{"id":126325,"date":"2018-02-22T06:30:00","date_gmt":"2018-02-21T22:30:00","guid":{"rendered":"\/\/m.iemloyee.com\/?p=126325"},"modified":"2018-02-21T20:23:18","modified_gmt":"2018-02-21T12:23:18","slug":"adv-energy-mater-%e5%be%ae%e4%b9%b3%e6%b6%b2%e8%af%b1%e5%af%bc%e5%90%88%e6%88%903d%e5%a4%9a%e5%ad%94%e7%a1%ab%e7%9f%b3%e5%a2%a8%e7%83%afg-c3n4%e5%a4%8d%e5%90%88%e6%b5%b7%e7%bb%b5%e4%bd%9c","status":"publish","type":"post","link":"\/\/m.iemloyee.com\/?p=126325","title":{"rendered":"Adv. Energy Mater. : \u5fae\u4e73\u6db2\u8bf1\u5bfc\u5408\u62103D\u591a\u5b54\u786b\/\u77f3\u58a8\u70ef@g-C3N4\u590d\u5408\u6d77\u7ef5\u4f5c\u4e3a\u81ea\u652f\u6491\u6b63\u6781\u7528\u4e8e\u9ad8\u80fd\u91cf\u5bc6\u5ea6Li\u2013S\u7535\u6c60"},"content":{"rendered":"

\u3010\u5f15\u8a00\u3011<\/strong><\/p>\n

\u968f\u7740\u4eba\u4eec\u5bf9\u7535\u52a8\u6c7d\u8f66\uff0c\u4fbf\u643a\u5f0f\u7535\u5b50\u8bbe\u5907\u4ee5\u53ca\u667a\u80fd\u7535\u7f51\u9700\u6c42\u7684\u65e5\u76ca\u5267\u589e\uff0c\u5f00\u53d1\u51fa\u5177\u6709\u9ad8\u80fd\u91cf\u5bc6\u5ea6\uff0c\u4f4e\u6210\u672c\u4ee5\u53ca\u957f\u5faa\u73af\u7a33\u5b9a\u6027\u7684\u7535\u5316\u5b66\u80fd\u91cf\u5b58\u50a8\u7cfb\u7edf\u5bf9\u4e8e\u672a\u6765\u793e\u4f1a\u7684\u53d1\u5c55\u6709\u91cd\u8981\u7684\u610f\u4e49\u3002\u5728\u4f17\u591a\u80fd\u91cf\u5b58\u50a8\u4f53\u7cfb\u4e2d\uff0cLi-S\u7535\u6c60\u56e0\u5177\u67092600 W h kg\u2212<\/sup>1<\/sup>\u7406\u8bba\u6bd4\u80fd\u91cf\u3001\u786b\u7684\u4e30\u5bcc\u6765\u6e90\u548c\u4f4e\u6bd2\u6027\u7b49\u4f18\u52bf\u800c\u5f15\u8d77\u4e86\u5e7f\u5927\u79d1\u7814\u4eba\u5458\u7684\u6ce8\u610f\u3002\u5c3d\u7ba1\u5982\u6b64\uff0cLi\u2013S\u7535\u6c60\u4ecd\u5b58\u5728\u4e00\u4e9b\u95ee\u9898\uff0c\u963b\u788d\u4e86\u5176\u5546\u4e1a\u5316\u8fdb\u7a0b\u7684\u63a8\u8fdb\uff1a(1)\u5355\u8d28\u786b\u53ca\u5176\u653e\u7535\u4ea7\u7269(Li2<\/sub>S\/Li2<\/sub>S2<\/sub>)\u56fa\u6709\u7684\u7535\u5b50\u7edd\u7f18\u6027\u5bfc\u81f4\u4e86\u5176\u8f83\u4f4e\u7684\u6d3b\u6027\u7269\u8d28\u5229\u7528\u7387\u548c\u7f13\u6162\u7684\u53cd\u5e94\u52a8\u529b\u5b66\uff1b(2)\u9ad8\u5ea6\u53ef\u6eb6\u7684\u4e2d\u95f4\u4ea7\u7269(Li2<\/sub>Sx<\/sub>, 4 \u2264 x \u2264 8)\u6781\u6613\u6269\u6563\u8fdb\u5165\u7535\u89e3\u6db2\u5e76\u6c89\u79ef\u4e8eLi\u8d1f\u6781\uff0c\u5bfc\u81f4\u4e0d\u53ef\u9006\u5bb9\u91cf\u7684\u635f\u5931\u4ee5\u53ca\u91d1\u5c5eLi\u8d1f\u6781\u7684\u8150\u8680\uff1b(3)\u5faa\u73af\u8fc7\u7a0b\u4e2d\u786b\u548cLi2<\/sub>S\u4e4b\u95f4\u7684\u7535\u5316\u5b66\u8f6c\u53d8\u4f1a\u4ea7\u751f\u8f83\u5927\u7684\u4f53\u79ef\u53d8\u5316\uff0c\u4ece\u800c\u5bfc\u81f4\u6b63\u6781\u7ed3\u6784\u4e0d\u7a33\u5b9a\u4ee5\u53ca\u5bb9\u91cf\u7684\u5feb\u901f\u964d\u4f4e\u3002\u8fd9\u4e9b\u95ee\u9898\u4e25\u91cd\u963b\u788d\u4e86\u5176\u5728\u5b9e\u9645\u4e2d\u7684\u5e94\u7528\u3002<\/p>\n

