\u5ea6\uff1bIa<\/sub>\u4e3a\u9ad8\u805a\u7269\u6837\u54c1\u975e\u6676\u90e8\u5206\u884d\u5c04\u79ef\u5206\u5f3a\u5ea6\uff1bK\u4e3a\u9ad8\u805a\u7269\u6837\u54c1\u7ed3\u6676\u548c\u975e\u6676\u90e8\u5206\u5355\u4f4d\u91cd\u91cf\u7684\u76f8\u5bf9\u6563\u5c04\u7cfb\u6570\u3002<\/p>\n

b.<\/strong>\u7814\u7a76\u9ad8\u805a\u7269\u53d6\u5411\u5ea6\u7684\u901a\u7528\u65b9\u6cd5\u6709X\u5c04\u7ebf\u884d\u5c04\u6cd5\u548c\u5149\u5b66\u65b9\u6cd5\u3002\u7528\u5149\u5b66\u65b9\u6cd5\u53ef\u6d4b\u5f97\u6574\u4e2a\u5206\u5b50\u94fe\u6216\u94fe\u6bb5\u7684\u53d6\u5411\uff0c\u800c\u7528X\u5c04\u7ebf\u884d\u5c04\u6cd5\u53ef\u6d4b\u91cf\u5fae\u6676\uff08\u6676\u533a\u5206\u5b50\u94fe\uff09\u7684\u53d6\u5411\u3002\u975e\u6676\u533a\u5206\u5b50\u94fe\u7684\u53d6\u5411\uff0c\u5219\u7531\u4e24\u79cd\u65b9\u6cd5\u6d4b\u5b9a\u7684\u7ed3\u679c\u52a0\u4ee5\u6362\u7b97\u5f97\u51fa\u3002\u5e38\u91c7\u7528\u4e0b\u9762\u7ecf\u9a8c\u516c\u5f0f\u8ba1\u7b97\u53d6\u5411\u5ea6\uff08\u03c0\uff09\uff1a<\/p>\n

\u03c0=\uff08180\u00b0-H\uff09\/180\u00b0\u00d7100<\/p>\n

H\u4e3a\u6cbf\u8d64\u9053\u7ebf\u4e0aDebye\u73af\uff08\u5e38\u7528\u6700\u5f3a\u73af\uff09\u7684\u5f3a\u5ea6\u5206\u5e03\u66f2\u7ebf\u7684\u534a\u9ad8\u5bbd\uff0c\u7528\u5ea6\u8868\u793a\u3002\u5b8c\u5168\u53d6\u5411\u65f6H=0\u00b0\uff0c\u03c0=100\u3002\u65e0\u89c4\u53d6\u5411\u65f6\uff0cH=180\u00b0\uff0c\u03c0=0\u3002<\/p>\n

c.<\/strong>\u9ad8\u805a\u7269\u6750\u6599\u7684\u7269\u6027\u9664\u4e86\u4e0e\u5176\u7ed3\u6676\u5ea6\u3001\u53d6\u5411\u5ea6\u6709\u5bc6\u5207\u5173\u7cfb\u5916\uff0c\u8fd8\u5e38\u5e38\u4e0e\u5176\u5fae\u6676\u5927\u5c0f\u6709\u5173\uff0c\u800c\u805a\u5408\u7269\u6750\u6599\u52a0\u5de5\u6210\u578b\u53ca\u70ed\u5904\u7406\u8fc7\u7a0b\uff0c\u5e38\u5e38\u5f71\u54cd\u8fd9\u4e2a\u503c\u7684\u5927\u5c0f\uff0c\u6545\u5fae\u6676\u5c3a\u5bf8\u7684\u6d4b\u91cf\u4e5f\u662f\u975e\u5e38\u91cd\u8981\u7684\u3002\u5fae\u6676\u5927\u5c0f\u4e00\u822c\u91c7\u7528\u8c22\u4e50\uff08Schorrer\uff09\u65b9\u7a0b\uff0c\u5982\u4e0b\uff1a<\/p>\n

Lhkl<\/sub>=K\u03bb\/\u03b2cos\u03b8<\/p>\n

\u5f0f\u4e2dLhkl<\/sub>\u7cfb\u5782\u76f4\u4e8e\uff08hkl\uff09\u6676\u9762\u7684\u5fae\u6676\u5c3a\u5bf8\uff1b\u03bb\u4e3a\u5165\u5c04X\u5c04\u7ebf\u7684\u6ce2\u957f\uff1b\u03b8\u4e3a\u5e03\u62c9\u683c\u89d2\uff1b\u03b2\u4e3a\u7eaf\u884d\u5c04\u7ebf\u589e\u5bbd\uff08\u7528\u5f27\u5ea6\u8868\u793a\uff09\u3002<\/p>\n