\u3010\u6210\u679c\u7b80\u4ecb\u3011<\/p>\n

\u8fd1\u65e5\uff0c\u6765\u81ea\u56fd\u5bb6\u7eb3\u7c73\u79d1\u5b66\u4e2d\u5fc3\u7684\u5f20\u5a1f\u535a\u58eb\uff08\u7b2c\u4e00\u4f5c\u8005\uff09\u3001\u891a\u536b\u56fd\u7814\u7a76\u5458\uff08\u5171\u540c\u901a\u8baf\uff09\u548c\u4e2d\u79d1\u9662\u5316\u5b66\u6240\u7684\u90ed\u7389\u56fd\u7814\u7a76\u5458\uff08\u5171\u540c\u901a\u8baf\uff09<\/strong>\u7b49\u4eba\u5728Advanced Energy Materials\u4e0a\u53d1\u6587\uff0c\u9898\u4e3a\u201cMicroemulsion Assisted Assembly of 3D Porous S\/Graphene@g-C3<\/sub>N4<\/sub> Hybrid Sponge as Free-Standing Cathodes for High Energy Density Li\u2013S Batteries\u201d\u3002\u7814\u7a76\u4eba\u5458\u91c7\u7528\u5fae\u4e73\u6db2\u8bf1\u5bfc\u6cd5\u6210\u529f\u5236\u5907\u4e863D\u591a\u5b54\u786b\/\u77f3\u58a8\u70ef@g-C3<\/sub>N4<\/sub>(S\/GCN)\u590d\u5408\u6d77\u7ef5\u5e76\u5c06\u5176\u76f4\u63a5\u4f5c\u4e3a\u81ea\u652f\u6491\u6b63\u6781\u7528\u4e8eLi\u2013S\u7535\u6c60\u3002\u5176\u4e2d\uff0c\u5fae\u4e73\u6ef4\u4f5c\u4e3a\u8f6f\u6a21\u677f\u5f62\u6210\u591a\u5b54\u7ed3\u6784\uff0c\u8868\u9762\u4eb2\u6c34\u7684GCN\u5728\u4e73\u6ef4\u5468\u56f4\u4e0d\u65ad\u5806\u53e0\u5f62\u6210\u76f8\u4e92\u4ea4\u8054\u76843D\u7f51\u7edc\uff0c\u7eb3\u7c73\u786b\u5747\u4e00\u5206\u6563\u4e8eGCN\u8868\u9762\u3002\u901a\u8fc7\u8be5\u5fae\u4e73\u6db2\u6cd5\uff0c\u7814\u7a76\u4eba\u5458\u5236\u5907\u51fa\u4e86\u786b\u8d1f\u8f7d\u91cf\u9ad8\u8fbe82wt%\u7684S\/GCN\u6b63\u6781\u3002\u540c\u65f6\uff0cGCN\u5927\u5b54\u9699\u4e2d\u4e30\u5bcc\u7684N\u4f4d\u70b9\u4e3a\u591a\u786b\u5316\u7269\u63d0\u4f9b\u4e86\u4f17\u591a\u7c98\u9644\u4f4d\u70b9\uff0c\u5b9e\u73b0\u4e86\u4e00\u4e2a\u201c\u7269\u7406\u2014\u5316\u5b66\u201d\u53cc\u91cd\u9632\u5fa1\u4f53\u7cfb\u6765\u9650\u5236\u591a\u786b\u5316\u7269\u7684\u6269\u6563\u3002\u6b64\u5916\uff0c\u4e09\u7ef4\u591a\u5b54\u7684\u77f3\u58a8\u70ef\u9aa8\u67b6\u4e3a\u5176\u63d0\u4f9b\u4e86\u9ad8\u6548\u7684\u7535\u5b50\/Li+<\/sup>\u4f20\u8f93\u901a\u9053\uff0c\u6709\u5229\u4e8e\u5b9e\u73b0\u5feb\u901f\u7684\u53cd\u5e94\u52a8\u529b\u5b66\u3002\u4e0e\u4f20\u7edf\u7684G-\u6d77\u7ef5\/Li2<\/sub>Sn<\/sub>\u6b63\u6781\u7535\u89e3\u6db2\u4f53\u7cfb\u76f8\u6bd4\uff0cS\/GCN\u53ef\u53d1\u6325\u51fa\u66f4\u9ad8\u7684\u6d3b\u6027\u7269\u8d28\u5229\u7528\u7387\uff0c\u9ad8\u500d\u7387\u6027\u80fd(612 mA h g\u2212<\/sup>1<\/sup> at 10 C)\uff0c\u4ee5\u53ca\u6709\u6548\u7f13\u89e3\u7684Li\u8d1f\u6781\u8150\u8680\u95ee\u9898\u3002\u503c\u5f97\u6ce8\u610f\u7684\u662f\uff0c\u57280.3C\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\uff0c\u8be5\u7535\u6c60\u4f53\u7cfb\u53ef\u5b9e\u73b01493 W h kg\u2212<\/sup>1<\/sup>\u7684\u9ad8\u80fd\u91cf\u5bc6\u5ea6 (\u57fa\u4e8e\u6b63\u6781\u603b\u8d28\u91cf\u8ba1\u7b97) \u548c\u4ec5\u4e3a0.017%\/\u7684\u5bb9\u91cf\u8870\u51cf\u7387\uff08800\u5468\u5faa\u73af\uff09\u3002<\/p>\n