7. \u7535\u5b50\u663e\u5fae\u955c<\/b><\/strong><\/p>\n

\u7535\u5b50\u663e\u5fae\u955c\u662f\u4e00\u79cd\u7535\u5b50\u5149\u5b66\u5fae\u89c2\u5206\u6790\u4eea\u5668\uff0c\u662f\u5c06\u805a\u7126\u5230\u5f88\u7ec6\u7684\u7535\u5b50\u675f\u6253\u5230\u8bd5\u6837\u4e0a\u5f85\u6d4b\u5b9a\u7684\u4e00\u4e2a\u5fae\u5c0f\u533a\u57df\uff0c\u4ea7\u751f\u4e0d\u540c\u7684\u4fe1\u606f\uff0c\u52a0\u4ee5\u6536\u96c6\u3001\u6574\u7406\u548c\u5206\u6790\uff0c\u5f97\u51fa\u6750\u6599\u7684\u5fae\u89c2\u5f62\u8c8c\u3001\u7ed3\u6784\u548c\u5316\u5b66\u6210\u5206\u7b49\u6709\u7528\u7684\u4fe1\u606f\uff0c\u5982\u900f\u5c04\u7535\u955c\uff08TEM\uff09\u3001\u626b\u63cf\u7535\u955c\uff08SEM\uff09\u548c\u7535\u5b50\u63a2\u9488\u5206\u6790\uff08EPA\uff09\u7b49\u3002\u7535\u5b50\u663e\u5fae\u955c\u5728\u5206\u6790\u7814\u7a76\u9ad8\u805a\u7269\u65f6\u6709\u4ee5\u4e0b\u5e94\u7528\uff1a<\/p>\n

a.<\/strong>\u7535\u955c\u53ef\u89c2\u5bdf\u975e\u6676\u6001\u9ad8\u805a\u7269\u5fae\u89c2\u5f62\u6001\uff0c\u5176\u5b58\u5728\u5927\u5c0f\u4e3a3\uff5e10nm\u7684\u201c\u7403\u7c92\u7ed3\u6784\u201d\u548c\u5c40\u90e8\u6709\u5e8f\u533a\u57df\uff1b<\/p>\n

b.<\/strong>\u7528\u7535\u955c\u53ef\u4ee5\u89c2\u5bdf\u5230\u805a\u5408\u7269\u7684\u5404\u79cd\u7ed3\u6676\u5f62\u6001\uff0c\u5982\u6298\u53e0\u94fe\u6676\u7247\u3001\u4e32\u6676\u3001\u4f38\u76f4\u94fe\u6676\u7b49<\/p>\n

c.<\/strong>\u7814\u7a76\u7ea4\u7ef4\u548c\u7ec7\u7269\u7684\u7ec7\u6784\u53ca\u5176\u7f3a\u9677\u7279\u5f81\uff0c\u540c\u65f6\u8fd8\u7528\u4e8e\u7814\u7a76\u7ea4\u7ef4\u7684\u65ad\u88c2\u7279\u5f81\uff0c\u4ece\u800c\u8fdb\u4e00\u6b65\u5f04\u6e05\u695a\u5404\u79cd\u7ea4\u7ef4\u7684\u65ad\u88c2\u673a\u7406\u7b49\uff1b<\/p>\n

d.<\/strong>\u7535\u955c\u5e7f\u6cdb\u7528\u4e8e\u5404\u79cd\u805a\u5408\u7269\u53ca\u5176\u5171\u6df7\u7269\u7684\u7ed3\u6784\uff0c\u4ee5\u53ca\u5b83\u4eec\u65ad\u53e3\u5f62\u6001\u7279\u5f81\u4e0e\u5176\u529b\u5b66\u884c\u4e3a\u5173\u7cfb\u7b49\uff1b<\/p>\n

e.<\/strong>\u6b64\u5916\uff0c\u7535\u955c\u8fd8\u5e7f\u6cdb\u7528\u4e8e\u590d\u5408\u6750\u6599\u7684\u5404\u79cd\u6545\u969c\u7ed3\u6784\u5206\u6790\uff0c\u4ee5\u53ca\u7814\u7a76\u9ad8\u805a\u7269\u6750\u6599\u4f5c\u4e3a\u6d82\u5c42\u3001\u80f6\u9ecf\u5242\u3001\u8584\u819c\u65f6\uff0c\u5f62\u6210\u9ad8\u805a\u7269\u819c\u7684\u7ed3\u6784\u53ca\u5176\u9ecf\u7ed3\u72b6\u6001\u3002<\/p>\n