\u3010\u56fe\u6587\u5bfc\u8bfb\u3011<\/p>\n

\u56fe1. \u7ed3\u6784\u8868\u5f81<\/p>\n

\"\"<\/p>\n

a)\u7531\u6df7\u5408\u7269\u5f97\u5230\u7684\u4e73\u6db2\u6ef4\u7684\u5149\u5b66\u663e\u5fae\u955c\u56fe\u50cf\uff1b<\/p>\n

b)\u901a\u8fc7\u5e38\u89c4\u65b9\u6cd5\u5f97\u5230\u7684G-\u6d77\u7ef5\uff08\u5de6\uff09\u4ee5\u53ca\u901a\u8fc7\u5fae\u4e73\u6db2\u6cd5\u5f97\u5230\u7684S\/GCN\u590d\u5408\u6d77\u7ef5\uff08\u53f3\uff09\u7684\u5149\u5b66\u663e\u5fae\u955c\u56fe\u50cf\uff1b<\/p>\n

c) S\/GCN\u7684SEM\u622a\u9762\u56fe\uff1bd) S\/GCN\u7684SEM\u9ad8\u5206\u8fa8\u56fe\uff1b<\/p>\n

e\u2013g) S\/GCN\u7684TEM\u56fe\uff1b<\/p>\n

S\/GCN\u7684\u5143\u7d20\u5206\u5e03\u56feh) N, i) C, j) S\uff1b<\/p>\n

S\/GCN\u7684\u7535\u5b50\u63a2\u9488\u663e\u5fae\u5206\u6790(EPMA)\u5143\u7d20\u5206\u5e03\u56fe\uff1ak)S,\u00a0 l) C\uff1b<\/p>\n

m) S\/GCN\u7684EDS\u56fe\uff1b<\/p>\n

\u56fe2. \u7ed3\u6784\u53ca\u5143\u7d20\u5206\u6790<\/p>\n

\"\"<\/p>\n

a) \u81ea\u7ec4\u88c5\u4e4b\u524d\u7684GO-C3<\/sub>N4<\/sub>-S\u524d\u9a71\u4f53\u4ee5\u53ca3D S\/GCN \u590d\u5408\u7269\u7684XRD\u56fe\uff1b<\/p>\n

b) \u81ea\u7ec4\u88c5\u4e4b\u524d\u7684GO-C3<\/sub>N4<\/sub>-S\u524d\u9a71\u4f53\u4ee5\u53ca3D S\/GCN \u590d\u5408\u7269\u7684Raman\u56fe\uff1b<\/p>\n

S\/GCN\u7684XPS\u56fe\uff1ac) N 1s\uff0cd) C 1s\uff1b<\/p>\n

\u56fe3. \u6027\u80fd\u8868\u5f81<\/p>\n

\"\"<\/p>\n

a) \u57281C\u6761\u4ef6\u4e0b\uff0cS\/GCN, GCN-Li2<\/sub>Sn<\/sub>, S-GCN\u6b63\u6781\u7684\u6052\u7535\u6d41\u5145\u653e\u7535\u66f2\u7ebf\u4ee5\u53ca\u76f8\u5e94\u7684b) dQ\/dV\u66f2\u7ebf\uff1b (b)\u7684\u63d2\u56fe\u4e3a\u662f3\u4e2a\u6b63\u6781\u7684\u5f52\u4e00\u5316\u540e\u7684\u7b2c\u4e8c\u5e73\u53f0\u653e\u7535\u66f2\u7ebf\uff1b.<\/p>\n

c) \u57281C\u6761\u4ef6\u4e0b\uff0cS\/GCN\u6b63\u6781200\u5468\u7684\u5faa\u73af\u6027\u80fd\uff1b<\/p>\n

d) 0.1 mV s\u2212<\/sup>1<\/sup>\u7684\u626b\u901f\u4e0b\uff0cS\/GCN\u6b63\u6781\u524d\u56db\u5708\u7684\u5faa\u73af\u4f0f\u5b89\u66f2\u7ebf\uff1b<\/p>\n

\u56fe4. \u6027\u80fd\u5206\u6790<\/p>\n

\"\"<\/p>\n

a) S\/GCN\u6b63\u6781\u5728\u4e0d\u540c\u5145\u653e\u7535\u500d\u7387\u4e0b\u7684\u6052\u7535\u6d41\u5145\u653e\u7535\u66f2\u7ebf(0.2, 0.5, 1, 2, 5, 8, 10 C)\uff1b<\/p>\n

b) S\/GCN, GCN-Li2<\/sub>Sn<\/sub>, S-GCN\u6b63\u6781\u7684\u500d\u7387\u6027\u80fd(\u5e93\u4f26\u6548\u7387\u5bf9\u5e94\u4e8eS\/GCN\u6b63\u6781)\uff1b<\/p>\n

c) S\/GCN, GCN-Li2<\/sub>Sn<\/sub>, S-GCN\u6b63\u6781\u5728\u4e0d\u540c\u500d\u7387\u4e0b\u7684\u653e\u7535\u5bb9\u91cf\u5bf9\u6bd4(\u6d45\u8272\u90e8\u5206\u5bf9\u5e94\u7684\u662f\u4f4e\u4e8e0 V\u7684\u6bd4\u5bb9\u91cf)\uff1b<\/p>\n

d) S\/GCN-73%S, S\/GCN-82%S, GCN-Li2<\/sub>Sn<\/sub>-70%, S-GCN-70%\u6b63\u6781\u57281C\u4e0b\u5faa\u73af150\u6b21\u7684\u5faa\u73af\u6027\u80fd\uff1b<\/p>\n

\u56fe5. \u957f\u5faa\u73af\u7a33\u5b9a\u6027\u6d4b\u8bd5<\/p>\n

\"\"<\/p>\n

a) S\/GCN, GCN-Li2<\/sub>Sn<\/sub>, S-GCN\u6b63\u6781\u57285 A g\u2212<\/sup>1<\/sup>(0.3 C)\u7684\u7535\u6d41\u5bc6\u5ea6\u4e0b\u7684\u957f\u5faa\u73af\u6027\u80fd\u5bf9\u6bd4\uff1b<\/p>\n

b)\u5bf9\u5404\u7c7bS\/C\u6b63\u6781\u7684\u6bd4\u5bb9\u91cf\u3001\u80fd\u91cf\u5bc6\u5ea6\u548cS wt% \u7684\u6bd4\u8f83(\u6240\u6709\u7684\u80fd\u91cf\u5bc6\u5ea6\u7684\u8ba1\u7b97\u5747\u57fa\u4e8e\u6b63\u6781\u603b\u8d28\u91cf)\uff1b<\/p>\n

\u3010\u603b\u7ed3\u3011<\/strong><\/p>\n

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\u6587\u732e\u94fe\u63a5\uff1aMicroemulsion Assisted Assembly of 3D Porous S\/Graphene@g-C3<\/sub>N4<\/sub> Hybrid Sponge as Free-Standing Cathodes for High Energy Density Li\u2013S Batteries<\/a>, (Advanced Energy Materials, 2018, DOI:\u00a010.1002\/aenm.201702839)<\/p>\n