8. X\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\u4eea<\/b><\/strong>\uff08XPS\uff09<\/b><\/strong><\/p>\n

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9. \u52a8\u6001\u70ed\u673a\u68b0\u5206\u6790<\/b><\/strong>\uff08DMA\uff09<\/b><\/strong><\/p>\n

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10. \u6d41\u53d8\u5206\u6790<\/b><\/strong><\/p>\n

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\u53e6\u5916\uff0c\u8fd1\u4e9b\u5e74\u6765\u5728\u8bb8\u591a\u79d1\u7814\u5de5\u4f5c\u8005\u6839\u636e\u9700\u8981\u4e5f\u7528\u5230\u4e86\u5176\u4ed6\u7684\u5206\u6790\u6d4b\u5b9a\u4eea\u5668\u548c\u65b9\u6cd5\uff0c\u5982\u4e07\u80fd\u8bd5\u9a8c\u673a\u3001\u504f\u5149\u5206\u6790\u3001\u5149\u58f0\u5149\u8c31\u5206\u6790\u3001\u4e2d\u5b50\u6563\u5c04\u6cd5\u3001\u5c0f\u89d2\u5149\u6563\u5c04\u6cd5\u3001\u626b\u63cf\u8d85\u58f0\u663e\u5fae\u955c\u7b49\uff0c\u4e3a\u9ad8\u5206\u5b50\u6750\u6599\u7684\u6df1\u5165\u7814\u7a76\u63d0\u4f9b\u4e86\u4e30\u5bcc\u800c\u6709\u529b\u7684\u8868\u5f81\u624b\u6bb5\u3002<\/p>\n

\u672c\u6587\u7531\u6750\u6599\u4eba\u4e13\u680f\u79d1\u6280\u987e\u95ee\u8d75\u6850\u8f89\u4f9b\u7a3f\uff0c\u6750\u6599\u4eba\u7f16\u8f91\u6574\u7406\u3002<\/p>\n

\u6750\u6599\u4eba\u63a8\u51fa\u6750\u6599\u6d4b\u8bd5\u89e3\u51b3\u65b9\u6848\uff0c\u626b\u7801\u63d0\u4ea4\u9700\u6c42\uff0c\u6216\u70b9\u51fb\u94fe\u63a5\u63d0\u4ea4\u9700\u6c42<\/a>\u3002\"\"<\/p>\n","protected":false},"excerpt":{"rendered":"

\u9ad8\u5206\u5b50\u6750\u6599\u7684\u94fe\u7ed3\u6784\uff0c\u51dd\u805a\u6001\u7ed3\u6784\uff0c\u529b\u5b66\u72b6\u6001\uff0c\u70ed\u8f6c\u53d8\u6e29\u5ea6\u4ee5\u53ca\u5728\u5916\u754c\u6761\u4ef6\u4e0b\u7684\u53cd\u5e94\u548c\u53d8\u5316\u8fc7\u7a0b\u7b49\u7b49\u5747\u5bf9\u9ad8\u5206\u5b50\u6750\u6599\u672c\u8eab\u7684\u4f7f\u7528\u6709\u7740\u91cd\u8981\u5f71\u54cd\uff0c\u800c\u8fd9\u4e9b\u5f71\u54cd\u56e0\u7d20\u90fd\u53d6\u51b3\u4e8e\u9ad8\u5206\u5b50\u6750\u6599\u7684…<\/p>\n","protected":false},"author":7350,"featured_media":127885,"comment_status":"open","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"footnotes":""},"categories":[4],"tags":[2890,42],"class_list":["post-127871","post","type-post","status-publish","format-standard","has-post-thumbnail","hentry","category-ganhuo","tag-2890","tag-gaofenzi"],"_links":{"self":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/127871"}],"collection":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts"}],"about":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/users\/7350"}],"replies":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcomments&post=127871"}],"version-history":[{"count":14,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/127871\/revisions"}],"predecessor-version":[{"id":128811,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/posts\/127871\/revisions\/128811"}],"wp:featuredmedia":[{"embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=\/wp\/v2\/media\/127885"}],"wp:attachment":[{"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fmedia&parent=127871"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Fcategories&post=127871"},{"taxonomy":"post_tag","embeddable":true,"href":"\/\/m.iemloyee.com\/index.php?rest_route=%2Fwp%2Fv2%2Ftags&post=127871"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}