\u901a\u8baf\u4f5c\u8005\u53ca\u56e2\u961f\u7b80\u4ecb<\/p>\n

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\u56e2\u961f\u5728\u8be5\u9886\u57df\u5de5\u4f5c\u6c47\u603b\uff1a<\/strong><\/p>\n

\u8fd1\u5e74\u6765\uff0c\u90ed\u7389\u56fd\u7814\u7a76\u5458\u8bfe\u9898\u7ec4\u5728\u9502\u786b\u7535\u6c60\u6b63\u8d1f\u6750\u6599\u53ca\u7535\u89e3\u8d28\u7684\u8bbe\u8ba1\u5408\u6210\u53ca\u5176\u7535\u5316\u5b66\u884c\u4e3a\u63a2\u7d22\u65b9\u9762\u5f00\u5c55\u4e86\u5927\u91cf\u7814\u7a76\uff0c\u5e76\u53d6\u5f97\u4e86\u4e00\u7cfb\u5217\u5177\u6709\u56fd\u9645\u5f71\u54cd\u529b\u7684\u8fdb\u5c55\u3002\u76f8\u5173\u6210\u679c\u76f8\u7ee7\u53d1\u8868\u5728J. Am. Chem. Soc.<\/em>, 2012, 134, 18510; Angew. Chem. Int. Ed.,<\/em> 2013, 52, 13186; J. Mater. Chem. A,<\/em> 2013, 1, 6602; Part. Part. Syst. Charact.,<\/em> 2013, 30, 321; Electrochim. Acta<\/em>, 2013, 91, 58; ACS Appl. Mater. Interfaces,<\/em> 2014, 6, 8789; Sci. China Chem.<\/em>, 2014, 57, 1564; J. Energy Chem.,<\/em> 2014, 3, 308; J. Am. Chem. Soc., <\/em>2015, 137, 2215; J. Mater. Chem. A<\/em>, 2015, 3, 4799; Adv. Mater, <\/em>2016, 28, 9539; Chem. Asian J.,<\/em> 2016, 11, 2690; ACS Appl. Mater. Interfaces,<\/em> 2016, 8, 3584; RSC Advances,<\/em> 2016, 6, 617; Chin. Phys. B<\/em>, 2016, 25, 018801; Angew. Chem. Int. Ed<\/em>., 2016, 55, 15835\uff1bACS Appl. Mater. Interfaces,<\/em> 2017, 9, 43696\uff1bACS Appl. Mater. Interfaces,<\/em> 2017, 9, 1553\uff1bAdv. Sci.<\/em> 2017, 4, 1600400\uff1bAdv. Sci.<\/em> 2017, 4, 1600445\uff1bNano Energy<\/em>, 2017, 36, 411\uff1bJoule<\/em>, 2017, 1, 563\uff1bNatl. Sci. Rev.<\/em>, 2017, 4, 54\uff1bACS Energy Lett.<\/em>, 2017, 2 , 1385\uff1bAdv. Energy Mater.<\/em>, 2017, 7, 1700530\uff1bAdv. Mater.<\/em>, 2017, 29, 1700389\uff1bAdv. Mater.<\/em>, 2017, 29, 1703729\uff1bJ. Am. Chem. Soc.<\/em>, 2017, 139, 5916\uff1bAngew. Chem. Int. Ed.<\/em>, 2018, 57, 1505; J. Am. Chem. Soc.<\/em>, 2018, 140, 1, 82; Chem<\/em>, 2018, 4, 298<\/p>\n

\u76f8\u5173\u4f18\u8d28\u6587\u732e\u63a8\u8350\uff1a<\/strong><\/p>\n

1\uff09S-H Chung, A. Manthiram*<\/sup> Rational Design of Statically and Dynamically Stable Lithium\u2013Sulfur Batteries with High Sulfur Loading and Low Electrolyte\/Sulfur Ratio. Adv. Mater., <\/em>2017, DOI: 10.1002\/adma.201705951.<\/p>\n

2\uff09W-L Wu, J. Pu, J. Wang, Z.-H. Shen, H.-Y. Tang, Z.-T. Deng, X.-Y. Tao, F. Pan, H.-G. Zhang*<\/sup> Biomimetic Bipolar Microcapsules Derived from Staphylococcus Aureus for Enhanced Properties of Lithium\u2013Sulfur Battery Cathodes. Adv. Energy Mater.,<\/em> 2018, DOI: 10.1002\/aenm.201702373<\/p>\n

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